CN108398403A - A kind of cone of wavelength modulation type four light fibre humidity transducer - Google Patents

A kind of cone of wavelength modulation type four light fibre humidity transducer Download PDF

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CN108398403A
CN108398403A CN201810253978.7A CN201810253978A CN108398403A CN 108398403 A CN108398403 A CN 108398403A CN 201810253978 A CN201810253978 A CN 201810253978A CN 108398403 A CN108398403 A CN 108398403A
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cone
optical fiber
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连延辉
连延钹
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Fujian Silicon Light Communication Technology Co Ltd
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/41Refractivity; Phase-affecting properties, e.g. optical path length
    • G01N21/45Refractivity; Phase-affecting properties, e.g. optical path length using interferometric methods; using Schlieren methods
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/41Refractivity; Phase-affecting properties, e.g. optical path length
    • G01N21/45Refractivity; Phase-affecting properties, e.g. optical path length using interferometric methods; using Schlieren methods
    • G01N2021/458Refractivity; Phase-affecting properties, e.g. optical path length using interferometric methods; using Schlieren methods using interferential sensor, e.g. sensor fibre, possibly on optical waveguide

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Abstract

本发明涉及一种波长调制型四锥光纤湿度传感器,包括光源、四锥光纤以及用于检测光的波长位置变化的探测器,所述四锥光纤两端分别与所述光源和探测器连接,所述四锥光纤的四锥结构上涂覆有湿敏材质的光学凝胶层。本发明检测湿度时,当不同湿度的空气与琼脂糖凝胶接薄膜触后,琼脂糖凝胶薄膜的折射率会发生改变,从而影响光纤中光的传输特性,通过测量干涉峰/谷的波长位置的变化,即可获得周围环境相应的湿度,并且,光纤采用四锥结构积累相位差,增强光耦合时干涉的变化量,在保证测量的灵敏度时,无需大幅度拉长四锥光纤锥腰部分的长度,其结构原理简单可靠,工艺步骤简便,操作制备容易,产品稳定性好,使用寿命长。

The invention relates to a wavelength-modulated four-cone optical fiber humidity sensor, which includes a light source, a four-cone optical fiber and a detector for detecting changes in the wavelength position of light. Both ends of the four-cone optical fiber are respectively connected to the light source and the detector. The four-cone structure of the four-cone optical fiber is coated with an optical gel layer of moisture-sensitive material. When the present invention detects humidity, when the air with different humidity is in contact with the agarose gel film, the refractive index of the agarose gel film will change, thereby affecting the transmission characteristics of light in the optical fiber, by measuring the wavelength of the interference peak/valley The corresponding humidity of the surrounding environment can be obtained by changing the position, and the optical fiber adopts a four-cone structure to accumulate phase difference, which enhances the change of interference during optical coupling. When ensuring the sensitivity of the measurement, there is no need to greatly lengthen the four-cone fiber cone waist The length of the part, its structural principle is simple and reliable, the process steps are simple, the operation and preparation are easy, the product stability is good, and the service life is long.

Description

一种波长调制型四锥光纤湿度传感器A wavelength-modulated four-cone fiber optic humidity sensor

技术领域technical field

本发明涉及光纤湿度传感器制作技术领域,更具体地说是指一种波长调制型四锥光纤湿度传感器。The invention relates to the technical field of making an optical fiber humidity sensor, and more specifically refers to a wavelength modulation type four-cone optical fiber humidity sensor.

背景技术Background technique

光纤湿度传感器相对于传统的电容电阻型湿度传感器具有许多优势。如:体积小、稳定性好,抗电磁干扰。现如今,光纤湿度传感器已经得到了广泛的应用,例如应用于农业上的粮食存储、锅炉内的高温环境、工业领域等等。近些年来,光纤湿度传感器的测量方法主要有以下几种:光谱法、光强度调制法、改变表面反射率、Bragg 和长周期光栅、干涉仪等。Fiber optic humidity sensors have many advantages over traditional capacitance-resistive humidity sensors. Such as: small size, good stability, anti-electromagnetic interference. Nowadays, fiber optic humidity sensors have been widely used, such as grain storage in agriculture, high temperature environment in boilers, industrial fields and so on. In recent years, the measurement methods of optical fiber humidity sensors mainly include the following: spectroscopy, light intensity modulation, changing surface reflectivity, Bragg and long-period gratings, interferometers, etc.

