CN110200311A - It is a kind of for the oolong tea of electronic cigarette and the composition of lemon and its application - Google Patents
It is a kind of for the oolong tea of electronic cigarette and the composition of lemon and its application Download PDFInfo
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- CN110200311A CN110200311A CN201910216284.0A CN201910216284A CN110200311A CN 110200311 A CN110200311 A CN 110200311A CN 201910216284 A CN201910216284 A CN 201910216284A CN 110200311 A CN110200311 A CN 110200311A
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- lemon
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- tea
- oolong tea
- cigarette
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- 235000005979 Citrus limon Nutrition 0.000 title claims abstract description 47
- 244000131522 Citrus pyriformis Species 0.000 title claims abstract description 47
- 235000006468 Thea sinensis Nutrition 0.000 title claims abstract description 44
- 235000020333 oolong tea Nutrition 0.000 title claims abstract description 44
- 239000000203 mixture Substances 0.000 title claims abstract description 41
- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 20
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 32
- 235000013616 tea Nutrition 0.000 claims abstract description 31
- 238000002360 preparation method Methods 0.000 claims abstract description 19
- 235000013361 beverage Nutrition 0.000 claims abstract description 4
- 241001122767 Theaceae Species 0.000 claims description 24
- 238000000605 extraction Methods 0.000 claims description 16
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 14
- 238000001694 spray drying Methods 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000007654 immersion Methods 0.000 claims description 8
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 7
- 239000001569 carbon dioxide Substances 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 claims description 5
- 239000013558 reference substance Substances 0.000 abstract description 9
- 238000012360 testing method Methods 0.000 abstract description 5
- 238000013329 compounding Methods 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000007812 deficiency Effects 0.000 abstract description 2
- 244000269722 Thea sinensis Species 0.000 abstract 3
- 230000000391 smoking effect Effects 0.000 description 19
- 241000208125 Nicotiana Species 0.000 description 14
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 14
- 239000000126 substance Substances 0.000 description 14
- 239000000047 product Substances 0.000 description 12
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 9
- 229960002715 nicotine Drugs 0.000 description 9
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- 239000001301 oxygen Substances 0.000 description 7
- 150000008442 polyphenolic compounds Chemical class 0.000 description 7
- 235000013824 polyphenols Nutrition 0.000 description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 229910002091 carbon monoxide Inorganic materials 0.000 description 6
- 206010028980 Neoplasm Diseases 0.000 description 5
- 230000000711 cancerogenic effect Effects 0.000 description 5
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- STNJBCKSHOAVAJ-UHFFFAOYSA-N Methacrolein Chemical compound CC(=C)C=O STNJBCKSHOAVAJ-UHFFFAOYSA-N 0.000 description 4
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
- 210000004556 brain Anatomy 0.000 description 4
- 201000011510 cancer Diseases 0.000 description 4
- 230000006378 damage Effects 0.000 description 4
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 108010054147 Hemoglobins Proteins 0.000 description 3
- 102000001554 Hemoglobins Human genes 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
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- 239000003183 carcinogenic agent Substances 0.000 description 3
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- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
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- 239000004615 ingredient Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 108010064719 Oxyhemoglobins Proteins 0.000 description 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 231100000315 carcinogenic Toxicity 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
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- 229910052757 nitrogen Inorganic materials 0.000 description 2
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- 239000004909 Moisturizer Substances 0.000 description 1
- HZEBHPIOVYHPMT-OUBTZVSYSA-N Polonium-210 Chemical compound [210Po] HZEBHPIOVYHPMT-OUBTZVSYSA-N 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
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- 240000003768 Solanum lycopersicum Species 0.000 description 1
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- 230000002503 metabolic effect Effects 0.000 description 1
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- 231100001143 noxa Toxicity 0.000 description 1
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- 208000005368 osteomalacia Diseases 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
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- 235000019505 tobacco product Nutrition 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/18—Extraction of water soluble tea constituents
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Tea And Coffee (AREA)
Abstract
It is the present invention relates to tealeaves spin-off field, in particular to a kind of for the oolong tea of electronic cigarette and the composition of lemon and its application.The raw material of the composition includes oolong tea and lemon.The present invention also provides a kind of preparation method of above-mentioned composition, the product obtained the present invention also provides a kind of above-mentioned composition or above-mentioned preparation method is in cigarette, electronic cigarette or the application for brewing beverage field.In technical solution provided by the invention, by the compounding of oolong tea and lemon, the faint scent of lemon burning can effectively integrate the bitter mouthfeel of tealeaves burning；Further, it smokes panel test through panelist, compared with commercially available tea cigarette, after electronic cigarette is made in composition of the invention, each item rating is superior to reference substance.It is provided by the invention it is a kind of contain tea composition, preparation method and applications, solve in the prior art, tea mouth taste is single, distasteful technological deficiency.
