CN105696320A - Flame-retardant finishing method for polyamide fabric - Google Patents
Flame-retardant finishing method for polyamide fabric Download PDFInfo
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- CN105696320A CN105696320A CN201610142952.6A CN201610142952A CN105696320A CN 105696320 A CN105696320 A CN 105696320A CN 201610142952 A CN201610142952 A CN 201610142952A CN 105696320 A CN105696320 A CN 105696320A
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- 239000004744 fabric Substances 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 22
- 239000003063 flame retardant Substances 0.000 title claims abstract description 18
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 239000004952 Polyamide Substances 0.000 title abstract description 6
- 229920002647 polyamide Polymers 0.000 title abstract description 6
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 13
- -1 methyl hydrogen Chemical class 0.000 claims abstract description 13
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 12
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims abstract description 12
- 238000005470 impregnation Methods 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 12
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- NQBXSWAWVZHKBZ-UHFFFAOYSA-N 2-butoxyethyl acetate Chemical compound CCCCOCCOC(C)=O NQBXSWAWVZHKBZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- RUPBZQFQVRMKDG-UHFFFAOYSA-M Didecyldimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCC[N+](C)(C)CCCCCCCCCC RUPBZQFQVRMKDG-UHFFFAOYSA-M 0.000 claims abstract description 6
- 239000010425 asbestos Substances 0.000 claims abstract description 6
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001257 hydrogen Substances 0.000 claims abstract description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 6
- 229910052895 riebeckite Inorganic materials 0.000 claims abstract description 6
- 229920001778 nylon Polymers 0.000 claims description 25
- 239000004677 Nylon Substances 0.000 claims description 24
- 238000001035 drying Methods 0.000 claims description 10
- MPPQGYCZBNURDG-UHFFFAOYSA-N 2-propionyl-6-dimethylaminonaphthalene Chemical compound C1=C(N(C)C)C=CC2=CC(C(=O)CC)=CC=C21 MPPQGYCZBNURDG-UHFFFAOYSA-N 0.000 claims description 5
- FAUKXDZDINMBSZ-UHFFFAOYSA-N 3-bis(methylperoxy)phosphoryl-n-(hydroxymethyl)propanamide Chemical compound COOP(=O)(OOC)CCC(=O)NCO FAUKXDZDINMBSZ-UHFFFAOYSA-N 0.000 claims description 5
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical group O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 5
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 239000004114 Ammonium polyphosphate Substances 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- LKJPYSCBVHEWIU-UHFFFAOYSA-N N-[4-cyano-3-(trifluoromethyl)phenyl]-3-[(4-fluorophenyl)sulfonyl]-2-hydroxy-2-methylpropanamide Chemical compound C=1C=C(C#N)C(C(F)(F)F)=CC=1NC(=O)C(O)(C)CS(=O)(=O)C1=CC=C(F)C=C1 LKJPYSCBVHEWIU-UHFFFAOYSA-N 0.000 abstract 1
- 235000019826 ammonium polyphosphate Nutrition 0.000 abstract 1
- 229920001276 ammonium polyphosphate Polymers 0.000 abstract 1
- 229960004670 didecyldimethylammonium chloride Drugs 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 229920002545 silicone oil Polymers 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 abstract 1
- 229920002554 vinyl polymer Polymers 0.000 abstract 1
- 239000008096 xylene Substances 0.000 abstract 1
- 239000000835 fiber Substances 0.000 description 5
- 239000004753 textile Substances 0.000 description 5
- 229920006052 Chinlon® Polymers 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 229920002292 Nylon 6 Polymers 0.000 description 2
- 229920002302 Nylon 6,6 Polymers 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 229920002994 synthetic fiber Polymers 0.000 description 2
- 239000004758 synthetic textile Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 229920006351 engineering plastic Polymers 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920006111 poly(hexamethylene terephthalamide) Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920006012 semi-aromatic polyamide Polymers 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
- D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/232—Organic carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/44—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing nitrogen and phosphorus
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a flame-retardant finishing method for polyamide fabric. The method comprises steps as follows: water is added to a finishing agent, an impregnation liquid is prepared, the fabric is put in the impregnation liquid to be padded, the pick-up ratio is 45%-70%, and finally, the fabric is washed with water 2-3 times, dewatered and dried; the finishing agent comprises components in parts by weight as follows: 3-10 parts of ethylene glycol monobutyl ether acetate, 3-6 parts of sodium fluosilicate, 3-7 parts of didecyl dimethyl ammonium chloride, 4-7 parts of barium sulfate, 3-8 parts of methylcyclosiloxane, 11-18 parts of N-hydroxymethyl-3-(dimethoxy phosphonyl) propanamide, 4-8 parts of methyl hydrogen silicone oil, 5-10 parts of vinyl versatate, 3-7 parts of vinyltriethoxysilane, 20-36 parts of butanol, 2-8 parts of xylene, 4-8 parts of asbestos powder and 2-10 parts of ammonium polyphosphate. By means of the finishing method, the flame retardant effect of the polyamide fabric is remarkably improved, the polyamide fabric is also endowed with good wash resistance, and the finishing method has good market promotion value.
