CN107780202A - A kind of dyeing and printing process of camouflage facing material - Google Patents

A kind of dyeing and printing process of camouflage facing material Download PDF

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Publication number
CN107780202A
CN107780202A CN201710981731.2A CN201710981731A CN107780202A CN 107780202 A CN107780202 A CN 107780202A CN 201710981731 A CN201710981731 A CN 201710981731A CN 107780202 A CN107780202 A CN 107780202A
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dyeing
concentration
facing material
printing process
flame
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潘学东
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Anhui Yayuan Printing And Dyeing Co Ltd
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Anhui Yayuan Printing And Dyeing Co Ltd
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/47—Oxides or hydroxides of elements of Groups 5 or 15 of the Periodic Table; Vanadates; Niobates; Tantalates; Arsenates; Antimonates; Bismuthates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
    • D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/262—Sulfated compounds thiosulfates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
    • D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Fireproofing Substances (AREA)

Abstract

The invention discloses a kind of dyeing and printing process of camouflage facing material, comprise the following steps：S1, singe；S2, cold pad--batch；S3, alkali cleaning；S4, alkali oxygen are washed；S5, mercerising；S6, dye ground；S7, stamp；S8, flame-proof treatment；S9, bake；S10, tentering and preshrunk；The step of flame-proof treatment is：By in the fabric dipping fire retarding treating liquid after revenue stamp process, process is rolled using two leachings two, fire retarding treating liquid is uniformly impregnated within the fiber of the fabric；In the fire retarding treating liquid, the concentration of fire retardant is 270 350g/L, and the concentration of bleeding agent is 9 13g/L, and the concentration of anti wrinkling agent is 5 9g/L, the concentration of polyoxyethylene nonylphenol ether 10 is 0.5 2g/L.The dyeing and printing process of camouflage facing material proposed by the present invention, its step is simple, and raw material is easy to get, and is easy to industrialized production, and obtained camouflage facing material has excellent anti-flammability.

Description

一种迷彩面料的印染工艺A kind of printing and dyeing process of camouflage fabric

技术领域technical field

本发明涉及印染技术领域，尤其涉及一种迷彩面料的印染工艺。The invention relates to the technical field of printing and dyeing, in particular to a printing and dyeing process for camouflage fabrics.

背景技术Background technique

迷彩系列纺织品最早因军事需要而生产。随着人们生活水平和欣赏水平的不断提高，欣赏层次也向多元化发展，迷彩系列产品已不仅仅作为军工产品，很多品种的迷彩已逐渐向民用方面发展。常见迷彩面料以纯棉、涤棉和锦棉类厚重的高密织物为主，具有吸湿性强，手感自然，穿着舒适，经济实惠的特点，受到人们的欢迎，然而作为棉织物的迷彩面料属于易燃物品，是火灾的潜在成因，大多需要进行阻燃整理以满足不同程度的防火需求，但是目前为止，迷彩面料存在阻燃性差的缺陷，限制了迷彩面料的应用。Camouflage series textiles were first produced for military needs. With the continuous improvement of people's living standards and appreciation levels, the appreciation level is also developing towards diversification. The camouflage series products are not only used as military products, but many varieties of camouflage have gradually been developed for civilian use. Common camouflage fabrics are mainly thick and high-density fabrics such as pure cotton, polyester cotton and nylon cotton, which have strong hygroscopicity, natural feel, comfortable wearing, and economical benefits. Combustible items are a potential cause of fire, and most of them need flame-retardant finishing to meet different degrees of fire protection requirements. However, so far, camouflage fabrics have the defect of poor flame retardancy, which limits the application of camouflage fabrics.

发明内容Contents of the invention

基于背景技术存在的技术问题，本发明提出了一种迷彩面料的印染工艺，其步骤简单，原料易得，便于工业化生产，得到的迷彩面料具有优异的阻燃性。Based on the technical problems existing in the background technology, the present invention proposes a printing and dyeing process for camouflage fabrics, which has simple steps, readily available raw materials, and is convenient for industrial production. The obtained camouflage fabrics have excellent flame retardancy.

