CN107675290A - A kind of preparation method of antiseptic nano-fiber mixed cloth - Google Patents
A kind of preparation method of antiseptic nano-fiber mixed cloth Download PDFInfo
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- CN107675290A CN107675290A CN201711003640.8A CN201711003640A CN107675290A CN 107675290 A CN107675290 A CN 107675290A CN 201711003640 A CN201711003640 A CN 201711003640A CN 107675290 A CN107675290 A CN 107675290A
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- 239000004744 fabric Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 30
- 230000002421 anti-septic effect Effects 0.000 title claims abstract description 21
- 239000002121 nanofiber Substances 0.000 title claims abstract description 21
- 239000000835 fiber Substances 0.000 claims abstract description 47
- 229920002472 Starch Polymers 0.000 claims abstract description 32
- 239000000843 powder Substances 0.000 claims abstract description 28
- 239000008107 starch Substances 0.000 claims abstract description 22
- 235000019698 starch Nutrition 0.000 claims abstract description 22
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 15
- 241001145009 Sophora alopecuroides Species 0.000 claims abstract description 15
- 241001116389 Aloe Species 0.000 claims abstract description 14
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 14
- 244000061121 Rauvolfia serpentina Species 0.000 claims abstract description 14
- 235000007303 Thymus vulgaris Nutrition 0.000 claims abstract description 14
- 235000011399 aloe vera Nutrition 0.000 claims abstract description 14
- 229910052802 copper Inorganic materials 0.000 claims abstract description 14
- 239000010949 copper Substances 0.000 claims abstract description 14
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 14
- UYTPUPDQBNUYGX-UHFFFAOYSA-N guanine Chemical compound O=C1NC(N)=NC2=C1N=CN2 UYTPUPDQBNUYGX-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000008390 olive oil Nutrition 0.000 claims abstract description 14
- 239000004006 olive oil Substances 0.000 claims abstract description 14
- 229920000728 polyester Polymers 0.000 claims abstract description 14
- 239000001585 thymus vulgaris Substances 0.000 claims abstract description 14
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims abstract description 13
- 240000003553 Leptospermum scoparium Species 0.000 claims abstract description 13
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 13
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 13
- 239000003921 oil Substances 0.000 claims abstract description 13
- 235000019198 oils Nutrition 0.000 claims abstract description 13
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 13
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 12
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229920002413 Polyhexanide Polymers 0.000 claims abstract description 11
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 11
- 229940072056 alginate Drugs 0.000 claims abstract description 11
- 229920000615 alginic acid Polymers 0.000 claims abstract description 11
- 235000010443 alginic acid Nutrition 0.000 claims abstract description 11
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 240000002657 Thymus vulgaris Species 0.000 claims abstract 2
- 238000009987 spinning Methods 0.000 claims description 32
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 20
- 239000003814 drug Substances 0.000 claims description 18
- 239000002002 slurry Substances 0.000 claims description 18
- 238000005406 washing Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 238000004043 dyeing Methods 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- 239000002253 acid Substances 0.000 claims description 13
- 238000004140 cleaning Methods 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- 229960000583 acetic acid Drugs 0.000 claims description 10
- 239000012362 glacial acetic acid Substances 0.000 claims description 10
- 229940100445 wheat starch Drugs 0.000 claims description 10
- 238000005516 engineering process Methods 0.000 claims description 8
- 238000005554 pickling Methods 0.000 claims description 8
- 238000002203 pretreatment Methods 0.000 claims description 8
- 239000011734 sodium Substances 0.000 claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- 229910052760 oxygen Inorganic materials 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 7
- 239000004902 Softening Agent Substances 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000000985 reactive dye Substances 0.000 claims description 6
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 6
- 239000006096 absorbing agent Substances 0.000 claims description 5
- 238000004061 bleaching Methods 0.000 claims description 5
- 239000007844 bleaching agent Substances 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 241000209140 Triticum Species 0.000 claims 1
- 235000021307 Triticum Nutrition 0.000 claims 1
- 230000009102 absorption Effects 0.000 claims 1
- 238000010521 absorption reaction Methods 0.000 claims 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 20
- 239000004753 textile Substances 0.000 abstract description 13
- 238000004332 deodorization Methods 0.000 abstract description 3
- 241000246358 Thymus Species 0.000 description 12
- 238000012360 testing method Methods 0.000 description 7
