CN1033461C - 消除含油功能流体形成油雾的方法 - Google Patents

消除含油功能流体形成油雾的方法 Download PDF

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Publication number: CN1033461C
Authority: CN; China
Prior art keywords: oil; multipolymer; butene; laurylene; composition
Prior art date: 1991-06-19
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Lifetime

Application number

CN93104651A

Other languages

English (en)

Chinese (zh)

Other versions

CN1093106A (zh

Inventor

H·E·巴克曼

史宗冈

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

ExxonMobil Chemical Patents Inc

Original Assignee

Exxon Chemical Patents Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1991-06-19

Filing date

1993-03-30

Publication date

1996-12-04

1991-06-19 Priority claimed from US07/717,433 external-priority patent/US5227551A/en

1993-03-22 Priority to AU38161/93A priority Critical patent/AU671625B2/en

1993-03-22 Priority to CA002156744A priority patent/CA2156744C/en

1993-03-22 Priority to DE69307931T priority patent/DE69307931T2/de

1993-03-22 Priority to BR9307827A priority patent/BR9307827A/pt

1993-03-22 Priority to AT93907626T priority patent/ATE148494T1/de

1993-03-22 Priority to JP6520971A priority patent/JPH08512334A/ja

1993-03-22 Priority to ES93907626T priority patent/ES2098731T3/es

1993-03-22 Priority to EP93907626A priority patent/EP0690902B1/en

1993-03-22 Priority to PCT/US1993/002605 priority patent/WO1994021760A1/en

1993-03-30 Priority to CN93104651A priority patent/CN1033461C/zh

1993-03-30 Application filed by Exxon Chemical Patents Inc filed Critical Exxon Chemical Patents Inc

1994-10-05 Publication of CN1093106A publication Critical patent/CN1093106A/zh

1995-09-21 Priority to NO19953727A priority patent/NO312910B1/no

1996-12-04 Publication of CN1033461C publication Critical patent/CN1033461C/zh

1996-12-04 Application granted granted Critical

2013-03-30 Anticipated expiration legal-status Critical

Status Expired - Lifetime legal-status Critical Current

Links

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125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
JFNLZVQOOSMTJK-KNVOCYPGSA-N norbornene Chemical group C1[C@@H]2CC[C@H]1C=C2 JFNLZVQOOSMTJK-KNVOCYPGSA-N 0.000 description 1
125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
239000003027 oil sand Substances 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
150000002899 organoaluminium compounds Chemical class 0.000 description 1
239000007800 oxidant agent Substances 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 1
125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
239000012071 phase Substances 0.000 description 1
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
150000003016 phosphoric acids Chemical class 0.000 description 1
OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 description 1
239000004033 plastic Substances 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
229920002401 polyacrylamide Polymers 0.000 description 1
229920001083 polybutene Polymers 0.000 description 1
229920000193 polymethacrylate Polymers 0.000 description 1
229920001155 polypropylene Polymers 0.000 description 1
229920005606 polypropylene copolymer Polymers 0.000 description 1
230000003449 preventive effect Effects 0.000 description 1
238000000197 pyrolysis Methods 0.000 description 1
229910052761 rare earth metal Inorganic materials 0.000 description 1
150000002910 rare earth metals Chemical class 0.000 description 1
239000011435 rock Substances 0.000 description 1
239000003079 shale oil Substances 0.000 description 1
238000010008 shearing Methods 0.000 description 1
229920002545 silicone oil Polymers 0.000 description 1
KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
229940051851 sulfurated lime Drugs 0.000 description 1
239000000725 suspension Substances 0.000 description 1
125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
150000007970 thio esters Chemical class 0.000 description 1
150000003608 titanium Chemical class 0.000 description 1
238000012549 training Methods 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
239000010913 used oil Substances 0.000 description 1
239000012808 vapor phase Substances 0.000 description 1
239000003981 vehicle Substances 0.000 description 1
239000001993 wax Substances 0.000 description 1
239000008096 xylene Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M143/00—Lubricating compositions characterised by the additive being a macromolecular hydrocarbon or such hydrocarbon modified by oxidation
- C10M143/08—Lubricating compositions characterised by the additive being a macromolecular hydrocarbon or such hydrocarbon modified by oxidation containing aliphatic monomer having more than 4 carbon atoms
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M161/00—Lubricating compositions characterised by the additive being a mixture of a macromolecular compound and a non-macromolecular compound, each of these compounds being essential
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/041—Mixtures of base-materials and additives the additives being macromolecular compounds only
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M171/00—Lubricating compositions characterised by purely physical criteria, e.g. containing as base-material, thickener or additive, ingredients which are characterised exclusively by their numerically specified physical properties, i.e. containing ingredients which are physically well-defined but for which the chemical nature is either unspecified or only very vaguely indicated
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/102—Aliphatic fractions
- C10M2203/1025—Aliphatic fractions used as base material
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/024—Propene
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/028—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers containing aliphatic monomers having more than four carbon atoms
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/287—Partial esters
- C10M2207/288—Partial esters containing free carboxyl groups
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
- C10N2020/01—Physico-chemical properties
- C10N2020/04—Molecular weight; Molecular weight distribution
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/02—Pour-point; Viscosity index
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/30—Anti-misting
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/38—Conveyors or chain belts

