CN103409959B - A kind of method of Tencel elastic force BLENDED FABRIC three-prevention finishing - Google Patents
A kind of method of Tencel elastic force BLENDED FABRIC three-prevention finishing Download PDFInfo
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- CN103409959B CN103409959B CN201310384130.5A CN201310384130A CN103409959B CN 103409959 B CN103409959 B CN 103409959B CN 201310384130 A CN201310384130 A CN 201310384130A CN 103409959 B CN103409959 B CN 103409959B
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- 239000002689 soil Substances 0.000 claims abstract description 22
- 230000001737 promoting effect Effects 0.000 claims abstract description 18
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 17
- 239000000460 chlorine Substances 0.000 claims abstract description 17
- 238000007730 finishing process Methods 0.000 claims abstract description 4
- 229920000570 polyether Polymers 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 229920002545 silicone oil Polymers 0.000 claims description 2
- 238000005406 washing Methods 0.000 abstract description 27
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- 238000002203 pretreatment Methods 0.000 abstract description 4
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- 239000004753 textile Substances 0.000 abstract description 2
- 230000002421 anti-septic effect Effects 0.000 description 17
- 238000005202 decontamination Methods 0.000 description 15
- 230000003588 decontaminative effect Effects 0.000 description 15
- 238000004043 dyeing Methods 0.000 description 11
- 239000000835 fiber Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000004519 grease Substances 0.000 description 5
- 238000009992 mercerising Methods 0.000 description 5
- 238000010186 staining Methods 0.000 description 5
- 230000007306 turnover Effects 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000000675 fabric finishing Substances 0.000 description 3
- 238000009962 finishing (textile) Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 230000006872 improvement Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- -1 perfluoro Chemical group 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 208000001300 Perinatal Death Diseases 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- 240000006413 Prunus persica var. persica Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
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- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- VQKFNUFAXTZWDK-UHFFFAOYSA-N alpha-methylfuran Natural products CC1=CC=CO1 VQKFNUFAXTZWDK-UHFFFAOYSA-N 0.000 description 1
- 230000003373 anti-fouling effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
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- 230000018044 dehydration Effects 0.000 description 1
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- 239000003599 detergent Substances 0.000 description 1
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- 238000011156 evaluation Methods 0.000 description 1
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- 230000002045 lasting effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
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- 210000002345 respiratory system Anatomy 0.000 description 1
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- GOLXNESZZPUPJE-UHFFFAOYSA-N spiromesifen Chemical compound CC1=CC(C)=CC(C)=C1C(C(O1)=O)=C(OC(=O)CC(C)(C)C)C11CCCC1 GOLXNESZZPUPJE-UHFFFAOYSA-N 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
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Abstract
The invention belongs to textile technology field, be specifically related to a kind of production method of Tencel elastic force BLENDED FABRIC.A kind of method of Tencel elastic force BLENDED FABRIC three-prevention finishing, it is characterized in that, in three-prevention finishing process, add softener 3305:5-20g/L, chlorine-resistant washes promoting agent: 20-40g/L, finishing agent CP-SLA:10-30g/L, finishing agent 7713:10-30g/L, soil-releasing finishing agent: CP-R:10-30g/L, promoting agent: LK-30:1-20g/L.Adopt method of the present invention to Tencel strong elastic BLENDED FABRIC three-prevention finishing, in the pre-treatment process of Tencel, adjustment three-prevention finishing and decontaminable consumption, strengthen the performance of Tencel; Adopt the Tencel after method process of the present invention also to have good soil release performance, also have good soil release performance to the heavy oil being difficult to wash away, and still have good soil release performance after washing 50 times, washing resistance is superior.
Description
Technical field
The invention belongs to textile technology field, be specifically related to a kind of production method of Tencel elastic force BLENDED FABRIC.
Background technology
Tencel fiber is the woody pulp based on coniferous tree is raw material, with the new cellulosic of solvent-spinning method explained hereafter, this fiber is by the reproduction strictly according to the facts of the natural characteristic of wooden pulp, and its molecule is simple carbohydrate, fiber naturally can return the earth, and Biodegradable is good.
