CN109682995A - A kind of scattering formula low-temperature scanning near-field optical microscope - Google Patents

A kind of scattering formula low-temperature scanning near-field optical microscope Download PDF

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Publication number
CN109682995A
CN109682995A CN201910053045.8A CN201910053045A CN109682995A CN 109682995 A CN109682995 A CN 109682995A CN 201910053045 A CN201910053045 A CN 201910053045A CN 109682995 A CN109682995 A CN 109682995A
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platform
scanning
sample
probe
needle tip
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王文杰
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Yisheng Scientific Instruments (jiaxing) Co Ltd
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Yisheng Scientific Instruments (jiaxing) Co Ltd
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Priority to CN201910053045.8A priority Critical patent/CN109682995A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/18SNOM [Scanning Near-Field Optical Microscopy] or apparatus therefor, e.g. SNOM probes
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/18SNOM [Scanning Near-Field Optical Microscopy] or apparatus therefor, e.g. SNOM probes
    • G01Q60/22Probes, their manufacture, or their related instrumentation, e.g. holders

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Radiology & Medical Imaging (AREA)
  • Microscoopes, Condenser (AREA)

Abstract

本发明公开了一种散射式低温扫描近场光学显微镜,包括冷台、设置于冷台底部的样品扫描平台和探针扫描平台、抛物面镜平台以及底座,所述样品扫描平台包括扫描台,扫描台上设置有弹性夹片和样品架,样品架可插拔的夹于扫描台和弹性夹片之间以便于更换样品;所述探针扫描平台位于样品扫描平台相对一侧,包括连接于冷台底部的针尖耦合提取平台和针尖托,针尖托上固定有探针,针尖托以磁吸式连接于针尖耦合提取平台并且与扫描台相对以便于更换探针对样品进行扫描;所述抛物面镜平台设置于底座上以会聚外部激光于探针处并收集带有样品信息的散射光于外部探测器。本发明可以同时实现原位换探针和换样品,操作简单兼容性强。

The invention discloses a scattering type low-temperature scanning near-field optical microscope, comprising a cold stage, a sample scanning platform and a probe scanning platform arranged at the bottom of the cold platform, a parabolic mirror platform and a base. An elastic clip and a sample holder are arranged on the stage, and the sample holder is pluggably clamped between the scanning stage and the elastic clip to facilitate sample replacement; the probe scanning platform is located on the opposite side of the sample scanning platform, including a The needle tip is coupled to the extraction platform and the needle tip holder at the bottom of the table, a probe is fixed on the needle tip holder, and the needle tip holder is magnetically connected to the needle tip coupling extraction platform and is opposite to the scanning table so that the probe can be replaced to scan the sample; the parabolic mirror The platform is arranged on the base to focus external laser light on the probe and collect scattered light with sample information on the external detector. The present invention can realize in-situ probe replacement and sample replacement at the same time, with simple operation and strong compatibility.

