CN107022902A - A kind of preparation method of shuttlecock feather piece - Google Patents
A kind of preparation method of shuttlecock feather piece Download PDFInfo
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- CN107022902A CN107022902A CN201710301723.9A CN201710301723A CN107022902A CN 107022902 A CN107022902 A CN 107022902A CN 201710301723 A CN201710301723 A CN 201710301723A CN 107022902 A CN107022902 A CN 107022902A
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- China
- Prior art keywords
- parts
- weight
- feather
- shuttlecock
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 210000003746 feather Anatomy 0.000 title claims abstract description 51
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000004061 bleaching Methods 0.000 claims abstract description 13
- 238000007654 immersion Methods 0.000 claims abstract description 13
- 238000005238 degreasing Methods 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 10
- 238000004140 cleaning Methods 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 8
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims abstract description 8
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 5
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 5
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 5
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 5
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000010265 sodium sulphite Nutrition 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
- 238000003756 stirring Methods 0.000 claims description 16
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 244000144977 poultry Species 0.000 claims description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000011259 mixed solution Substances 0.000 claims description 6
- 239000004094 surface-active agent Substances 0.000 claims description 5
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 3
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 235000006408 oxalic acid Nutrition 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 6
- 239000007844 bleaching agent Substances 0.000 abstract description 4
- 239000000377 silicon dioxide Substances 0.000 abstract description 3
- 238000004043 dyeing Methods 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 235000012239 silicon dioxide Nutrition 0.000 abstract description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- WWSNLNXXISONLQ-UHFFFAOYSA-N C(CCCCCCCCCCCCCCC)Cl(C)(C)C Chemical compound C(CCCCCCCCCCCCCCC)Cl(C)(C)C WWSNLNXXISONLQ-UHFFFAOYSA-N 0.000 description 1
- 229910008051 Si-OH Inorganic materials 0.000 description 1
- 229910002808 Si–O–Si Inorganic materials 0.000 description 1
- 229910006358 Si—OH Inorganic materials 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 125000005909 ethyl alcohol group Chemical group 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000007781 pre-processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M19/00—Treatment of feathers
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of preparation method of shuttlecock with feather piece, first oxidation bleaching and reducing bleach are carried out by feather progress cleaning and degreasing, ferrous sulfate mordant dyeing pretreatment and then respectively with hydrogen peroxide and sodium sulfite, silane coupler KH 560 is added in reducing bleach process to be handled, then the feather piece after bleaching is obtained into slice of shuttlecock finished product in the silicon dioxide gel that sol-gal process is obtained after immersion treatment, drying.The shuttlecock that the present invention is obtained feather piece not only has good whiteness and presentation quality, and with good intensity and toughness, good mechanical property, combination property is high.
Description
Technical field
The present invention relates to feather processing technology field, more particularly to a kind of shuttlecock preparation method of feather piece.
Background technology
In China, shuttlecock is a kind of very high motion of popularity, with it is easy, view and admire, entertain, salubrity the features such as,
It is deep to be liked by the people.Feather piece is the topmost raw material of shuttlecock, and its intensity, toughness have to the quality of shuttlecock
Important influence.At present, during the working process of shuttlecock, essential technique be by feather by bleaching obtain white
The feather piece of color.However, bleaching is easily destroyed the structure of feather, reduce the mechanical performance of feather, so as to get feather piece
It is difficult to reach requirement in terms of intensity, toughness, it is impossible to produce the feather piece of high-quality, so as to influence the quality of shuttlecock.Cause
How this, improve the mechanical performance of feather piece while presentation quality of the bleaching to improve feather piece is carried out, accord with it
The requirement of actual use is closed, as current urgent problem.
The content of the invention
The object of the invention is exactly that there is provided a kind of shuttlecock plumage of satisfactory mechanical property in order to make up the defect of prior art
The preparation method of workprint.
