CN106145698B - Vacuum glass and its manufacturing method of batch synthesis - Google Patents
Vacuum glass and its manufacturing method of batch synthesis Download PDFInfo
- Publication number
- CN106145698B CN106145698B CN201610417659.6A CN201610417659A CN106145698B CN 106145698 B CN106145698 B CN 106145698B CN 201610417659 A CN201610417659 A CN 201610417659A CN 106145698 B CN106145698 B CN 106145698B
- Authority
- CN
- China
- Prior art keywords
- glass
- vacuum
- plate glass
- edge sealing
- sealing material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000011521 glass Substances 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 8
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 8
- 239000005357 flat glass Substances 0.000 claims abstract description 25
- 239000003566 sealing material Substances 0.000 claims abstract description 15
- 239000004744 fabric Substances 0.000 claims abstract description 9
- 238000005245 sintering Methods 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 4
- 239000006066 glass batch Substances 0.000 claims abstract 2
- 239000000758 substrate Substances 0.000 claims description 6
- 238000007688 edging Methods 0.000 claims description 4
- 241001074085 Scophthalmus aquosus Species 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 230000003247 decreasing effect Effects 0.000 claims description 3
- 239000003292 glue Substances 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 8
- 238000004134 energy conservation Methods 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 230000007547 defect Effects 0.000 abstract description 2
- 239000002184 metal Substances 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C27/00—Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
- C03C27/06—Joining glass to glass by processes other than fusing
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Joining Of Glass To Other Materials (AREA)
Abstract
The invention discloses a kind of manufacturing methods of vacuum glass batch synthesis, it is supportted by cloth after getting the blind hole for placing getter on one flat plate glass, another sintering curing after edge coats special edge sealing material, using the glass of cloth support cured glass is covered the bottom of as, two fixed with special-purpose high temperature metal clip it is compound, it is put into the method that the edge sealing material on plate glass is melted to by heating up sealing-in again after extracting air in vacuum kettle out, batch micro operations vacuum glass, this method step is simple, manufacturing process energy conservation and environmental protection, vacuum degree is high, and defect rate is low.
Description
Technical field
The present invention relates to vacuum glass method field of manufacturing, and in particular to a kind of energy-saving and environment-friendly vacuum glass and its batch
The manufacturing method of synthesis.
Background technology
In the building of cold district, it is installation double glazing to prevent the most common method of the rapid heat dissipations such as door and window, however
Double glazing still results in energy leakage, for example when interior is turned on the aircondition, about 25% energy can all be dissipated from door and window
It sends out, virtually results in the waste of the energy.How so that becoming vacuum state between double glazing to avoid the energy
Waste is many scientific research personnel all in the project of thinking, the production method of existing vacuum glass be all monolithic production and there are one
Vacuum noz(zle), cost high finished product rate are low.The present invention changes the state of existing time-consuming expense resource, energy-efficient.
Getter be for obtaining, maintaining vacuum and purified gases etc., can effectively certain (kind) gas molecules of sorption
Preparation or device common name.There are the diversified forms such as powdery, disk like, band-like, tubulose, ring-type, cup-shaped.
Invention content
Goal of the invention：The purpose of the invention is to make up the deficiency of existing investigative technique, a kind of energy conservation and environmental protection is provided
Batch synthesis vacuum glass manufacturing method.
Technical solution：A kind of manufacturing method of batch synthesis vacuum glass, includes the following steps：
a：By two blocks of plate glass, cuts, edging and cleans, obtain two plate substrate plate glass, for use；
b：The two plate substrate plate glass obtained in step a are supported with 2~5cm square cloth with ball-type, while arbitrary
Arm of angle brill grinds a diameter of 6mm to 12mm, and depth is the blind hole of 2~3mm；
c：Another sheet glass is coated into edge sealing material, a piece of is put into together in sintering furnace with 250~450 DEG C of temperature ranges with preceding
Lower sintering 5~20 minutes, edge sealing material becomes solid-state after cooling；
d：The two panels plate glass sintered is placed in getter or more as egative film using cloth blade in blind hole to be overlapped, edge
Alignment, is used in combination clip to clip together, puts into vacuum kettle, closes vacuum kettle, and after kettle Inner is vacuumized, gradually heating makes temperature to vacuum kettle
Degree rises to 250~450 DEG C again, and edge sealing material is molten into glue, seals the existing gap between two panels plate glass originally, together
Shi Zidong activated degassers so that close sealing-in between two panels plate glass；
e：Continuously decreasing the temperature in vacuum kettle so that edge sealing cures, and deflates, after being normal temperature and pressure in vacuum kettle,
It takes out to get vacuum glass.
Advantageous effect：The present invention is put into true by the special edge sealing material of coating after the cloth support between two blocks of plate glass, sintering
It realizes that batch vacuumizes in empty kettle, and is placed in getter in blind hole and vacuum degree is further increased, finally by plate glass
On the method for edge sealing material fusing sealing-in manufacture vacuum glass, this method step is simple, manufacturing process energy conservation and environmental protection, and vacuum degree is high
And defect rate is low.