- 238000002074 melt spinning Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 210000004243 sweat Anatomy 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- ZRALSGWEFCBTJO-UHFFFAOYSA-N Guanidine Chemical compound NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 description 4
- CHJJGSNFBQVOTG-UHFFFAOYSA-N methylguanidine Chemical compound CNC(N)=N CHJJGSNFBQVOTG-UHFFFAOYSA-N 0.000 description 4
- 241000195493 Cryptophyta Species 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 230000001408 fungistatic effect Effects 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 2
- 241000255789 Bombyx mori Species 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- SWSQBOPZIKWTGO-UHFFFAOYSA-N dimethylaminoamidine Natural products CN(C)C(N)=N SWSQBOPZIKWTGO-UHFFFAOYSA-N 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 229920002674 hyaluronan Polymers 0.000 description 2
- 229960003160 hyaluronic acid Drugs 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 2
- 238000002715 modification method Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 206010011409 Cross infection Diseases 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 244000284380 Hibiscus rosa sinensis Species 0.000 description 1
- 206010029803 Nosocomial infection Diseases 0.000 description 1
- 102000004020 Oxygenases Human genes 0.000 description 1
- 108090000417 Oxygenases Proteins 0.000 description 1
- QOSMNYMQXIVWKY-UHFFFAOYSA-N Propyl levulinate Chemical compound CCCOC(=O)CCC(C)=O QOSMNYMQXIVWKY-UHFFFAOYSA-N 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 238000007306 functionalization reaction Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009940 knitting Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 239000008363 phosphate buffer Substances 0.000 description 1
- 238000000554 physical therapy Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000012958 reprocessing Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/106—Radiation shielding agents, e.g. absorbing, reflecting agents
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Woven Fabrics (AREA)
Abstract
The invention discloses a kind of preparation method of antiseptic nano-fiber mixed cloth, it is made from the following raw materials in parts by weight：75 85 parts of copper modified polyester fiber, 5 10 parts of wheaten starch, 25 parts of aloe, 10 20 parts of alginate fibre, 24 parts of nano zine oxide, 12 parts of nano-silver powder, 13 parts of pearl essence, 23 parts of M82 emulsifying agents, 25 parts of propylben, 23 parts of polyhexamethylene guanide, 24 parts of olive oil, 35 parts of synthesis silk oil, 13 parts of Sodium Hyaluronate, 25 parts of devilpepper, 24 parts of folium artemisiae argyi, 12 parts of bitter dish, 12 parts of Sophora alopecuroide, 13 parts of tea tree, 13 parts of thyme, 12 parts of pearl powder.The antiseptic nano-fiber mixed cloth that the present invention makes, there is the functional characteristics such as natural antibacterial, deodorization, anti-uv, be widely used in making the field such as clothes and household textiles.
Description
Technical field
The invention belongs to textile technology field, and in particular to a kind of preparation method of antiseptic nano-fiber mixed cloth.
Background technology
With progress, expanding economy and the growth in the living standard of society, requirement of the people to textile is also increasingly
Extensively, while comfortableness is pursued, the functionalization of textile product is also increasingly paid close attention to.The progress of modern science and technology, not only
The developmental research and popularization of tech Textiles are promoted, the applications expanding of textile has also been arrived into frontier.By high-tech
Means, high-performance, multi-functional, high added value new textile product have been developed both at home and abroad, realize the industry of functional fiber
Change, because textile easily adsorbs various impurity, turn into breeding, the carrier of parasitic bacteria, not only influence human health, and
Easily trigger the cross-infection of public place, therefore anti-bacterial fibre has become international development trend, especially in health care
Industry seems even more important.Knitting product using anti-bacterial fibre, the particularly yarn production of natural antibacterial fibre spinning resists
Bacterium effect is lasting, and washability is good.
Antibacterial fabric can improve value-added content of product, meet the needs of people are to health environment-friendly, thus increasingly by
It is very big to the attention of vast textile research person, market potential.In the research field of antibacterial fabric, the system of antibacterial fabric
Preparation Method mainly has fibre modification method and fabric post-treatment method.Fibre modification method adds nanometer in fiber-forming polymer first
Gold, then carries out wet method or melt spinning, and antibiotic fabric is made in reprocessing；Fabric post-treatment is then by being applied in fabric face
Layer or impregnating mode, textile material surface is set to form nanogold antibiotic layer, but during antibiotic facing material of the prior art use
Between do not grow, fungistatic effect is still undesirable.