本发明提出的一种迷彩面料的印染工艺，包括以下步骤：S1、烧毛；S2、冷轧堆；S3、碱洗；S4、碱氧洗；S5、丝光；S6、染地；S7、印花；S8、阻燃整理；S9、焙烘；S10、拉幅和预缩；The printing and dyeing process of a camouflage fabric proposed by the present invention comprises the following steps: S1, singeing; S2, cold pad-batch; S3, alkali washing; S4, alkali-oxygen washing; S5, mercerizing; S6, ground dyeing; S7, printing; S8, flame retardant finishing; S9, baking; S10, tentering and pre-shrinking;

其中，所述阻燃整理的步骤为：将经过印花工序后的面料浸渍阻燃整理液中，采用二浸二轧工序，使阻燃整理液均匀浸渍在所述面料的纤维上；Wherein, the step of the flame-retardant finishing is: dipping the fabric after the printing process into the flame-retardant finishing liquid, and adopting two dipping and two-rolling processes, so that the flame-retardant finishing liquid is evenly impregnated on the fibers of the fabric;

所述阻燃整理液中，阻燃剂的浓度为270-350g/L，渗透剂的浓度为9-13g/L，抗皱剂的浓度为5-9g/L、乳化剂OP-10的浓度为0.5-2g/L。In the flame retardant finishing solution, the concentration of the flame retardant is 270-350g/L, the concentration of the penetrating agent is 9-13g/L, the concentration of the anti-wrinkle agent is 5-9g/L, and the concentration of the emulsifier OP-10 is 0.5-2g/L.

优选地，在二浸二轧过程中，阻燃整理液的温度为25-40℃，第一次浸泡时间为35-50min，第二次浸泡时间为4-10min；压轧压力为0.35-0.65MPa，轧余率为80-100％。Preferably, during the second dipping and second rolling process, the temperature of the flame retardant finishing solution is 25-40°C, the first soaking time is 35-50 minutes, the second soaking time is 4-10 minutes; the rolling pressure is 0.35-0.65 MPa, the surplus rate is 80-100%.

优选地，所述阻燃剂的原料包括改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵。Preferably, the raw materials of the flame retardant include modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, Dihydroxymethyl Phosphate, Ammonium Dimethoxy Phosphate.

优选地，改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵的重量比为2-10：2-12：3-15：4-20：3-8：10-20：3-8：1-7。Preferably, modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl, urea, dimethylol phosphoric acid, dimethyl The weight ratio of ammonium oxyphosphate is 2-10:2-12:3-15:4-20:3-8:10-20:3-8:1-7.

优选地，所述改性蒙脱土为二乙烯三胺改性蒙脱土。Preferably, the modified montmorillonite is diethylenetriamine modified montmorillonite.

优选地，焙烘的具体工艺为：将经阻燃整理后的面料在85-105℃下预烘3-5min，然后在130-145℃下焙烘2-4.5min。Preferably, the specific process of baking is: pre-baking the flame-retardant finished fabric at 85-105°C for 3-5 minutes, and then baking at 130-145°C for 2-4.5 minutes.

优选地，所述渗透剂为烷基硫酸酯钠、脂肪醇聚氧乙烯醚JFC中的一种或者两种的混合物。Preferably, the penetrating agent is one or a mixture of sodium alkyl sulfate and fatty alcohol polyoxyethylene ether JFC.

优选地，所述抗皱剂为丁烷四羧酸、柠檬酸、马来酸、聚马来酸中的一种或者多种的混合物。Preferably, the anti-wrinkle agent is one or a mixture of butane tetracarboxylic acid, citric acid, maleic acid and polymaleic acid.