Tencel fiber has natural fabric and synthetic fiber advantage separately, and not only moisture absorption is breathed freely, powerful good, and it is bright-coloured to paint, and fabric fall is splendid, and have peach face effect and silk style, feel is soft and smooth, and its manufactured goods have higher added value.
Tencel fiber can interweave with other fiber blend, produces the weaving face fabric with individual style.
Namely fabric three-prevention finishing, three anti-refuse water, refuse oil, soil-repellent finishing, is on fabric, apply one or several finishing agents, changes the surface property of fabric, make fabric not easily by water and common greasy dirt soak or stain.Its purposes is as the coat, wind coat, jacket, leisure wear etc. of high-end women and man, various protective clothing is as oil field Work Clothes, mine Work Clothes, fire-entry suit (with flame-proof treatment compound) and special uniform etc., and high-grade dinner cloth, molten curtain and light-duty fluffy account etc.Fluorinated fabric finishing agent, particularly perfluoro capryl sulfonyl compound (PFOS) fabric finishing agent, because having excellent hydrophobic and lyophobic property, gas permeability, and washable, antifouling and soil release performance energy, occupy an important position in fabric finishing industry.
But research finds, PFOS is also that one is very lasting simultaneously, and biological accumulation and poisonous chemicals, not only can cause respiratory system to injure, cause neonatal death, and be distributed in blood and liver, is difficult to by metabolism and decomposes.Swedish government issues circular on July 6th, 2005, and regulation PFOS is prohibited from entering Sweden market with the material that can be degraded to PFOS, and European Union's meeting is passed through the sale of suggestion PFOS on October 25th, 2006 and used restriction.According to international environmental science scholarly forecast, will limit use in the world containing the surfactant of PFOS and finishing agent within 5 years, until forbid completely, therefore, various countries researcher expands the tide of PFOS substitute research.
Fabric three-proof finishing agent is comparatively large for fabric impact, therefore researchs and develops three-proof finishing agent, uses suitable three-proof finishing agent to act on fabric, has very important effect for the performance improving fabric.
But in the dyeing and finishing technology of the weaving of tencel fiber or Tencel, it is not alkaline-resisting that the pre-treatment common process of Tencel easily produces broken hole sky silk, cotton alkaline-resisting, and the effect that soil-releasing finiss and water-proof finish two kinds of this modes will reach is difficult to find equalization point, difficult realization, therefore needs the old process of change pre-treatment and adjusts the three-prevention finishing consumption different with easy decontamination, making it to reach intermediate equilibria point, Final finishing two leaching methods solve padding of 8 kinds of auxiliary agents, thus reach its medical performance.
Summary of the invention
In order to solve above-mentioned technical problem, the invention provides a kind of alkaline-resisting and method of the Tencel elastic force BLENDED FABRIC three-prevention finishing of soil-releasing finiss.
The present invention is realized by following technical scheme:
A kind of method of Tencel elastic force BLENDED FABRIC three-prevention finishing, the feature of the method is, adds softener 3305:5-20g/L, chlorine-resistant washes promoting agent: 20-40g/L, finishing agent CP-SLA: 10-30g/L, finishing agent 7713:10-30g/L, soil-releasing finishing agent: CP-R:10-30g/L, promoting agent: LK-30:1-20g/L in three-prevention finishing process.
Antiseptic A:5-30g/L, antiseptic B:5-30g/L is also added in three-prevention finishing process.
Concrete, the method for above-mentioned Tencel elastic force BLENDED FABRIC three-prevention finishing, comprises following step:
Turn over seam → bound edge → contracting width → cylinder chlorine drift ice of singing → roll up wash → dry → shape → mercerising → dyeing → Final finishing roll antibacterially → rear wholely roll three anti-easy decontaminations, chlorine-resistant floats → bakes interlinkage → preshrunk;
After staining procedure, product clot;
After dyeing, cropping temperature is less than 50 degree, and above rolls up immediately, and upper volume temperature 120-130 degree, the speed of a motor vehicle 60 ms/min, fabric width: 132-133CM, clot internal layer shield 50 meters, main purpose prevents the backfin falling into cloth car.