The content of the invention
In order to overcome the above-mentioned deficiencies of the prior art, it is an object of the invention to provide a kind of antiseptic nano-fiber flour mixed with adulterants
The preparation method of material, there is the functional characteristics such as natural antibacterial, deodorization, anti-uv, be widely used in making clothes and household textile
The fields such as product.
To achieve these goals, the technical solution adopted by the present invention is：A kind of system of antiseptic nano-fiber mixed cloth
Method, it is made from the following raw materials in parts by weight：Copper modified polyester fiber 75-85 parts, wheaten starch 5-10 parts, aloe 2-5 parts, sea
Algae fiber 10-20 parts, nano zine oxide 2-4 parts, nano-silver powder 1-2 parts, pearl essence 1-3 parts, M82 emulsifying agent 2-3 parts, Ni Bo
Golden propyl ester 2-5 parts, polyhexamethylene guanide 2-3 parts, olive oil 2-4 parts, synthesis silk oil 3-5 parts, Sodium Hyaluronate 1-3 parts, trailing plants
Cottonrose hibiscus wood 2-5 parts, folium artemisiae argyi 2-4 parts, bitter dish 1-2 parts, Sophora alopecuroide 1-2 parts, tea tree 1-3 parts, thyme 1-3 parts, pearl powder 1-2 parts.
Preferably, preparation method comprises the following steps：(1) mixing medicine slurry is prepared；(2) wheaten starch is ground to grain
Footpath is 50-80um, is placed in beaker, is 1 by the weight of wheaten starch and water ratio:3 add water, are mixed evenly, add
Silk oil, propylben, Sodium Hyaluronate and olive oil are synthesized, is uniformly mixed, is eventually adding obtained by step (1)
Mixing medicine slurry is stirred 1-3h, is dried to constant weight under the conditions of 100-120 DEG C, obtains modified wheat starch；(3) copper is modified
Double screw extruder is fed after polyester fiber, alginate fibre are well mixed, spinning melt is made；(4) modified wheat starch is added
And nano zine oxide, nano-silver powder, pearl essence, M82 emulsifying agents, polyhexamethylene guanide, it is uniformly mixed, obtains modified
Spinning melt；(5) modified spinning melt is subjected to melt spinning, obtains spinning fibre；(6) by spinning fibre through washing, floating
In vain, oil, dry；(7) dye；(8) acid cleaning process prescription and condition:HAc glacial acetic acid 0.6g/L, 25 DEG C of temperature, time
10min；(9) shape：It is 140 DEG C to select setting temperature, speed 20.16m/min；(10) fabric is woven into, is produced.
Any of the above-described scheme is preferably, and the mixing medicine slurry preparation method of the step (1) is：Claim according to formula rate
Aloe, devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, tea tree, thyme, pearl powder are taken, mixing adds the 15-20 of total medicinal material weight
Amount water again, 0.5-1h is soaked, be heated to 90-100 DEG C, decoct 3-5h, filter to obtain filtrate with 3 layers of gauze, heating is concentrated into always
3-6 times of medicinal material weight, is filtered with double gauze, stand-by.
Any of the above-described scheme is preferably, and also includes pre-treating technology, pre-treatment prescription and condition before dyeing:C-180
Deoil yarn agent 0.5g/L, C-MS200 oxygen bleaching agent 2.0g/L, H2O2, 4.0g/L, 95 DEG C of temperature, time 30min.
Any of the above-described scheme is preferably, and also includes pickling, acid cleaning process prescription and condition after pre-treatment:HAc ice vinegar
Sour 0.5g/L, temperature 60 C, time 10min.
Any of the above-described scheme is preferably, and washing, washing process prescription and condition are also included after pickling:Deoxyenzyme
0.1g/L, 30 DEG C of temperature, time 15min.
Any of the above-described scheme is preferably, the technical recipe and condition of step (7) dyeing:Reactive dye 1.6%,
UV-330 ultra-violet absorbers 2.2%, JH-PPM 120 moisture absorbing and sweat releasing softening agent 1.2g/L, Na2S0426g/L, Na2C03
12g/L, 62 DEG C of temperature, dyeing time 60-60min.
