CN113756104B - Perfume composition for textiles - Google Patents

Perfume composition for textiles Download PDF

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Publication number
CN113756104B
CN113756104B CN202111130096.XA CN202111130096A CN113756104B CN 113756104 B CN113756104 B CN 113756104B CN 202111130096 A CN202111130096 A CN 202111130096A CN 113756104 B CN113756104 B CN 113756104B
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Prior art keywords
solution
stirring
silk
perfume composition
suspension
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CN113756104A (en
Inventor
王天义
汪洋
张政
王毅
何云飞
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Anhui Hyea Aromas Co ltd
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Anhui Hyea Aromas Co ltd
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
    • D06M23/12—Processes in which the treating agent is incorporated in microcapsules
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/005—Compositions containing perfumes; Compositions containing deodorants
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/12—Aldehydes; Ketones
    • D06M13/13—Unsaturated aldehydes, e.g. acrolein; Unsaturated ketones; Ketenes ; Diketenes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/15—Proteins or derivatives thereof

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention relates to a perfume composition for textile, which is prepared by the following steps: step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80% to prepare a protein solution, dialyzing, separating out impurities, and preparing a purified protein solution, namely a solution a; s2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, uniformly stirring, adding tween-80, and stirring at a rotating speed of 350r/min for 2 hours to prepare a suspension; s3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, and dialyzing for 1h to form microspheres to obtain the perfume composition for textiles; the microsphere particles have smaller particle size, can be easily attached to the surface of the fabric, and slowly release fragrance, so that the fragrance storage time of the fabric is longer.