近年来,许多人在光纤表面涂敷湿敏材料使得传感器的特性得以提高。但是光强调制型的传感器容易受到光源功率波动的影响如专利号:CN 107561039 A,采用的是光强调制的方法,易受光源波动的影响。采用布拉格光纤光栅的传感器,成本高。In recent years, many people have improved the characteristics of the sensor by coating moisture-sensitive materials on the surface of optical fibers. However, light intensity modulation sensors are easily affected by light source power fluctuations, such as patent number: CN 107561039 A, which uses a light intensity modulation method, which is easily affected by light source fluctuations. Sensors using Bragg fiber gratings are expensive.

为解决上述问题,授权公告号为CN 203287311U的中国实用新型专利公开了一种基于双锥型细芯单模光纤的透射式光纤湿度传感器,包括第一单模光纤、双锥型细芯单模光纤、第二单模光纤和湿度敏感膜四部分。双锥型细芯单模光纤的锥腰表面涂有湿度敏感膜;第一单模光纤,第二单模光纤分别与宽带光源和光纤光谱仪相连。该传感器器虽然能够根据环境湿度的改变引起湿度敏感膜折射率的改变,进而引起传感器的透射光谱特性发生变化。根据透射光谱中特征峰的波长变化量即可获得环境的湿度值。虽然该传感采用波长解调的方法,克服了光源光强稳定的影响,但是,该传感器基于双锥细芯的结构,其细芯单模必须拉得足够长,即细芯非常细,如10微米以下,否则难以通过光纤光谱仪测量传感器透光谱中的特征峰波长的改变量。另外,现有的光纤湿度传感器通常工作在1.3微米或者1.5微米的波段上,但是该波段没有很强的水分子吸收,灵敏度不高。In order to solve the above problems, the Chinese utility model patent with the authorized announcement number CN 203287311U discloses a transmission optical fiber humidity sensor based on biconical thin-core single-mode optical fiber, including the first single-mode optical fiber, biconical thin-core single-mode fiber The optical fiber, the second single-mode optical fiber and the humidity sensitive film are composed of four parts. The surface of the cone waist of the biconical thin-core single-mode fiber is coated with a moisture-sensitive film; the first single-mode fiber and the second single-mode fiber are respectively connected with a broadband light source and a fiber optic spectrometer. Although the sensor device can cause changes in the refractive index of the humidity-sensitive film according to changes in ambient humidity, thereby causing changes in the transmission spectrum characteristics of the sensor. According to the wavelength change of the characteristic peak in the transmission spectrum, the humidity value of the environment can be obtained. Although the sensor adopts the method of wavelength demodulation to overcome the influence of the light intensity stability of the light source, the sensor is based on the structure of the double cone thin core, and the single mode of the thin core must be drawn long enough, that is, the thin core is very thin, such as Otherwise, it is difficult to measure the change of the characteristic peak wavelength in the transmission spectrum of the sensor by a fiber optic spectrometer. In addition, the existing optical fiber humidity sensors usually work in the 1.3 micron or 1.5 micron waveband, but this waveband has no strong absorption of water molecules, and the sensitivity is not high.

发明内容Contents of the invention

本发明提供一种波长调制型四锥光纤湿度传感器,目的在于克服现有技术的不足,提供一种结构简单、成本低廉、灵敏度高的光纤湿度传感器。The invention provides a wavelength-modulated four-cone optical fiber humidity sensor, aiming at overcoming the deficiencies of the prior art and providing an optical fiber humidity sensor with simple structure, low cost and high sensitivity.

本发明采用如下技术方案:The present invention adopts following technical scheme:

一种波长调制型四锥光纤湿度传感器,包括光源、四锥光纤以及用于检测光的波长位置变化的探测器,所述四锥光纤两端分别与所述光源和探测器连接,所述四锥光纤的四锥结构上涂覆有湿敏材质的光学凝胶层。A wavelength-modulated four-cone optical fiber humidity sensor, including a light source, a four-cone optical fiber, and a detector for detecting changes in the wavelength position of light. Both ends of the four-cone optical fiber are respectively connected to the light source and the detector. The four-cone structure of the tapered optical fiber is coated with an optical gel layer of moisture-sensitive material.

进一步地,所述光源为宽度光源或者可调谐光源,光源的波长范围是1900nm~2400nm,优选为2000nm,即两微米的光源。Further, the light source is a width light source or a tunable light source, and the wavelength range of the light source is 1900nm-2400nm, preferably 2000nm, that is, a light source of two microns.

进一步地,所述四锥光纤采用单模光纤研制,包括纤芯和包层,所述单模光纤上拉锥形成一段四锥结构,该段四锥结构纤芯涂覆所述光学凝胶层。Further, the four-cone optical fiber is developed by using a single-mode optical fiber, including a core and a cladding, and the single-mode optical fiber is tapered to form a section of a four-cone structure, and the core of the four-cone structure is coated with the optical gel layer .