The beneficial effects of the invention are as follows：A kind of preparation method of antiseptic nano-fiber mixed cloth is provided, by following parts by weight
Raw material is made：Copper modified polyester fiber 75-85 parts, wheaten starch 5-10 parts, aloe 2-5 parts, alginate fibre 10-20 parts, nanometer
Zinc oxide 2-4 parts, nano-silver powder 1-2 parts, pearl essence 1-3 parts, M82 emulsifying agent 2-3 parts, propylben 2-5 parts, poly- six Asia
Methylguanidine 2-3 parts, olive oil 2-4 parts, synthesis silk oil 3-5 parts, Sodium Hyaluronate 1-3 parts, devilpepper 2-5 parts, folium artemisiae argyi 2-4
Part, bitter dish 1-2 parts, Sophora alopecuroide 1-2 parts, tea tree 1-3 parts, thyme 1-3 parts, pearl powder 1-2 parts.The nanometer that the present invention makes
Anti-bacterial fibre mixed cloth, there is the functional characteristics such as natural antibacterial, deodorization, anti-uv, be widely used in making clothes
With the field such as household textiles.
Embodiment
The structural principle and operation principle of the present invention are described in further detail below.
Embodiment 1
A kind of preparation method of antiseptic nano-fiber mixed cloth, is made from the following raw materials in parts by weight：Copper modified polyester fiber
78 parts, 6 parts of wheaten starch, 3 parts of aloe, 12 parts of alginate fibre, 2.5 parts of nano zine oxide, 1.5 parts of nano-silver powder, pearl essence
1.5 parts, 2.2 parts of M82 emulsifying agents, 3 parts of propylben, 2.2 parts of polyhexamethylene guanide, 2.5 parts of olive oil, synthesis silk oil
3.5 parts, 1.5 parts of Sodium Hyaluronate, 2.5 parts of devilpepper, 2.5 parts of folium artemisiae argyi, 1.2 parts of bitter dish, 1.2 parts of Sophora alopecuroide, 1.5 parts of tea tree,
1.8 parts of thyme, 1.6 parts of pearl powder.
Preparation method comprises the following steps：(1) mixing medicine slurry is prepared；(2) it is 50- wheaten starch to be ground into particle diameter
80um, it is placed in beaker, is 1 by the weight of wheaten starch and water ratio:3 add water, are mixed evenly, and add synthesis silkworm
Silk oil, propylben, Sodium Hyaluronate and olive oil, are uniformly mixed, and are eventually adding the mixing medicine obtained by step (1)
Slurry is stirred 1.5h, is dried to constant weight under the conditions of 108 DEG C, obtains modified wheat starch；(3) by copper modified polyester fiber, sea
Double screw extruder is fed after algae fiber is well mixed, spinning melt is made；(4) modified wheat starch and nano oxygen are added
Change zinc, nano-silver powder, pearl essence, M82 emulsifying agents, polyhexamethylene guanide, be uniformly mixed, obtain modified spinning melt；
(5) modified spinning melt is subjected to melt spinning, obtains spinning fibre；(6) by spinning fibre through washing, bleaching, oiling,
Dry；(7) dye；(8) acid cleaning process prescription and condition:HAc glacial acetic acid 0.6g/L, 25 DEG C of temperature, time 10min；(9) it is fixed
Shape：It is 140 DEG C to select setting temperature, speed 20.16m/min；(10) fabric is woven into, is produced.
The technical scheme that the present invention further optimizes, the mixing medicine slurry preparation method of the step (1) are：According to formula
Ratio weighs aloe, devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, tea tree, thyme, pearl powder, and mixing adds total medicinal material weight
18 times of amount water, soak 0.6h, are heated to 95 DEG C, decoct 3.5h, filter to obtain filtrate with 3 layers of gauze, heating is concentrated into total medicinal material
4 times of weight, are filtered with double gauze, stand-by.
The technical scheme that the present invention further optimizes, also include pre-treating technology, pre-treatment prescription and bar before dyeing
Part:C-180 deoils yarn agent 0.5g/L, C-MS200 oxygen bleaching agent 2.0g/L, H2O2, 4.0g/L, 95 DEG C of temperature, time 30min.
The technical scheme that the present invention further optimizes, also include pickling, acid cleaning process prescription and condition after pre-treatment:
HAc glacial acetic acid 0.5g/L, temperature 60 C, time 10min.
