CN106245147A - A kind of flame-proof polylactic acid fabric lining - Google Patents
A kind of flame-proof polylactic acid fabric lining Download PDFInfo
- Publication number
- CN106245147A CN106245147A CN201610619302.6A CN201610619302A CN106245147A CN 106245147 A CN106245147 A CN 106245147A CN 201610619302 A CN201610619302 A CN 201610619302A CN 106245147 A CN106245147 A CN 106245147A
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- Prior art keywords
- polylactic acid
- raw material
- acid
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- flame
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- 229920000747 poly(lactic acid) Polymers 0.000 title claims abstract description 50
- 239000004626 polylactic acid Substances 0.000 title claims abstract description 50
- 239000004744 fabric Substances 0.000 title claims abstract description 25
- 239000002253 acid Substances 0.000 claims abstract description 27
- 239000002994 raw material Substances 0.000 claims abstract description 26
- 238000002156 mixing Methods 0.000 claims abstract description 24
- 239000000835 fiber Substances 0.000 claims abstract description 22
- 239000000843 powder Substances 0.000 claims abstract description 16
- 238000009987 spinning Methods 0.000 claims abstract description 16
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- 238000002074 melt spinning Methods 0.000 claims abstract description 9
- 229920001661 Chitosan Polymers 0.000 claims abstract description 8
- 239000004594 Masterbatch (MB) Substances 0.000 claims abstract description 8
- UQZIYBXSHAGNOE-USOSMYMVSA-N Stachyose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO[C@@H]2[C@@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O2)O1 UQZIYBXSHAGNOE-USOSMYMVSA-N 0.000 claims abstract description 8
- 229910052599 brucite Inorganic materials 0.000 claims abstract description 8
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000001125 extrusion Methods 0.000 claims abstract description 8
- 239000010445 mica Substances 0.000 claims abstract description 8
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 229910052901 montmorillonite Inorganic materials 0.000 claims abstract description 8
- 230000000979 retarding effect Effects 0.000 claims abstract description 8
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 8
- UQZIYBXSHAGNOE-XNSRJBNMSA-N stachyose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO[C@@H]3[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O3)O)O2)O)O1 UQZIYBXSHAGNOE-XNSRJBNMSA-N 0.000 claims abstract description 8
- 229940070527 tourmaline Drugs 0.000 claims abstract description 8
- 229910052613 tourmaline Inorganic materials 0.000 claims abstract description 8
- 239000011032 tourmaline Substances 0.000 claims abstract description 8
- -1 and be vacuum dried Substances 0.000 claims description 7
- 238000004804 winding Methods 0.000 claims description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 238000005406 washing Methods 0.000 description 5
- 239000003063 flame retardant Substances 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 210000000582 semen Anatomy 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000003856 thermoforming Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/07—Addition of substances to the spinning solution or to the melt for making fire- or flame-proof filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses the preparation method of a kind of flame-proof polylactic acid fabric lining: (1) is equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing raw material: PLA polylactic acid 65 89 parts；PBS0.2 part；Tourmaline powder 0.2 part；Montmorillonite 0.8 1 parts；1 part of stachyose；Chitosan 0.2 04 parts；Brucite 0.3 0.5 parts；Mica powder 0.8 part；Carborundum 0.3 part；(2) above-mentioned mixed uniformly polydactyl acid mixing raw material being prepared polydactyl acid master batch by double screw extruder melt blending, extrusion, and is vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
Description
Technical field
The present invention relates to a kind of flame-proof polylactic acid fabric lining, belong to field of textiles.
Background technology
Acid fiber by polylactic is with amyloid agricultural product such as Semen Maydis, Semen Tritici aestivi, Radix Betaes as raw material, after fermented generation lactic acid,
To make through polycondensation and melt spinning again. acid fiber by polylactic is that a kind of raw material can be planted, easily be planted, and garbage can be certainly in nature
So synthetic fibers of degraded.It can be analyzed to carbon dioxide and water through microbial action in soil or sea water, during burning, and will not
Distribute poison, do not result in pollution, be the ecological fiber of a kind of sustainable development.Its fabric feel, drapability are good, anti-purple
Outside line, has relatively low combustibility and excellent processing characteristics, is applicable to various fashionable dress, easy dress, sports goods and health and uses
Product etc., have broad application prospects.
