CN109727693B - Connector for I-131 absorption bottle - Google Patents
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- CN109727693B CN109727693B CN201910014083.2A CN201910014083A CN109727693B CN 109727693 B CN109727693 B CN 109727693B CN 201910014083 A CN201910014083 A CN 201910014083A CN 109727693 B CN109727693 B CN 109727693B
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Abstract
Description
技术领域technical field
本发明属于放射性同位素制备技术领域,具体涉及一种用于I-131吸收瓶的连接器。The invention belongs to the technical field of radioisotope preparation, and in particular relates to a connector for an I-131 absorption bottle.
背景技术Background technique
放射性碘-131是生产Na131I胶囊等放射性药品重要原料,主要通过高温(约750℃)干馏反应堆辐照后的TeO2并用稀碱液吸收馏出的碘蒸气制得。中国工程物理研究院核物理与化学研究所,及国内的中国原子能科学研究院和中国核动力研究院,均曾采用卧式装置进行商业化放射性碘-131生产。现有的碘-131生产装置的气路系统一般包括依次连接的蒸馏管、吸收瓶、碱洗涤瓶、活性炭吸附柱和真空泵,由于蒸馏管、吸收瓶、碱洗涤瓶多为玻璃材质制作,这些部件之间的连接只能采用塑料或橡胶管道;而且,在吸收瓶上最基本的设置有碘蒸气(载气)进口、稀碱液加注口、含碘-131吸收液(即产品溶液)取出口、尾气排出口,在具有水冷却功能的吸收瓶上还设置有进、出水等接口,这些输送气体、液体的管道必需由工作人员手动连接。由于连接各部件所用的塑料管或乳胶管在载气的高温和载气中放射性碘-131的高强度γ射线长时间作用下容易老化开裂,往往导致载气流速不稳定和碘蒸气泄漏污染环境并影响碘-131收率,而且对沾有放射性碘-131的老化塑料管或乳胶管的更换比较麻烦和危险,往往需要工作人员对生产现场严格去污后进入热室处理,维护维修人员会受到较多辐照剂量,特别是在需要解决生产过程中出现管道破裂等突发情况时。尽管已有碘-131生产单位将蒸馏管与吸收瓶做成一体,消除了载气的高温对蒸馏管与吸收瓶之间连接管道损害的安全隐患,但热室内的强电离辐射对其它塑料管或乳胶管损伤的安全隐患并未消减。Radioactive iodine - 131 is an important raw material for the production of radioactive drugs such as Na 131 I capsules. The Institute of Nuclear Physics and Chemistry of the Chinese Academy of Engineering Physics, as well as the China Institute of Atomic Energy and the China Institute of Nuclear Power in China have all used horizontal devices for commercial production of radioactive iodine-131. The gas circuit system of the existing iodine-131 production device generally includes a distillation tube, an absorption bottle, an alkali washing bottle, an activated carbon adsorption column and a vacuum pump, which are connected in sequence. The connection between components can only be made of plastic or rubber pipes; moreover, the most basic configuration on the absorption bottle is the inlet of iodine vapor (carrier gas), the filling port of dilute lye, and the absorption liquid containing iodine-131 (ie, the product solution) The intake port and the exhaust gas discharge port are also provided with inlet and outlet ports on the absorption bottle with water cooling function. These pipes for transporting gas and liquid must be manually connected by the staff. Due to the high temperature of the carrier gas and the high-intensity γ-ray of radioactive iodine-131 in the carrier gas, the plastic tubes or latex tubes used to connect the components are prone to aging and cracking for a long time, which often leads to unstable carrier gas flow rate and iodine vapor leakage to pollute the environment. And affect the yield of iodine-131, and the replacement of aging plastic tubes or latex tubes stained with radioactive iodine-131 is troublesome and dangerous, often requiring staff to strictly decontaminate the production site and then enter the hot room for treatment, and maintenance personnel will Exposure to high doses of radiation, especially when it is necessary to solve emergencies such as pipe ruptures during the production process. Although some iodine-131 production units have integrated the distillation tube and the absorption bottle, which eliminates the potential safety hazard that the high temperature of the carrier gas will damage the connecting pipeline between the distillation tube and the absorption bottle, the strong ionizing radiation in the hot chamber can cause damage to other plastic tubes. Or the safety hazard of latex tube damage has not been reduced.
