CN103835126A - Novel mildew preventive for textile, and preparation method thereof - Google Patents
Novel mildew preventive for textile, and preparation method thereof Download PDFInfo
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- CN103835126A CN103835126A CN201310671046.1A CN201310671046A CN103835126A CN 103835126 A CN103835126 A CN 103835126A CN 201310671046 A CN201310671046 A CN 201310671046A CN 103835126 A CN103835126 A CN 103835126A
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- textiles
- smilax
- benzoic acid
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- 239000004753 textile Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 230000003449 preventive effect Effects 0.000 title 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 22
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000005711 Benzoic acid Substances 0.000 claims abstract description 11
- 235000010233 benzoic acid Nutrition 0.000 claims abstract description 11
- 235000019260 propionic acid Nutrition 0.000 claims abstract description 11
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims abstract description 11
- XEFQLINVKFYRCS-UHFFFAOYSA-N Triclosan Chemical compound OC1=CC(Cl)=CC=C1OC1=CC=C(Cl)C=C1Cl XEFQLINVKFYRCS-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229960003500 triclosan Drugs 0.000 claims abstract description 7
- 241000362909 Smilax <beetle> Species 0.000 claims abstract description 6
- 239000000126 substance Substances 0.000 claims abstract description 3
- 241000110847 Kochia Species 0.000 claims abstract 3
- 239000003429 antifungal agent Substances 0.000 claims abstract 3
- 229940121375 antifungal agent Drugs 0.000 claims abstract 3
- 241000304195 Salvia miltiorrhiza Species 0.000 claims abstract 2
- 235000011135 Salvia miltiorrhiza Nutrition 0.000 claims abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 10
- 235000004347 Perilla Nutrition 0.000 claims description 9
- 230000008569 process Effects 0.000 claims description 7
- 241000605422 Asparagus asparagoides Species 0.000 claims description 5
- 235000010894 Artemisia argyi Nutrition 0.000 claims 1
- 241001435059 Artemisia argyi Species 0.000 claims 1
- 241000037740 Coptis chinensis Species 0.000 claims 1
- 244000124853 Perilla frutescens Species 0.000 claims 1
- 241001072909 Salvia Species 0.000 claims 1
- 235000017276 Salvia Nutrition 0.000 claims 1
- 240000000513 Santalum album Species 0.000 claims 1
- 235000008632 Santalum album Nutrition 0.000 claims 1
- 238000007654 immersion Methods 0.000 claims 1
- 238000002791 soaking Methods 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 230000007613 environmental effect Effects 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 239000003814 drug Substances 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract description 2
- 230000035699 permeability Effects 0.000 abstract description 2
- 240000003870 Ageratum houstonianum Species 0.000 abstract 1
- 241000737241 Cocos Species 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 abstract 1
- 238000005260 corrosion Methods 0.000 abstract 1
- OEYQBKYISMRWQB-UHFFFAOYSA-N Santal Chemical compound C=1C(OC)=CC(O)=C(C2=O)C=1OC=C2C1=CC=C(O)C(O)=C1 OEYQBKYISMRWQB-UHFFFAOYSA-N 0.000 description 16
- 240000004510 Agastache rugosa Species 0.000 description 8
- 240000001851 Artemisia dracunculus Species 0.000 description 8
- 235000003092 Artemisia dracunculus Nutrition 0.000 description 8
- 241001645380 Bassia scoparia Species 0.000 description 8
- 244000247747 Coptis groenlandica Species 0.000 description 8
- 235000002991 Coptis groenlandica Nutrition 0.000 description 8
- 241000229722 Perilla <angiosperm> Species 0.000 description 8
- 240000007164 Salvia officinalis Species 0.000 description 8
- 241001671204 Stemona Species 0.000 description 8
- 235000013399 edible fruits Nutrition 0.000 description 8
- 235000005412 red sage Nutrition 0.000 description 8
- 239000003112 inhibitor Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 230000002421 anti-septic effect Effects 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 230000002070 germicidal effect Effects 0.000 description 4
- 238000009413 insulation Methods 0.000 description 4
- 239000004744 fabric Substances 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 241000628997 Flos Species 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 229920002972 Acrylic fiber Polymers 0.000 description 1
