CN104179006A - Mould inhibitor for nylon fabric - Google Patents
Mould inhibitor for nylon fabric Download PDFInfo
- Publication number
- CN104179006A CN104179006A CN201410423580.5A CN201410423580A CN104179006A CN 104179006 A CN104179006 A CN 104179006A CN 201410423580 A CN201410423580 A CN 201410423580A CN 104179006 A CN104179006 A CN 104179006A
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- CN
- China
- Prior art keywords
- mould inhibitor
- parts
- stir
- ethanol
- cooled
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000003112 inhibitor Substances 0.000 title claims abstract description 42
- 239000004677 Nylon Substances 0.000 title claims abstract description 29
- 229920001778 nylon Polymers 0.000 title claims abstract description 29
- 239000004744 fabric Substances 0.000 title claims abstract description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 42
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 42
- GDDNTTHUKVNJRA-UHFFFAOYSA-N 3-bromo-3,3-difluoroprop-1-ene Chemical compound FC(F)(Br)C=C GDDNTTHUKVNJRA-UHFFFAOYSA-N 0.000 claims abstract description 21
- 235000011187 glycerol Nutrition 0.000 claims abstract description 21
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 235000017281 sodium acetate Nutrition 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims description 30
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 20
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000001632 sodium acetate Substances 0.000 claims description 18
- 229940117958 vinyl acetate Drugs 0.000 claims description 18
- BTJIUGUIPKRLHP-UHFFFAOYSA-N 4-nitrophenol Chemical compound OC1=CC=C([N+]([O-])=O)C=C1 BTJIUGUIPKRLHP-UHFFFAOYSA-N 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 10
- PVEOYINWKBTPIZ-UHFFFAOYSA-N but-3-enoic acid Chemical class OC(=O)CC=C PVEOYINWKBTPIZ-UHFFFAOYSA-N 0.000 claims description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 235000011091 sodium acetates Nutrition 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- BDKLKNJTMLIAFE-UHFFFAOYSA-N 2-(3-fluorophenyl)-1,3-oxazole-4-carbaldehyde Chemical compound FC1=CC=CC(C=2OC=C(C=O)N=2)=C1 BDKLKNJTMLIAFE-UHFFFAOYSA-N 0.000 abstract 1
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 abstract 1
- 230000005764 inhibitory process Effects 0.000 abstract 1
- 238000000465 moulding Methods 0.000 abstract 1
- 229940087562 sodium acetate trihydrate Drugs 0.000 abstract 1
- 239000004753 textile Substances 0.000 description 5
- 244000005700 microbiome Species 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 229920002972 Acrylic fiber Polymers 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 229920002978 Vinylon Polymers 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a mould inhibitor for a nylon fabric. The mould inhibitor consists of the following components in parts by weight: 4-6 parts of tetrabutyl titanate, 10-15 parts of sodium acetate trihydrate, 2-3 parts of ammonium perchlorate, 3-5 parts of glycerin, 8-10 parts of vinyl acetate and 30-40 parts of ethanol. By virtue of the mould inhibitor, the moulding problem of the nylon fabric can be well solved and permanent mould inhibition can be achieved; besides, the mould inhibitor has good heat stability and cannot discolor easily, thereby meeting the temperature requirement of a normal production technology.
Description
Technical field
The invention belongs to textile technology field, be specifically related to a kind of nylon fabrics mould inhibitor.
Background technology
Along with social development, the raising of economic level, large-scale light industry enterprise particularly textile enterprise's quantity rolls up.Textiles is various in style, and majority easily goes mouldy, as cotton, fiber crops, hair, vinylon, nylon, acrylic fibers spray silk etc.Thereby the storage of textile product and raw material also becomes a difficult problem for these enterprises.For the control that textile product goes mouldy, many factories have to strengthen expect that from former product processes the administration of health of whole process.But under many circumstances, control the initial contaminant capacity of microorganism or arrange that all environmental conditions that is unfavorable for growth of microorganism normally can not accomplish, also need to use mould inhibitor to control the pollution and harm of microorganism to production environment, material, product.
Summary of the invention
The invention provides a kind of nylon fabrics mould inhibitor, for preventing going mouldy of nylon fabrics.
The invention provides a kind of nylon fabrics mould inhibitor, described mould inhibitor is made up of each component of following mass fraction: butyl titanate 4-6 part, sodium acetate 10-15 part, ammonium perchlorate 2-3 part, glycerine 3-5 part, vinylacetate 8-10 part, ethanol 30-40 part.