进一步地,所述光学凝胶层为琼脂糖凝胶薄膜。Further, the optical gel layer is an agarose gel film.

进一步地,所述探测器为光谱仪。Further, the detector is a spectrometer.

由上述对本发明结构的描述可知,和现有技术相比,本发明具有如下优点:As can be seen from the above description of the structure of the present invention, compared with the prior art, the present invention has the following advantages:

1、 本发明检测湿度时,当不同湿度的空气与琼脂糖凝胶接薄膜触后,琼脂糖凝胶薄膜的折射率会发生改变,从而影响光纤中光的传输特性,通过测量干涉峰/谷的波长的变化,即可推算周围环境相应的湿度,不仅能够避免测试结果受光源光强稳定性的影响,而且光纤采用四锥结构积累相位差,增强光耦合时干涉的变化量,在保证测量的灵敏度时,无需大幅度拉长光纤锥腰部分的长度,其结构原理简单可靠,工艺步骤简便,操作制备容易,产品稳定性好,使用寿命长。1. When the present invention detects humidity, when the air of different humidity is in contact with the agarose gel film, the refractive index of the agarose gel film will change, thereby affecting the transmission characteristics of light in the optical fiber. By measuring the interference peak/valley The change of the wavelength can calculate the corresponding humidity of the surrounding environment, which can not only avoid the test results from being affected by the stability of the light intensity of the light source, but also use the four-cone structure of the optical fiber to accumulate the phase difference and enhance the interference change during optical coupling. When the sensitivity is high, there is no need to greatly lengthen the length of the tapered part of the optical fiber. The structure and principle are simple and reliable, the process steps are simple, the operation is easy to prepare, the product is stable, and the service life is long.

2、 本发明采用两微米的光源,两微米的光有很强的水分子吸收能力,并且涂覆有琼脂糖凝胶薄膜的四锥光纤,使传感器输出的损耗谱在1900-2000nm波段有若干个近似等间距的干涉峰/谷,其波长变化对湿度非常敏感,小的湿度变化,即可产生明显的波长变化,利用该特性,可以极大限度的提高湿度传感器的灵敏度。2, the present invention adopts the light source of two micrometers, and the light of two micrometers has very strong water molecule absorption capacity, and is coated with the four-tapered optical fiber of agarose gel film, makes the loss spectrum of sensor output have several in 1900-2000nm band An approximately equidistant interference peak/valley, its wavelength change is very sensitive to humidity, a small change in humidity can produce obvious wavelength change, using this feature, can greatly improve the sensitivity of the humidity sensor.

附图说明Description of drawings

图1为本发明结构框图;Fig. 1 is a structural block diagram of the present invention;

图2为四锥光纤结构示意图;Fig. 2 is a schematic diagram of the structure of a four-tapered optical fiber;

图3为本发明随外界环境湿度的改变的干涉损耗谱示意图;Fig. 3 is the interference loss spectrum schematic diagram of the present invention with the change of external environment humidity;

图4为特定波谷随外界湿度漂移的示意图。FIG. 4 is a schematic diagram of a specific trough drifting with external humidity.

具体实施方式Detailed ways

下面参照附图说明本发明实施例的具体实施方式。The specific implementation manners of the embodiments of the present invention will be described below with reference to the accompanying drawings.

参照图1和图2,一种波长调制型四锥光纤湿度传感器,包括光源1、四锥光纤2和用于检测光的波长位置变化的探测器3组成,探测器3优选为光谱仪。所述四锥光纤2两端分别与光源1和探测器3连接,四锥光纤2的四锥结构上涂覆有湿敏材质的光学凝胶层4。Referring to Figures 1 and 2, a wavelength-modulated four-cone optical fiber humidity sensor includes a light source 1, a four-cone optical fiber 2 and a detector 3 for detecting changes in the wavelength position of light. The detector 3 is preferably a spectrometer. Both ends of the four-cone fiber 2 are respectively connected to the light source 1 and the detector 3, and the four-cone structure of the four-cone fiber 2 is coated with an optical gel layer 4 of a moisture-sensitive material.

参照图1和图2,光源1采用宽度光源1或者可调谐光源1。光源1的波长范围为1900nm~2400nm,本实施例中优选为2000nm,即两微米的光源1,两微米的光有很强的水分子吸收能力,利用该特性,可以极大限度的提高湿度传感器的灵敏度。Referring to FIG. 1 and FIG. 2 , the light source 1 adopts a width light source 1 or a tunable light source 1 . The wavelength range of the light source 1 is 1900nm to 2400nm. In this embodiment, it is preferably 2000nm, that is, the light source 1 of two microns, and the light of two microns has a strong water molecule absorption capacity. Using this feature, the humidity sensor can be greatly improved. sensitivity.