- 241000255789 Bombyx mori Species 0.000 description 1
- 229910000906 Bronze Inorganic materials 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 229920002978 Vinylon Polymers 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000010974 bronze Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 210000004209 hair Anatomy 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明提供了一种纺织品新型防霉剂及其制备方法，由以下重量份的物质制备而成：丹参 0.1-0.5份，黄芬 0.2-0.6份；地肤子 0.3-0.7份；黄连 0.1-0.5份；百部0.8-1.5份；白藿香 0.4-0.9份；土茯苓 1.2-1.8份；科子0.5-1.5份；紫苏0.1-1.0份；艾叶0.5-1.5份；檀香 0.7-1.4份；丙酸8.5-12.5份；三氯新5-10份；苯甲酸 8-15份。本发明防霉效果好，且成本低、安全环保。其包含有中药成分绿色安全，对纺织品无腐蚀无损伤，能使纺织品保持干燥和良好透气性，且能持久均匀地作用，综合性能好，适于工业化应用。The invention provides a novel antifungal agent for textiles and a preparation method thereof, which is prepared from the following substances in parts by weight: 0.1-0.5 parts of Salvia miltiorrhiza, 0.2-0.6 parts of Huangfen; 0.3-0.7 parts of Kochia chinensis; 0.5 parts; 0.8-1.5 parts of Baibu; 0.4-0.9 parts of white ageratum; 1.2-1.8 parts of Smilax cocos; 8.5-12.5 parts of propionic acid; 5-10 parts of triclosan; 8-15 parts of benzoic acid. The invention has good anti-mildew effect, low cost, safety and environmental protection. It contains green and safe traditional Chinese medicine ingredients, has no corrosion and no damage to textiles, can keep textiles dry and has good air permeability, and can act persistently and evenly. It has good comprehensive performance and is suitable for industrial applications.
Description
Technical field
The present invention relates to a kind of textiles New Type Antiseptic Germicide and preparation method thereof.
Background technology
Textiles has long history.As far back as the Stone Age southern Europe just there is linen, to the Bronze Age, Northern Europe has produced wool fabric.China is world-famous silk big country, and before several thousand, just having breeds silkworms controls an industry, and many ancient tombs, the silk goods that ancient site is unearthed are exactly best witness
.in ruins, there is large quantities of silk goods and silk in the Neolithic Age (being equivalent to the Shang dynasty) of excavating out at Wu County, Zhejiang.To the Zhou Dynasty, existing a large amount of literature records about silk thing.No. 1, Mawangdui, Changsha tomb of Han dynasty is especially for we have opened one underground " silk treasure-house " silk such as a large amount of intact thin,tough silk, yarn, sieve, figured woven silk material, silk floss, fluffing silk floss, embroidery, the burlap linen fabrics that have been unearthed.Textiles is of a great variety, and except the artificial synthetic fiber who occurred modern age, the textiles in ancient times mainly contains silk goods, woolen knitwear, cotton goods and the linen fabrics.Front two generic animal fibers, rear two generic strings.Textiles is the organic substance by atomic buildings such as carbon, hydrogen, oxygen, nitrogen; in moist, warm, improper ventilation, light irradiation and oxidizing atmosphere, be easy to occur oxidation reaction and hydrolysis; cause its rot mouldy, lose intensity, therefore particularly important to the mildew-resistant protection of textiles.
Along with social development, the raising of economic level, large-scale light industry enterprise particularly textile enterprise's quantity rolls up.Textiles is various in style, and majority easily goes mouldy, as cotton, fiber crops, hair, vinylon, nylon, acrylic fibers spray silk etc.Thereby the storage of textile product and raw material also becomes a difficult problem for these enterprises.For the control that textile product goes mouldy, many factories have to strengthen expect that from former product processes the administration of health of whole process.But under many circumstances, control the initial contaminant capacity of microorganism or arrange that all environmental conditions that is unfavorable for growth of microorganism normally can not accomplish, also need to use mould inhibitor to control the pollution and harm of microorganism to production environment, material, product.
Along with, the enhancing of people's environmental consciousness, the effect cheaply of studying a kind of environmental protection significantly mould inhibitor becomes important topic.
Summary of the invention
The invention provides a kind of textiles New Type Antiseptic Germicide and preparation method thereof.