The technical scheme that the present invention further optimizes, washing, washing process prescription and condition are also included after pickling:Remove
Oxygenase 0.1g/L, 30 DEG C of temperature, time 15min.
The technical scheme that the present invention further optimizes, the technical recipe and condition of step (7) dyeing:Reactive dye
1.5%, UV-330 ultra-violet absorber 2.0%, JH-PPM 120 moisture absorbing and sweat releasing softening agent 1.0g/L, Na2S0424g/L,
Na2C0310g/L, 65 DEG C of temperature, dyeing time 60min.
Embodiment 2
A kind of preparation method of antiseptic nano-fiber mixed cloth, is made from the following raw materials in parts by weight：Copper modified polyester fiber
80 parts, 8 parts of wheaten starch, 4 parts of aloe, 16 parts of alginate fibre, 3 parts of nano zine oxide, 1.7 parts of nano-silver powder, pearl essence 2.5
Part, 2.5 parts of M82 emulsifying agents, 4 parts of propylben, 2.5 parts of polyhexamethylene guanide, 3.5 parts of olive oil, synthesis silk oil 4.5
Part, 2.4 parts of Sodium Hyaluronate, 4.5 parts of devilpepper, 3.6 parts of folium artemisiae argyi, 1.4 parts of bitter dish, 1.6 parts of Sophora alopecuroide, 2.4 parts of thyme,
1.2 parts of pearl powder.
Preparation method comprises the following steps：(1) mixing medicine slurry is prepared；(2) it is 50- wheaten starch to be ground into particle diameter
80um, it is placed in beaker, is 1 by the weight of wheaten starch and water ratio:3 add water, are mixed evenly, and add synthesis silkworm
Silk oil, propylben, Sodium Hyaluronate and olive oil, are uniformly mixed, and are eventually adding the mixing medicine obtained by step (1)
Slurry is stirred 2.4h, is dried to constant weight under the conditions of 110 DEG C, obtains modified wheat starch；(3) by copper modified polyester fiber, sea
Double screw extruder is fed after algae fiber is well mixed, spinning melt is made；(4) modified wheat starch and nano oxygen are added
Change zinc, nano-silver powder, pearl essence, M82 emulsifying agents, polyhexamethylene guanide, be uniformly mixed, obtain modified spinning melt；
(5) modified spinning melt is subjected to melt spinning, obtains spinning fibre；(6) by spinning fibre through washing, bleaching, oiling,
Dry；(7) dye：The technical recipe and condition of dyeing:Reactive dye 1.8%, UV-330 ultra-violet absorbers 2.4%, JH-
PPM 120 moisture absorbing and sweat releasing softening agent 1.4g/L, Na2S0424g/L, Na2C0311g/L, 65 DEG C of temperature, dyeing time
65min；(8) acid cleaning process prescription and condition:HAc glacial acetic acid 0.65g/L, 28 DEG C of temperature, time 10min；(9) shape：Selection
Setting temperature is 135 DEG C, speed 20.18m/min；(10) fabric is woven into, is produced.
The technical scheme that the present invention further optimizes, the mixing medicine slurry preparation method of the step (1) are：According to formula
Ratio weighs aloe, devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, thyme, pearl powder, and mixing adds 18 times of total medicinal material weight
Water is measured, soaks 0.8h, is heated to 96 DEG C, decocts 4h, filters to obtain filtrate with 3 layers of gauze, heating is concentrated into the 5 of total medicinal material weight
Times, filtered with double gauze, it is stand-by.
The technical scheme that the present invention further optimizes, also include pre-treating technology, pre-treatment prescription and bar before dyeing
Part:C-180 deoils yarn agent 0.6g/L, C-MS200 oxygen bleaching agent 2.2g/L, H2O2, 4.0g/L, 98 DEG C of temperature, time 30min.Before
Also include pickling, acid cleaning process prescription and condition after processing:HAc glacial acetic acid 0.6g/L, temperature 60 C, time 10min.Acid
Also include washing, washing process prescription and condition after washing:The 5g/L of deoxyenzyme 0.1,30 DEG C of temperature, time 15min.