发明内容SUMMARY OF THE INVENTION
为了提高放射性碘-131生产的安全性和可靠性,本发明提供一种用于I-131吸收瓶的连接器。In order to improve the safety and reliability of radioactive iodine-131 production, the present invention provides a connector for an I-131 absorption bottle.
本发明的连接器能够通过操作热室机械手对放射性碘-131生产装置中各部件之间连接管道实施远程、快速、安全地安装或更换,采用金属管连接更有利于提高生产装置的可靠性并降低安全风险。The connector of the invention can remotely, quickly and safely install or replace the connecting pipes between the various components in the radioactive iodine-131 production device by operating the hot cell manipulator, and the use of metal pipe connection is more conducive to improving the reliability of the production device and improving the reliability of the production device. Reduce security risks.
实现本发明的技术方案如下:The technical scheme that realizes the present invention is as follows:
本发明的一种用于I-131吸收瓶的连接器,其特点是,所述的连接器包括牵引器部分、插接器部分、套箍、滑轨和支架。上述连接器的连接关系是,所述的套箍、牵引器部分沿X轴向依次设置,牵引器部分、插接器部分、滑轨、支架自上而下依次设置,牵引器部分的一端放置在套箍内并与套箍滑动连接,插接器部分与滑轨滑动连接,滑轨与支架固定连接。A connector for an I-131 absorption bottle of the present invention is characterized in that the connector includes a retractor part, a plug connector part, a ferrule, a slide rail and a bracket. The connection relationship of the above-mentioned connector is that the ferrule and the tractor part are arranged in turn along the X axis, the tractor part, the connector part, the slide rail and the bracket are arranged in order from top to bottom, and one end of the tractor part is placed. Inside the ferrule and slidably connected with the ferrule, the connector part is slidably connected with the slide rail, and the slide rail is fixedly connected with the bracket.
所述的套箍为两端结构对称的金属片构件,套箍的两端由螺钉固定连接形成一个圆环和一个上方敞口的方盒,在方盒X轴向壁中央向上有竖直的开口。所述的牵引器部分包含丝杆、三角块、半球体和手柄,插接器部分包含滑座、托架Ⅰ、托架Ⅱ、挡板。The ferrule is a metal sheet member with symmetrical structure at both ends, and the two ends of the ferrule are fixedly connected by screws to form a ring and a square box with an upper opening, and there is a vertical upward in the center of the X-axis wall of the square box. Open your mouth. The retractor part includes a screw rod, a triangular block, a hemisphere and a handle, and the connector part includes a sliding seat, a bracket I, a bracket II, and a baffle.
所述的插接器部分中的托架Ⅰ、托架Ⅱ、挡板均设置有开口向上的插槽、卡槽,滑座放置在滑轨上并与滑轨滑动连接,托架Ⅰ、托架Ⅱ、挡板固定设置在滑座上,托架Ⅰ与托架Ⅱ位于滑座Y轴线的一侧并以滑座X轴线对称设置,挡板位于滑座Y轴线的另一侧并设置于滑座X轴线上,沿X轴向在托架Ⅰ上安装有插接头Ⅰ、在托架Ⅱ上安装有插接头Ⅱ、在挡板上安装有牵引器部分中的丝杆、三角块。The brackets I, brackets II and baffles in the connector part are all provided with slots and card slots with upward openings. The frame II and the baffle are fixed on the sliding seat, the bracket I and the bracket II are located on one side of the Y axis of the sliding seat and are arranged symmetrically with the X axis of the sliding seat, and the baffle is located on the other side of the Y axis of the sliding seat and is arranged on the side of the sliding seat. On the X axis of the sliding seat, along the X axis, a plug connector I is installed on the bracket I, a plug connector II is installed on the bracket II, and the lead screw and triangle block in the retractor part are installed on the baffle plate.