Described Final finishing rolls in aseptic procedures:
Add antiseptic A:5-30g/L and antiseptic B:5-30g/L;
Described rear wholely roll in three anti-easy decontamination steps:
Add finishing agent CP-SLA: 10-30g/L, finishing agent 7713:10-30g/L, soil-releasing finishing agent: CP-R:10-30g/L, promoting agent: LK-30:1-20g/L; Softener 3305:5-20g/L; The pH value of regulator solution is transferred between 5-6;
Described bakes in interlinkage step: bake 2 minutes at 140-180 DEG C.
The addition of above-mentioned various materials is respectively:
Add antiseptic A:15g/L and antiseptic B:15g/L; Add finishing agent CP-SLA: 20g/L, finishing agent 7713:20g/L, soil-releasing finishing agent: CP-R:20g/L, promoting agent: LK-30:30g/L, softener 3305:10g/L.
Softener is: any one in softener 3305, polyethers amino modified hydrophilic silicone oil.
It is DFC-39 that chlorine-resistant washes promoting agent.
Soil-releasing finishing agent is CP-R.
Antiseptic B adhesive.
In raw material of the present invention, three-proof finishing agent: CP-SLA, lays particular emphasis on waterproof, has grease proofing effect concurrently;
Three-proof finishing agent: 7713, lays particular emphasis on grease proofing, has waterproof effect concurrently;
The catalyst of CP-SLA, can improve the washable effect of repeatedly washing.
Beneficial effect of the present invention is, adopts method of the present invention to Tencel strong elastic BLENDED FABRIC three-prevention finishing, and in the pre-treatment process of Tencel, adjustment three-prevention finishing and decontaminable consumption, strengthen the performance of Tencel; Adopt the Tencel after method process of the present invention also to have good soil release performance, also have good soil release performance to the heavy oil being difficult to wash away, and still have good soil release performance after washing 50 times, washing resistance is superior.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, so that those skilled in the art more understands the present invention, but does not therefore limit the present invention.
Embodiment 1
This Collator Mode contains antiseptic A15g/L, antiseptic B:15g/L, three-proof finishing agent: CP-SLA: 20g/L three-proof finishing agent 7713: 20g/L soil-releasing finishing agent: CP-R:20g/L;
Chlorine-resistant washes promoting agent: 30g/L
Promoting agent LK-30:10g/L
Softener 3305:10g/L
First material cylinder water is added to 300L, open mixer 1000r/min first to add softener 3305 10g/L → chlorine-resistant and wash promoting agent 30g/L → three-proof finishing agent CP-SLA:20g/L → three-proof finishing agent 7713:20g/L → soil-releasing finishing agent CP-R:20g/L → promoting agent LK-30: 10g/L and often prop up and to need upper material stirring 1 minute before material adds, finally add water down 500L, is transferred between 5-6 by solution ph.
Roll material to dry
Temperature 160 DEG C makes cloth cover finishing agent and fiber fully react for 2 minutes, thus reaches requirement index.
Before Tencel elastic force process change with after index contrast:
TEN 55/C45 40*32+40D 230*80 is golden
Index before improvement:
Waterproof (before washing) 3 grades (after washing): 2.5 grades
Grease proofing (before washing) 3 grades (after washing) 2 grades
Easy decontamination (before washing) 3 grades (after washing) 2 grades
Index after improvement:
Waterproof (before washing) 4 grades (after washing): 3 grades
Grease proofing (before washing) 4 grades (after washing) 3 grades
Easy decontamination (before washing) 4 grades (after washing) 3 grades
By above arrangement
Pass through: notary test meets the requirements of the Work Clothes that finishing functions can make hospital, school.
Embodiment 2
Turn over seam → bound edge → contracting width → cylinder chlorine drift ice of singing → roll up wash → dry → shape → mercerising → dyeing → Final finishing roll antibacterially → rear wholely roll three anti-easy decontaminations, chlorine-resistant floats → bakes interlinkage → preshrunk;
After described staining procedure, product clot;
After dyeing, cropping temperature is less than 50 DEG C, and above rolls up immediately, upper volume temperature 120-130 DEG C, the speed of a motor vehicle 60 ms/min, fabric width: 132-133CM, clot internal layer shield 50 meters;
Described Final finishing rolls in aseptic procedures:
Add antiseptic A:20g/L and antiseptic B:20g/L;
Described rear wholely roll in three anti-easy decontamination steps:
Add finishing agent CP-SLA: 20g/L, finishing agent 7713:20g/L, soil-releasing finishing agent: CP-R:20g/L, promoting agent: LK-30:12g/L; Softener 3305:12g/L; The pH value of regulator solution is 5.5;
Described bakes in interlinkage step: bake 2 minutes at 150 DEG C.