The present invention is achieved by the following technical solutions：
A kind of shuttlecock preparation method of feather piece, comprises the following steps：
（1）1-1.5 parts by weight of sodium hydroxide and 0.3-0.5 parts by weight lauryl sodium sulfate are added in 80-100 parts by weight water
Stirring and dissolving, then adds 80-100 parts by weight poultry feather and 2-4h progress cleaning and degreasing processing is stirred in 50-60 DEG C, then will
Poultry feather after cleaning and degreasing is cleaned with clear water, dry for standby；
（2）0.3-0.5 parts by weight of ferrous sulfate and 0.1-0.2 parts surfactants are added and stirred in 80-100 parts by weight water
Mix and be uniformly dissolved, then add step（1）Poultry feather immersion treatment 15-30min after middle degreasing, is cleaned with clear water and obtains pre-
Handle feather；
（3）By step（2）Obtained pretreatment feather add 5-10 parts by weight hydrogen peroxide, 0.1-0.2 parts by weight sodium tripolyphosphate,
60-80 DEG C of stir process 2-4h in the mixed solution of 0.1-0.2 parts by weight pull open powder and 80-100 parts by weight water, is cleaned with clear water
After add 0.3-0.5 parts by weight sodium sulfite, 0.6-0.8 parts by weight oxalic acid, 0.5-1 parts by weight silane coupler KH-560 and
50-60 DEG C of stir process 0.5-1h in the mixed solution of 80-100 parts by weight water, obtains bleaching feather piece after being cleaned with clear water；
（4）It is 0.05- by 0.5-1 parts by weight tetraethyl orthosilicate, 3-5 parts by weight absolute ethyl alcohol and 1-1.5 parts by weight mass fraction
0.1% hydrochloric acid solution mixing stirs 0.5-1h after 40-50 DEG C, is then slowly added into 80-100 parts by weight water and stirs,
Add step（3）In bleaching feather piece immersion treatment 12-24h, then take out drying, obtain slice of shuttlecock.
Described surfactant is selected from NPE, empgen BB or cetyl trimethyl chlorine
Change the one or more in ammonium.
The step（2）The temperature of middle immersion treatment is 35-45 DEG C.
The mass fraction of the hydrogen peroxide is 15-30%.
The step（4）The temperature of middle immersion treatment is 50-60 DEG C, and the temperature of drying is 90-100 DEG C.
It is an advantage of the invention that：
Feather is first carried out cleaning and degreasing, ferrous sulfate mordant dyeing pretreatment and then uses hydrogen peroxide and sodium sulfite respectively by the present invention
Oxidation bleaching and reducing bleach are carried out, silane coupler KH-560 processing is added in reducing bleach process, it is fine to feather
Si-OH groups are introduced in dimension, then soak the feather piece after bleaching in the silicon dioxide gel that sol-gel process is obtained
Silica, is firmly bonded to inside feather fiber by bubble processing by Si-O-Si keys, forms steady in feather piece after drying
Fixed three-dimensional net structure, so as to obtain slice of shuttlecock finished product.The shuttlecock feather piece that the present invention is obtained not only has
Good whiteness and presentation quality, and with good intensity and toughness, good mechanical property, combination property is high.
Embodiment
A kind of shuttlecock preparation method of feather piece, comprises the following steps：
（1）1 parts by weight of sodium hydroxide and 0.3 parts by weight lauryl sodium sulfate are added into stirring and dissolving in 80 parts by weight water, so
After add 80 parts by weight poultry feathers in 50 DEG C stir 2h carry out cleaning and degreasing processing, then by the poultry feather after cleaning and degreasing
Cleaned with clear water, dry for standby；
（2）Stirring and dissolving in 0.3 parts by weight of ferrous sulfate and 0.1 parts surfactant, 80 parts by weight water of addition is uniform,
Then step is added（1）Poultry feather immersion treatment 15min after middle degreasing, is cleaned with clear water and obtains pre-processing feather；
（3）By step（2）Obtained pretreatment feather adds 5 parts by weight hydrogen peroxide, 0.1 parts by weight sodium tripolyphosphate, 0.1 weight
60 DEG C of stir process 2h in the mixed solution of part pull open powder and 80 parts by weight water, add 0.3 parts by weight sub- after being cleaned with clear water
50 DEG C are stirred in sodium sulphate, 0.6 parts by weight oxalic acid, the mixed solution of 0.5 parts by weight silane coupler KH-560 and 80 parts by weight water
Processing 0.5h is mixed, obtains bleaching feather piece after being cleaned with clear water；
（4）0.5 parts by weight tetraethyl orthosilicate, 3 parts by weight absolute ethyl alcohols and 1 parts by weight mass fraction is molten for 0.05% hydrochloric acid
Liquid mixing stirs 0.5h after 40 DEG C, is then slowly added into 80 parts by weight water and stirs, adds step（3）In bleaching
Feather piece immersion treatment 12h, then takes out drying, obtains slice of shuttlecock.
Described surfactant is NPE.
The step（2）The temperature of middle immersion treatment is 35 DEG C.
The mass fraction of the hydrogen peroxide is 15%.
The step（4）The temperature of middle immersion treatment is 50 DEG C, and the temperature of drying is 90 DEG C.