Description

A kind of scattering formula low-temperature scanning near-field optical microscope
Technical field
The invention belongs near field optic Instrument technology fields, and in particular to a kind of scattering formula low temperature scanning near field optic is micro- Mirror.
Background technique
With being constantly progressive for modern micro-nano technology technology and scanning probe microscopy, near-field optical microscope is not yet There is the near-field optical microscope of various feedback forms and working method in disconnected development, these near-field optical microscope obtain closely For the resolution ratio of field optics image compared with being difficult to break through the diffraction limit of light, obtained resolution ratio is lower.In order to by resolution ratio into One step improves, scientists by the AFM probe of metallization, obtained in the way of scattering resolution ratio in~10nm or so or Better near field optic image, thus the research in the near field optic field pushed, meanwhile, the breakthrough of high vacuum and liquid helium region The near field imaging system of diffraction limit also has important application in fields such as physics, chemistry, material, biology, national defence, information.
But currently, the scattering formula that can obtain liquid helium region is infrared or far infrared near field imaging system only has a company It is making, product cannot achieve needle exchange in situ or vary product, and its scattering formula near field imaging system cannot be according to the actual situation Each platform is positioned, working environment and vacuum degree do not reach the requirement of ultrahigh vacuum yet, in research application and reality It is all very inconvenient in the operation of border, adverse effect is also generated to experimental data.
Therefore, it is necessary to propose expansible, compatible scattering under easy to operate, the extremely low mild ultra-high vacuum environment of one kind Formula low-temperature scanning near-field optical microscope.
Summary of the invention
The present invention is directed to the situation of the prior art, overcomes drawbacks described above, proposes a kind of scattering formula low temperature scanning near field optic Microscope.
The present invention use following technical scheme, a kind of scattering formula low-temperature scanning near-field optical microscope, including cold bench, Sample Scan platform, probe scanning platform, paraboloidal mirror platform and pedestal, in which:
The Sample Scan platform is set to cold bench bottom, and the Sample Scan platform includes scan table, the scan table On be provided with elastic clip and specimen holder, the specimen holder is pluggable to be sandwiched between scan table and elastic clip in order to replace Sample;
The probe scanning platform is set to cold bench bottom and is located at Sample Scan platform opposite side, the probe scanning Platform includes the needle point coupling extraction platform and needle point support for being connected to cold bench bottom, is fixed with probe in the needle point support, described Needle point support is connected to needle point coupling extraction platform and opposite with the scan table in order to replacing probe pair with magnetic-type Sample is scanned;
The paraboloidal mirror platform is set on pedestal, and the paraboloidal mirror platform is for assembling external laser at probe And the scattering light with sample message is collected in outer locator.
As a further improvement of the above technical scheme, the Sample Scan platform further includes having to be fixed on cold bench bottom First XYZ mobile mechanism, the scan table are connected to the first XYZ mobile mechanism and are driven and move in XYZ space.
As a further improvement of the above technical scheme, the probe scanning platform further includes be fixed on cold bench bottom Two XYZ mobile mechanisms, the needle point coupling extraction platform are connected to the 2nd XYZ mobile mechanism and are driven in XYZ space Interior movement is to adjust needle point support in the position of XYZ space.
As a further improvement of the above technical scheme, the paraboloidal mirror platform includes the 3rd XYZ mobile mechanism and throwing Object plane mirror, the 3rd XYZ mobile mechanism are fixed on pedestal, and the paraboloidal mirror is connected to the 3rd XYZ mobile mechanism And it is driven and is moved in XYZ space to assemble external laser at probe and collect the scattering light with sample message in outside Detector.
As a further improvement of the above technical scheme, the paraboloidal mirror preferred dimension is off-axis no more than 1 inch Paraboloidal mirror.
