CN105821669A - Manufacturing method for multifunctional flame-retardant polyester fabric - Google Patents

Manufacturing method for multifunctional flame-retardant polyester fabric Download PDF

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Publication number
CN105821669A
CN105821669A CN201610187025.6A CN201610187025A CN105821669A CN 105821669 A CN105821669 A CN 105821669A CN 201610187025 A CN201610187025 A CN 201610187025A CN 105821669 A CN105821669 A CN 105821669A
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dacron
minutes
primer
fabric
follows
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CN105821669B (en
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刘伟建
钱立军
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Suzhou Najin New Material Technology Co Ltd
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Suzhou Najin New Material Technology Co Ltd
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
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    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
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    • D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
    • D06M13/03—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons with unsaturated hydrocarbons, e.g. alkenes, or alkynes
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    • D06M13/08—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with halogenated hydrocarbons
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    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/35—Heterocyclic compounds
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    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
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    • D06M13/44—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing nitrogen and phosphorus
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    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
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    • D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
    • D06M13/503—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms without bond between a carbon atom and a metal or a boron, silicon, selenium or tellurium atom
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    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/244—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
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    • D06M2200/30—Flame or heat resistance, fire retardancy properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention relates to a processing and finishing method for a multifunctional flame-retardant polyester fabric. The method is used for improving the multifunctionality, the perforation preventing performance and the flame retardance of the fabric, so that the fabric has the advantages of inhibiting smoke, being free of molten drops, preventing burning perforation, repelling water and oil, resisting acid and alkali and being permeable to moisture and conductive, and the problems that a conventional flame-retardant fabric is single in function and prone to perforation to cause the molten drops are solved. The method mainly comprises the steps that 1, padding and high-temperature drying are conducted to form a conductive, water-repellent, oil-repellent and acid-alkali-resistant layer; 2, a waterproof and breathable base adhesive containing a charring agent and a phosphate flame retardant is applied and cured; 3, a waterproof and breathable surface adhesive containing the charring agent and the phosphate flame retardant is applied and cured.