本发明所述迷彩面料的印染工艺，采用了二浸二轧的工序对面料进行了阻燃处理，赋予面料优异的阻燃性，且使面料手感柔软，在阻燃剂中，选择了改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵为原料，通过控制阻燃剂中各原料的含量，并控制焙烘的工艺条件，在防止各原料分解的同时使各原料的性能实现了最佳的协同，赋予迷彩面料优异的阻燃性，其中，阻燃剂中加入了二羟甲基磷酸和二甲氧基磷酸铵与尿素配合，在防止织物泛黄的同时能生成不含离子的纤维素磷酸酯，避免硬水洗时发生离子交换，赋予织物优异的耐久阻燃性，实现了织物白度和阻燃之间的综合平衡；改性蒙脱土与多聚磷酸铵配合后赋予面料优异的成炭率，克服了多聚磷酸铵在织物表面迁移所造成的发白和强度不足的缺陷，并使面料更加柔软；氧化铋加入体系中，能减少面料燃烧过程中的烟释放量，进一步提高面料的阻燃性。The printing and dyeing process of the camouflage fabric of the present invention adopts the process of two dipping and two rolling to carry out flame retardant treatment on the fabric, endows the fabric with excellent flame retardancy, and makes the fabric feel soft. Among the flame retardants, modified Montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, dimethylol phosphoric acid, ammonium dimethoxy phosphate as Raw materials, by controlling the content of each raw material in the flame retardant and controlling the baking process conditions, while preventing the decomposition of each raw material, the performance of each raw material can be optimally coordinated, and the camouflage fabric is endowed with excellent flame retardancy, among which , adding dimethylol phosphoric acid and ammonium dimethoxy phosphate to the flame retardant, combined with urea, can generate ion-free cellulose phosphate while preventing the fabric from yellowing, avoiding ion exchange during hard washing, and imparting The excellent durable flame retardancy of the fabric has achieved a comprehensive balance between the whiteness of the fabric and the flame retardancy; the combination of modified montmorillonite and ammonium polyphosphate endows the fabric with an excellent char formation rate, which overcomes the effect of ammonium polyphosphate on the fabric. The defects of whitening and insufficient strength caused by surface migration can make the fabric softer; adding bismuth oxide to the system can reduce the amount of smoke released during the combustion process of the fabric and further improve the flame retardancy of the fabric.

具体实施方式Detailed ways

下面，通过具体实施例对本发明的技术方案进行详细说明。Below, the technical solution of the present invention will be described in detail through specific examples.

实施例1Example 1

本发明提出的一种迷彩面料的印染工艺，包括以下步骤：S1、烧毛；S2、冷轧堆；S3、碱洗；S4、碱氧洗；S5、丝光；S6、染地；S7、印花；S8、阻燃整理；S9、焙烘；S10、拉幅和预缩；The printing and dyeing process of a camouflage fabric proposed by the present invention comprises the following steps: S1, singeing; S2, cold pad-batch; S3, alkali washing; S4, alkali-oxygen washing; S5, mercerizing; S6, ground dyeing; S7, printing; S8, flame retardant finishing; S9, baking; S10, tentering and pre-shrinking;

其中，所述阻燃整理的步骤为：将经过印花工序后的面料浸渍阻燃整理液中，采用二浸二轧工序，使阻燃整理液均匀浸渍在所述面料的纤维上；Wherein, the step of the flame-retardant finishing is: dipping the fabric after the printing process into the flame-retardant finishing liquid, and adopting two dipping and two-rolling processes, so that the flame-retardant finishing liquid is evenly impregnated on the fibers of the fabric;

所述阻燃整理液中，阻燃剂的浓度为350g/L，渗透剂的浓度为9g/L，抗皱剂的浓度为9g/L、乳化剂OP-10的浓度为0.5g/L。In the flame retardant finishing liquid, the concentration of the flame retardant is 350g/L, the concentration of the penetrating agent is 9g/L, the concentration of the anti-wrinkle agent is 9g/L, and the concentration of the emulsifier OP-10 is 0.5g/L.