Preferably, described mould inhibitor is made up of each component of following mass fraction: 5 parts of butyl titanates, 12 parts of sodium acetates, 2.5 parts of ammonium perchlorate, 4 parts of glycerine, 9 parts of vinylacetates, 35 parts of ethanol.
Further, described mould inhibitor also comprises 2-3 part p-nitrophenol.
Second object of the present invention is to provide the preparation method of above-mentioned mould inhibitor, that butyl titanate 4-6 part, ethanol 30-40 part are heated to 80-90 DEG C, stir 1-2 hour, add successively again sodium acetate 10-15 part, ammonium perchlorate 2-3 part, stir after 0.5-1 hour, be cooled to 70-75 DEG C, add glycerine 3-5 part, vinylacetate 8-10 part to stir, be cooled to and obtain after room temperature.
The 3rd object of the present invention is to provide the preparation method of above-mentioned mould inhibitor, that butyl titanate 4-6 part, ethanol 30-40 part are heated to 80-90 DEG C, stir 1-2 hour, add successively again sodium acetate 10-15 part, ammonium perchlorate 2-3 part, p-nitrophenol 2-3 part, stir after 0.5-1 hour, be cooled to 70-75 DEG C, add glycerine 3-5 part, vinylacetate 8-10 part to stir, be cooled to and obtain after room temperature.
Apply the mouldization problem that mould inhibitor of the present invention can well solve nylon fabrics, can reach permanent mildew-resistant.And Heat stability is good, not easy to change, meet normal production technology temperature requirement.
Detailed description of the invention
Following embodiment is convenient to understand better the present invention, but does not limit the present invention.Experimental technique in following embodiment, if no special instructions, is conventional method.
embodiment 1
Nylon fabrics provided by the invention is as follows with mould inhibitor formula: butyl titanate 5kg, sodium acetate 12kg, ammonium perchlorate 2.5kg, glycerine 4kg, vinylacetate 9kg, ethanol 35kg.
Nylon fabrics provided by the invention is as follows by the preparation method of mould inhibitor: butyl titanate 5kg, ethanol 35kg are heated to 85 DEG C, stir 1.5 hours, add successively again sodium acetate 12kg, ammonium perchlorate 2.5kg, stir after 0.5 hour, be cooled to 72 DEG C, add glycerine 4kg, vinylacetate 9kg to stir, obtain nylon fabrics mould inhibitor of the present invention after being cooled to room temperature.
embodiment 2
Nylon fabrics provided by the invention is as follows with mould inhibitor formula: butyl titanate 4kg, sodium acetate 10kg, ammonium perchlorate 3kg, glycerine 5kg, vinylacetate 8kg, ethanol 40kg.
Nylon fabrics provided by the invention is as follows by the preparation method of mould inhibitor: butyl titanate 4kg, ethanol 40kg are heated to 80 DEG C, stir 2 hours, add successively again sodium acetate 10kg, ammonium perchlorate 3kg, stir after 1 hour, be cooled to 75 DEG C, add glycerine 5kg, vinylacetate 8kg to stir, obtain nylon fabrics mould inhibitor of the present invention after being cooled to room temperature.
embodiment 3
Nylon fabrics provided by the invention is as follows with mould inhibitor formula: butyl titanate 6kg, sodium acetate 15kg, ammonium perchlorate 2kg, glycerine 3kg, vinylacetate 10kg, ethanol 30kg.
Nylon fabrics provided by the invention is as follows by the preparation method of mould inhibitor: butyl titanate 6kg, ethanol 30kg are heated to 90 DEG C, stir 1 hour, add successively again sodium acetate 15kg, ammonium perchlorate 2kg, stir after 0.5 hour, be cooled to 70 DEG C, add glycerine 3kg, vinylacetate 10kg to stir, obtain nylon fabrics mould inhibitor of the present invention after being cooled to room temperature.
embodiment 4
Nylon fabrics provided by the invention is as follows with mould inhibitor formula: butyl titanate 6kg, sodium acetate 15kg, ammonium perchlorate 2kg, glycerine 3kg, vinylacetate 10kg, p-nitrophenol 2kg, ethanol 30kg.
