CN107603399A - A kind of high attachment coating in rattan wicker plaiting article surface - Google Patents
A kind of high attachment coating in rattan wicker plaiting article surface Download PDFInfo
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- CN107603399A CN107603399A CN201710849261.4A CN201710849261A CN107603399A CN 107603399 A CN107603399 A CN 107603399A CN 201710849261 A CN201710849261 A CN 201710849261A CN 107603399 A CN107603399 A CN 107603399A
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- CN
- China
- Prior art keywords
- coating
- plaiting article
- polyvinyl alcohol
- wicker plaiting
- rattan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000011248 coating agent Substances 0.000 title claims abstract description 38
- 238000000576 coating method Methods 0.000 title claims abstract description 38
- 241000345998 Calamus manan Species 0.000 title claims abstract description 33
- 235000012950 rattan cane Nutrition 0.000 title claims abstract description 33
- 238000009954 braiding Methods 0.000 title claims abstract description 30
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 39
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000203 mixture Substances 0.000 claims abstract description 23
- 229920002307 Dextran Polymers 0.000 claims abstract description 14
- 238000012986 modification Methods 0.000 claims abstract description 14
- 230000004048 modification Effects 0.000 claims abstract description 14
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 11
- -1 hydroxyalkyl amides Chemical class 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 21
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 20
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 20
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 15
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 15
- 238000002360 preparation method Methods 0.000 claims description 15
- 229920001503 Glucan Polymers 0.000 claims description 14
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 235000019441 ethanol Nutrition 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 5
- 239000000194 fatty acid Substances 0.000 claims description 5
- 229930195729 fatty acid Natural products 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 238000002390 rotary evaporation Methods 0.000 claims description 5
- 239000001334 starch sodium octenyl succinate Substances 0.000 claims description 5
- 235000013826 starch sodium octenyl succinate Nutrition 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims 2
- 210000000481 breast Anatomy 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract description 7
- 239000000839 emulsion Substances 0.000 abstract description 7
- 229920001296 polysiloxane Polymers 0.000 abstract description 7
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 29
- 230000000052 comparative effect Effects 0.000 description 7
- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000003973 paint Substances 0.000 description 2
- PXFBZOLANLWPMH-UHFFFAOYSA-N 16-Epiaffinine Natural products C1C(C2=CC=CC=C2N2)=C2C(=O)CC2C(=CC)CN(C)C1C2CO PXFBZOLANLWPMH-UHFFFAOYSA-N 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 241001330002 Bambuseae Species 0.000 description 1
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of high attachment coating in rattan wicker plaiting article surface, it is related to wicker plaiting article processing technology field, is made up of following component：Silicone acrylic emulsion, dextran modification polyvinyl alcohol, β hydroxyalkyl amides, compounded mix, emulsifying agent, water；Basic ingredient of the present invention using silicone acrylic emulsion as coating, by adding β hydroxyalkyl amides in coating system, surface compatibility of the coating to rattan wicker plaiting article made of can effectively improving, so as to improve adhesion of the rattan wicker plaiting article to coating, by using dextran modification polyvinyl alcohol, so that dextran modification polyvinyl alcohol can be with occurring chemical bond in coating system on the film forming matter strand of composition coating, so that whole film architecture is greatly improved, dextran modification polyvinyl alcohol has more significant absorption affinity simultaneously, surface adhesion force of the coating to rattan wicker plaiting article can be increased substantially, raising is effectively obtained by the addition coating hardness of compounded mix.
Description
Technical field
The invention belongs to wicker plaiting article technical field, and in particular to a kind of high attachment coating in rattan wicker plaiting article surface.
Background technology
The liana that rattan is strong but pliable in texture, figure is extremely long.Rattan crust is bright in luster, and feel is smooth, and elasticity is splendid, seemingly
Slight rather than slight.Also the daily apparatus such as this establishment rattan chair, rattan case are commonly used.Wherein rattan intensity and toughness are all higher, are very suitable for making
For the raw material of wicker plaiting article, the leatherware of rattan has very big toughness；Rattan wicker plaiting article accepts extensively for many people currently on the market
Handicraft, its shape is varied, function also very abundant, existing to be used to fill large bamboo or wicker basket, fruit basket of thing etc., has again for filling
The various products of decorations, a variety of wicker productses are all the articles of people's close contact, therefore can often be touched, and generation frequently rubs
Wipe, the adhesive force of this surfacecti proteon coating to rattan wicker plaiting article requires great test, and the poor coating of adhesive force exists
After often touching friction, the easily cracked, phenomenon that comes off, so as to lose protection effect.