实施例2Example 2

本发明提出的一种迷彩面料的印染工艺，包括以下步骤：S1、烧毛；S2、冷轧堆；S3、碱洗；S4、碱氧洗；S5、丝光；S6、染地；S7、印花；S8、阻燃整理；S9、焙烘；S10、拉幅和预缩；The printing and dyeing process of a camouflage fabric proposed by the present invention comprises the following steps: S1, singeing; S2, cold pad-batch; S3, alkali washing; S4, alkali-oxygen washing; S5, mercerizing; S6, ground dyeing; S7, printing; S8, flame retardant finishing; S9, baking; S10, tentering and pre-shrinking;

其中，所述阻燃整理的步骤为：将经过印花工序后的面料浸渍阻燃整理液中，采用二浸二轧工序，使阻燃整理液均匀浸渍在所述面料的纤维上；Wherein, the step of the flame-retardant finishing is: dipping the fabric after the printing process into the flame-retardant finishing liquid, and adopting two dipping and two-rolling processes, so that the flame-retardant finishing liquid is evenly impregnated on the fibers of the fabric;

所述阻燃整理液中，阻燃剂的浓度为270g/L，渗透剂的浓度为13g/L，抗皱剂的浓度为5g/L、乳化剂OP-10的浓度为2g/L。In the flame retardant finishing liquid, the concentration of the flame retardant is 270g/L, the concentration of the penetrating agent is 13g/L, the concentration of the anti-wrinkle agent is 5g/L, and the concentration of the emulsifier OP-10 is 2g/L.

实施例3Example 3

本发明提出的一种迷彩面料的印染工艺，包括以下步骤：S1、烧毛；S2、冷轧堆；S3、碱洗；S4、碱氧洗；S5、丝光；S6、染地；S7、印花；S8、阻燃整理；S9、焙烘；S10、拉幅和预缩；The printing and dyeing process of a camouflage fabric proposed by the present invention comprises the following steps: S1, singeing; S2, cold pad-batch; S3, alkali washing; S4, alkali-oxygen washing; S5, mercerizing; S6, ground dyeing; S7, printing; S8, flame retardant finishing; S9, baking; S10, tentering and pre-shrinking;

其中，所述阻燃整理的步骤为：将经过印花工序后的面料浸渍阻燃整理液中，采用二浸二轧工序，使阻燃整理液均匀浸渍在所述面料的纤维上；Wherein, the step of the flame-retardant finishing is: dipping the fabric after the printing process into the flame-retardant finishing liquid, and adopting two dipping and two-rolling processes, so that the flame-retardant finishing liquid is evenly impregnated on the fibers of the fabric;

所述阻燃整理液中，阻燃剂的浓度为330g/L，渗透剂的浓度为10g/L，抗皱剂的浓度为8.3g/L、乳化剂OP-10的浓度为1g/L；In the flame retardant finishing liquid, the concentration of the flame retardant is 330g/L, the concentration of the penetrant is 10g/L, the concentration of the anti-wrinkle agent is 8.3g/L, and the concentration of the emulsifier OP-10 is 1g/L;

在二浸二轧过程中，阻燃整理液的温度为40℃，第一次浸泡时间为35min，第二次浸泡时间为10min；压轧压力为0.35MPa，轧余率为100％；In the second dipping and second rolling process, the temperature of the flame retardant finishing solution is 40°C, the first soaking time is 35 minutes, and the second soaking time is 10 minutes; the rolling pressure is 0.35MPa, and the rolling rate is 100%;

所述阻燃剂的原料包括改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵，且改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵的重量比为2：12：3：20：3：20：3：7；The raw materials of the flame retardant include modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, dimethylol Ammonium phosphoric acid, ammonium dimethoxyphosphate, and modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, The weight ratio of dimethylol phosphoric acid and ammonium dimethoxy phosphate is 2:12:3:20:3:20:3:7;

所述改性蒙脱土为二乙烯三胺改性蒙脱土；The modified montmorillonite is diethylenetriamine modified montmorillonite;

所述渗透剂为烷基硫酸酯钠；The penetrating agent is sodium alkyl sulfate;

所述抗皱剂为柠檬酸、马来酸、聚马来酸的混合物，且柠檬酸、马来酸、聚马来酸的重量比为3:5:2；Described anti-wrinkle agent is the mixture of citric acid, maleic acid, polymaleic acid, and the weight ratio of citric acid, maleic acid, polymaleic acid is 3:5:2;

焙烘的具体工艺为：将经阻燃整理后的面料在85℃下预烘5min，然后在130℃下焙烘4.5min。The specific process of baking is as follows: pre-baking the flame-retardant finished fabric at 85°C for 5 minutes, and then baking at 130°C for 4.5 minutes.