Heavy oil soil release performance is tested
Choose the test film that 4 block sizes are identical, this test film is Tencel fabric, and wherein 1 piece is pollution judgement code test sheet;
Placed on a glass by test film, heavy oil is dropped in the central authorities of test film, put glass plate in the above, the load imposing 2N places 1 minute;
Removing load and glass plate, move on to soft tissue in filter paper upper cover by test film, from rollably wiping greasy dirt away above, place more than 24 hours, air dry under level;
The change of the color of test film and code test sheet after polluting, compares with pollution gray scale the grade distinguishing pollution level, represents with the mean value of 3 pieces:
Continue the alkalescent synthesis of detergent liquid 25L putting into 40 DEG C in the sink of full-automatic or 2 machine sylvan life slot types, put into test film 2 pieces and load cloth after the pollution of weight 500 grams altogether, carry out washing in 5 minutes by the strong condition of rinsing maching;
Washing 2 minutes after dehydration in 30 seconds, repeatedly this operation 2 times;
Do not twist dry taking-up test film, press gently with filter paper and anhydrate, air dry under level;
The change color of the test film after washing and code test sheet, compares with pollution grey packet card the grade distinguishing washability, represents with the mean value of 3 pieces.
In embodiment 2, easy decontamination (before washing) 4 grades (after washing) 3 grades
Waterproof (before washing) 4 grades (after washing): 3 grades
Grease proofing (before washing) 4 grades (after washing) 3 grades.
Tencel, after washing 50 times, goes up heavy oil, adopts its easy decontamination grade of above-mentioned method evaluation, washs first 4 grades, wash latter 3 grades.
Embodiment 3
Turn over seam → bound edge → contracting width → cylinder chlorine drift ice of singing → roll up wash → dry → shape → mercerising → dyeing → Final finishing roll antibacterially → rear wholely roll three anti-easy decontaminations, chlorine-resistant floats → bakes interlinkage → preshrunk;
After described staining procedure, product clot;
After dyeing, cropping temperature is less than 50 DEG C, and above rolls up immediately, upper volume temperature 120-130 DEG C, the speed of a motor vehicle 60 ms/min, fabric width: 132-133CM, clot internal layer shield 50 meters;
Described Final finishing rolls in aseptic procedures:
Add antiseptic A:20g/L and antiseptic B:20g/L;
Described rear wholely roll in three anti-easy decontamination steps:
Add finishing agent CP-SLA: 10g/L, finishing agent 7713:10g/L, soil-releasing finishing agent: CP-R:10g/L, promoting agent: LK-30:12g/L; Softener 3305:5g/L; The pH value of regulator solution is 5;
Described bakes in interlinkage step: bake 2 minutes at 140 DEG C.
Embodiment 4
Turn over seam → bound edge → contracting width → cylinder chlorine drift ice of singing → roll up wash → dry → shape → mercerising → dyeing → Final finishing roll antibacterially → rear wholely roll three anti-easy decontaminations, chlorine-resistant floats → bakes interlinkage → preshrunk;
After described staining procedure, product clot;
After dyeing, cropping temperature is less than 50 DEG C, and above rolls up immediately, upper volume temperature 120-130 DEG C, the speed of a motor vehicle 60 ms/min, fabric width: 132-133CM, clot internal layer shield 50 meters;
Described Final finishing rolls in aseptic procedures:
Add antiseptic A:20g/L and antiseptic B:20g/L;
Described rear wholely roll in three anti-easy decontamination steps:
Add finishing agent CP-SLA: 30g/L, finishing agent 7713:30g/L, soil-releasing finishing agent: CP-R:30g/L, promoting agent: LK-30:20g/L; Softener 3305:20g/L; The pH value of regulator solution is 6;
Described bakes in interlinkage step: bake 2 minutes at 140 DEG C.