Embodiment 3
A kind of preparation method of antiseptic nano-fiber mixed cloth, is made from the following raw materials in parts by weight：Copper modified polyester fiber
82 parts, 8 parts of wheaten starch, 5 parts of aloe, 20 parts of alginate fibre, 4 parts of nano zine oxide, 2 parts of nano-silver powder, 3 parts of pearl essence,
3 parts of M82 emulsifying agents, 5 parts of propylben, 3 parts of polyhexamethylene guanide, 4 parts of olive oil, synthesis silk oily 5 parts, hyaluronic acid
3 parts of sodium, 5 parts of devilpepper, 4 parts of folium artemisiae argyi, 2 parts of bitter dish, 2 parts of Sophora alopecuroide, 3 parts of tea tree, 3 parts of thyme, 2 parts of pearl powder.
Preparation method comprises the following steps：(1) mixing medicine slurry is prepared, mixing medicine slurry preparation method is：According to formula rate
Aloe, devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, tea tree, thyme, pearl powder are weighed, mixing adds 20 times of total medicinal material weight
Water is measured, soaks 1h, is heated to 100 DEG C, decocts 5h, filters to obtain filtrate with 3 layers of gauze, heating is concentrated into the 6 of total medicinal material weight
Times, filtered with double gauze, it is stand-by；
(2) it is 80um wheaten starch to be ground into particle diameter, is placed in beaker, is 1 by the weight of wheaten starch and water ratio:3
Water is added, is mixed evenly, synthesis silk oil, propylben, Sodium Hyaluronate and olive oil is added, is stirred
Uniformly, it is eventually adding the mixing medicine slurry obtained by step (1) and is stirred 3h, is dried to constant weight under the conditions of 120 DEG C, is modified
Wheaten starch；
(3) double screw extruder is fed after being well mixed copper modified polyester fiber, alginate fibre, spinning melt is made；
(4) modified wheat starch and nano zine oxide, nano-silver powder, pearl essence, M82 emulsifying agents, poly- six methylene are added
Base guanidine, is uniformly mixed, and obtains modified spinning melt；
(5) modified spinning melt is subjected to melt spinning, obtains spinning fibre；
(6) by spinning fibre through washing, bleaching, oiling, dry；
(7) dye, the technical recipe and condition of dyeing:Reactive dye 1.6%, UV-330 ultra-violet absorbers 2.2%,
JH-PPM 120 moisture absorbing and sweat releasing softening agent 1.2g/L, Na2S0426 g/L, Na2C0312g/L, 62 DEG C of temperature, dyeing time 60-
60min；
(8) acid cleaning process prescription and condition:HAc glacial acetic acid 0.6g/L, 25 DEG C of temperature, time 10min；
(9) shape：It is 140 DEG C to select setting temperature, speed 20.16m/min；(10) fabric is woven into, is produced.
The technical scheme that the present invention further optimizes, also include pre-treating technology, pre-treatment prescription and bar before dyeing
Part:C-180 deoils yarn agent 0.5g/L, C-MS200 oxygen bleaching agent 2.0g/L, H2O2, 4.0g/L, 95 DEG C of temperature, time 30min.Before
Also include pickling, acid cleaning process prescription and condition after processing:HAc glacial acetic acid 0.5g/L, temperature 60 C, time 10min.Acid
Also include washing, washing process prescription and condition after washing:Deoxyenzyme 0.1g/L, 30 DEG C of temperature, time 15min.
Embodiment 4
A kind of preparation method of antiseptic nano-fiber mixed cloth, is made from the following raw materials in parts by weight：Copper modified polyester fiber
82 parts, 8 parts of wheaten starch, 5 parts of aloe, 20 parts of alginate fibre, 4 parts of nano zine oxide, 2 parts of nano-silver powder, 3 parts of pearl essence,
3 parts of M82 emulsifying agents, 5 parts of propylben, 3 parts of polyhexamethylene guanide, 4 parts of olive oil, synthesis silk oily 5 parts, hyaluronic acid
3 parts of sodium, 5 parts of devilpepper, 4 parts of folium artemisiae argyi, 2 parts of bitter dish, 2 parts of Sophora alopecuroide, 3 parts of tea tree, 3 parts of thyme, 2 parts of pearl powder.