Description
Technical field
It is the present invention relates to tealeaves spin-off field, in particular to a kind of for the oolong tea of electronic cigarette and the composition of lemon
And its application.
Background technique
Due to containing the particular matters such as nicotine in tobacco, the people of long-term smoking can generate anaclisis to cigarette, we
It is usually to have dependent form smoker the person of smoking addiction.Smoking can lead to laryngocarcinoma.Patients with laryngeal carcinoma is in the majority with male.
Tobacco contains benzene and tar, radioactive substance also carcinogenic there are many energy.Some researches show that 90% patients with lung cancer
It is as caused by smoking.The past bladder carcinoma in males case at least 60% being proved in western countries of studying is that smoking is drawn
It rises, there are also carcinoma of mouth and laryngocarcinoma etc..Past tobacco product because made one containing mould cancer danger it is bigger.Smoking can cause
Lung, angiocarpy, the disease of intestines and stomach and various tumours and exacerbation diabetes, cause the common disease such as senile dementia.Smoking
Man's infertility chance is six times higher than non-smoker, and smoking can not only reduce sperm quantity, moreover it is possible to lead to cacospermia and impotence.It inhales
Cigarette promotes blood moderate stimulation element is horizontal to reduce, and can damage to the vital blood vessel of skin elasticity and connective tissue is kept, stand erect skin
Become dry relaxation, to cause apparent " smoking face ", destroys youth beautiful beauty.There is the machine of wrinkle in smoking women
Rate is 3 times of non-smoker.A possibility that smoking compared with the women of non-smoking, suffering from infertility wants 2.7 times high.Mother of smoking
The health that not only will affect oneself body can also bring disaster to the next generation, and such as neonatal constitution is poor, weight is light, the death rate is high；Baby
A possibility that suffering from congenital heart disease, is 2 times bigger than ordinary person.Smoking is also possible to make gastric ulcer to deteriorate disease and subtract to suffer from wound healing.Women inhales
Cigarette also results in amenorrhoea and increases the danger for suffering from osteomalacia.Research shows that the smoker of half is middle age or senescence phase to die of and cause
Disease.
The health of harmfulness of smoking people is known together by numerous people, and for teenager, harmfulness is just bigger.According to physician
Studies have shown that teenager is in growth and development period, each physiological system, organ are all not yet mature, have to external environment
The resistance of noxa element is more adult to be weak, is easy to absorb the normal growth of poisonous substance damage body.Smoking damage brain, make intelligence by
To influence.In the smog of tobacco, carbon monoxide content is very high.After sucking human body, carbon is combined into the hemoglobin in blood
Oxygen hemoglobin prevents hemoglobin from being normally combined into oxyhemoglobin with oxygen, thus loses the function of oxygen carrying.This
Outside, carbon monoxide and Hb-BC are 260 times bigger than oxygen, and carbon monoxide is dissociated from carbonyl haemoglobin
Speed is again more much slower than isolating the speed of oxygen from oxyhemoglobin.Since the brain of people is big to the requirement of oxygen, to scarce
Oxygen is very sensitive, and therefore, having inhaled mostly cigarette will feel that energy is not concentrated, or even headache, dizzy phenomenon occurs.Long it, brain is just
It is damaged, thinking is made to slow up, failure of memory.In this way, necessarily will affect study and work, make the study of student at
Achievement decline.