实施例4Example 4

本发明提出的一种迷彩面料的印染工艺，包括以下步骤：S1、烧毛；S2、冷轧堆；S3、碱洗；S4、碱氧洗；S5、丝光；S6、染地；S7、印花；S8、阻燃整理；S9、焙烘；S10、拉幅和预缩；The printing and dyeing process of a camouflage fabric proposed by the present invention comprises the following steps: S1, singeing; S2, cold pad-batch; S3, alkali washing; S4, alkali-oxygen washing; S5, mercerizing; S6, ground dyeing; S7, printing; S8, flame retardant finishing; S9, baking; S10, tentering and pre-shrinking;

其中，所述阻燃整理的步骤为：将经过印花工序后的面料浸渍阻燃整理液中，采用二浸二轧工序，使阻燃整理液均匀浸渍在所述面料的纤维上；Wherein, the step of the flame-retardant finishing is: dipping the fabric after the printing process into the flame-retardant finishing liquid, and adopting two dipping and two-rolling processes, so that the flame-retardant finishing liquid is evenly impregnated on the fibers of the fabric;

所述阻燃整理液中，阻燃剂的浓度为280g/L，渗透剂的浓度为12g/L，抗皱剂的浓度为6.5g/L、乳化剂OP-10的浓度为1.8g/L；In the flame retardant finishing liquid, the concentration of flame retardant is 280g/L, the concentration of penetrant is 12g/L, the concentration of anti-wrinkle agent is 6.5g/L, and the concentration of emulsifier OP-10 is 1.8g/L;

在二浸二轧过程中，阻燃整理液的温度为25℃，第一次浸泡时间为50min，第二次浸泡时间为4min；压轧压力为0.65MPa，轧余率为80％；During the second dipping and second rolling process, the temperature of the flame retardant finishing solution is 25°C, the first soaking time is 50 minutes, and the second soaking time is 4 minutes; the rolling pressure is 0.65MPa, and the rolling ratio is 80%;

所述阻燃剂的原料包括改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵，且改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵的重量比为10：2：15：4：8：10：8：1；The raw materials of the flame retardant include modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, dimethylol Ammonium phosphoric acid, ammonium dimethoxyphosphate, and modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, The weight ratio of dimethylol phosphoric acid and ammonium dimethoxy phosphate is 10:2:15:4:8:10:8:1;

所述改性蒙脱土为二乙烯三胺改性蒙脱土；The modified montmorillonite is diethylenetriamine modified montmorillonite;

所述渗透剂为脂肪醇聚氧乙烯醚JFC；The penetrating agent is fatty alcohol polyoxyethylene ether JFC;

所述抗皱剂为丁烷四羧酸；The anti-wrinkle agent is butane tetracarboxylic acid;

焙烘的具体工艺为：将经阻燃整理后的面料在105℃下预烘3min，然后在145℃下焙烘2min。The specific process of baking is: pre-baking the flame-retardant finished fabric at 105°C for 3 minutes, and then baking at 145°C for 2 minutes.

实施例5Example 5

本发明提出的一种迷彩面料的印染工艺，包括以下步骤：S1、烧毛；S2、冷轧堆；S3、碱洗；S4、碱氧洗；S5、丝光；S6、染地；S7、印花；S8、阻燃整理；S9、焙烘；S10、拉幅和预缩；The printing and dyeing process of a camouflage fabric proposed by the present invention comprises the following steps: S1, singeing; S2, cold pad-batch; S3, alkali washing; S4, alkali-oxygen washing; S5, mercerizing; S6, ground dyeing; S7, printing; S8, flame retardant finishing; S9, baking; S10, tentering and pre-shrinking;