Preparation method comprises the following steps：(1) mixing medicine slurry is prepared, mixing medicine slurry preparation method is：According to formula rate
Aloe, devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, tea tree, thyme, pearl powder are weighed, mixing adds 20 times of total medicinal material weight
Water is measured, soaks 1h, is heated to 100 DEG C, decocts 5h, filters to obtain filtrate with 3 layers of gauze, heating is concentrated into the 6 of total medicinal material weight
Times, filtered with double gauze, it is stand-by；
(2) it is 80um wheaten starch to be ground into particle diameter, is placed in beaker, is 1 by the weight of wheaten starch and water ratio:3
Water is added, is mixed evenly, synthesis silk oil, propylben, Sodium Hyaluronate and olive oil is added, is stirred
Uniformly, it is eventually adding the mixing medicine slurry obtained by step (1) and is stirred 3h, is dried to constant weight under the conditions of 120 DEG C, is modified
Wheaten starch；
(3) double screw extruder is fed after being well mixed copper modified polyester fiber, alginate fibre, spinning melt is made；
(4) modified wheat starch and nano zine oxide, nano-silver powder, pearl essence, M82 emulsifying agents, poly- six methylene are added
Base guanidine, is uniformly mixed, and obtains modified spinning melt；
(5) modified spinning melt is subjected to melt spinning, obtains spinning fibre；
(6) by spinning fibre through washing, bleaching, oiling, dry；
(7) dye, the technical recipe and condition of dyeing:Reactive dye 1.6%, UV-330 ultra-violet absorbers 2.2%,
JH-PPM 120 moisture absorbing and sweat releasing softening agent 1.2g/L, Na2S0426 g/L, Na2C0312g/L, 62 DEG C of temperature, dyeing time 60-
60min；
(8) acid cleaning process prescription and condition:HAc glacial acetic acid 0.6g/L, 25 DEG C of temperature, time 10min；
(9) shape：It is 140 DEG C to select setting temperature, speed 20.16m/min；(10) fabric is woven into, is produced.
Embodiment 5
The antibacterial tests test method of antiseptic nano-fiber mixed cloth and characteristic index：
Antibacterial test uses GB/T 20944.3-2008《The evaluation Part III of antibacterial textile performance:Succusion》.
Sterilizing methods-high pressure steam sterilization
Vibrate liquid -0.03mol/L phosphate buffers
Contact Temperature-(24 scholar 1) DEG C
Time of contact 18h
Fungistatic effect evaluation index is:Staphylococcus aureus and the bacteriostasis rate of Escherichia coli) >=70%, or white thought
The bacteriostasis rate of pearl bacterium) >=60%, show that sample has antibacterial functions.
The antiseptic nano-fiber mixed cloth prepared using embodiment 1- embodiments 4 carries out antibacterial test.
1 embodiment of table, 1 antibacterial test effect
1 embodiment of table, 2 antibacterial test effect
1 embodiment of table, 3 antibacterial test effect
1 embodiment of table, 4 antibacterial test effect
From the above results, the nanometer silver antimicrobial functional fabric prepared by embodiment 1 and embodiment 3, have excellent
Fungistatic effect, and wash 50 times after bacteriostasis rate it is substantially unchanged, there is lasting bacteria resistance function.Simultaneously because the original of the present invention
Expect also containing devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, tea tree, thyme, pearl powder etc. in component, not only with antibacterial bacteriostatic
Effect, additionally it is possible to play physiotherapy function to body indirectly, such as improve immunity.
It should be noted that various embodiments above is merely illustrative of the technical solution of the present invention, rather than its limitations；To the greatest extent
The present invention is described in detail with reference to foregoing embodiments for pipe, it will be understood by those within the art that：Its according to
The technical scheme described in foregoing embodiments can so be modified, either to which part or all technical characteristic
Carry out equivalent substitution；And these modifications or replacement, the essence of appropriate technical solution is departed from various embodiments of the present invention
The scope of technical scheme.
Claims (7)
1. a kind of preparation method of antiseptic nano-fiber mixed cloth, it is characterised in that be made from the following raw materials in parts by weight：Copper is modified
Polyester fiber 75-85 parts, wheaten starch 5-10 parts, aloe 2-5 parts, alginate fibre 10-20 parts, nano zine oxide 2-4 parts, nanometer
Silver powder 1-2 parts, pearl essence 1-3 parts, M82 emulsifying agent 2-3 parts, propylben 2-5 parts, polyhexamethylene guanide 2-3 parts, olive oil
2-4 parts, synthesis silk oil 3-5 parts, Sodium Hyaluronate 1-3 parts, devilpepper 2-5 parts, folium artemisiae argyi 2-4 parts, bitter dish 1-2 parts, Sophora alopecuroide
1-2 parts, tea tree 1-3 parts, thyme 1-3 parts, pearl powder 1-2 parts.