所述的插接头Ⅰ包含X轴向水平设置的锥头棒Ⅰ、钢管Ⅰ及竖直设置的插片Ⅰ,插接头Ⅱ包含X轴向水平设置的L形空心的锥头棒Ⅱ、钢管Ⅱ、Y轴向水平设置的波纹管及竖直设置的插片Ⅱ。所述的锥头棒Ⅰ放置在托架Ⅰ的卡槽中,插片Ⅰ向下插在托架Ⅰ的插槽中,锥头棒Ⅰ垂直穿过插片Ⅰ中央并与插片Ⅰ固定连接,钢管Ⅰ穿过锥头棒Ⅰ并与锥头棒Ⅰ密封固定连接。所述的锥头棒Ⅱ放置在托架Ⅱ的卡槽中,插片Ⅱ向下插在托架Ⅱ的插槽中,锥头棒Ⅱ垂直穿过插片Ⅱ中央并与插片Ⅱ固定连接,钢管Ⅱ穿过锥头棒Ⅱ并与锥头棒Ⅱ密封固定连接,波纹管与锥头棒Ⅱ固定连通;所述的锥头棒Ⅰ、锥头棒Ⅱ的锥头部各设置有两个环形的凹槽,在凹槽内配合设置有密封圈。The plug joint I includes a taper rod I, a steel pipe I and a vertical insert I arranged horizontally in the X axis, and the plug joint II includes an L-shaped hollow taper rod II and a steel pipe II arranged horizontally in the X axis. , Y-axis horizontally arranged bellows and vertically arranged inserts II. The tapered rod I is placed in the slot of the bracket I, the insert piece I is inserted downward into the slot of the bracket I, and the tapered head rod I vertically passes through the center of the insert piece I and is fixedly connected with the insert piece I. , the steel pipe I passes through the cone head rod I and is sealed and fixed with the cone head rod I. The taper-head rod II is placed in the slot of the bracket II, the insert piece II is inserted downward into the slot of the bracket II, and the taper-head rod II vertically passes through the center of the insert piece II and is fixedly connected with the insert piece II. , the steel pipe II passes through the cone head rod II and is sealed and fixedly connected with the cone head rod II, and the bellows is fixedly connected with the cone head rod II; the cone head rod I and the cone head rod II are each provided with two cone heads. The annular groove is fitted with a sealing ring in the groove.
所述的牵引器部分中的半球体、手柄分别固定设置在水平设置的丝杆的两端,三角块竖直设置在丝杆的中部,在三角块的中央设置有一螺纹孔,丝杆穿过螺纹孔并与三角块滑动连接。所述的丝杆与滑轨平行设置,丝杆放置在挡板的卡槽中,三角块向下插在挡板的插槽中,半球体放置在套箍的方盒内并与方盒内壁滑动连接。所述的滑轨为双辐滑轨,由两条平行的轨道构成。The hemisphere and the handle in the retractor part are respectively fixed on both ends of the horizontally arranged screw rod, the triangular block is vertically arranged in the middle of the screw rod, and a threaded hole is arranged in the center of the triangular block, and the screw rod passes through it. Threaded hole and sliding connection with triangle block. The screw rod is arranged in parallel with the slide rail, the screw rod is placed in the slot of the baffle, the triangular block is inserted downward in the slot of the baffle, and the hemisphere is placed in the square box of the hoop and is connected to the inner wall of the square box. Slide to connect. The sliding rail is a double-spoke sliding rail composed of two parallel rails.
所述的套箍固定连接在外接的吸收瓶上,在吸收瓶上配合设置有与锥头棒Ⅰ、锥头棒Ⅱ对应的管道。The ferrule is fixedly connected to the external absorption bottle, and the absorption bottle is matched with pipes corresponding to the cone-head rod I and the cone-head rod II.
所述的套箍、丝杆、滑座和滑轨的X轴心线设置在同一立面上。所述的钢管Ⅰ与锥头棒Ⅰ的X轴心线、钢管Ⅱ与锥头棒Ⅱ的X轴心线分别重合设置。The X-axis lines of the ferrule, the screw rod, the sliding seat and the sliding rail are arranged on the same elevation. The X-axis centers of the steel pipe I and the taper rod I, and the X-axis centers of the steel pipe II and the taper rod II are respectively overlapped and arranged.