The present invention is achieved in that a kind of textiles New Type Antiseptic Germicide, is prepared from by the material of following weight portion: red sage root 0.1-0.5 part, Huang Fen 0.2-0.6 part; Fruit of summer cypress 0.3-0.7 part; Coptis 0.1-0.5 part; Tuber of stemona 0.8-1.5 part; White wrinkled giant hyssop 0.4-0.9 part; Smilax 1.2-1.8 part; The sub-0.5-1.5 part of section; Purple perilla 0.1-1.0 part; Tarragon 0.5-1.5 part; Santal 0.7-1.4 part; Propionic acid 8.5-12.5 part; Triclosan 5-10 part; Benzoic acid 8-15 part; Water 15-30 part.
The method of preparing mould inhibitor as claimed in claim 1, is characterized in that, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, cold water soak, pulverizes;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation;
C) by B) in the mixture that obtains dry, cooling.
Preferably, A) described in the cold water soak time be 120-140min.
Preferably, A) described in cold water temperature be 8-10 DEG C.
Preferably, B) in temperature retention time be 130-160min.
Advantage of the present invention is:
Anti-mold effect of the present invention is good, and cost is low, safety and environmental protection.It includes traditional Chinese medicine ingredients green safety, to the corrosion-free not damaged of textiles, can make textiles keep dry and fine air permeability, and can act on equably lastingly, and good combination property, is suitable for industrial applications.
Detailed description of the invention
Embodiment 1
Prepare the material of following weight portion: 0.1 part of the red sage root, 0.2 part of Huang Fen; 0.3 part of the fruit of summer cypress; 0.1 part of the coptis; 0.8 part of the tuber of stemona; 0.4 part of white wrinkled giant hyssop; 1.2 parts of smilaxs; 0.5 part of section's; 0.1 part of purple perilla; 0.5 part of tarragon; 0.7 part, santal; 8.5 parts of propionic acid; 5 parts of triclosans; 8 parts, benzoic acid; 15 parts, water.
The method of the mould inhibitor described in preparation, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation 130-160min;
C) by B) in the mixture that obtains dry, cooling.
Embodiment 2
Prepare the material of following weight portion: 0.3 part of the red sage root, 0.5 part of Huang Fen; 0.5 part of the fruit of summer cypress; 0.4 part of the coptis; 1.0 parts of the tubers of stemona; 0.6 part of white wrinkled giant hyssop; 1.5 parts of smilaxs; 1.0 parts of section's; 0.8 part of purple perilla; 1.0 parts of tarragons; 1.0 parts, santal; 10 parts of propionic acid; 7 parts of triclosans; 10 parts, benzoic acid; 25 parts, water.
The method of the mould inhibitor described in preparation, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation 130-160min;
C) by B) in the mixture that obtains dry, cooling.
Embodiment 3
Prepare the material of following weight portion: 0.5 part of the red sage root, 0.6 part of Huang Fen; 0.7 part of the fruit of summer cypress; 0.5 part of the coptis; 1.5 parts of the tubers of stemona; 0.9 part of white wrinkled giant hyssop; 1.8 parts of smilaxs; 1.5 parts of section's; 1.0 parts of purple perillas; 1.5 parts of tarragons; 1.4 parts, santal; 12.5 parts of propionic acid; 10 parts of triclosans; 15 parts, benzoic acid; 30 parts, water.
The method of the mould inhibitor described in preparation, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation 130-160min;
C) by B) in the mixture that obtains dry, cooling.
Finally it should be noted that: above embodiment is only in order to illustrate the present invention and unrestricted technical scheme described in the invention; Therefore, although this description has been described in detail the present invention with reference to each above-mentioned embodiment,, those of ordinary skill in the art should be appreciated that still and can modify or be equal to replacement the present invention; And all do not depart from technical scheme and the improvement thereof of invention spirit and scope, it all should be encompassed in the middle of claim scope of the present invention.