In recent years, polylactic acid is due to its excellent biodegradability, abundant source and good machining property
Paid close attention to widely.At present, as general thermoplastic polyester, polylactic acid is in different processing and forming sides
FAXIA can be prepared as thin film, sheet material, bar etc..Its fiber after the secondary operations such as thermoforming, spinning weaving, packaging, agriculture
The most increasingly extensive being employed in field such as industry, health care, daily living article.At current plastics industry circle, polylactic acid quilt
It is referred to as the most promising " green plastic ".But polylactic acid easily burns, limited oxygen index only has 19%.
It is desirable to provide a kind of flame-proof polylactic acid fabric lining, it makes simple, good flame retardation effect.
Summary of the invention
The present invention is directed to shortcoming of the prior art, it is desirable to provide a kind of flame-proof polylactic acid fabric lining, its system
Make simple, good flame retardation effect.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of preparation method of flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 65-89 part；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 0.8-1 part；
1 part of stachyose；
Chitosan 0.2-04 part；
Brucite 0.3-0.5 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
Described spinning temperature is 200 DEG C, and winding speed is 1300 m/min；Drawing temperature is 95 DEG C, and drafting multiple is 2.5 times；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
The invention have benefit that:
(1) present invention process is simple, it is easy to industrialization operates, it is not necessary to adds fire retardant and just can reach extraordinary fire-retardant effect
Really, energy-conserving and environment-protective.
(2) the modified polylactic acid fiber fabric that the present invention prepares has good heat-proof combustion-resistant effect, additionally has easily
Upper dye, the advantage of good spinnability.
Detailed description of the invention
Embodiment 1:
A kind of preparation method of flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 65 parts；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 1 part；
1 part of stachyose；
Chitosan 0.2 part；
Brucite 0.5 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
Described spinning temperature is 200 DEG C, and winding speed is 1300 m/min；Drawing temperature is 95 DEG C, and drafting multiple is 2.5 times；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
Result: limited oxygen index is 26%, dye-uptake 98%, washing fastness (AATCC test) reaches 5 grades.
Embodiment 2:
A kind of preparation method of flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 89 parts；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 0.8 part；
1 part of stachyose；
Chitosan 0.4 part；
Brucite 0.3 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
Described spinning temperature is 200 DEG C, and winding speed is 1300 m/min；Drawing temperature is 95 DEG C, and drafting multiple is 2.5 times；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
Result: limited oxygen index is 39%, dye-uptake 95%, washing fastness (AATCC test) reaches 5 grades.
Embodiment 3:
A kind of preparation method of flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 70 parts；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 0.9 part；
1 part of stachyose；
Chitosan 0.3 part；
Brucite 0.4 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
Described spinning temperature is 200 DEG C, and winding speed is 1300 m/min；Drawing temperature is 95 DEG C, and drafting multiple is 2.5 times；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
Result: limited oxygen index is 28%, dye-uptake 97%, washing fastness (AATCC test) reaches 5 grades.
Embodiment 4:
A kind of preparation method of flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 80 parts；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 0.8 part；
1 part of stachyose；
Chitosan 0.4 part；
Brucite 0.5 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
Described spinning temperature is 200 DEG C, and winding speed is 1300 m/min；Drawing temperature is 95 DEG C, and drafting multiple is 2.5 times；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
Result: limited oxygen index is 35%, dye-uptake 96%, washing fastness (AATCC test) reaches 5 grades.
Embodiment 5:
A kind of preparation method of flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 75 parts；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 1 part；
1 part of stachyose；
Chitosan 0.2 part；
Brucite 0.3 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
Described spinning temperature is 200 DEG C, and winding speed is 1300 m/min；Drawing temperature is 95 DEG C, and drafting multiple is 2.5 times；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
Result: limited oxygen index is 30%, dye-uptake 98%, washing fastness (AATCC test) reaches 5 grades.
As can be seen here, present invention process is simple, it is easy to industrialization operates, it is not necessary to adds fire retardant and just can reach very
Good flame retardant effect, energy-conserving and environment-protective.The modified polylactic acid fiber fabric that the present invention prepares has good heat-proof combustion-resistant effect, this
Outward also there is Yi Shangran, the advantage of good spinnability.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, according to technical scheme and
Inventive concept equivalent or change in addition, all should contain within protection scope of the present invention.