As a further improvement of the above technical scheme, the cold bench is fixed on external cryostat.
As a further improvement of the above technical scheme, shock-absorbing arms is also set up between the cold bench and pedestal.
A kind of scattering formula low-temperature scanning near-field optical microscope disclosed by the invention, the beneficial effect is that, in the present invention Needle point support is fixed in a manner of magnetic, it can be achieved that needle exchange in situ and being applicable to various types of probes, and specimen holder passes through elasticity Intermediate plate is fixed on scan table, while original position may be implemented and vary product, and compatibility easy to operate is strong;The configuration of the present invention is simple configuration is small Ingeniously, the intracavitary use of ultrahigh vacuum, strong applicability can be placed directly in;Using three XYZ mobile mechanisms to each flat in the present invention Platform carries out spatial position adjustment and paraboloidal mirror is using off axis paraboloidal mirror convergent laser and collection scattering light, can effectively mention Take near-field signals, signal-to-noise ratio with higher;Shock-absorbing arms is also set up between cold bench and pedestal, so that present invention work is in low vibration Environment, experimental result are reliable.
Detailed description of the invention
Fig. 1 is the general structure schematic diagram of the preferred embodiment of the present invention.
Fig. 2 is a visual angle schematic diagram of Sample Scan platform in the present invention.
Fig. 3 is the partial enlarged view of part A in Fig. 1.
Appended drawing reference includes: 1- cold bench, 2- Sample Scan platform, 22- scan table, the first XYZ mobile mechanism of 21-, 23- bullet Property intermediate plate, 24- specimen holder, 25- lug, 3- probe scanning platform, the 2nd XYZ mobile mechanism of 31-, the coupling of 32- needle point is extracted flat Platform, 33- needle point support, 34- magnet, 4- paraboloidal mirror platform, the 3rd XYZ mobile mechanism of 41-, 42- paraboloidal mirror, 5- pedestal, 51- Shock-absorbing arms.
Specific embodiment
The invention discloses a kind of scattering formula low-temperature scanning near-field optical microscopes, below with reference to preferred embodiment, to this The specific embodiment of invention is further described.
Specific structure of the invention is shown to Fig. 3, Fig. 1 to Fig. 3 referring to Figure 1 of the drawings.A kind of scattering formula low temperature Optical microscope for scanning near field, including cold 1, Sample Scan platform 2, probe scanning platform 3, paraboloidal mirror platform 4 and pedestal 5, in which:
The Sample Scan platform 2 is set to 1 bottom of cold bench, and the Sample Scan platform 2 includes scan table 22, described to sweep It retouches and is provided with elastic clip 23 and specimen holder 24 on platform 22, the specimen holder 24 is pluggable to be sandwiched in scan table 22 and elastic clip In order to replacing sample between 23;
The probe scanning platform 3 is set to 1 bottom of cold bench and is located at 2 opposite side of Sample Scan platform, the probe Scanning platform 3 includes the needle point coupling extraction platform 32 and needle point support 33 for being connected to 1 bottom of cold bench, is fixed in the needle point support 33 Have a probe, the needle point support 33 with it is magnetic-type be connected to the needle point coupling extraction platform 32 and with the scan table 22 it is opposite It is scanned in order to replace probe to sample;
The paraboloidal mirror platform 4 is set on pedestal 5, and the paraboloidal mirror platform 4 is for assembling external laser in spy At needle and the scattering light with sample message is collected in outer locator.
Cold bench 1 provides low temperature environment for near-field optical microscope in the present invention, can use various forms of refrigeration platforms, Versatile, scan table 22 provides placement platform for sample, elastic clip 23 and specimen holder 24 is provided on scan table 22, in reality Sample is to be affixed on specimen holder 24 in a manner of gluing, and specimen holder 24 is pluggable to be sandwiched in scan table 22 and bullet in the application of border Property intermediate plate 23 between, specimen holder 24 need to only be extracted to the insertion that more renew, further at this when needing replacing sample Specimen holder 24 is additionally provided with a lug 25 far from the side of elastic clip 23 in embodiment, which conveniently exchanges specimen holder for, Probe scanning platform 3 is used to obtain the optical imagery of sample, is wherein provided with magnet 34, needle point in needle point coupling extraction