参照图1和图2,四锥光纤2采用普通的单模光纤拉锥制成,其制作步骤如下:Referring to Figures 1 and 2, the four-tapered optical fiber 2 is made of a common single-mode optical fiber tapered, and its manufacturing steps are as follows:

1、取市面销售的单模光纤50cm,内外芯经为9/125um,其结构由纤芯和包层组成。1. Take a 50cm commercially available single-mode optical fiber, the inner and outer core diameters are 9/125um, and its structure is composed of a core and a cladding.

2、用光纤剥除器剥除长度为2~8cm的包层。2. Use a fiber stripper to strip the cladding with a length of 2-8cm.

3、采用拉锥的方法,如用二氧化碳激光器熔融拉制形成四锥结构的四锥光纤2。四锥光纤两个锥腰均为50-70微米,两个锥腰之间的距离为10-30微米。3. Adopt the tapering method, such as melting and drawing the four-tapered optical fiber 2 with a four-tapered structure by using a carbon dioxide laser. The two cone waists of the four-taper fiber are both 50-70 microns, and the distance between the two cone waists is 10-30 microns.

4、在裸露四锥结构的纤芯上涂覆有湿敏材质的光学凝胶层4。4. An optical gel layer 4 of a moisture-sensitive material is coated on the bare four-cone structure fiber core.

参照图1和图2,光学凝胶层4采用湿敏材质制成,可以为琼脂糖凝胶薄膜、PVA薄膜、氧化石墨烯薄膜等湿敏材质薄膜。本实施例中优选为琼脂糖凝胶薄膜。琼脂糖凝胶薄膜含有多个羟基,可吸收水分,将琼脂糖凝胶与光纤相结合,琼脂糖凝胶会影响光纤的有效折射率,进而影响到光纤中的传输特性。由于简单及低廉的制作方法,与光纤系统的高度兼容性,使得琼脂糖凝胶成为四锥光纤2传感的理想材料。Referring to Fig. 1 and Fig. 2, the optical gel layer 4 is made of a moisture-sensitive material, which may be a moisture-sensitive material film such as an agarose gel film, a PVA film, or a graphene oxide film. In this embodiment, an agarose gel film is preferred. The agarose gel film contains multiple hydroxyl groups, which can absorb water and combine the agarose gel with the optical fiber. The agarose gel will affect the effective refractive index of the optical fiber, and then affect the transmission characteristics in the optical fiber. Due to the simple and cheap fabrication method and high compatibility with fiber optic systems, agarose gel is an ideal material for quadruple cone fiber optic 2 sensing.

参照图1至图4,本发明的基本工作原理如下:With reference to Fig. 1 to Fig. 4, the basic operating principle of the present invention is as follows:

采用2微米的光源1发出的光在四锥光纤2中传播,当光从单模光纤的纤芯中传输到四锥结构的第一个双锥区域时,入射光等效地变成二束光,即分成纤芯中的光和包层及光学凝胶层4的光。这二束光经过第二个双锥区域时,积累了相位差,当它们耦合回单模光纤纤芯后会发生干涉,干涉输出的干涉损耗谱呈若干个损耗峰/谷,当外界环境湿度发生变化时,损耗峰/谷的位置也跟着变化,具体表现为某特定峰/谷位置处波长随着湿度的变化做出规律性的移动。该干涉峰/谷的波长λ变化与湿度RH如图3所示,近似成线性关系,其函数为λ=λ0+a*RH(RH是相对湿度,单位是%,a是传感器的灵敏度,P0是传感器参数)。从上面方程可以看出,λ与湿度RH近似成线性关系,通过测量损耗谱特定波长的λ,就可以获得相对湿度,即RH=(λ-λ0)/a。传感器的灵敏度a和传感器参数P0由实验标定。The light emitted by the 2-micron light source 1 propagates in the four-cone fiber 2. When the light is transmitted from the core of the single-mode fiber to the first double-cone region of the four-cone structure, the incident light becomes equivalently two beams Light, that is, split into the light in the core and the light in the cladding and the optical gel layer 4 . When the two beams of light pass through the second biconical region, the phase difference is accumulated. When they are coupled back to the core of the single-mode fiber, interference will occur. The interference loss spectrum of the interference output shows several loss peaks/valleys. When the external environment humidity When the change occurs, the position of the loss peak/valley also changes, which is specifically manifested in the regular movement of the wavelength at a specific peak/valley position as the humidity changes. The wavelength λ change of the interference peak/valley and the humidity RH are shown in Figure 3, which is approximately linear, and its function is λ=λ0+a*RH (RH is the relative humidity, the unit is %, a is the sensitivity of the sensor, P0 is the sensor parameter). It can be seen from the above equation that λ is approximately linearly related to the humidity RH, and the relative humidity can be obtained by measuring the λ of a specific wavelength of the loss spectrum, that is, RH=(λ-λ0)/a. The sensitivity a of the sensor and the sensor parameter P0 are calibrated by experiments.