其中，所述阻燃整理的步骤为：将经过印花工序后的面料浸渍阻燃整理液中，采用二浸二轧工序，使阻燃整理液均匀浸渍在所述面料的纤维上；Wherein, the step of the flame-retardant finishing is: dipping the fabric after the printing process into the flame-retardant finishing liquid, and adopting two dipping and two-rolling processes, so that the flame-retardant finishing liquid is evenly impregnated on the fibers of the fabric;

所述阻燃整理液中，阻燃剂的浓度为300g/L，渗透剂的浓度为10g/L，抗皱剂的浓度为8.5g/L、乳化剂OP-10的浓度为1.5g/L；In the flame retardant finishing solution, the concentration of flame retardant is 300g/L, the concentration of penetrant is 10g/L, the concentration of anti-wrinkle agent is 8.5g/L, and the concentration of emulsifier OP-10 is 1.5g/L;

在二浸二轧过程中，阻燃整理液的温度为35℃，第一次浸泡时间为42min，第二次浸泡时间为6min；压轧压力为0.5MPa，轧余率为95％；During the second dipping and second rolling process, the temperature of the flame retardant finishing solution is 35°C, the first soaking time is 42 minutes, and the second soaking time is 6 minutes; the rolling pressure is 0.5MPa, and the rolling rate is 95%;

所述阻燃剂的原料包括改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵，且改性蒙脱土、多聚磷酸铵、氧化铋、聚氨酯、N,N-双(2-羟甲基)氨基乙基膦酸二甲酯、尿素、二羟甲基磷酸、二甲氧基磷酸铵的重量比为8：11：12：14：6：15：5：6；The raw materials of the flame retardant include modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, dimethylol Ammonium phosphoric acid, ammonium dimethoxyphosphate, and modified montmorillonite, ammonium polyphosphate, bismuth oxide, polyurethane, N,N-bis(2-hydroxymethyl)aminoethylphosphonic acid dimethyl ester, urea, The weight ratio of dimethylol phosphoric acid and ammonium dimethoxy phosphate is 8:11:12:14:6:15:5:6;

所述改性蒙脱土为二乙烯三胺改性蒙脱土；The modified montmorillonite is diethylenetriamine modified montmorillonite;

所述渗透剂为烷基硫酸酯钠、脂肪醇聚氧乙烯醚的混合物，且烷基硫酸酯钠、脂肪醇聚氧乙烯醚的重量比为3：4；The penetrating agent is a mixture of sodium alkyl sulfate and fatty alcohol polyoxyethylene ether, and the weight ratio of sodium alkyl sulfate and fatty alcohol polyoxyethylene ether is 3:4;

所述抗皱剂为丁烷四羧酸、柠檬酸、马来酸、聚马来酸的混合物，且丁烷四羧酸、柠檬酸、马来酸、聚马来酸的重量比为4：6：3：1；The anti-wrinkle agent is a mixture of butane tetracarboxylic acid, citric acid, maleic acid and polymaleic acid, and the weight ratio of butane tetracarboxylic acid, citric acid, maleic acid and polymaleic acid is 4:6 :3:1;

焙烘的具体工艺为：将经阻燃整理后的面料在100℃下预烘4min，然后在140℃下焙烘3.8min。The specific process of baking is: pre-baking the flame-retardant finished fabric at 100°C for 4 minutes, and then baking at 140°C for 3.8 minutes.

以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。The above is only a preferred embodiment of the present invention, but the scope of protection of the present invention is not limited thereto, any person familiar with the technical field within the technical scope disclosed in the present invention, according to the technical solution of the present invention Any equivalent replacement or change of the inventive concepts thereof shall fall within the protection scope of the present invention.