Claims (5)
1. a kind of shuttlecock preparation method of feather piece, it is characterised in that comprise the following steps：
（1）1-1.5 parts by weight of sodium hydroxide and 0.3-0.5 parts by weight lauryl sodium sulfate are added in 80-100 parts by weight water
Stirring and dissolving, then adds 80-100 parts by weight poultry feather and 2-4h progress cleaning and degreasing processing is stirred in 50-60 DEG C, then will
Poultry feather after cleaning and degreasing is cleaned with clear water, dry for standby；
（2）0.3-0.5 parts by weight of ferrous sulfate and 0.1-0.2 parts surfactants are added and stirred in 80-100 parts by weight water
Mix and be uniformly dissolved, then add step（1）Poultry feather immersion treatment 15-30min after middle degreasing, is cleaned with clear water and obtains pre-
Handle feather；
（3）By step（2）Obtained pretreatment feather add 5-10 parts by weight hydrogen peroxide, 0.1-0.2 parts by weight sodium tripolyphosphate,
60-80 DEG C of stir process 2-4h in the mixed solution of 0.1-0.2 parts by weight pull open powder and 80-100 parts by weight water, is cleaned with clear water
After add 0.3-0.5 parts by weight sodium sulfite, 0.6-0.8 parts by weight oxalic acid, 0.5-1 parts by weight silane coupler KH-560 and
50-60 DEG C of stir process 0.5-1h in the mixed solution of 80-100 parts by weight water, obtains bleaching feather piece after being cleaned with clear water；
（4）It is 0.05- by 0.5-1 parts by weight tetraethyl orthosilicate, 3-5 parts by weight absolute ethyl alcohol and 1-1.5 parts by weight mass fraction
0.1% hydrochloric acid solution mixing stirs 0.5-1h after 40-50 DEG C, is then slowly added into 80-100 parts by weight water and stirs,
Add step（3）In bleaching feather piece immersion treatment 12-24h, then take out drying, obtain slice of shuttlecock.
2. the preparation method of a kind of shuttlecock feather piece according to claim 1, it is characterised in that live on described surface
One or more of the property agent in NPE, empgen BB or hexadecyltrimethylammonium chloride.
3. a kind of preparation method of shuttlecock feather piece according to claim 1, it is characterised in that the step（2）
The temperature of middle immersion treatment is 35-45 DEG C.
4. the preparation method of a kind of shuttlecock feather piece according to claim 1, it is characterised in that the hydrogen peroxide
Mass fraction is 15-30%.
5. a kind of preparation method of shuttlecock feather piece according to claim 1, it is characterised in that the step（4）
The temperature of middle immersion treatment is 50-60 DEG C, and the temperature of drying is 90-100 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710301723.9A CN107022902A (en) | 2017-05-02 | 2017-05-02 | A kind of preparation method of shuttlecock feather piece |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710301723.9A CN107022902A (en) | 2017-05-02 | 2017-05-02 | A kind of preparation method of shuttlecock feather piece |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107022902A true CN107022902A (en) | 2017-08-08 |
Family
ID=59528278
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710301723.9A Pending CN107022902A (en) | 2017-05-02 | 2017-05-02 | A kind of preparation method of shuttlecock feather piece |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107022902A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114164673A (en) * | 2021-12-01 | 2022-03-11 | 安徽芙芮雅羽绒有限公司 | Surface treatment process for improving feather processing characteristics |
| CN116427178A (en) * | 2023-05-25 | 2023-07-14 | 宁波东港体育用品有限公司 | Badminton feather tablet toughening agent and preparation method and application thereof |
| CN116497607A (en) * | 2023-05-25 | 2023-07-28 | 宁波东港体育用品有限公司 | A kind of badminton flakes treatment agent and its preparation method and application |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102720052A (en) * | 2012-07-02 | 2012-10-10 | 北京泛博化学股份有限公司 | Method for bleaching black feathers and adopted bleaching agent, bleaching auxiliary and bleacher |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN104294577A (en) * | 2013-07-16 | 2015-01-21 | 威海市锐达羽毛制品有限公司 | A bleaching method of colored badminton ball feathers |
-
2017
- 2017-05-02 CN CN201710301723.9A patent/CN107022902A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102720052A (en) * | 2012-07-02 | 2012-10-10 | 北京泛博化学股份有限公司 | Method for bleaching black feathers and adopted bleaching agent, bleaching auxiliary and bleacher |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN104294577A (en) * | 2013-07-16 | 2015-01-21 | 威海市锐达羽毛制品有限公司 | A bleaching method of colored badminton ball feathers |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114164673A (en) * | 2021-12-01 | 2022-03-11 | 安徽芙芮雅羽绒有限公司 | Surface treatment process for improving feather processing characteristics |
| CN116427178A (en) * | 2023-05-25 | 2023-07-14 | 宁波东港体育用品有限公司 | Badminton feather tablet toughening agent and preparation method and application thereof |
| CN116497607A (en) * | 2023-05-25 | 2023-07-28 | 宁波东港体育用品有限公司 | A kind of badminton flakes treatment agent and its preparation method and application |
| CN116427178B (en) * | 2023-05-25 | 2025-08-29 | 宁波东港体育用品有限公司 | A badminton feather toughening agent and its preparation method and application |
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Application publication date: 20170808 |