Description
Technical field
The invention belongs to textile technology field, be specifically related to a kind of nylon fabric flame-retardant finishing method。
Technical background
Chinlon is exactly the nylon fiber generally said, nylon fabric is that nylon material is pulled into very thin fiber, then weave cotton cloth, the concrete formal name used at school of nylon is called polyamide, is broad-spectrum engineering plastics。Polyamide (PA) is that DuPont develops the resin for fiber at first, realizes industrialization in nineteen thirty-nine。Start exploitation the 1950's and produce injection-molded item, meeting downstream industry goods lightweight with substituted metal, reduce the requirement of cost。PA's is various in style, has PA6, PA66, PAll, PAl2, PA46, PA610, PA612, PAl010 etc. and a lot of new varieties such as the semi-aromatic nylon PA6T developed in recent years and extraordinary nylon。Material according to nylon is different, it can be common that chinlon 6 and chinlon 66, the fiber namely made with nylon 6 and nylon66 fiber。
Nylon fabric is famous with the wearability of its excellence, and it is not only the optimum selection of down jackets, anorak dress material, and often and other fiber blend or intertexture, to improve intensity and the fastness of fabric。The anti-wear performance of nylon fabric occupies first of each kind fabric, much higher times of other fabric of like product of ratio, and therefore, its ruggedness is splendid。The hygroscopicity of nylon fabric belongs to better kind in synthetic fabrics, and therefore the clothing with chinlon making are more comfortable and easy to wear than terylene clothes。Nylon fabric belongs to light fabric, is only listed in after polypropylene, acrylic fabric in synthetic fabrics, therefore, is suitable for making anorak, water clothes etc.。Simultaneously the elasticity of nylon fabric and elastic recovery are fabulous。
Fire is the major hidden danger threatening human life's safety。The fire exceeding half according to statistics in the world is all caused by textile, additionally, textile can produce harmful gas mostly when burning。Therefore, safety is also paid attention to by people gradually, and a lot of occasions are desirable that fabric used has anti-flaming function, and the research and development of flame retardant textiles are significant。Nylon fabric belongs to inflammable articles, so flame-proof treatment is particularly important to it。Fabric after being processed is nonflammable after meeting fire, has significantly expanded its application。Having a variety of fire retardant on the market now, after fabric is processed, the intensity of fabric self, feel, outward appearance, dyestuff color and luster and color fastness aspect all receive impact in various degree, and on flame retardant effect and durable degree, also not fully up to expectations。Therefore how overcoming the deficiencies in the prior art is the problem that current field of textiles needs solution badly。
Summary of the invention
To achieve these goals, the invention provides a kind of nylon fabric flame-retardant finishing method。
It is an object of the invention to be achieved through the following technical solutions:
A kind of nylon fabric flame-retardant finishing method, the method has following steps: first being added water by finishing agent is configured to impregnation liquid, is then put in impregnation liquid by fabric and pads, pick-up 45-70%, finally washing 2-3 time, last dewatered drying；Described finishing agent is made up of the component of following parts by weight: 2-Butoxyethyl acetate 3-10 part, prodan 3-6 part, DDAC 3-7 part, barium sulfate 4-7 part, methyl cyclosiloxane 3-8 part, N-methylol-3-(dimethoxy phosphono) propionic acid amide. 11-18 part, Methyl Hydrogen Polysiloxane Fluid 4-8 part, tertiary ethylene carbonate 5-10 part, VTES 3-7 part, butanol 20-36 part, dimethylbenzene 2-8 part, flake asbestos 4-8 part, APP 2-10 part。
The preparation technology of finishing agent is common process, skillfully grasps for those of ordinary skill in the art。
Described fabric impregnates 20-30 minute at 50-85 DEG C。
Described drying temperature is 50-60 DEG C, and the time is 3 minutes。
The concentration of described aqueous solution is 800-1500ppm。
The method have the advantages that method for sorting of the present invention significantly improves the flame retardant effect of nylon fabric, give the water-wash resistance that nylon fabric is good simultaneously, there is good market popularization value。
Detailed description of the invention