platform 32 Support 33 is pulled in needle point coupling extraction platform 32 in a manner of magnetic, and probe is mounted in needle point support 33, can be with this Needle point support 33 is easily removed to the replacement for carrying out probe, in practice, can according to need hyperphoric various probes (not only can be more It is changed to AFM probe and is also replaced by STM probe), paraboloidal mirror platform 4 can converge to external laser at probe to make probe It is effective extract near-field signals (laser include visible light, infrared and terahertz wave band light) and collect have sample message Light is scattered in outer locator.The replacement of progress sample and probe that the present invention can be convenient, compatibility easy to operate are strong.
Further, the Sample Scan platform 2 further includes having the first XYZ mobile mechanism 21 for being fixed on 1 bottom of cold bench, The scan table 22 is connected to the first XYZ mobile mechanism 21 and is driven and moves in XYZ space.
Further, the probe scanning platform 3 further includes the 2nd XYZ mobile mechanism 31 for being fixed on 1 bottom of cold bench, institute Needle point coupling extraction platform 32 is stated to be connected to the 2nd XYZ mobile mechanism 31 and be driven in XYZ space movement to adjust Needle point support 33 is in the position of XYZ space.
Further, the paraboloidal mirror platform 4 includes the 3rd XYZ mobile mechanism 41 and paraboloidal mirror 42, the third XYZ mobile mechanism 41 is fixed on pedestal 5, and the paraboloidal mirror 42 is connected in the 3rd XYZ mobile mechanism 41 and by band It moves and is moved in XYZ space to assemble external laser at probe and collect the scattering light with sample message in external detection Device.
Specifically, the first XYZ mobile mechanism 21, the 2nd XYZ mobile mechanism 31 and the 3rd XYZ mobile mechanism 41 adopt With the prior art known in those skilled in the art, the first XYZ mobile mechanism 21, the 2nd XYZ mobile mechanism 31 and the 3rd XYZ Mobile mechanism 41 itself is not inventive point of the invention, the first XYZ mobile mechanism 21,31 and of the 2nd XYZ mobile mechanism 3rd XYZ mobile mechanism 41 includes X to stepper motor, Y-direction stepping motor and Z-direction stepping motor, and the X is to stepper motor, Y It is respectively used to control the X-direction displacement, Y-direction displacement and Z-direction displacement of each platform to stepper motor and Z-direction stepping motor. In the present embodiment by three XYZ mobile mechanisms (21,31,41) respectively to Sample Scan platform 2, probe scanning platform 3 and The spatial position of paraboloidal mirror platform 4 is adjusted, so as to high-precision adjusting probe at a distance from sample, laser convergence Orientation, allow the invention to effectively extract near-field signals, signal-to-noise ratio with higher.
Further, 42 preferred dimension of paraboloidal mirror is the off axis paraboloidal mirror no more than 1 inch.
Further, the cold bench 1 is fixed on external cryostat, so that present invention may apply to each The cryostat of kind form, it is applied widely.
Further, shock-absorbing arms 51 is also set up between the cold bench 1 and pedestal 5.
Specifically, since each platform that will drive of each XYZ mobile mechanism carries out motion scan, in order to prevent each Vibration influence experimental result is generated during platform motion scan, and shock-absorbing arms 51 is provided between cold bench 1 and pedestal 5, so that The present invention works in low shake environment, and experimental result is true and reliable.
It is noted that the metal material part of scattering formula low-temperature scanning near-field optical microscope proposed by the invention Using oxygen-free copper or aluminium alloy (such as pedestal, shock-absorbing arms, Sample Scan platform) and surface polishing is passed through in its metal material part Or it is gold-plated, since oxygen-free copper and aluminium alloy are that (it is high that other thermal conductivitys also can be selected in the high metal of thermal conductivity in practical applications Metal), on metal material polishing or it is gold-plated, enhance thermal isolation effect of the invention, allow the invention to be subjected to height Temperature baking, is suitable for ultra-high vacuum environment.
For a person skilled in the art, technical solution documented by foregoing embodiments can still be repaired Change or equivalent replacement of some of the technical features, it is all within the spirits and principles of the present invention, made any to repair Change, equivalent replacement, improvement etc., should be included in protection scope of the present invention.