The content of the invention
The purpose of the present invention is to be directed to the problem of existing, there is provided a kind of high attachment coating in rattan wicker plaiting article surface.
The present invention is achieved by the following technical solutions：
A kind of high attachment coating in rattan wicker plaiting article surface, is made up of following component by weight：Silicone acrylic emulsion 70-80, Portugal gather
Sugared modified polyvinylalcohol 5-10, beta-hydroxy alkylamide 3-5, compounded mix 12-18, emulsifying agent 1.2-1.5, water 30-50；It is described multiple
Close filler and press 3 by nano-calcium carbonate, talcum powder：1.3-1.6 mass ratios mix.
Further, the dextran modification polyvinyl alcohol preparation method is：
（1）Polyvinyl alcohol is evenly spread in deionized water, is configured to the polyvinyl alcohol water solution that mass fraction is 20%,
It is incubated at 55 DEG C；
（2）To step（1）The glucan aqueous solution of its quality 20% is added in the polyvinyl alcohol water solution of middle preparation, is stirred
Afterwards, then the starch Sodium Octenyl Succinate of polyvinyl alcohol water solution quality 1.5% is added, reacts 1 hour at 60 DEG C, then adopt
Reaction solution pH to 8.5 is adjusted with ammoniacal liquor, at 40 DEG C, is stirred 2 hours with 1500r/min rotating speeds, then naturally cools to room temperature,
Rotary evaporation is carried out again and removes moisture, is produced.
Further, the glucan aqueous solution mass fraction is 2.5-3.5%.
Further, the ammoniacal liquor is saturation ammoniacal liquor.
Further, the emulsifying agent is methyl glycol fatty acid ester.
Further, the nano-calcium carbonate granularity is 60-70nm.
Further, the talcum Powder Particle Size is 1250 mesh.
Further, the compounded mix preparation method is：Nano-calcium carbonate and talcum powder are weighed by proportioning, is added successively
Into ethanol solution, wherein absolute ethyl alcohol quality is 80 times of nano-calcium carbonate quality, then at 50 DEG C, with 3000r/
Min rotating speeds stir 2 hours, are then filtered, and dry, produce.
The present invention has advantages below compared with prior art：Basic ingredient of the present invention using silicone acrylic emulsion as coating, passes through
Beta-hydroxy alkylamide is added in coating system, it is affine to the surface of rattan wicker plaiting article can effectively to improve manufactured coating
Property, so as to improve adhesion of the rattan wicker plaiting article to coating, by using dextran modification polyvinyl alcohol so that glucan
Chemical bond occurs on the film forming matter strand that modified polyvinylalcohol can be with forming coating in coating system so that whole
Film architecture is greatly improved, while dextran modification polyvinyl alcohol has more significant absorption affinity, Neng Gou great
Amplitude improves surface adhesion force of the coating to rattan wicker plaiting article, the internal affinity increase of film, is made by the addition of compounded mix
Obtain coating hardness and be effectively obtained raising.
Embodiment
Embodiment 1
A kind of high attachment coating in rattan wicker plaiting article surface, is made up of following component by weight：Silicone acrylic emulsion 70, glucan change
Property polyvinyl alcohol 5, beta-hydroxy alkylamide 3, compounded mix 12, emulsifying agent 1.2, water 30；The compounded mix by nano-calcium carbonate,
Talcum powder presses 3：1.3 mass ratios mix.
Further, the dextran modification polyvinyl alcohol preparation method is：
（1）Polyvinyl alcohol is evenly spread in deionized water, is configured to the polyvinyl alcohol water solution that mass fraction is 20%,
It is incubated at 55 DEG C；
（2）To step（1）The glucan aqueous solution of its quality 20% is added in the polyvinyl alcohol water solution of middle preparation, is stirred
Afterwards, then the starch Sodium Octenyl Succinate of polyvinyl alcohol water solution quality 1.5% is added, reacts 1 hour at 60 DEG C, then adopt
Reaction solution pH to 8.5 is adjusted with ammoniacal liquor, at 40 DEG C, is stirred 2 hours with 1500r/min rotating speeds, then naturally cools to room temperature,
Rotary evaporation is carried out again and removes moisture, is produced.
Further, the glucan aqueous solution mass fraction is 2.5%.
Further, the ammoniacal liquor is saturation ammoniacal liquor.
Further, the emulsifying agent is methyl glycol fatty acid ester.
Further, the nano-calcium carbonate granularity is 60nm.
Further, the talcum Powder Particle Size is 1250 mesh.
Further, the compounded mix preparation method is：Nano-calcium carbonate and talcum powder are weighed by proportioning, is added successively
Into ethanol solution, wherein absolute ethyl alcohol quality is 80 times of nano-calcium carbonate quality, then at 50 DEG C, with 3000r/
Min rotating speeds stir 2 hours, are then filtered, and dry, produce.