The following stated is only the preferred embodiments of the present invention, it is not limited to the present invention, although the present invention being described in detail with reference to previous embodiment, for a person skilled in the art, technical scheme described in foregoing embodiments still can be modified by it, or wherein portion of techniques feature carries out equivalent replacement。All within the spirit and principles in the present invention, any amendment of making, equivalent replacement, improvement etc., should be included within protection scope of the present invention。
Embodiment 1
A kind of nylon fabric flame-retardant finishing method, it has following steps: first being added water by finishing agent is configured to impregnation liquid, is then put in impregnation liquid by fabric and pads, pick-up 45-70%, finally washing 2-3 time, last dewatered drying；Described finishing agent is made up of the component of following parts by weight: 2-Butoxyethyl acetate 3 parts, prodan 3 parts, DDAC 3 parts, 4 parts of barium sulfate, methyl cyclosiloxane 3 parts, N-methylol-3-(dimethoxy phosphono) propionic acid amide. 11 parts, Methyl Hydrogen Polysiloxane Fluid 4 parts, tertiary ethylene carbonate 5 parts, VTES 3 parts, 20 parts of butanol, dimethylbenzene 2 parts, flake asbestos 4 parts, APP 2 parts。
Described fabric impregnates 20-30 minute at 50-85 DEG C。
Described drying temperature is 50-60 DEG C, and the time is 3 minutes。
The concentration of described aqueous solution is 800-1500ppm。
Embodiment 2
A kind of nylon fabric flame-retardant finishing method, it has following steps: first being added water by finishing agent is configured to impregnation liquid, is then put in impregnation liquid by fabric and pads, pick-up 45-70%, finally washing 2-3 time, last dewatered drying；Described finishing agent is made up of the component of following parts by weight: 2-Butoxyethyl acetate 10 parts, prodan 6 parts, DDAC 7 parts, 7 parts of barium sulfate, methyl cyclosiloxane 8 parts, N-methylol-3-(dimethoxy phosphono) propionic acid amide. 18 parts, Methyl Hydrogen Polysiloxane Fluid 8 parts, tertiary ethylene carbonate 10 parts, VTES 7 parts, 36 parts of butanol, dimethylbenzene 8 parts, flake asbestos 8 parts, APP 10 parts。
Described fabric impregnates 20-30 minute at 50-85 DEG C。
Described drying temperature is 50-60 DEG C, and the time is 3 minutes。
The concentration of described aqueous solution is 800-1500ppm。
Embodiment 3
A kind of nylon fabric flame-retardant finishing method, it has following steps: first being added water by finishing agent is configured to impregnation liquid, is then put in impregnation liquid by fabric and pads, pick-up 45-70%, finally washing 2-3 time, last dewatered drying；Described finishing agent is made up of the component of following parts by weight: 2-Butoxyethyl acetate 6 parts, prodan 4 parts, DDAC 5 parts, 6 parts of barium sulfate, methyl cyclosiloxane 5 parts, N-methylol-3-(dimethoxy phosphono) propionic acid amide. 15 parts, Methyl Hydrogen Polysiloxane Fluid 6 parts, tertiary ethylene carbonate 7 parts, VTES 5 parts, 28 parts of butanol, dimethylbenzene 5 parts, flake asbestos 6 parts, APP 6 parts。
Described fabric impregnates 20-30 minute at 50-85 DEG C。
Described drying temperature is 50-60 DEG C, and the time is 3 minutes。
The concentration of described aqueous solution is 800-1500ppm。
Claims (4)
1. a nylon fabric flame-retardant finishing method, it is characterised in that the step of described method is as follows: first added water by finishing agent and be configured to impregnation liquid, then puts into fabric in impregnation liquid and pads, pick-up 45-70%, finally washing 2-3 time, last dewatered drying；Described finishing agent is made up of the component of following parts by weight: 2-Butoxyethyl acetate 3-10 part, prodan 3-6 part, DDAC 3-7 part, barium sulfate 4-7 part, methyl cyclosiloxane 3-8 part, N-methylol-3-(dimethoxy phosphono) propionic acid amide. 11-18 part, Methyl Hydrogen Polysiloxane Fluid 4-8 part, tertiary ethylene carbonate 5-10 part, VTES 3-7 part, butanol 20-36 part, dimethylbenzene 2-8 part, flake asbestos 4-8 part, APP 2-10 part。
2. a kind of nylon fabric flame-retardant finishing method according to claim 1, it is characterised in that: described fabric impregnates 20-30 minute at 50-85 DEG C。
3. a kind of nylon fabric flame-retardant finishing method according to claim 1, it is characterised in that: described drying temperature is 50-60 DEG C, and the time is 3 minutes。
4. a kind of nylon fabric flame-retardant finishing method according to claim 1, it is characterised in that: the concentration of described aqueous solution is 800-1500ppm。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610142952.6A CN105696320A (en) | 2016-03-14 | 2016-03-14 | Flame-retardant finishing method for polyamide fabric |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN118223286A (en) * | 2024-03-21 | 2024-06-21 | 昆山怡家居纺织有限公司 | Flame retardant finishing method for nylon textile and flame retardant nylon textile |
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Application publication date: 20160622 |