Nylon fabrics provided by the invention is as follows by the preparation method of mould inhibitor: butyl titanate 6kg, ethanol 30kg are heated to 90 DEG C, stir 1 hour, add successively again sodium acetate 15kg, ammonium perchlorate 2kg, p-nitrophenol 2kg, stir after 0.5 hour, be cooled to 70 DEG C, add glycerine 3kg, vinylacetate 10kg to stir, obtain nylon fabrics mould inhibitor of the present invention after being cooled to room temperature.
embodiment 5
Nylon fabrics provided by the invention is as follows with mould inhibitor formula: butyl titanate 5kg, sodium acetate 12kg, ammonium perchlorate 2.5kg, glycerine 4kg, vinylacetate 9kg, p-nitrophenol 2kg, ethanol 35kg.
Nylon fabrics provided by the invention is as follows by the preparation method of mould inhibitor: butyl titanate 5kg, ethanol 35kg are heated to 85 DEG C, stir 1.5 hours, add successively again sodium acetate 12kg, ammonium perchlorate 2.5kg, p-nitrophenol 2kg, stir after 0.5 hour, be cooled to 72 DEG C, add glycerine 4kg, vinylacetate 9kg to stir, obtain nylon fabrics mould inhibitor of the present invention after being cooled to room temperature.
embodiment 6
Nylon fabrics provided by the invention is as follows with mould inhibitor formula: butyl titanate 4kg, sodium acetate 13kg, ammonium perchlorate 3kg, glycerine 3kg, vinylacetate 8kg, p-nitrophenol 3kg, ethanol 40kg.
Nylon fabrics provided by the invention is as follows by the preparation method of mould inhibitor: butyl titanate 4kg, ethanol 40kg are heated to 80 DEG C, stir 2 hours, add successively again sodium acetate 13kg, ammonium perchlorate 3kg, p-nitrophenol 3kg, stir after 1 hour, be cooled to 75 DEG C, add glycerine 3kg, vinylacetate 8kg to stir, obtain nylon fabrics mould inhibitor of the present invention after being cooled to room temperature.
Finally it should be noted that: the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although the present invention is had been described in detail with reference to previous embodiment, for a person skilled in the art, its technical scheme that still can record aforementioned each embodiment is modified, or part technical characterictic is wherein equal to replacement.Within the spirit and principles in the present invention all, any amendment of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (5)
1. a nylon fabrics mould inhibitor, is characterized in that: described mould inhibitor is made up of each component of following mass fraction: butyl titanate 4-6 part, sodium acetate 10-15 part, ammonium perchlorate 2-3 part, glycerine 3-5 part, vinylacetate 8-10 part, ethanol 30-40 part.
2. mould inhibitor according to claim 1, is characterized in that: described mould inhibitor is made up of each component of following mass fraction: 5 parts of butyl titanates, 12 parts of sodium acetates, 2.5 parts of ammonium perchlorate, 4 parts of glycerine, 9 parts of vinylacetates, 35 parts of ethanol.
3. mould inhibitor according to claim 1, is characterized in that: described mould inhibitor also comprises 2-3 part p-nitrophenol.
4. the preparation method of the arbitrary described mould inhibitor of claim 1-2, it is characterized in that: be that butyl titanate 4-6 part, ethanol 30-40 part are heated to 80-90 DEG C, stir 1-2 hour, add successively again sodium acetate 10-15 part, ammonium perchlorate 2-3 part, stir after 0.5-1 hour, be cooled to 70-75 DEG C, add glycerine 3-5 part, vinylacetate 8-10 part to stir, be cooled to and obtain after room temperature.