A kind of 2. preparation method of antiseptic nano-fiber mixed cloth according to claim 1, it is characterised in that preparation method bag
Include following steps：(1) mixing medicine slurry is prepared；(2) it is 50-80um wheaten starch to be ground into particle diameter, is placed in beaker, by wheat
The weight of starch and water ratio is 1:3 add water, are mixed evenly, and add synthesis silk oil, propylben, hyaluronic acid
Sodium and olive oil, are uniformly mixed, and are eventually adding the mixing medicine slurry obtained by step (1) and are stirred 1-3h, 100-120 DEG C of bar
Constant weight is dried under part, obtains modified wheat starch；(3) fed after being well mixed copper modified polyester fiber, alginate fibre double
Screw extruder, spinning melt is made；(4) modified wheat starch and nano zine oxide, nano-silver powder, pearl essence, M82 are added
Emulsifying agent, polyhexamethylene guanide, are uniformly mixed, and obtain modified spinning melt；(5) modified spinning melt is melted
Spinning, obtain spinning fibre；(6) by spinning fibre through washing, bleaching, oiling, dry；(7) dye；(8) acid cleaning process prescription
And condition:HAc glacial acetic acid 0.6g/L, 25 DEG C of temperature, time 10min；(9) shape：It is 140 DEG C to select setting temperature, and speed is
20.16m/min；(10) fabric is woven into, is produced.
A kind of 3. preparation method of antiseptic nano-fiber mixed cloth according to claim 2, it is characterised in that the step
(1) mixing medicine slurry preparation method is：Aloe, devilpepper, folium artemisiae argyi, bitter dish, Sophora alopecuroide, tea tree, hundred are weighed according to formula rate
In fragrant, pearl powder, mixing add total medicinal material weight 15-20 times measure water, soak 0.5-1h, be heated to 90-100 DEG C, decoct 3-
5h, filtrate is filtered to obtain with 3 layers of gauze, heating is concentrated into 3-6 times of total medicinal material weight, filtered with double gauze, stand-by.
4. the preparation method of a kind of antiseptic nano-fiber mixed cloth according to claim 2, it is characterised in that before dyeing also
Including pre-treating technology, pre-treatment prescription and condition:C-180 deoils yarn agent 0.5g/L, C-MS200 oxygen bleaching agent 2.0g/L, H2O2,
4.0g/L, 95 DEG C of temperature, time 30min.
5. the preparation method of a kind of antiseptic nano-fiber mixed cloth according to claim 4, it is characterised in that after pre-treatment
Also include pickling, acid cleaning process prescription and condition:HAc glacial acetic acid 0.5g/L, temperature 60 C, time 10min.
6. the preparation method of a kind of antiseptic nano-fiber mixed cloth according to claim 5, it is characterised in that after pickling also
Including washing, washing process prescription and condition:Deoxyenzyme 0.1g/L, 30 DEG C of temperature, time 15min.
A kind of 7. preparation method of antiseptic nano-fiber mixed cloth according to claim 2, it is characterised in that the step
(7) technical recipe and condition of dyeing:Reactive dye 1.6%, UV-330 ultra-violet absorbers 2.2%, the moisture absorptions of JH-PPM 120
Perspire softening agent 1.2g/L, Na2S0426g/L, Na2C0312g/L, 62 DEG C of temperature, dyeing time 60-60min.
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| CN109468690A (en) * | 2018-10-17 | 2019-03-15 | 李涛 | A kind of antibacterial aloe fabric lining and preparation method thereof |
| CN115323574A (en) * | 2022-08-10 | 2022-11-11 | 宜昌市毕生纺织有限公司 | Preparation method of super-soft antibacterial yarn fiber fabric for infant pregnant women |
| EP3995198A4 (en) * | 2019-07-02 | 2023-08-23 | LG Electronics Inc. | ANTIBACTERIAL COMPOSITION, FILTER WITH IT AND HOUSEHOLD APPLIANCE WITH FILTER |
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Application publication date: 20180209 |