The ingredient mainly contained in traditional tobacco: pipe tobacco, smoked sheet, flavors and fragrances, moisturizer, filter tip, cigarette paper, tradition
Cigarette contains more harmful substances, and the pipe tobacco and smoked sheet in traditional tobacco are all tobacco objects, and perfume (or spice) is mainly sold in China at present
Cigarette type is all flue-cured tobacco." statistics of 1998-2004 tobacco germplasm modulation tobacco leaf " announced according to Zhong Yan group, is baked
The average content of chemical component is respectively as follows: total reducing sugar 23.08%, reduced sugar 19.63%, total nitrogen 2.00%, nicotine in cigarette
1.99%, protein 10.32%, schmuck value 2.45, total reducing sugar/nicotine 14.21, total nitrogen/nicotine 1.15.Also containing micro- in tobacco
The radioactive substance polonium -210 of amount.The ingredient of cigarette paper is: bleaching jute pulp also mixes partial bleaching wood pulp or straw pulp, glutinous through height
Shape mashing is filled with (calcium carbonate) and a small amount of combustion adjuvant (to coordinate the burning velocity of cigarette paper and tobacco filament).It is main to human body
Harmful substance is all the substance generated by burning.Such as: tar (carcinogen and rush cancer substance), BaP (high activity
Indirect-acting carcinogen), heavy metal (Cd, Cr, As, Pb etc.), gas pollutant (carbon monoxide, methacrylaldehyde, hydrogen cyanide, nitric oxide,
Nitrogen dioxide, acetone, sulfide, ammonia, phenol, acetaldehyde etc.).The unique purpose of cigarette of enfleuraging is exactly to obtain nicotine in fact, when Buddhist nun's Gu
Fourth enters in vivo, can transmit via blood, and can be average after sucking only to need 7 seconds i.e. reachable brains by blood-brain barrier.Buddhist nun
Gu Ding is about 2 hours intracorporal half-life period in people.Liver is the organ of main metabolic nicotine, amylase Cytochrome
P450, in recent years many experts both at home and abroad think the nicotine in cigarette there is no too many harm, and real carcinogenic assailant is
Tar and carbon monoxide exist among the fruit of a variety of plants of Solanaceae because nicotine not only exists only among tobacco leaf,
Such as just contain nicotine in the plants such as tomato, fructus lycii, and these vegetables and medicinal material be acknowledged as it is beneficial to human body
Health food.
Therefore, in the environment of accomplishing total ban cigarette not yet, accomplish meet the needs of smoker as far as possible, have simultaneously
The control of effect and the harmful substance human body for removing cigarette, compliance requirements and demand for security, have important practical significance.
Summary of the invention
In view of this, the present invention provide it is a kind of for the oolong tea of electronic cigarette and the composition of lemon and its application.
The present invention passes through the compounding of oolong tea and lemon, and the faint scent of lemon burning can effectively integrate the bitter mouthfeel of tealeaves burning；Into one
Step ground, smokes panel test, compared with commercially available tea cigarette, after electronic cigarette is made in composition of the invention, each item rating is superior to through panelist
Reference substance.
In order to achieve the above-mentioned object of the invention, the present invention the following technical schemes are provided:
The present invention provides a kind of compositions, including oolong tea and lemon.
In some specific embodiments of the invention, in terms of mass parts, including 70~99 parts of oolong tea and 1~30
The lemon of part.
The present invention also provides the preparation methods of the composition, include the following steps:
Step 1: it is filtered after taking oolong tea to mix extraction with water, collects filtrate, be concentrated, spray drying, through overcritical dioxy
Change the extraction of carbon extraction, oolong tea extract is made；
Step 2: taking the lemon to crush, impregnate and obtain lemon extract；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
In some specific embodiments of the invention, the extraction temperature of supercritical carbon dioxide extraction method described in step 1
Degree is 51~64 DEG C, and the extracting pressure of the supercritical carbon dioxide extraction method is 12Mpa-15Mpa, the overcritical titanium dioxide
The extraction time of carbon extraction is 9~12h.