所述的套箍、牵引器部分、滑轨、支架、钢管Ⅰ和钢管Ⅱ采用不锈钢制作。所述的插接器部分中的滑座、托架Ⅰ、托架Ⅱ、挡板、锥头棒Ⅰ、锥头棒Ⅱ、插片Ⅰ和插片Ⅱ采用聚乙烯制作。所述的密封圈采用硅橡胶制作。The ferrule, the part of the tractor, the slide rail, the bracket, the steel pipe I and the steel pipe II are made of stainless steel. The sliding seat, bracket I, bracket II, baffle plate, taper rod I, taper rod II, insert piece I and insert piece II in the connector part are made of polyethylene. The sealing ring is made of silicone rubber.
本发明的一种用于I-131吸收瓶的连接器的简要工作原理是:操作机械手将插接头Ⅰ、插接头Ⅱ分别安装在托架上,旋转手柄通过丝杆传动驱使插接器部分向套箍方向移动,将插接头Ⅰ、插接头Ⅱ分别插入外接吸收瓶上对应的管道中插紧,实现吸收瓶与其它部件金属连接管道的过渡连接。The brief working principle of the connector for the I-131 absorbing bottle of the present invention is as follows: the manipulator is operated to install the plug connector I and the plug connector II on the bracket respectively, and the rotating handle drives the connector part to the bracket through the screw drive. The ferrule is moved in the direction, and the plug connector I and the plug connector II are respectively inserted into the corresponding pipes on the external absorption bottle and inserted tightly, so as to realize the transition connection between the absorption bottle and the metal connecting pipes of other components.
本发明的有益效果是,采用耐辐照性能更好的金属管道替换现用的塑料或橡胶管道以延长Na131I生产装置的工作寿命,并通过采用适用于热室内放射性碘-131生产环境的专用连接器实现生产装置相关部件之间连接管道的远程更换,显著降低维护维修人员的安全风险。本发明的连接器的结构紧凑、小巧,易于操作,安全性和可靠性好。The beneficial effect of the present invention is that the existing plastic or rubber pipes are replaced by metal pipes with better radiation resistance to prolong the working life of the Na 131 I production device, and by adopting the metal pipes suitable for the production environment of radioactive iodine-131 in the hot room Dedicated connectors enable remote replacement of connecting pipes between related components of the production plant, significantly reducing safety risks for maintenance personnel. The connector of the invention has a compact and small structure, is easy to operate, and has good safety and reliability.
附图说明Description of drawings
图1是本发明的一种用于I-131吸收瓶的连接器的结构示意图;Fig. 1 is the structural representation of a kind of connector used for I-131 absorption bottle of the present invention;
图2是本发明的一种用于I-131吸收瓶的连接器的俯视示意图;2 is a schematic top view of a connector for an I-131 absorption bottle of the present invention;
图3是本发明中的锥头棒Ⅰ的剖视图;Fig. 3 is the sectional view of the taper rod I in the present invention;
图4是本发明中的锥头棒Ⅱ的剖视图;Fig. 4 is the sectional view of the taper rod II in the present invention;
图中 1.套箍 2.滑轨 3.支架 4.丝杆 5.三角块 6.半球体 7.手柄 8.滑座 9.托架Ⅰ 10.托架Ⅱ 11.挡板 12.锥头棒Ⅰ 13.钢管Ⅰ 14.插片Ⅰ 15.密封圈 16.锥头棒Ⅱ 17.钢管Ⅱ 18.波纹管 19.插片Ⅱ。In the figure 1.
具体实施方式Detailed ways
下面结合附图和实施例对本发明进一步说明。The present invention will be further described below in conjunction with the accompanying drawings and embodiments.