Specific implementation mode：
In the present invention, edge sealing material may be used application No. is 201310584824.3, entitled《One kind being used for negative pressure kettle method
Manufacture the edging material of vacuum glass》In edge sealing material.Getter is commercially available.Clip is special-purpose high temperature metal clip.
Embodiment 1：
A kind of manufacturing method of batch synthesis vacuum glass, includes the following steps：
a：By two blocks of plate glass, cuts, edging and cleans, obtain two plate substrate plate glass, for use；
b：The two plate substrate plate glass obtained in step a are supported with 2~5cm square cloth with ball-type, while arbitrary
Arm of angle brill grinds a diameter of 6mm to 12mm, and depth is the blind hole of 2~3mm；
c：Another sheet glass is coated into edge sealing material, a piece of is put into together in sintering furnace with 250~450 DEG C of temperature ranges with preceding
Lower sintering 5~20 minutes, edge sealing material becomes solid-state after cooling；
d：The two panels plate glass sintered is placed in getter or more as egative film using cloth blade in blind hole to be overlapped, edge
Alignment, is used in combination clip to clip together, puts into vacuum kettle, closes vacuum kettle, and after kettle Inner is vacuumized, gradually heating makes temperature to vacuum kettle
Degree rises to 250~450 DEG C again, and edge sealing material is molten into glue, seals the existing gap between two panels plate glass originally, together
Shi Zidong activated degassers so that close sealing-in between two panels plate glass,；
e：Continuously decreasing the temperature in vacuum kettle so that edge sealing cures, and deflates, after being normal temperature and pressure in vacuum kettle,
It takes out to get vacuum glass.
Step of the present invention is simple, product energy conservation and environmental protection, and the vacuum degree between vacuum glass is more than national standard.
Claims (1)
1. a kind of manufacturing method of vacuum glass batch synthesis, it is characterised in that：Include the following steps：
a：By two blocks of plate glass, cuts, edging and cleans, obtain two plate substrate plate glass, for use；
b：The plate substrate plate glass obtained in step a is supported with 2~5cm square cloth with ball-type, while in the arbitrary arm of angle
Brill grinds a diameter of 6mm to 12mm, and depth is the blind hole of 2~3mm；
c：Another sheet glass is coated into edge sealing material, a piece of is put into together in sintering furnace to be burnt under 250~450 DEG C of temperature ranges with preceding
Knot 5~20 minutes, edge sealing material becomes solid-state after cooling；
d：The two panels plate glass sintered is placed in getter or more as egative film using cloth blade in blind hole to be overlapped, edge pair
Together, it is used in combination clip to clip together, puts into vacuum kettle, close vacuum kettle, after kettle Inner is vacuumized, gradually heating makes temperature to vacuum kettle
250~450 DEG C are risen to again, and edge sealing material is molten into glue, seals the existing gap between two panels plate glass originally, simultaneously
Automatic activated degasser so that close sealing-in between two panels plate glass；
e：Continuously decreasing the temperature in vacuum kettle so that edge sealing cures, and deflates, and after being normal temperature and pressure in vacuum kettle, takes out,
Up to vacuum glass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610417659.6A CN106145698B (en) | 2016-06-12 | 2016-06-12 | Vacuum glass and its manufacturing method of batch synthesis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610417659.6A CN106145698B (en) | 2016-06-12 | 2016-06-12 | Vacuum glass and its manufacturing method of batch synthesis |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106145698A CN106145698A (en) | 2016-11-23 |
| CN106145698B true CN106145698B (en) | 2018-11-13 |
Family
ID=57353240
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610417659.6A Active CN106145698B (en) | 2016-06-12 | 2016-06-12 | Vacuum glass and its manufacturing method of batch synthesis |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106145698B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114671630B (en) * | 2020-12-24 | 2024-12-10 | 唐健正 | Splicing component and vacuum glass made of the splicing component |
| CN119528461B (en) * | 2024-10-31 | 2025-10-03 | 皓晶控股集团股份有限公司 | Vacuum glass and preparation method thereof |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3082046B2 (en) * | 1989-08-23 | 2000-08-28 | ザ ユニバーシティ オブ シドニー | Thermal insulation glass panel and method of constructing the same |
| CN2522579Y (en) * | 2001-12-07 | 2002-11-27 | 唐健正 | Vacuum glass with getter |
| CN101215076B (en) * | 2008-01-07 | 2012-07-04 | 左树森 | Method for preparing vacuum glass |
| CN101792253B (en) * | 2010-04-14 | 2012-07-11 | 左树森 | Encapsulation method for vacuum glass getter |
| CN103723911B (en) * | 2013-11-19 | 2018-05-04 | 江苏圣帝真空玻璃科技有限公司 | A kind of method using negative pressure kettle manufacture vacuum glass |
| CN104230186B (en) * | 2014-08-21 | 2017-04-26 | 江苏凯尚真空玻璃制造有限公司 | Method for manufacturing vacuum glass based on edge sealing technique and negative pressure kettle |
| CN104193155A (en) * | 2014-08-22 | 2014-12-10 | 徐良 | Manufacturing method of three-glass-two-cavity vacuum glass |
-
2016
- 2016-06-12 CN CN201610417659.6A patent/CN106145698B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN106145698A (en) | 2016-11-23 |
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| GR01 | Patent grant |