Claims (8)

1. a kind of dyeing and printing process of camouflage facing material, it is characterised in that comprise the following steps：S1, singe；S2, cold pad--batch；S3, alkali Wash；S4, alkali oxygen are washed；S5, mercerising；S6, dye ground；S7, stamp；S8, flame-proof treatment；S9, bake；S10, tentering and preshrunk；
Wherein, the step of flame-proof treatment is：By in the fabric dipping fire retarding treating liquid after revenue stamp process, soaked using two Two roll process, fire retarding treating liquid is uniformly impregnated within the fiber of the fabric；
In the fire retarding treating liquid, the concentration of fire retardant is 270-350g/L, and the concentration of bleeding agent is 9-13g/L, anti wrinkling agent Concentration is 5-9g/L, the concentration of emulsifier op-10 is 0.5-2g/L.
2. the dyeing and printing process of camouflage facing material according to claim 1, it is characterised in that fire-retardant whole during two leachings two are rolled The temperature for managing liquid is 25-40 DEG C, and first time soak time is 35-50min, and second of soak time is 4-10min；Pressure rolling pressure For 0.35-0.65MPa, pick-up 80-100%.
3. the dyeing and printing process of camouflage facing material according to claim 1 or claim 2, it is characterised in that the raw material of the fire retardant includes Modified montmorillonoid, ammonium polyphosphate, bismuth oxide, polyurethane, N, double (2- methylols) the aminoethyl phosphonic acid dimethyl esters of N-, urea, Dihydroxymethyl phosphoric acid, dimethoxy ammonium phosphate.
4. the dyeing and printing process of camouflage facing material according to claim 3, it is characterised in that modified montmorillonoid, ammonium polyphosphate, oxygen Change bismuth, polyurethane, N, N- double (2- methylols) aminoethyl phosphonic acid dimethyl ester, urea, dihydroxymethyl phosphoric acid, dimethoxy phosphoric acid The weight ratio of ammonium is 2-10：2-12：3-15：4-20：3-8：10-20：3-8：1-7.
5. according to the dyeing and printing process of the camouflage facing material of claim 3 or 4, it is characterised in that the modified montmorillonoid is diethyl Alkene triamine modified montmorillonoid.
6. according to the dyeing and printing process of camouflage facing material any one of claim 1-5, it is characterised in that the concrete technology baked For：By the fabric after flame-proof treatment at 85-105 DEG C preliminary drying 3-5min, then bake 2-4.5min at 130-145 DEG C.
7. according to the dyeing and printing process of camouflage facing material any one of claim 1-6, it is characterised in that the bleeding agent is alkane One or two kinds of mixture in base sodium sulfovinate, AEO JFC.
8. according to the dyeing and printing process of camouflage facing material any one of claim 1-7, it is characterised in that the anti wrinkling agent is fourth One or more kinds of mixtures in alkane tetrabasic carboxylic acid, citric acid, maleic acid, poly.
CN201710981731.2A 2017-10-20 2017-10-20 A kind of dyeing and printing process of camouflage facing material Withdrawn CN107780202A (en)

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CN109137211A (en) * 2018-07-13 2019-01-04 浙江盛发纺织印染有限公司 A kind of duplex pringing camouflage inflaming retarding fabric
CN110747666A (en) * 2019-11-15 2020-02-04 四川鑫敬业化纤织带有限公司 Nylon 56 flame-retardant infrared-resistant camouflage ribbon

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CN103266468A (en) * 2013-05-30 2013-08-28 东华大学 Flame retardant conditioning method of intumescent flame retardant system on pure cotton fabrics
CN105040490A (en) * 2015-06-11 2015-11-11 芜湖市瑞都服装贸易有限公司 A printing and dyeing process of camouflage fabric
CN106049092A (en) * 2016-06-21 2016-10-26 安徽亚源印染有限公司 Anti-infrared military camouflage fabric and printing and dyeing process thereof

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Publication number Priority date Publication date Assignee Title
CN103266468A (en) * 2013-05-30 2013-08-28 东华大学 Flame retardant conditioning method of intumescent flame retardant system on pure cotton fabrics
CN105040490A (en) * 2015-06-11 2015-11-11 芜湖市瑞都服装贸易有限公司 A printing and dyeing process of camouflage fabric
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109137211A (en) * 2018-07-13 2019-01-04 浙江盛发纺织印染有限公司 A kind of duplex pringing camouflage inflaming retarding fabric
CN110747666A (en) * 2019-11-15 2020-02-04 四川鑫敬业化纤织带有限公司 Nylon 56 flame-retardant infrared-resistant camouflage ribbon

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Application publication date: 20180309