参照图1和图2,综上所述,本发明检测湿度时,当不同湿度的空气与琼脂糖凝胶接薄膜触后,琼脂糖凝胶薄膜的折射率会发生改变,从而影响光纤中光的传输特性,通过测量干涉峰/谷的波长变化,即可获得周围环境相应的湿度,并且,光纤采用四锥结构积累相位差,增强光耦合时干涉的变化量,在保证测量的灵敏度时,无需大幅度拉长光纤锥腰部分的长度,其结构原理简单可靠,工艺步骤简便,操作制备容易,产品稳定性好,使用寿命长。Referring to Fig. 1 and Fig. 2, in summary, when the present invention detects humidity, when the air of different humidity contacts the agarose gel contact film, the refractive index of the agarose gel film will change, thereby affecting the light in the optical fiber. By measuring the wavelength change of the interference peak/valley, the corresponding humidity of the surrounding environment can be obtained, and the optical fiber adopts a four-cone structure to accumulate the phase difference to enhance the interference change during optical coupling. While ensuring the measurement sensitivity, There is no need to greatly lengthen the length of the optical fiber taper waist, the structure principle is simple and reliable, the process steps are simple, the operation and preparation are easy, the product stability is good, and the service life is long.

上述仅为本发明的具体实施方式,但本发明的设计构思并不局限于此,凡利用此构思对本发明进行非实质性的改动,均应属于侵犯本发明保护范围的行为。The above is only a specific embodiment of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial changes made to the present invention by using this concept should be an act of violating the protection scope of the present invention.

Claims (6)

1.一种波长调制型四锥光纤湿度传感器,其特征在于:包括光源、四锥光纤以及用于检测光的波长位置变化的探测器,所述四锥光纤两端分别与所述光源和探测器连接,所述四锥光纤的四锥结构上涂覆有湿敏材质的光学凝胶层。1. A wavelength-modulated four-cone optical fiber humidity sensor, characterized in that: comprise a light source, a four-cone optical fiber and a detector for detecting changes in the wavelength position of light, the two ends of the four-cone optical fiber are respectively connected to the light source and the detector The four-cone structure of the four-cone optical fiber is coated with an optical gel layer of moisture-sensitive material. 2.根据权利要求 1 所述的一种波长调制型四锥光纤湿度传感器,其特征在于:所述光源的波长范围是1900nm~2400nm。2. A wavelength-modulated four-cone fiber optic humidity sensor according to claim 1, characterized in that: the wavelength range of the light source is 1900nm-2400nm. 3.根据权利要求 1 所述的一种波长调制型四锥光纤湿度传感器,其特征在于:所述四锥光纤采用单模光纤,所述单模光纤上拉锥形成一段四锥结构,该段四锥结构纤芯涂覆所述光学凝胶层。3. A wavelength-modulated four-cone optical fiber humidity sensor according to claim 1, characterized in that: the four-cone optical fiber adopts a single-mode optical fiber, and the single-mode optical fiber is drawn up to form a four-cone structure. The four-cone structure core is coated with the optical gel layer. 4.根据权利要求 1 所述的一种波长调制型四锥光纤湿度传感器,其特征在于:所述四锥光纤四锥结构中两个锥腰均为50-70微米,两个锥腰之间的距离为10-30微米。4. A kind of wavelength modulation type four-cone optical fiber humidity sensor according to claim 1, characterized in that: in the four-cone optical fiber four-cone structure, two cone waists are 50-70 microns, and between the two cone waists The distance is 10-30 microns. 5.根据权利要求 1 所述的一种波长调制型四锥光纤湿度传感器,其特征在于:所述光学凝胶层为琼脂糖凝胶薄膜。5. A wavelength-modulated four-cone optical fiber humidity sensor according to claim 1, characterized in that: the optical gel layer is an agarose gel film. 6.根据权利要求 1 所述的一种波长调制型四锥光纤湿度传感器,其特征在于:所述探测器为光谱仪。6. A wavelength-modulated four-cone fiber optic humidity sensor according to claim 1, wherein the detector is a spectrometer.
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Application publication date: 20180814