In some specific embodiments of the invention, the mass ratio of oolong tea and water is 1:(10~20 in step 1).
In some specific embodiments of the invention, (15 DEG C) of cocnentration factor of concentration described in step 1 for 1:(1.2~
1.3)。
In some specific embodiments of the invention, the inlet temperature of spray drying described in step 1 is 90~95
DEG C, the outlet temperature of the spray drying is 45~55 DEG C, and the mixing speed of the spray drying is 200~230rpm, described
The time of spray drying is 1~2h.
In some specific embodiments of the invention, the temperature of immersion described in step 2 is 80~100 DEG C, the leaching
The time of bubble is 40~90min.
The present invention also provides compositions made from the composition or the preparation method to prepare cigarette, electronic cigarette
Or brew application in beverage.
On the basis of the studies above, the present invention also provides cigarette or electronic cigarette, including the composition or described
Composition made from preparation method.
It is accurate, quick, easy by supercritical carbon dioxide extracting, it can also be in line traffic control while improving product purity
Quality processed realizes industrialization production.Tea polyphenols are extracted using method of the invention, tea polyphenols purity is made to be increased to 99% by 95%
More than, it needs 15-20 tons of stem teas to be reduced to 5-6 tons of stem teas by extracting 1 ton of tea polyphenols using tea raw material, is extracted with this method
Tea polyphenols thoroughly solve harmful substance residue, to expand application of the tea polyphenols product on food and medicine, significantly
Product cost is reduced, the antioxidant cost well below chemical industry synthesis is allowed to, accelerates and expand products application range.
In conclusion the raw material of the composition includes: oolong tea and lemon the present invention provides a kind of composition.This
Invention additionally provides a kind of preparation method of above-mentioned composition, and the present invention also provides a kind of above-mentioned composition or above-mentioned preparation sides
The product that method obtains is in cigarette, electronic cigarette or the application for brewing beverage field.In technical solution provided by the invention, pass through crow
The faint scent of the compounding of imperial tea and lemon, lemon burning can effectively integrate the bitter mouthfeel of tealeaves burning；Further, through panelist
It smokes panel test, compared with commercially available tea cigarette, after electronic cigarette is made in composition of the invention, each item rating is superior to reference substance.The present invention
One kind of offer contains tea composition, preparation method and applications, solves in the prior art, tea mouth taste is single, distasteful
Technological deficiency.
Composition provided by the invention can be avoided the harmful substance of sucking cigarette, obtain smoker under non-burning state
The satisfaction of smoking, while harmful substance being blocked to injure smoker, so the research of this composition has compliance requirements and safety
Meaning.It is prepared into product appropriate using composition provided by the invention, is given up smoking scope applied to substitution conventional cigarette and help,
So this composition also has apparent innovative and industrialization social benefit.
Technical solution provided by the invention, has the advantage that
1, compounding by oolong tea and lemon, can effectively enhance fragrance when tealeaves burning, and faint scent when burning has
Good acceptance；
2, tea polyphenols when tealeaves burns, can effectively play the effect refreshed oneself, and drink tea similar with traditional, can play and mention
The effect of mind, can substitute traditional cigarette products to a certain extent, and the transitional product that also can be used as the smoking cessation stage uses；
3, benefit materials, the long-time services such as the substance that the tea polyphenols generated when tealeaves burns and lemon burning generate can
It plays a role in health care；
4, in preparation method provided by the invention, the accurate control for tea processing is realized, with traditional tea product
Processing needs to compare by the experience of technical staff, and technical solution provided by the invention is more stable, controllable, alleviates for warp
The dependence tested, strong operability；
5, different from conventional smoking article, composition provided by the invention can be not only used for the tea cigarette of traditional cigarette form
And the preparation of new electronic cigarette smoke grenade form tea smoke grenade, can also brew as traditional tea product drinking.