5. the preparation method of a mould inhibitor claimed in claim 3, it is characterized in that: be that butyl titanate 4-6 part, ethanol 30-40 part are heated to 80-90 DEG C, stir 1-2 hour, add successively again sodium acetate 10-15 part, ammonium perchlorate 2-3 part, p-nitrophenol 2-3 part, stir after 0.5-1 hour, be cooled to 70-75 DEG C, add glycerine 3-5 part, vinylacetate 8-10 part to stir, be cooled to and obtain after room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410423580.5A CN104179006B (en) | 2014-08-26 | 2014-08-26 | A kind of nylon fabrics mould inhibitor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410423580.5A CN104179006B (en) | 2014-08-26 | 2014-08-26 | A kind of nylon fabrics mould inhibitor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104179006A true CN104179006A (en) | 2014-12-03 |
| CN104179006B CN104179006B (en) | 2016-04-13 |
Family
ID=51960329
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410423580.5A Expired - Fee Related CN104179006B (en) | 2014-08-26 | 2014-08-26 | A kind of nylon fabrics mould inhibitor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104179006B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105821652A (en) * | 2016-04-21 | 2016-08-03 | 潘红 | Mildew preventive for nylon fabrics |
| CN105887476A (en) * | 2016-06-29 | 2016-08-24 | 广西美男子文化传媒有限公司 | Anti-mold agent for nylon fabric |
| CN106012516A (en) * | 2016-06-24 | 2016-10-12 | 广德毅维纺织有限公司 | Mildewing-proof and sun-proof treating liquid for clothing fabric |
| CN106192375A (en) * | 2016-06-29 | 2016-12-07 | 广西美男子文化传媒有限公司 | A kind of medicated clothing antifungus agent and preparation method thereof |
| CN107996591A (en) * | 2017-11-30 | 2018-05-08 | 安徽宏远无纺布业有限公司 | A kind of cloth mould inhibitor and preparation method thereof |
| CN113290952A (en) * | 2021-03-27 | 2021-08-24 | 浙江国富纺织科技有限公司 | Deodorizing mildew-proof wall cloth and preparation method thereof |
| CN115595791A (en) * | 2022-10-24 | 2023-01-13 | 绍兴市越发纺织有限公司（Cn） | A breathable knitted fabric and its preparation method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1072776A (en) * | 1996-08-23 | 1998-03-17 | Lion Corp | Emulsion type laundry paste and method for producing the same |
| CN102772049A (en) * | 2011-05-10 | 2012-11-14 | 纳德·哈桑·萨布里 | Orthopedic kneeling pad |
| CN103741463A (en) * | 2013-12-31 | 2014-04-23 | 吴江市七都镇庙港雅迪针织制衣厂 | Mothproofing agent for silk fabric |
| CN103774431A (en) * | 2014-01-20 | 2014-05-07 | 南通全技纺织涂层有限公司 | Antibacterial mildew-proof nylon fabric |
| CN103924444A (en) * | 2014-04-24 | 2014-07-16 | 南雄鼎成化工有限公司 | Preparation method and application of hydrophilic anti-bacteria conditioner for fabric |
-
2014
- 2014-08-26 CN CN201410423580.5A patent/CN104179006B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1072776A (en) * | 1996-08-23 | 1998-03-17 | Lion Corp | Emulsion type laundry paste and method for producing the same |
| CN102772049A (en) * | 2011-05-10 | 2012-11-14 | 纳德·哈桑·萨布里 | Orthopedic kneeling pad |
| CN103741463A (en) * | 2013-12-31 | 2014-04-23 | 吴江市七都镇庙港雅迪针织制衣厂 | Mothproofing agent for silk fabric |
| CN103774431A (en) * | 2014-01-20 | 2014-05-07 | 南通全技纺织涂层有限公司 | Antibacterial mildew-proof nylon fabric |
| CN103924444A (en) * | 2014-04-24 | 2014-07-16 | 南雄鼎成化工有限公司 | Preparation method and application of hydrophilic anti-bacteria conditioner for fabric |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105821652A (en) * | 2016-04-21 | 2016-08-03 | 潘红 | Mildew preventive for nylon fabrics |
| CN106012516A (en) * | 2016-06-24 | 2016-10-12 | 广德毅维纺织有限公司 | Mildewing-proof and sun-proof treating liquid for clothing fabric |
| CN105887476A (en) * | 2016-06-29 | 2016-08-24 | 广西美男子文化传媒有限公司 | Anti-mold agent for nylon fabric |
| CN106192375A (en) * | 2016-06-29 | 2016-12-07 | 广西美男子文化传媒有限公司 | A kind of medicated clothing antifungus agent and preparation method thereof |
| CN107996591A (en) * | 2017-11-30 | 2018-05-08 | 安徽宏远无纺布业有限公司 | A kind of cloth mould inhibitor and preparation method thereof |
| CN113290952A (en) * | 2021-03-27 | 2021-08-24 | 浙江国富纺织科技有限公司 | Deodorizing mildew-proof wall cloth and preparation method thereof |
| CN115595791A (en) * | 2022-10-24 | 2023-01-13 | 绍兴市越发纺织有限公司（Cn） | A breathable knitted fabric and its preparation method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104179006B (en) | 2016-04-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Lu Zhuangling Inventor before: Zhou Min |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170524 Address after: 322100 Jiangbei hi tech Industrial Park, Zhejiang, Dongyang Patentee after: Limited company is weaved in Asia by Zhejiang Australia Address before: 214000 Jiangsu Province, Wuxi city Xishan District Yang Jian Zhen Li an Cun Xi Hu Lu Bei Patentee before: WUXI QISHENG KNITTING GLOVES FACTORY |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160413 Termination date: 20170826 |