Embodiment 5
Turn over seam → bound edge → contracting width → cylinder chlorine drift ice of singing → roll up wash → dry → shape → mercerising → dyeing → Final finishing roll antibacterially → rear wholely roll three anti-easy decontaminations, chlorine-resistant floats → bakes interlinkage → preshrunk;
After described staining procedure, product clot;
After dyeing, cropping temperature is less than 50 DEG C, and above rolls up immediately, upper volume temperature about 125 DEG C, the speed of a motor vehicle 60 ms/min, fabric width: 132-133CM, clot internal layer shield 50 meters;
Described Final finishing rolls in aseptic procedures:
Add antiseptic A:15g/L and antiseptic B:15g/L;
Described rear wholely roll in three anti-easy decontamination steps:
Add finishing agent CP-SLA: 20g/L, finishing agent 7713:20g/L, soil-releasing finishing agent: CP-R:20g/L, promoting agent: LK-30:20g/L; Softener 3305:15g/L; The pH value of regulator solution is 6;
Described bakes in interlinkage step: bake 2 minutes at 140 DEG C.
Claims (3)
1. the method for a Tencel elastic force BLENDED FABRIC three-prevention finishing, it is characterized in that, in three-prevention finishing process, add softener 3305:5-20g/L, chlorine-resistant washes promoting agent: 20-40g/L, finishing agent CP-SLA: 10-30g/L, finishing agent 7713:10-30g/L, soil-releasing finishing agent: CP-R:10-30g/L, promoting agent: LK-30:1-20g/L.
2. the method for a kind of Tencel elastic force BLENDED FABRIC three-prevention finishing as claimed in claim 1, it is characterized in that, softener is polyethers amino modified hydrophilic silicone oil.
3. the method for a kind of Tencel elastic force BLENDED FABRIC three-prevention finishing as claimed in claim 1, it is characterized in that, it is DFC-39 that described chlorine-resistant washes promoting agent.
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| CN105568696B (en) * | 2014-10-31 | 2018-05-04 | 南通大学 | The preparation method of nano silver three-protection anti-microbial finishing agent |
| CN104674575A (en) * | 2015-02-15 | 2015-06-03 | 浙江兆新织造有限公司 | Novel three-prevention, easy-stain-removal and super-soft-comfortable shell fabric for throw pillow |
| CN107447327A (en) * | 2017-09-06 | 2017-12-08 | 四川航天系统工程研究所 | Space flight special type antibacterial and mouldproof fiber cloth based on chitin fiber and preparation method thereof |
| CN107794790A (en) * | 2017-11-10 | 2018-03-13 | 新乡市新科防护科技有限公司 | A kind of method for improving waterproof polyester-cotton fabric color fastness |
| CN113774684B (en) * | 2021-10-08 | 2024-04-05 | 华纺股份有限公司 | Preparation method of polyester-cotton blended weft double-covered elastic fabric |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1614129A (en) * | 2003-11-05 | 2005-05-11 | 北京中科安康医疗用品有限公司 | Bactericidal and anti-virus fabrics and its production and garment for patients therefrom |
| CN101715499A (en) * | 2007-04-17 | 2010-05-26 | 海克原料股份公司 | Water-, oil-, and dirt-repellent finishes on fibers and textile fabrics |
| CN102465403A (en) * | 2011-06-09 | 2012-05-23 | 上海嘉乐股份有限公司 | New finishing process of copolymerization fluorine antifouling easy-to-clean finishing liquid |
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2013
- 2013-08-29 CN CN201310384130.5A patent/CN103409959B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1614129A (en) * | 2003-11-05 | 2005-05-11 | 北京中科安康医疗用品有限公司 | Bactericidal and anti-virus fabrics and its production and garment for patients therefrom |
| CN101715499A (en) * | 2007-04-17 | 2010-05-26 | 海克原料股份公司 | Water-, oil-, and dirt-repellent finishes on fibers and textile fabrics |
| CN102465403A (en) * | 2011-06-09 | 2012-05-23 | 上海嘉乐股份有限公司 | New finishing process of copolymerization fluorine antifouling easy-to-clean finishing liquid |
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