Embodiment 2
A kind of high attachment coating in rattan wicker plaiting article surface, is made up of following component by weight：Silicone acrylic emulsion 80, glucan change
Property polyvinyl alcohol 10, beta-hydroxy alkylamide 5, compounded mix 18, emulsifying agent 1.5, water 50；The compounded mix is by nano-calcium carbonate
Calcium, talcum powder press 3：1.6 mass ratios mix.
Further, the dextran modification polyvinyl alcohol preparation method is：
（1）Polyvinyl alcohol is evenly spread in deionized water, is configured to the polyvinyl alcohol water solution that mass fraction is 20%,
It is incubated at 55 DEG C；
（2）To step（1）The glucan aqueous solution of its quality 20% is added in the polyvinyl alcohol water solution of middle preparation, is stirred
Afterwards, then the starch Sodium Octenyl Succinate of polyvinyl alcohol water solution quality 1.5% is added, reacts 1 hour at 60 DEG C, then adopt
Reaction solution pH to 8.5 is adjusted with ammoniacal liquor, at 40 DEG C, is stirred 2 hours with 1500r/min rotating speeds, then naturally cools to room temperature,
Rotary evaporation is carried out again and removes moisture, is produced.
Further, the glucan aqueous solution mass fraction is 3.5%.
Further, the ammoniacal liquor is saturation ammoniacal liquor.
Further, the emulsifying agent is methyl glycol fatty acid ester.
Further, the nano-calcium carbonate granularity is 60-70nm.
Further, the talcum Powder Particle Size is 1250 mesh.
Further, the compounded mix preparation method is：Nano-calcium carbonate and talcum powder are weighed by proportioning, is added successively
Into ethanol solution, wherein absolute ethyl alcohol quality is 80 times of nano-calcium carbonate quality, then at 50 DEG C, with 3000r/
Min rotating speeds stir 2 hours, are then filtered, and dry, produce.
Embodiment 3
A kind of high attachment coating in rattan wicker plaiting article surface, is made up of following component by weight：Silicone acrylic emulsion 75, glucan change
Property polyvinyl alcohol 6, beta-hydroxy alkylamide 4, compounded mix 15, emulsifying agent 1.3, water 40；The compounded mix by nano-calcium carbonate,
Talcum powder presses 3：1.5 mass ratios mix.
Further, the dextran modification polyvinyl alcohol preparation method is：
（1）Polyvinyl alcohol is evenly spread in deionized water, is configured to the polyvinyl alcohol water solution that mass fraction is 20%,
It is incubated at 55 DEG C；
（2）To step（1）The glucan aqueous solution of its quality 20% is added in the polyvinyl alcohol water solution of middle preparation, is stirred
Afterwards, then the starch Sodium Octenyl Succinate of polyvinyl alcohol water solution quality 1.5% is added, reacts 1 hour at 60 DEG C, then adopt
Reaction solution pH to 8.5 is adjusted with ammoniacal liquor, at 40 DEG C, is stirred 2 hours with 1500r/min rotating speeds, then naturally cools to room temperature,
Rotary evaporation is carried out again and removes moisture, is produced.
Further, the glucan aqueous solution mass fraction is 2.5-3.5%.
Further, the ammoniacal liquor is saturation ammoniacal liquor.
Further, the emulsifying agent is methyl glycol fatty acid ester.
Further, the nano-calcium carbonate granularity is 65nm.
Further, the talcum Powder Particle Size is 1250 mesh.
Further, the compounded mix preparation method is：Nano-calcium carbonate and talcum powder are weighed by proportioning, is added successively
Into ethanol solution, wherein absolute ethyl alcohol quality is 80 times of nano-calcium carbonate quality, then at 50 DEG C, with 3000r/
Min rotating speeds stir 2 hours, are then filtered, and dry, produce.
Comparative example 1：Differed only in embodiment 1 and do not add dextran modification polyvinyl alcohol.
Comparative example 2：Differed only in embodiment 1 and dextran modification polyvinyl alcohol is replaced with into common polythene alcohol.
Comparative example 3：Differed only in embodiment 1 and do not add beta-hydroxy alkylamide.
Experiment：
Paint film is prepared in rattan wicker plaiting article by GB/T1727-79, the adhesive force of film is then determined by GB/T1720-79, is adopted
Tested with Coating adhesion test instrument, embodiment and comparative example coating are tested respectively, film thickness is 30 μm：
Table 1
| Paint film adhesion/level | |
| Embodiment 1 | 1 |
| Embodiment 2 | 1 |
| Embodiment 3 | 1 |
| Comparative example 1 | 4 |
| Comparative example 2 | 3 |
| Comparative example 3 | 3 |
The rattan wicker plaiting article coating that as can be seen from Table 1 prepared by the present invention has higher adhesive force.