Claims (3)
1. a preparation method for flame-proof polylactic acid fabric lining, its step is as follows:
(1) being equipped with raw material by following parts by weight, being subsequently adding in high-speed mixer is uniformly dispersed obtains polydactyl acid mixing
Raw material:
PLA polylactic acid 65-89 part；
PBS0.2 part；
Tourmaline powder 0.2 part；
Montmorillonite 0.8-1 part；
1 part of stachyose；
Chitosan 0.2-04 part；
Brucite 0.3-0.5 part；
Mica powder 0.8 part；
Carborundum 0.3 part；
(2) above-mentioned mixed uniformly polydactyl acid mixing raw material is passed through double screw extruder melt blending, extrusion prepares and changes
Property polylactic acid master batch, and be vacuum dried, mixture obtains modified polylactic acid fiber through circular spinneret orifice spinning on melt spinning machine；
(3) above-mentioned acid fiber by polylactic is woven into inflaming retarding fabric.
2. described in claim 1 preparation method, it is characterised in that:
Described step (2 parameters be spinning temperature be 200 DEG C, winding speed is 1300 m/min；Drawing temperature is 95 DEG C, drawing-off
Multiple is 2.5 times.
3. the fabric that claim 1-2 preparation method prepares.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610619302.6A CN106245147A (en) | 2016-08-02 | 2016-08-02 | A kind of flame-proof polylactic acid fabric lining |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610619302.6A CN106245147A (en) | 2016-08-02 | 2016-08-02 | A kind of flame-proof polylactic acid fabric lining |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106245147A true CN106245147A (en) | 2016-12-21 |
Family
ID=57606518
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610619302.6A Pending CN106245147A (en) | 2016-08-02 | 2016-08-02 | A kind of flame-proof polylactic acid fabric lining |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106245147A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107630261A (en) * | 2017-10-24 | 2018-01-26 | 安徽亚源印染有限公司 | A kind of preparation method of high intensity acid fiber by polylactic |
| CN107630260A (en) * | 2017-10-24 | 2018-01-26 | 安徽亚源印染有限公司 | A kind of preparation method of stretch-proof acid fiber by polylactic |
| CN107723843A (en) * | 2017-10-24 | 2018-02-23 | 安徽亚源印染有限公司 | A kind of preparation method of tear-resistant acid fiber by polylactic |
| CN107868993A (en) * | 2017-10-24 | 2018-04-03 | 安徽亚源印染有限公司 | A kind of flame-proof polylactic acid fabric lining and preparation method thereof |
| CN109706539A (en) * | 2018-12-25 | 2019-05-03 | 上海德福伦化纤有限公司 | A kind of anion acid fiber by polylactic and preparation method thereof |
| CN112813528A (en) * | 2020-12-30 | 2021-05-18 | 浪莎针织有限公司 | Degradable flame-retardant polylactic acid elastic fiber and preparation method thereof |
| CN114921870A (en) * | 2022-06-24 | 2022-08-19 | 武汉纺织大学 | Flame-retardant polylactic acid fabric and preparation method thereof |
| CN119083030A (en) * | 2024-10-11 | 2024-12-06 | 杭州高健展览装饰工程有限公司 | Heat-resistant and flame-retardant polylactic acid fiber cloth and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107630261A (en) * | 2017-10-24 | 2018-01-26 | 安徽亚源印染有限公司 | A kind of preparation method of high intensity acid fiber by polylactic |
| CN107630260A (en) * | 2017-10-24 | 2018-01-26 | 安徽亚源印染有限公司 | A kind of preparation method of stretch-proof acid fiber by polylactic |
| CN107723843A (en) * | 2017-10-24 | 2018-02-23 | 安徽亚源印染有限公司 | A kind of preparation method of tear-resistant acid fiber by polylactic |
| CN107868993A (en) * | 2017-10-24 | 2018-04-03 | 安徽亚源印染有限公司 | A kind of flame-proof polylactic acid fabric lining and preparation method thereof |
| CN109706539A (en) * | 2018-12-25 | 2019-05-03 | 上海德福伦化纤有限公司 | A kind of anion acid fiber by polylactic and preparation method thereof |
| CN112813528A (en) * | 2020-12-30 | 2021-05-18 | 浪莎针织有限公司 | Degradable flame-retardant polylactic acid elastic fiber and preparation method thereof |
| CN114921870A (en) * | 2022-06-24 | 2022-08-19 | 武汉纺织大学 | Flame-retardant polylactic acid fabric and preparation method thereof |
| CN114921870B (en) * | 2022-06-24 | 2024-05-28 | 武汉纺织大学 | Flame retardant polylactic acid fabric and preparation method thereof |
| CN119083030A (en) * | 2024-10-11 | 2024-12-06 | 杭州高健展览装饰工程有限公司 | Heat-resistant and flame-retardant polylactic acid fiber cloth and preparation method thereof |
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Application publication date: 20161221 |