Claims (7)

1.一种散射式低温扫描近场光学显微镜,其特征在于,包括冷台、样品扫描平台、探针扫描平台、抛物面镜平台以及底座,其中:1. a scattering type cryogenic scanning near-field optical microscope, is characterized in that, comprises cold stage, sample scanning platform, probe scanning platform, parabolic mirror platform and base, wherein: 所述样品扫描平台设置于冷台底部,所述样品扫描平台包括扫描台,所述扫描台上设置有弹性夹片和样品架,所述样品架可插拔的夹于扫描台和弹性夹片之间以便于更换样品;The sample scanning platform is arranged at the bottom of the cold stage, and the sample scanning platform includes a scanning stage. The scanning stage is provided with an elastic clip and a sample holder, and the sample holder is pluggable and clipped between the scanning stage and the elastic clip. between to facilitate the replacement of samples; 所述探针扫描平台设置于冷台底部且位于样品扫描平台相对一侧,所述探针扫描平台包括连接于冷台底部的针尖耦合提取平台和针尖托,所述针尖托上固定有探针,所述针尖托以磁吸式连接于所述针尖耦合提取平台并且与所述扫描台相对以便于更换探针对样品进行扫描;The probe scanning platform is arranged at the bottom of the cold stage and is located on the opposite side of the sample scanning platform, and the probe scanning platform includes a needle tip coupling extraction platform and a needle tip support connected to the bottom of the cold stage, and a probe is fixed on the needle tip support , the needle tip holder is magnetically connected to the needle tip coupling extraction platform and is opposite to the scanning platform so as to facilitate the replacement of the probe to scan the sample; 所述抛物面镜平台设置于底座上,所述抛物面镜平台用于会聚外部激光于探针处并收集带有样品信息的散射光于外部探测器。The parabolic mirror platform is arranged on the base, and the parabolic mirror platform is used for condensing external laser light at the probe and collecting scattered light with sample information to the external detector. 2.根据权利要求1所述的一种散射式低温扫描近场光学显微镜,其特征在于,所述样品扫描平台还包括有固定于冷台底部的第一XYZ移动机构,所述扫描台连接于第一XYZ移动机构并被带动在XYZ空间内运动。2 . The scattering-type cryogenic scanning near-field optical microscope according to claim 1 , wherein the sample scanning platform further comprises a first XYZ moving mechanism fixed on the bottom of the cold stage, and the scanning stage is connected to 2 . The first XYZ moving mechanism is driven to move in the XYZ space. 3.根据权利要求1所述的一种散射式低温扫描近场光学显微镜,其特征在于,所述探针扫描平台还包括固定于冷台底部的第二XYZ移动机构,所述针尖耦合提取平台连接于所述第二XYZ移动机构并被带动在XYZ空间内运动以调整针尖托在XYZ空间的位置。3 . The scattering type cryogenic scanning near-field optical microscope according to claim 1 , wherein the probe scanning platform further comprises a second XYZ moving mechanism fixed on the bottom of the cold stage, and the needle tip is coupled to the extraction platform 3 . It is connected to the second XYZ moving mechanism and is driven to move in the XYZ space to adjust the position of the needle tip holder in the XYZ space. 4.根据权利要求1所述的一种散射式低温扫描近场光学显微镜,其特征在于,所述抛物面镜平台包括第三XYZ移动机构和抛物面镜,所述第三XYZ移动机构固定于底座上,所述抛物面镜连接于于所述第三XYZ移动机构并被带动在XYZ空间内运动以会聚外部激光于探针处并收集带有样品信息的散射光于外部探测器。4 . The scattering type cryogenic scanning near-field optical microscope according to claim 1 , wherein the parabolic mirror platform comprises a third XYZ moving mechanism and a parabolic mirror, and the third XYZ moving mechanism is fixed on the base. 5 . , the parabolic mirror is connected to the third XYZ moving mechanism and is driven to move in the XYZ space to condense external laser light at the probe and collect scattered light with sample information to the external detector. 5.根据权利要求4所述的一种散射式低温扫描近场光学显微镜,其特征在于,所述抛物面镜选用尺寸为不大于1英寸的离轴抛物面镜。5 . The scattering type cryogenic scanning near-field optical microscope according to claim 4 , wherein the parabolic mirror is an off-axis parabolic mirror with a size of not more than 1 inch. 6 . 6.根据权利要求1所述的一种散射式低温扫描近场光学显微镜,其特征在于,所述冷台固定于外部的低温恒温器上。6 . The scattering low-temperature scanning near-field optical microscope according to claim 1 , wherein the cold stage is fixed on an external cryostat. 7 . 7.根据权利要求1或6任一权利要求所述的一种散射式低温扫描近场光学显微镜,其特征在于,所述冷台与底座之间还设置减震臂。7 . The scattering low-temperature scanning near-field optical microscope according to claim 1 , wherein a shock absorbing arm is further arranged between the cold stage and the base. 8 .
CN201910053045.8A 2019-01-21 2019-01-21 A kind of scattering formula low-temperature scanning near-field optical microscope Pending CN109682995A (en)

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CN112665966A (en) * 2020-12-15 2021-04-16 Oppo(重庆)智能科技有限公司 Precision controller
CN113884706A (en) * 2020-07-02 2022-01-04 中国科学院苏州纳米技术与纳米仿生研究所 Vacuum interconnection system and transfer vacuum sample support
CN114018921A (en) * 2021-11-02 2022-02-08 仪晟科学仪器(嘉兴)有限公司 A near-field optical microscope based on a probe optical positioning system

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Publication number Priority date Publication date Assignee Title
CN113884706A (en) * 2020-07-02 2022-01-04 中国科学院苏州纳米技术与纳米仿生研究所 Vacuum interconnection system and transfer vacuum sample support
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CN114018921A (en) * 2021-11-02 2022-02-08 仪晟科学仪器(嘉兴)有限公司 A near-field optical microscope based on a probe optical positioning system

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