Description

A kind of manufacture method of multifunctional flame-proof dacron
Technical field
The present invention relates to a kind of method utilizing Final finishing technology to carry out the functionalization fabric including fire-retardant, belong to function textile material technical field.
Background technology
For adapting to the current social demand demand for the specific function of fabric, particularly in some special fields, such as fields such as military project, frock, fire-fightings, the fabric of simple function is difficult in adapt to the application demand of special environment；Therefore, using environment and different purposes to carry out combined fabric Final finishing technology for difference, exploitation has several functions in the functional fabric product of one, has important technological value and commercial value.
If several functions auxiliary agent being bestowed during Final finishing fabric, the conflicting and effect of antagonism may be there is again between various functions, therefore should consider each orthofunction, consider the formulation condition many-side cross influence such as related auxiliaries, additive again；The hydraulic pressure that the mass ratio that the CH-key of the water and oil repellant auxiliary agent that ratio solves if desired for emphasis and fire-retardant powder body auxiliary agent can reduce carrier adhesive is brought declines problem, and the generation of this problem will cause the problem that fabric moisture-penetrability declines；To be exactly also fabric can produce when burning has a strong impact on the phenomenon that the perforation of human-body safety, drippage are melted, and multifunctional flame-proof fabric is all manufactured and designed and proposes challenge by these problems.
And at present both at home and abroad relevant research and development and industrialized development for this series products are relatively slow, therefore by extremely important to the development of this area functional textile product for the exploitation of the flame-retardant textile of several functions superposition based on anti-flaming function.
Summary of the invention
It is an object of the invention to improve the multifunctionality of solution fabric and anti-perforation is fire-retardant, make fabric have press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting, the characteristic of conduction, solving the perforation single, easy of conventional flame retardant fabric functional can the difficult problem of molten drop.
A kind of multifunctional flame-proof fabric processing and sorting method of the present invention, it is characterised in that the first step forms conduction, water repellent by padding with high temperature drying, refuses oily and anti-soda acid layer；Second step contains carbon forming agent and the water-proof air-permeable primer of phosphate flame retardant by coating and solidifies；3rd step is that coating contains carbon forming agent and the water-proof air-permeable face glue of phosphate flame retardant and solidifies；By above-mentioned three steps for the Final finishing process technology of dacron, make this dacron obtain press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting and the overall characteristic of conduction.
Wherein carbon forming agent is tetramethylolmethane, Bis(pentaerythritol), ethylenediamine triazine macromole, 1-oxo-4-methylol-2, one or more in 6,7-trioxa-1-phosphabicyclo [2,2,2] octanes (being called for short PEPA)；One or more during wherein phosphine flame retardant is hexaphenoxycyclotriphosphazene, poly bisphenol phenyl phosphate ester and poly-resorcinol phenyl phosphate ester.
Three step Final finishing processing methods of the present invention realize particular by techniques below scheme, comprise the following steps:
The first step is padded carrying out the dacron after warning fluorescence high-temperature dyeing at 100-130 DEG C in first step padding liquid, then by dacron in 80 DEG C of-130 DEG C of preliminary dryings 1.5 minutes-3 minutes, 160 DEG C-180 DEG C bakee 1.5 minutes-3 minutes, after finalizing cloth cooling, then by fabric backing through 100 DEG C-160 DEG C high temperature pasta press polish 2-3 time；After process completes, dacron weight increases 0.3%-3%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Second step, in the one side that dacron is processed by press polish, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, bakes at dacron is placed in 80-160 DEG C, and the time of baking needs 0.5-5 minute；After dacron gluing, weight increases 2%-10%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
3rd step is scribbling the dacron side of primer, coat the 3rd step face rubber cement liquid, form homogeneous glued membrane on dacron surface, dacron is placed in 80 DEG C-160 DEG C and bakes, the time that bakes needs 0.5 minute-5 minutes, and having baked rear dacron weight increases 2%-10%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
The dacron processed be provided with press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting and the overall characteristic of conduction；After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:
The present invention is unique in that application method can obtain a kind of multifunctional flame-proof dacron after dacron is carried out Final finishing processing, can have simultaneously press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting and the overall characteristic of conduction；After dacron being carried out Final finishing processing especially with this method, will not produce to melt in combustion testing and drip broken hole, the highest protection fire rating (ENISO14116-20083 level) of frock protective garment can be reached；Owing to being provided with conduction, high visual fluorescence staining, water repellent, refusing soda acid characteristic oily, anti-so that the dacron after process can reach high-visibility warning standard (ENISO20471-2013), by protective garment electrostatic standard EN1149.CLASS3；Coating material in the present invention has water resistant, moisture-inhibiting and anti-flaming function so that treated dacron can reach the highest rainproof moisture-inhibiting rank (EN343class3/3 level) of rain and snow mist class protection clothes simultaneously；The dacron using this method to carry out rear processing finishing can apply to multiple personal protection industry.
Detailed description of the invention:
Embodiment 1