Claims (8)
1. the high attachment coating in a kind of rattan wicker plaiting article surface, it is characterised in that be made up by weight of following component：The breast of silicon third
Liquid 70-80, dextran modification polyvinyl alcohol 5-10, beta-hydroxy alkylamide 3-5, compounded mix 12-18, emulsifying agent 1.2-1.5, water
30-50；The compounded mix presses 3 by nano-calcium carbonate, talcum powder：1.3-1.6 mass ratios mix.
A kind of 2. high attachment coating in rattan wicker plaiting article surface as claimed in claim 1, it is characterised in that the dextran modification
Polyvinyl alcohol preparation method is：
（1）Polyvinyl alcohol is evenly spread in deionized water, is configured to the polyvinyl alcohol water solution that mass fraction is 20%,
It is incubated at 55 DEG C；
（2）To step（1）The glucan aqueous solution of its quality 20% is added in the polyvinyl alcohol water solution of middle preparation, is stirred
Afterwards, then the starch Sodium Octenyl Succinate of polyvinyl alcohol water solution quality 1.5% is added, reacts 1 hour at 60 DEG C, then adopt
Reaction solution pH to 8.5 is adjusted with ammoniacal liquor, at 40 DEG C, is stirred 2 hours with 1500r/min rotating speeds, then naturally cools to room temperature,
Rotary evaporation is carried out again and removes moisture, is produced.
3. the high attachment coating in a kind of rattan wicker plaiting article surface as claimed in claim 2, it is characterised in that the glucan is water-soluble
Liquid mass fraction is 2.5-3.5%.
4. the high attachment coating in a kind of rattan wicker plaiting article surface as claimed in claim 2, it is characterised in that the ammoniacal liquor is saturation
Ammoniacal liquor.
5. the high attachment coating in a kind of rattan wicker plaiting article surface as claimed in claim 1, it is characterised in that the emulsifying agent is third
Diol fatty acid ester.
A kind of 6. high attachment coating in rattan wicker plaiting article surface as claimed in claim 1, it is characterised in that the nano-calcium carbonate
Granularity is 60-70nm.
A kind of 7. high attachment coating in rattan wicker plaiting article surface as claimed in claim 1, it is characterised in that the talcum Powder Particle Size
For 1250 mesh.
A kind of 8. high attachment coating in rattan wicker plaiting article surface as claimed in claim 1, it is characterised in that the compounded mix system
Preparation Method is：Nano-calcium carbonate and talcum powder are weighed by proportioning, is added to successively in ethanol solution, wherein absolute ethyl alcohol matter
Measure as 80 times of nano-calcium carbonate quality, then at 50 DEG C, stirred 2 hours with 3000r/min rotating speeds, then filtered, dried
It is dry, produce.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710849261.4A CN107603399A (en) | 2017-09-20 | 2017-09-20 | A kind of high attachment coating in rattan wicker plaiting article surface |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710849261.4A CN107603399A (en) | 2017-09-20 | 2017-09-20 | A kind of high attachment coating in rattan wicker plaiting article surface |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107603399A true CN107603399A (en) | 2018-01-19 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710849261.4A Pending CN107603399A (en) | 2017-09-20 | 2017-09-20 | A kind of high attachment coating in rattan wicker plaiting article surface |
Country Status (1)
| Country | Link |
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| CN (1) | CN107603399A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108753083A (en) * | 2018-06-26 | 2018-11-06 | 阜南县腾博工艺品有限公司 | A kind of wicker plaiting article stain resistant imitation stone lacquer |
| CN108864871A (en) * | 2018-08-07 | 2018-11-23 | 安徽嘉美工艺品有限公司 | A kind of wicker products coating of insect prevention toughening |
| CN108948907A (en) * | 2018-05-09 | 2018-12-07 | 阜南县勤艺工艺品有限公司 | A kind of high life rattan braided article |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108948907A (en) * | 2018-05-09 | 2018-12-07 | 阜南县勤艺工艺品有限公司 | A kind of high life rattan braided article |
| CN108753083A (en) * | 2018-06-26 | 2018-11-06 | 阜南县腾博工艺品有限公司 | A kind of wicker plaiting article stain resistant imitation stone lacquer |
| CN108864871A (en) * | 2018-08-07 | 2018-11-23 | 安徽嘉美工艺品有限公司 | A kind of wicker products coating of insect prevention toughening |
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