实施例1Example 1
图1是本发明的一种用于I-131吸收瓶的连接器的结构示意图,图2是本发明的一种用于I-131吸收瓶的连接器的俯视示意图,图3是本发明中的锥头棒Ⅰ的剖视图,图,4是本发明中的锥头棒Ⅱ的剖视图。在图1~图4中,本发明的一种用于I-131吸收瓶的连接器,包括牵引器部分、插接器部分、套箍1、滑轨2和支架3。上述连接器的连接关系是,所述的套箍1、牵引器部分沿X轴向依次设置,牵引器部分、插接器部分、滑轨2、支架3自上而下依次设置,牵引器部分的一端放置在套箍1内并与套箍1滑动连接,插接器部分与滑轨2滑动连接,滑轨2与支架3固定连接。所述的套箍1为两端结构对称的金属片构件,套箍1的两端由螺钉固定连接形成一个圆环和一个上方敞口的方盒,在方盒X轴向壁中央向上有竖直的开口,用于放置丝杆4。所述的牵引器部分包含丝杆4、三角块5、半球体6和手柄7,插接器部分包含滑座8、托架Ⅰ9、托架Ⅱ10和挡板11。Fig. 1 is a schematic view of the structure of a connector used for an I-131 absorbing bottle of the present invention, Fig. 2 is a schematic top view of a connector used for an I-131 absorbing bottle of the present invention, and Fig. 3 is a schematic diagram of the present invention. The sectional view of the taper rod I, Figure 4 is the sectional view of the taper rod II in the present invention. In FIGS. 1 to 4 , a connector for an I-131 absorption bottle of the present invention includes a retractor part, a connector part, a
所述的插接器部分中的托架Ⅰ9、托架Ⅱ10、挡板11均设置有开口向上的插槽、卡槽,滑座8放置在滑轨2上并与滑轨2滑动连接,托架Ⅰ9、托架Ⅱ10、挡板11固定设置在滑座8上,托架Ⅰ9与托架Ⅱ10位于滑座8Y轴线的一侧并以滑座8X轴线对称设置,挡板11位于滑座8Y轴线的另一侧并设置于滑座8X轴线上,沿X轴向在托架Ⅰ9上安装有插接头Ⅰ、在托架Ⅱ10上安装有插接头Ⅱ、在挡板11上安装有牵引器部分中的丝杆4、三角块5。The bracket I9, bracket II10, and baffle
所述的插接头Ⅰ包含X轴向水平设置的锥头棒Ⅰ12、钢管Ⅰ13及竖直设置的插片Ⅰ14,插接头Ⅱ包含X轴向水平设置的L形空心的锥头棒Ⅱ16、钢管Ⅱ17、Y轴向水平设置的波纹管18及竖直设置的插片Ⅱ19。所述的锥头棒Ⅰ12放置在托架Ⅰ9的卡槽中,插片Ⅰ14向下插在托架Ⅰ9的插槽中,锥头棒Ⅰ12垂直穿过插片Ⅰ14中央并与插片Ⅰ14固定连接,钢管Ⅰ13穿过锥头棒Ⅰ12并与锥头棒Ⅰ12密封固定连接。所述的锥头棒Ⅱ16放置在托架Ⅱ10的卡槽中,插片Ⅱ19向下插在托架Ⅱ10的插槽中,锥头棒Ⅱ16垂直穿过插片Ⅱ19中央并与插片Ⅱ19固定连接,钢管Ⅱ17穿过锥头棒Ⅱ16并与锥头棒Ⅱ16密封固定连接,波纹管18与锥头棒Ⅱ16固定连通。所述的锥头棒Ⅰ12、锥头棒Ⅱ16的锥头部各设置有两个环形的凹槽,在凹槽内配合设置有密封圈15。The plug connector I includes a taper rod I12 horizontally arranged in the X axis, a steel pipe I13 and a vertical insert I14, and the plug connector II includes an L-shaped hollow taper rod II16, a steel pipe II17, which are horizontally arranged in the X axis. , The bellows 18 arranged horizontally in the Y axis and the insert II 19 arranged vertically. The tapered rod I12 is placed in the slot of the bracket I9, the insert I14 is inserted downward into the slot of the bracket I9, and the tapered rod I12 vertically passes through the center of the insert I14 and is fixedly connected with the insert I14. , the