Claims (5)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310671046.1A CN103835126B (en) | 2013-12-12 | 2013-12-12 | A kind of anti-mildew agent for textiles and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310671046.1A CN103835126B (en) | 2013-12-12 | 2013-12-12 | A kind of anti-mildew agent for textiles and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
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| CN103835126A true CN103835126A (en) | 2014-06-04 |
| CN103835126B CN103835126B (en) | 2016-08-17 |
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| CN201310671046.1A Expired - Fee Related CN103835126B (en) | 2013-12-12 | 2013-12-12 | A kind of anti-mildew agent for textiles and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104389169A (en) * | 2014-11-18 | 2015-03-04 | 太仓市宏亿化纤有限公司 | Mildew preventive used for textiles and preparation method thereof |
| CN105274835A (en) * | 2015-12-01 | 2016-01-27 | 江苏太林纺织品有限公司 | Grey fabric |
| CN105369603A (en) * | 2015-12-22 | 2016-03-02 | 常熟市泽众家用纺织品有限公司 | Pillow interior fabric |
| CN105401436A (en) * | 2015-12-18 | 2016-03-16 | 苏州富美纺织科技有限公司 | Preparation method for flame-retardation finishing liquid for fabrics |
| CN105401439A (en) * | 2015-12-24 | 2016-03-16 | 常熟市馨格家纺有限公司 | Lambwool fabric |
| CN106351001A (en) * | 2016-08-26 | 2017-01-25 | 相里海霞 | Method for manufacturing ultraviolet-proof textile fabric based on moxa |
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| JPS5641257A (en) * | 1979-09-08 | 1981-04-17 | Nissan Chem Ind Ltd | Industrial antifungal agent |
| CN101077079A (en) * | 2006-05-25 | 2007-11-28 | 西安格润森生物制药股份有限公司 | Plant-type antibacterial agent |
| CN101215781A (en) * | 2007-12-27 | 2008-07-09 | 浙江嘉得莱有限公司 | Chinese herbal medicine antibiotic finishing method for knitting plus material |
| CN102071573A (en) * | 2009-11-20 | 2011-05-25 | 戚冬梅 | Anti-mildew agent for textiles |
| CN102310966A (en) * | 2010-07-01 | 2012-01-11 | 郑州大学 | Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof |
| CN102561029A (en) * | 2010-12-15 | 2012-07-11 | 戚冬梅 | Mildew-proof agent for textile |
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2013
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| JPS5641257A (en) * | 1979-09-08 | 1981-04-17 | Nissan Chem Ind Ltd | Industrial antifungal agent |
| CN101077079A (en) * | 2006-05-25 | 2007-11-28 | 西安格润森生物制药股份有限公司 | Plant-type antibacterial agent |
| CN101215781A (en) * | 2007-12-27 | 2008-07-09 | 浙江嘉得莱有限公司 | Chinese herbal medicine antibiotic finishing method for knitting plus material |
| CN102071573A (en) * | 2009-11-20 | 2011-05-25 | 戚冬梅 | Anti-mildew agent for textiles |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104389169A (en) * | 2014-11-18 | 2015-03-04 | 太仓市宏亿化纤有限公司 | Mildew preventive used for textiles and preparation method thereof |
| CN105274835A (en) * | 2015-12-01 | 2016-01-27 | 江苏太林纺织品有限公司 | Grey fabric |
| CN105401436A (en) * | 2015-12-18 | 2016-03-16 | 苏州富美纺织科技有限公司 | Preparation method for flame-retardation finishing liquid for fabrics |
| CN105369603A (en) * | 2015-12-22 | 2016-03-02 | 常熟市泽众家用纺织品有限公司 | Pillow interior fabric |
| CN105401439A (en) * | 2015-12-24 | 2016-03-16 | 常熟市馨格家纺有限公司 | Lambwool fabric |
| CN106351001A (en) * | 2016-08-26 | 2017-01-25 | 相里海霞 | Method for manufacturing ultraviolet-proof textile fabric based on moxa |
Also Published As
| Publication number | Publication date |
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| CN103835126B (en) | 2016-08-17 |
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Inventor after: Shi Hongsheng Inventor after: Ma Ningning Inventor after: Li Zhengrong Inventor before: Li Benming |
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Effective date of registration: 20170504 Address after: 528400 Guangdong province Zhongshan City Triangle Town Hing Road No. 18 first floor Patentee after: ZHONGSHAN ZHONGKE CHEMICAL Co.,Ltd. Address before: Room 2, building 158, Haier Road, Laoshan District, Shandong, Qingdao, 266061 Patentee before: QINGDAO WUWEI THERMAL INSULATION MATERIAL Co.,Ltd. |
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Effective date of registration: 20220329 Address after: 528437 room H40, building 7, Rhine garden, Ligang City, Torch Development Zone, Zhongshan City, Guangdong Province Patentee after: Wang Weixia Address before: 528400 first floor, No. 18, Tongxing Road, Sanjiao Town, Zhongshan City, Guangdong Province Patentee before: ZHONGSHAN ZHONGKE CHEMICAL Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160817 |