Pad carrying out the dacron after warning fluorescence high-temperature dyeing at 100-130 DEG C in first step padding liquid, then by dacron in 110 DEG C of-130 DEG C of preliminary dryings 3 minutes, 160 DEG C-180 DEG C bakee 3 minutes, after finalizing cloth cooling, then by fabric backing through 140 DEG C-160 DEG C high temperature pasta press polish 3 times, having processed rear dacron weight increases by 0.8%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Then the one side processed by press polish at dacron, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, bakes at dacron is placed in 140-160 DEG C, bake the time 5 minutes, and having processed rear dacron weight increases by 6%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
Finally scribbling the dacron side of primer, coating the 3rd step face rubber cement liquid, form homogeneous glued membrane on dacron surface, dacron is placed in 140 DEG C-160 DEG C and bakes, bake the time 5 minutes, having processed rear dacron weight increases by 6%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:
Embodiment 2
Pad carrying out the dacron after warning fluorescence high-temperature dyeing at 100-130 DEG C in first step padding liquid, then by dacron in 110 DEG C of-120 DEG C of preliminary dryings 1.5 minutes, 160 DEG C-180 DEG C bakee 1.5 minutes, after finalizing cloth cooling, then by fabric backing through 100 DEG C-160 DEG C high temperature pasta press polish 2 times；After process completes, dacron weight increases by 0.5%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Then the one side processed by press polish at dacron, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, bakes at dacron is placed in 140-150 DEG C, and the time that bakes needs 3 minutes；After dacron gluing, weight increases by 4%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
Finally scribbling the dacron side of primer, coat the 3rd step face rubber cement liquid, form homogeneous glued membrane on dacron surface, dacron is placed in 140 DEG C-150 DEG C and bakes, the time that bakes needs 2 minutes, and having baked rear dacron weight increases by 3%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:
Embodiment 3
Pad carrying out the dacron after warning fluorescence high-temperature dyeing at 120-130 DEG C in first step padding liquid, then by dacron in 110 DEG C of-120 DEG C of preliminary dryings 2 minutes, 160 DEG C-180 DEG C bakee 2 minutes, after finalizing cloth cooling, then by fabric backing through 140 DEG C-150 DEG C high temperature pasta press polish 3 times；After process completes, dacron weight increases by 1%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Then the one side processed by press polish at dacron, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, bakes at dacron is placed in 130-140 DEG C, and the time that bakes needs 3 minutes；After dacron gluing, weight increases by 5%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
Finally scribbling the dacron side of primer, coating the 3rd step face rubber cement liquid, form homogeneous glued membrane on dacron surface, dacron is placed in 130 DEG C-140 DEG C and bakes, bake the time 3 minutes, having baked rear dacron weight increases by 5%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:
Embodiment 4
The first step is padded carrying out the dacron after warning fluorescence high-temperature dyeing at 120-130 DEG C in first step padding liquid, then by dacron in 110 DEG C of-130 DEG C of preliminary dryings 2 minutes, 160 DEG C-170 DEG C bakee 1.5 minutes, after finalizing cloth cooling, then by fabric backing through 110 DEG C-120 DEG C high temperature pasta press polish 2 times；After process completes, dacron weight increases by 2%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Then the one side processed by press polish at dacron, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, bakes at dacron is placed in 140-160 DEG C, and the time that bakes needs 4 minutes；After dacron gluing, weight increases by 3%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
Finally scribbling the dacron side of primer, coat the 3rd step face rubber cement liquid, form homogeneous glued membrane on dacron surface, dacron is placed in 150 DEG C-160 DEG C and bakes, the time that bakes needs 5 minutes, and having baked rear dacron weight increases by 8%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:
Embodiment 5
Pad carrying out the dacron after warning fluorescence high-temperature dyeing at 130 DEG C in first step padding liquid, then by dacron in 120 DEG C of-130 DEG C of preliminary dryings 3 minutes, 160 DEG C bakee 3 minutes, after finalizing cloth cooling, are then pressed 3 times through 150 DEG C-160 DEG C high temperature pastas by fabric backing；After process completes, dacron weight increases by 1.1%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Then the one side processed by press polish at dacron, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, is placed in by dacron at 150 DEG C and bakes, and the time that bakes needs 3 minutes；After dacron gluing, weight increases by 4%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
3rd step is scribbling the dacron side of primer, coats the 3rd step face rubber cement liquid, forms homogeneous glued membrane on dacron surface, dacron is placed in 150 DEG C and bakes, and the time that bakes needs 3 minutes, and having baked rear dacron weight increases by 5%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
The dacron processed be provided with press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting and the overall characteristic of conduction；After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:
Embodiment 6
Pad carrying out the dacron after warning fluorescence high-temperature dyeing at 130 DEG C in first step padding liquid, then by dacron in 130 DEG C of preliminary dryings 3 minutes, 180 DEG C bakee 3 minutes, after finalizing cloth cooling, then by fabric backing through 150 DEG C-160 DEG C high temperature pasta press polish 3 times；After process completes, dacron weight increases by 2%.
It is as follows that wherein said first step padding liquid calculates composition with mass parts:
Then the one side processed by press polish at dacron, coats second step primer serosity, after dacron surface forms homogeneous glued membrane, bakes at dacron is placed in 150-160 DEG C, and the time that bakes needs 3 minutes；After dacron gluing, weight increases by 5%.
It is as follows that wherein said second step primer slurry counts composition with mass parts:
Finally scribbling the dacron side of primer, coat the 3rd step face rubber cement liquid, form homogeneous glued membrane on dacron surface, dacron is placed in 150 DEG C-160 DEG C and bakes, the time that bakes needs 3 minutes, and having baked rear dacron weight increases by 5%.
It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
The dacron processed be provided with press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting and the overall characteristic of conduction；After a kind of multifunctional flame-proof fabric using the technology of the present invention to be obtained is tested, performance indications are as follows:

Claims (5)

1. the manufacture method of a multifunctional flame-proof dacron, it is characterized in that the first step is passed through to pad and high temperature drying, second step contains carbon forming agent and the water-proof air-permeable primer of phosphate flame retardant by coating and solidifies, 3rd step is that coating contains carbon forming agent and the water-proof air-permeable face glue of phosphate flame retardant and solidifies, by above-mentioned three steps for the Final finishing process technology of dacron, make this dacron obtain press down cigarette, without molten drop, anti-burning perforation, water repellent, refuse soda acid oily, anti-, moisture-inhibiting and the overall characteristic of conduction.
2. the carbon forming agent described in claim 1 is tetramethylolmethane, Bis(pentaerythritol), ethylenediamine triazine macromole, 1-oxo-4-methylol-2, one or more in 6,7-trioxa-1-phosphabicyclo [2,2,2] octanes (being called for short PEPA)；Phosphine flame retardant is one or more in hexaphenoxycyclotriphosphazene, poly bisphenol phenyl phosphate ester and poly-resorcinol phenyl phosphate ester.
3. the first step described in claim 1 is padded and high temperature drying, it is characterised by padding carrying out the dacron after warning fluorescence high-temperature dyeing at 100-130 DEG C in first step padding liquid, then by dacron in 80 DEG C of-130 DEG C of preliminary dryings 1.5 minutes-3 minutes, 160 DEG C-180 DEG C bakee 1.5 minutes-3 minutes, after finalizing cloth cooling, then by fabric backing through 100 DEG C-160 DEG C high temperature pasta press polish 2-3 time；After process completes, dacron weight increases 0.3%-3%；It is as follows that wherein said first step padding liquid calculates composition with mass parts:
4. the manufacture method of a multifunctional flame-proof dacron, second step contains carbon forming agent and the water-proof air-permeable primer of phosphate flame retardant by coating and solidifies, it is characterized in that in the one side that dacron is processed by press polish, coating second step primer serosity, after dacron surface forms homogeneous glued membrane, baking at dacron is placed in 80-160 DEG C, the time of baking needs 0.5-5 minute；After dacron gluing, weight increases 2%-10%；It is as follows that wherein said second step primer slurry counts composition with mass parts:
5. the manufacture method of a multifunctional flame-proof dacron, 3rd step is that coating contains carbon forming agent and the water-proof air-permeable face glue of phosphate flame retardant and solidifies, it is characterized in that scribbling the dacron side of primer, coat the 3rd step face rubber cement liquid, homogeneous glued membrane is formed on dacron surface, dacron being placed in 80 DEG C-160 DEG C bake, the time that bakes needs 0.5 minute-5 minutes, and having baked rear dacron weight increases 2%-10%；It is as follows that the 3rd wherein said step face rubber cement material counts composition with mass parts:
CN201610187025.6A 2016-03-30 2016-03-30 A kind of manufacturing method of multifunctional flame-proof dacron Active CN105821669B (en)

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CN109652984A (en) * 2018-12-12 2019-04-19 上海雅运新材料有限公司 A kind of fabrics flame resistance coating finishing agent composition and preparation method thereof

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CN105064017A (en) * 2015-08-03 2015-11-18 章丽珍 Making method of fireproof heat insulation curtain cloth

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CN101798759A (en) * 2009-12-21 2010-08-11 愉悦家纺有限公司 Finishing method of flocking fabric
CN102121196A (en) * 2010-12-25 2011-07-13 江苏联宏纺织有限公司 Water-proof and air-permeable coating process based on polysulfonamide fabric
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CN107282374A (en) * 2017-08-16 2017-10-24 湖州荣能达燃料贸易有限公司 A kind of efficient applicator system of yarn fabric flame-retardant layer
CN109652984A (en) * 2018-12-12 2019-04-19 上海雅运新材料有限公司 A kind of fabrics flame resistance coating finishing agent composition and preparation method thereof
CN109652984B (en) * 2018-12-12 2021-07-20 太仓宝霓实业有限公司 A kind of fabric flame retardant coating finishing agent composition and preparation method thereof

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