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Oil, Petroleum & Natural Gas (AREA)
Organic Chemistry (AREA)
Lubricants (AREA)
Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Treating Waste Gases (AREA)

CN93104651A 1991-06-19 1993-03-30 消除含油功能流体形成油雾的方法 Expired - Lifetime CN1033461C (zh)

Priority Applications (11)

Application Number	Priority Date	Filing Date	Title
PCT/US1993/002605 WO1994021760A1 (en)	1991-06-19	1993-03-22	Method of suppressing mist formation from oil-containing functional fluids
DE69307931T DE69307931T2 (de)	1991-06-19	1993-03-22	Verfahren zu unterdrückung der nebelbildung von einzel verwendung schmieröl
BR9307827A BR9307827A (pt)	1991-06-19	1993-03-22	Processo de eliminação de formação de névoa de fluidos funcionais contendo óleo
AT93907626T ATE148494T1 (de)	1991-06-19	1993-03-22	Verfahren zu unterdrückung der nebelbildung von einzel verwendung schmieröl
JP6520971A JPH08512334A (ja)	1991-06-19	1993-03-22	油含有機能液からミスト発生を抑制する方法
ES93907626T ES2098731T3 (es)	1991-06-19	1993-03-22	Metodo para suprimir la formacion de nebulizacion a partir de un aceite lubricante de un solo uso.
AU38161/93A AU671625B2 (en)	1991-06-19	1993-03-22	Method of suppressing mist formation from oil-containing functional fluids
EP93907626A EP0690902B1 (en)	1991-06-19	1993-03-22	Method of suppressing mist formation from single use lubricating oil
CA002156744A CA2156744C (en)	1991-06-19	1993-03-22	Method of suppressing mist formation from oil-containing functional fluids
CN93104651A CN1033461C (zh)	1991-06-19	1993-03-30	消除含油功能流体形成油雾的方法
NO19953727A NO312910B1 (no)	1991-06-19	1995-09-21	Anvendelse av en kopolymer med höy molekylvekt som tilsats til en ±nbruksmöreolje for undertrykkelse av disdannelse

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
US07/717,433 US5227551A (en)	1989-11-19	1991-06-19	Method of suppressing mist formation from oil-containing functional fluids
PCT/US1993/002605 WO1994021760A1 (en)	1991-06-19	1993-03-22	Method of suppressing mist formation from oil-containing functional fluids
CN93104651A CN1033461C (zh)	1991-06-19	1993-03-30	消除含油功能流体形成油雾的方法
US08/061,899 US5329055A (en)	1991-06-19	1993-05-14	Method of suppressing mist formation from oil-containing functional fluids

Publications (2)

Publication Number	Publication Date
CN1093106A CN1093106A (zh)	1994-10-05
CN1033461C true CN1033461C (zh)	1996-12-04

Family

ID=36809251

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CN93104651A Expired - Lifetime CN1033461C (zh)	1991-06-19	1993-03-30	消除含油功能流体形成油雾的方法

Country Status (11)