steel pipe I13 passes through the taper rod I12 and is sealed and fixedly connected with the taper rod I12. The tapered rod II16 is placed in the slot of the bracket II10, the insert II19 is inserted downward into the slot of the bracket II10, and the tapered rod II16 vertically passes through the center of the insert II19 and is fixedly connected with the insert II19. , the steel pipe II17 passes through the cone head rod II16 and is sealed and fixedly connected with the cone head rod II16, and the
所述的牵引器部分中的半球体6、手柄7分别固定设置在水平设置的丝杆4的两端,三角块5竖直设置在丝杆4的中部,在三角块5的中央设置有一螺纹孔,丝杆4穿过螺纹孔并与三角块5滑动连接;所述的丝杆4与滑轨2平行设置,丝杆4放置在挡板11的卡槽中,三角块5向下插在挡板11的插槽中,半球体6放置在套箍1的方盒内并与方盒内壁滑动连接。所述的滑轨2为双辐滑轨,由两条平行的轨道构成。The
所述的套箍1固定连接在外接的吸收瓶上,在吸收瓶上配合设置有与锥头棒Ⅰ12、锥头棒Ⅱ16对应的管道。所述的套箍1、丝杆4、滑座8和滑轨2的X轴心线设置在同一立面上。所述的钢管Ⅰ13与锥头棒Ⅰ12的X轴心线、钢管Ⅱ17与锥头棒Ⅱ16的X轴心线分别重合设置。所述的套箍1、牵引器部分、滑轨2、支架3、钢管Ⅰ13和钢管Ⅱ17采用不锈钢制作。所述的插接器部分中的滑座8、托架Ⅰ9、托架Ⅱ10、挡板11、锥头棒Ⅰ12、锥头棒Ⅱ16、插片Ⅰ14和插片Ⅱ19采用聚乙烯制作。所述的密封圈15采用硅橡胶制作。如图1~图4所示。The
所述的套箍1的圆环和方盒由对称结构的不锈钢薄片折叠而成,方盒壁上开口的宽度与牵引器部分中的丝杆4、半球体6的直径配合设置。所述的钢管Ⅰ13穿出锥头棒Ⅰ12锥头的部分较短,有利于减少锥头与外接吸收瓶排液口的间距所造成液体在接头处的残留量,而钢管Ⅱ17穿出锥头棒Ⅱ16锥头的部分较长,有利于通过钢管Ⅱ17输送的吸收液全部注入外接吸收瓶而不被抽吸入波纹管造成损失。所述的插片Ⅰ14、插片Ⅱ19、三角块5分别对应与托架Ⅰ9、托架Ⅱ10、挡板11上的卡槽非紧密配合设置,保持插片Ⅰ14、插片Ⅱ19有一定移动空间,有利于避免锥头棒插接时吸收瓶玻璃管道的损坏,保持三角块5在卡槽内有较大X轴向位移空间有利于牵引器部分的装卸。The circular ring and the square box of the
本实施例中,所述的锥头棒Ⅰ12、锥头棒Ⅱ16中的每一个凹槽内均配合设置有一个密封圈,密封圈15是其中的一个。In this embodiment, a sealing ring is fitted in each groove of the cone-head rod I12 and the cone-head rod II16, and the sealing
本发明的工作流程如下,操作机械手将插接头Ⅰ、插接头Ⅱ分别安装在托架Ⅰ、托架Ⅱ的卡槽内,再将牵引器部分水平放置在套箍1的方盒内和挡板11的卡槽内,并将三角块5插在挡板11的插槽内,旋转手柄7通过丝杆4传动驱使插接器部分向套箍1方向移动,将锥棒头Ⅰ12、锥棒头Ⅱ16分别插入外接吸收瓶上对应的管道中插紧,实现吸收瓶与其它部件金属连接管道的过渡连接,并在外接真空泵等设备的支持下实现通过波纹管18、钢管Ⅰ13、钢管Ⅱ17分别从吸收瓶抽气、抽出含碘-131溶液和向吸收瓶加注吸收液。反向旋转手柄7,可将锥棒头Ⅰ12、锥棒头Ⅱ16分别从外接吸收瓶上对应的管道中退出,利用机械手将取下的插接器部分通过检修门转移出热室进行维护维修,实现热室内强电离辐射环境下放射性碘-131生产装置连接管道的远程、快速、安全装卸。The working process of the present invention is as follows: operate the manipulator to install the plug connector I and the plug connector II in the slots of the bracket I and bracket II respectively, and then place the retractor part horizontally in the square box of the
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