CN105102440A - 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化 - Google Patents

单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化 Download PDF

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Publication number
CN105102440A
CN105102440A CN201380057105.4A CN201380057105A CN105102440A CN 105102440 A CN105102440 A CN 105102440A CN 201380057105 A CN201380057105 A CN 201380057105A CN 105102440 A CN105102440 A CN 105102440A
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CN
China
Prior art keywords
phase
cmf
liquid
hydrochloric acid
methods
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Pending
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CN201380057105.4A
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English (en)
Chinese (zh)
Inventor
阿维亚德·卡哈纳
爱德华·尼基丁
杰里米·斯坦迪福德
凯尔·埃利斯
张吕正
蒂莫西·乔治
彼得·米考奇克
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XF TECHNOLOGIES Inc
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XF TECHNOLOGIES Inc
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Publication of CN105102440A publication Critical patent/CN105102440A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
CN201380057105.4A 2012-10-16 2013-09-03 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化 Pending CN105102440A (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261714225P 2012-10-16 2012-10-16
US61/714,225 2012-10-16
US201361818418P 2013-05-01 2013-05-01
US61/818,418 2013-05-01
PCT/US2013/057795 WO2014062303A2 (en) 2012-10-16 2013-09-03 Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde

Publications (1)

Publication Number Publication Date
CN105102440A true CN105102440A (zh) 2015-11-25

Family

ID=50488863

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380057105.4A Pending CN105102440A (zh) 2012-10-16 2013-09-03 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化

Country Status (10)

Country Link
US (1) US9102644B2 (2)
EP (1) EP2909187A4 (2)
CN (1) CN105102440A (2)
BR (1) BR112015008477B1 (2)
CA (1) CA2888298C (2)
IN (1) IN2015DN03835A (2)
MX (1) MX363821B (2)
PH (1) PH12015500818A1 (2)
SG (1) SG11201502939WA (2)
WO (1) WO2014062303A2 (2)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111936478A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936477A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX346916B (es) 2011-06-09 2017-04-05 Micromidas Inc Utilizacion de reactor de fases multiples para la conversion de biomasa para producir furanos substituidos.
BR112015009121A2 (pt) 2012-10-26 2017-07-04 Micromidas Inc métodos para produzir 5-(halometil)furfural
MY193787A (en) 2013-03-14 2022-10-27 Micromidas Inc Solid forms of 5-(halomethyl) furfural and methods for preparing thereof
KR102247145B1 (ko) 2013-03-14 2021-05-04 마이크로마이다스, 인코포레이티드 5-(할로메틸)푸르푸랄의 정제 방법
ES2932619T3 (es) 2013-09-20 2023-01-23 Origin Mat Operating Inc Métodos para producir 5-(halometil)furfural
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
EP3740662B1 (en) 2018-01-19 2023-08-16 Qmaxx Products Group, Inc. Metal cleaning compositions comprising furoate esters and uses therefor
EP3840746A1 (en) 2018-08-23 2021-06-30 Novartis AG New pharmaceutical use for the treatment of heart failure
WO2020039394A1 (en) 2018-08-24 2020-02-27 Novartis Ag New drug combinations
BR112022018316A2 (pt) 2020-04-17 2022-10-25 Dow Global Technologies Llc Formulação agrícola
MX2024010807A (es) * 2022-03-04 2024-09-11 Avantium Knowledge Centre Bv Metodo de extraccion de 5-clorometilfurfural con un disolvente organico de fibras celulosicas y fibras no celulosicas artificiales hidrolizadas en conjunto con acido clorhidrico.

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4335049A (en) * 1980-07-16 1982-06-15 Sumitomo Chemical Company, Limited Process for producing 5-methylfurfural
US20090234142A1 (en) * 2008-03-17 2009-09-17 The Regents Of The Unversity Of California High-yield conversion of cellulosic biomass into furanic biofuels and value-added products

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4154744A (en) * 1976-10-12 1979-05-15 Sumitomo Chemical Company, Limited Process for producing a furan derivative
DE3842825A1 (de) * 1988-01-08 1989-07-20 Krupp Gmbh Verfahren und vorrichtung zur herstellung von furfural
CA2864086C (en) * 2011-02-28 2018-07-10 Midori Renewables, Inc. Polymeric acid catalysts and uses thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4335049A (en) * 1980-07-16 1982-06-15 Sumitomo Chemical Company, Limited Process for producing 5-methylfurfural
US20090234142A1 (en) * 2008-03-17 2009-09-17 The Regents Of The Unversity Of California High-yield conversion of cellulosic biomass into furanic biofuels and value-added products

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
HÉCTOR QUIROZ-FLORENTINO ET AL.: "Total Synthesis of Naturally Occurring Furan Compounds 5-{[(4-Hydroxybenzyl)oxy]methyl}-2-furaldehyde and Pichiafuran C", 《SYNTHESIS》 *
MALTE BRASHOLZ ET AL.,: "Highly efficient dehydration of carbohydrates to 5-(chloromethyl)furfural(CMF),5-(hydroxymethyl)furfural(HMF)and levulinic acid by biphasic continuous flow processing", 《GREEN CHEM》 *
MARK MASCAL AND EDWARD B. NIKITIN: "Dramatic Advancements in the Saccharide to 5-(Chloromethyl)furfural Conversion Reaction", 《CHEMSUSCHEM》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111936478A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936477A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936478B (zh) * 2018-01-31 2023-10-10 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936477B (zh) * 2018-01-31 2023-10-10 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺

Also Published As

Publication number Publication date
US9102644B2 (en) 2015-08-11
EP2909187A4 (en) 2016-05-11
BR112015008477B1 (pt) 2020-12-08
CA2888298A1 (en) 2014-04-24
PH12015500818A1 (en) 2015-06-08
IN2015DN03835A (2) 2015-10-02
EP2909187A2 (en) 2015-08-26
MX2015004716A (es) 2016-08-17
BR112015008477A2 (pt) 2017-07-04
WO2014062303A3 (en) 2015-07-16
WO2014062303A2 (en) 2014-04-24
MX363821B (es) 2019-04-04
CA2888298C (en) 2022-05-31
SG11201502939WA (en) 2015-05-28
US20140187802A1 (en) 2014-07-03

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Application publication date: 20151125