Country	Link
EP (1)	EP0690902B1 (ja)
JP (1)	JPH08512334A (ja)
CN (1)	CN1033461C (ja)
AT (1)	ATE148494T1 (ja)
AU (1)	AU671625B2 (ja)
BR (1)	BR9307827A (ja)
CA (1)	CA2156744C (ja)
DE (1)	DE69307931T2 (ja)
ES (1)	ES2098731T3 (ja)
NO (1)	NO312910B1 (ja)
WO (1)	WO1994021760A1 (ja)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE19530816A1 (de)	1995-08-23	1997-02-27	Cognis Bio Umwelt	Verwendung von mutierter Subtilisin-Protease in kosmetischen Produkten
JP5170969B2 (ja) *	2006-03-17	2013-03-27	昭和シェル石油株式会社	潤滑油組成物
JP5138965B2 (ja) *	2007-03-30	2013-02-06	三井化学株式会社	潤滑油組成物、ミスト発生抑制剤
WO2012047949A1 (en) *	2010-10-06	2012-04-12	The Lubrizol Corporation	Lubricating oil composition with anti-mist additive
CN106635309A (zh) *	2016-09-21	2017-05-10	广西大学	一种环境友好低速重载防锈抗盐雾开式齿轮齿条传动润滑剂组合物
CN109679756B (zh) *	2019-01-24	2022-01-11	苏州市神顺新晨科技有限公司	一种微乳切削液及其制备方法
CN110628493B (zh) *	2019-10-01	2021-09-21	中科孚迪科技发展有限公司	一种高抗氧化性微量润滑切削油及其制备方法和应用

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3919098A (en) *	1973-11-05	1975-11-11	Chevron Res	Cutting oil of reduced stray fog
CA1059111A (en) *	1974-12-20	1979-07-24	Dominic A. Apikos	Metal working lubricant comprising ethylene copolymers
US4400281A (en) *	1981-08-19	1983-08-23	Atlantic Richfield Co.	Yarn processing lubricants
US5227551A (en) *	1989-11-19	1993-07-13	Exxon Chemical Patents Inc.	Method of suppressing mist formation from oil-containing functional fluids

1993
- 1993-03-22 JP JP6520971A patent/JPH08512334A/ja active Pending
- 1993-03-22 AT AT93907626T patent/ATE148494T1/de active
- 1993-03-22 CA CA002156744A patent/CA2156744C/en not_active Expired - Lifetime
- 1993-03-22 EP EP93907626A patent/EP0690902B1/en not_active Expired - Lifetime
- 1993-03-22 ES ES93907626T patent/ES2098731T3/es not_active Expired - Lifetime
- 1993-03-22 WO PCT/US1993/002605 patent/WO1994021760A1/en not_active Ceased
- 1993-03-22 BR BR9307827A patent/BR9307827A/pt not_active IP Right Cessation
- 1993-03-22 DE DE69307931T patent/DE69307931T2/de not_active Expired - Lifetime
- 1993-03-22 AU AU38161/93A patent/AU671625B2/en not_active Ceased
- 1993-03-30 CN CN93104651A patent/CN1033461C/zh not_active Expired - Lifetime
1995
- 1995-09-21 NO NO19953727A patent/NO312910B1/no unknown

Also Published As

Publication number	Publication date
JPH08512334A (ja)	1996-12-24
ATE148494T1 (de)	1997-02-15
AU671625B2 (en)	1996-09-05
EP0690902B1 (en)	1997-01-29
CA2156744A1 (en)	1994-09-29
NO953727L (no)	1995-09-21
NO953727D0 (no)	1995-09-21
BR9307827A (pt)	1995-11-14
NO312910B1 (no)	2002-07-15
ES2098731T3 (es)	1997-05-01
WO1994021760A1 (en)	1994-09-29
DE69307931D1 (de)	1997-03-13
CA2156744C (en)	2002-11-12
CN1093106A (zh)	1994-10-05
EP0690902A1 (en)	1996-01-10
AU3816193A (en)	1994-10-11
DE69307931T2 (de)	1997-05-15

Legal Events

Date	Code	Title	Description
1994-10-05	C06	Publication
1994-10-05	PB01	Publication
1995-07-26	C10	Entry into substantive examination
1995-07-26	SE01	Entry into force of request for substantive examination
1996-12-04	C14	Grant of patent or utility model
1996-12-04	GR01	Patent grant
2013-05-15	C17	Cessation of patent right
2013-05-15	CX01	Expiry of patent term	Expiration termination date: 20130330 Granted publication date: 19961204

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