Under the flames of anger heating temperature not higher than 300 DEG C, stablizes the original taste of release cigarette and ingredient, do not generate cause
Cancer substance and the tar for promoting cancer substance；The BaP of high activity indirect-acting carcinogen is not generated；Do not generate carbon monoxide, methacrylaldehyde,
The hazardous air pollutants such as hydrogen cyanide, nitric oxide, nitrogen dioxide, acetone, sulfide, ammonia, phenol, acetaldehyde.
In addition, composition of the present invention, quality controllable, it is safe and convenient to use.Composition of the present invention is suitble to
In industrialized production.
Specific embodiment
The invention discloses a kind of for the oolong tea of electronic cigarette and the composition of lemon and its application, this field skill
Art personnel can use for reference present disclosure, be suitably modified realization of process parameters.In particular, it should be pointed out that all similar replacements and
Change apparent to those skilled in the art, they are considered as being included in the present invention.Method of the invention and
Using being described by preferred embodiment, related personnel can obviously not depart from the content of present invention, spirit and scope
It is interior that method described herein and application are modified or appropriate changes and combinations, carry out implementation and application the technology of the present invention.
It is provided by the invention a kind of for original involved in the oolong tea of electronic cigarette and the composition of lemon and its application
Material and reagent are available on the market.
Below with reference to embodiment, the present invention is further explained:
Embodiment 1
70 parts of oolong tea and 1~30 part of lemon are accurately weighed respectively.
Step 1: being filtered after taking oolong tea to mix extraction with the water of 10 times (w/w), collect filtrate, concentration (is concentrated at 15 DEG C
Than for 1:1.2), spray drying (inlet temperature is 90 DEG C, and outlet temperature is 50 DEG C, mixing speed 200rpm, time 2h),
Oolong tea extract is made in the supercritical carbon dioxide extracting 9h under conditions of 51 DEG C, 12Mpa；
Step 2: taking the lemon to crush, obtain lemon extract in 100 DEG C of immersion 40min；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
Embodiment 2
99 parts of oolong tea and 1~30 part of lemon are accurately weighed respectively.
Step 1: being filtered after taking oolong tea to mix extraction with the water of 20 times (w/w), collect filtrate, concentration (is concentrated at 15 DEG C
Than for 1:1.3), spray drying (inlet temperature is 95 DEG C, and outlet temperature is 55 DEG C, mixing speed 230rpm, time 1h),
Oolong tea extract is made in the supercritical carbon dioxide extracting 12h under conditions of 64 DEG C, 15Mpa；
Step 2: taking the lemon to crush, obtain lemon extract in 80 DEG C of immersion 90min；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
Embodiment 3
85 parts of oolong tea and 1~30 part of lemon are accurately weighed respectively.
Step 1: being filtered after taking oolong tea to mix extraction with the water of 15 times (w/w), collect filtrate, concentration (is concentrated at 15 DEG C
Than for 1:1.25), (inlet temperature is 93 DEG C, and outlet temperature is 45 DEG C, mixing speed 220rpm, and the time is for spray drying
1.5h), oolong tea extract is made in the supercritical carbon dioxide extracting 10h under conditions of 58 DEG C, 13Mpa；
Step 2: taking the lemon to crush, obtain lemon extract in 90 DEG C of immersion 60min；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
Comparative example 1
65 parts of oolong tea and 35 parts of lemon are accurately weighed respectively.
Step 1: being filtered after taking oolong tea to mix extraction with the water of 5 times (w/w), collect filtrate, concentration (cocnentration factor at 15 DEG C
For 1:1.1), it is spray-dried (inlet temperature is 85 DEG C, and outlet temperature is 60 DEG C, mixing speed 180rpm, time 2.5h),
Oolong tea extract is made in the supercritical carbon dioxide extracting 8h under conditions of 45 DEG C, 10Mpa；
Step 2: taking the lemon to crush, obtain lemon extract in 60 DEG C of immersion 120min；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
Comparative example 2
50 parts of oolong tea and 50 parts of lemon are accurately weighed respectively.
Step 1: being filtered after taking oolong tea to mix extraction with the water of 25 times (w/w), collect filtrate, concentration (is concentrated at 15 DEG C
Than for 1:1.4), (inlet temperature is 100 DEG C, and outlet temperature is 40 DEG C, mixing speed 250rpm, and the time is for spray drying
0.5h), oolong tea extract is made in the supercritical carbon dioxide extracting 13h under conditions of 67 DEG C, 17Mpa；
Step 2: taking the lemon to crush, obtain lemon extract in 110 DEG C of immersion 30min；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
Embodiment 4
Composition prepared by the present invention is detected.Referring to table 1.
Table 1
Note:*Show that compared with the control group there is significant difference (P < 0.05)；#Show has extremely significant difference compared with the control group
(P < 0.01).
Embodiment 5
Experimental group 1~3: electronic cigarette made from composition made from Examples 1 to 3；
Control group: reference substance is commercially available tea smoke product.
Choose 30 panelists and carry out measurement of smokeing panel test, carry out blind suction in continuous mode, i.e., panelist smoke panel test give a mark when simultaneously
The number of sample to be tested is not known.Panelist is in suction, from cigarette flavor, mouthfeel, effect of refreshing oneself and comprehensive score four dimensions
Degree is given a mark, and scoring is 1~5 point, and 5 points are optimal.Measure the scoring average mark of electronic cigarette 1~3 and reference substance, gained knot
Fruit please refers to table 2.
Table 2
Note: *, which shows compared with reference substance, has significant difference (P < 0.05)；# shows has extremely significant difference compared with reference substance
(P < 0.01).
As can be drawn from Table 2, compared with commercially available tea cigarette (reference substance), technical solution provided by the invention combination obtained
Electronic cigarette made from object, fragrance and effect of refreshing oneself are superior to commercially available traditional cigarette, and comprehensive score is better than reference substance, show that product has
There is good market acceptance.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. one kind contains tea composition, which is characterized in that including oolong tea and lemon.
2. containing tea composition as described in claim 1, which is characterized in that in terms of mass parts, including 70~99 parts of oolong tea
With 1~30 part of lemon.
3. as claimed in claim 1 or 2 containing the preparation method of tea composition, which comprises the steps of:
Step 1: it is filtered after taking oolong tea to mix extraction with water, collects filtrate, be concentrated, spray drying, through supercritical carbon dioxide
Extraction extraction, is made oolong tea extract；
Step 2: taking the lemon to crush, impregnate and obtain lemon extract；
Step 3: the oolong tea extract made from step 1 is mixed with lemon extract made from step 2.
4. preparation method as claimed in claim 3, which is characterized in that supercritical carbon dioxide extraction method described in step 1
Extraction temperature is 51~64 DEG C, and the extracting pressure of the supercritical carbon dioxide extraction method is 12Mpa-15Mpa, described overcritical
The extraction time of carbon dioxide extraction method is 9~12h.
5. preparation method as described in claim 3 or 4, which is characterized in that the mass ratio of oolong tea and water is 1 in step 1:
(10~20).
6. such as the described in any item preparation methods of claim 3 to 5, which is characterized in that the cocnentration factor of concentration described in step 1
(15 DEG C) are 1:(1.2~1.3).
7. such as the described in any item preparation methods of claim 3 to 6, which is characterized in that the entrance of spray drying described in step 1
Temperature is 90~95 DEG C, and the outlet temperature of the spray drying is 45~55 DEG C, the mixing speed of the spray drying is 200~
230rpm, the time of the spray drying are 1~2h.
8. such as the described in any item preparation methods of claim 3 to 7, which is characterized in that the temperature of immersion described in step 2 is 80
~100 DEG C, the time of the immersion is 40~90min.
9. as claimed in claim 1 or 2 containing made from tea composition or the preparation method as described in any one of claim 3 to 7
Composition is preparing cigarette, electronic cigarette or is brewing application in beverage.
10. cigarette or electronic cigarette, which is characterized in that including containing tea composition as claimed in claim 1 or 2 or such as claim
Composition made from any one of 3 to 7 preparation methods.
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Cited By (1)
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