Description

Perfume composition for textiles
Technical Field
The invention belongs to the technical field of perfumes, and particularly relates to a perfume composition for textiles.
Background
In order to meet the increasing demand of aromatic textiles, many essence manufacturers are continuously developing the after-finishing technology of perfuming, soaking and perfuming. From the original process of spraying perfume powder and perfume onto clothing or sewing perfume bag onto clothing, the prior method of using perfume is developed, the perfumed soap or perfume bag with lavender with very large fragrance is sealed in a suitcase, the perfume volatilizes and permeates into fiber pores, and the clothing can keep the fragrance in a short time. In order to improve the fragrance adsorption capacity of fabrics, a method of attaching activated carbon fibers to clothes and a method of attaching fragrances to fabrics through washing liquid are adopted, but the fragrances are easy to volatilize, have poor stability and short fragrance storage time, and cannot be stored on textiles for a long time.
Disclosure of Invention
In order to solve the technical problems, the invention aims to provide a perfume composition for textiles.
The aim of the invention can be achieved by the following technical scheme:
a perfume composition for textiles, the composition comprising the steps of:
s1, adding degummed silk into 80% lithium bromide solution by mass fraction, completely immersing, putting into a 50-60 ℃ oven for dissolution, oscillating for 1 time every 1 hour to obtain protein solution, dialyzing, centrifuging for 2 times at 10000r/min for 10min each time, separating out impurities to obtain purified protein solution, namely solution a, and controlling the dosage ratio of degummed silk to lithium bromide to be 25g to 80g;
s2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, stirring at a constant speed, adding tween-80, stirring for 2 hours at a rotating speed of 350r/min to obtain a suspension, controlling the dosage ratio of bergamot oil, rose alcohol, alpha-ionone and deionized water to be 5 mg:5:5 mg:10 mL, wherein the dosage of tween-80 is 1-1.5% of the dosage of bergamot oil;
in the step S2, bergamot oil, rose alcohol, alpha-ionone and the like are taken as perfume components to be added into water, tween-80 is taken as a surfactant to be stirred to prepare suspension.
And S3, adding the suspension into the solution a, uniformly stirring for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing for 1h in an ammonium sulfate saturated aqueous solution, uniformly stirring in the dialysis process to form microspheres, and obtaining the perfume composition for textiles, wherein the volume ratio of the suspension to the solution a is controlled to be 1:10-15.
Further: the degummed silk comprises the following steps:
adding sodium carbonate into boiling water, stirring at uniform speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring every 15min, fishing out the steamed silk, rubbing with deionized water for three times, removing residual sericin, and obtaining degummed silk, wherein the dosage ratio of the sodium carbonate, the boiling water and the silk is controlled to be 24.65 g/10L/30 g.
Further: the duration of the dialysis in step S1 was 36h, the total water was changed 6 times during the dialysis, the first two times each 3h, and the last four times each 6 h.
Further: the perfume composition is orange and rose type.
The invention has the beneficial effects that:
the spice composition is characterized in that a protein solution is prepared by degumming silk in the preparation process, bergamot oil, rosol, alpha-ionone and the like are added into water as spice components, tween-80 is added into the water and is stirred to prepare suspension, and then the suspension is blended and dialyzed to prepare microsphere particles by a salting-out method.
Detailed Description
The technical solutions of the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into 80% lithium bromide solution by mass fraction, completely immersing, putting into a 50 ℃ oven for dissolution, oscillating for 1 time every 1 hour to obtain protein solution, dialyzing for 36 hours, changing water for 6 times in the dialyzing process, changing water for 3 hours in the first two times, changing water for 6 hours in the last four times, centrifuging for 2 times at a rotating speed of 10000r/min and 10 minutes each time, separating impurities to obtain purified protein solution which is solution a, and controlling the dosage ratio of degummed silk and lithium bromide to be 25g to 80g;
adding sodium carbonate into boiling water, stirring at uniform speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring every 15min, fishing out the steamed silk, rubbing with deionized water for three times, removing residual sericin, and obtaining degummed silk, wherein the dosage ratio of the sodium carbonate, the boiling water and the silk is controlled to be 24.65 g/10L/30 g.
S2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, stirring at a constant speed, adding tween-80, stirring for 2 hours at a rotating speed of 350r/min to obtain a suspension, controlling the dosage ratio of the bergamot oil to the rose alcohol to the alpha-ionone to the deionized water to be 5 mg:5:5 mg:10 mL, wherein the dosage of the tween-80 is 1% of the dosage of the bergamot oil;
and S3, adding the suspension into the solution a, uniformly stirring for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing for 1h in an ammonium sulfate saturated aqueous solution, uniformly stirring in the dialysis process to form microspheres, and preparing the perfume composition for textiles, wherein the volume ratio of the suspension to the solution a is controlled to be 1:10.
Example 2
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into 80% lithium bromide solution by mass fraction, completely immersing, putting into a 55 ℃ oven for dissolution, oscillating for 1 time every 1 hour to obtain protein solution, dialyzing for 36 hours, changing water for 6 times in the dialyzing process, changing water for 3 hours in the first two times, changing water for 6 hours in the last four times, centrifuging for 2 times at a rotating speed of 10000r/min and 10 minutes each time, separating impurities to obtain purified protein solution which is solution a, and controlling the dosage ratio of degummed silk and lithium bromide to be 25g to 80g;
adding sodium carbonate into boiling water, stirring at uniform speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring every 15min, fishing out the steamed silk, rubbing with deionized water for three times, removing residual sericin, and obtaining degummed silk, wherein the dosage ratio of the sodium carbonate, the boiling water and the silk is controlled to be 24.65 g/10L/30 g.
S2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, stirring at a constant speed, adding tween-80, stirring for 2 hours at a rotating speed of 350r/min to obtain a suspension, controlling the dosage ratio of the bergamot oil to the rose alcohol to the alpha-ionone to the deionized water to be 5 mg/10 mL, wherein the dosage of the tween-80 is 1.2% of the dosage of the bergamot oil;
and S3, adding the suspension into the solution a, uniformly stirring for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing for 1h in an ammonium sulfate saturated aqueous solution, uniformly stirring in the dialysis process to form microspheres, and preparing the perfume composition for textiles, wherein the volume ratio of the suspension to the solution a is controlled to be 1:12.
Example 3
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into 80% lithium bromide solution by mass percent, completely immersing, putting into a 60 ℃ oven for dissolution, oscillating for 1 time every 1 hour to obtain protein solution, dialyzing for 36 hours, changing water for 6 times in the dialyzing process, changing water for 3 hours in the first two times, changing water for 6 hours in the last four times, centrifuging for 2 times at a rotating speed of 10000r/min and 10 minutes each time, separating impurities to obtain purified protein solution which is solution a, and controlling the dosage ratio of degummed silk and lithium bromide to be 25g to 80g;
adding sodium carbonate into boiling water, stirring at uniform speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring every 15min, fishing out the steamed silk, rubbing with deionized water for three times, removing residual sericin, and obtaining degummed silk, wherein the dosage ratio of the sodium carbonate, the boiling water and the silk is controlled to be 24.65 g/10L/30 g.
S2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, stirring at a constant speed, adding tween-80, stirring for 2 hours at a rotating speed of 350r/min to obtain a suspension, controlling the dosage ratio of the bergamot oil to the rose alcohol to the alpha-ionone to the deionized water to be 5 mg/10 mL, wherein the dosage of the tween-80 is 1.4% of the dosage of the bergamot oil;
and S3, adding the suspension into the solution a, uniformly stirring for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing for 1h in an ammonium sulfate saturated aqueous solution, uniformly stirring in the dialysis process to form microspheres, and preparing the perfume composition for textiles, wherein the volume ratio of the suspension to the solution a is controlled to be 1:14.
Example 4
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into 80% lithium bromide solution by mass percent, completely immersing, putting into a 60 ℃ oven for dissolution, oscillating for 1 time every 1 hour to obtain protein solution, dialyzing for 36 hours, changing water for 6 times in the dialyzing process, changing water for 3 hours in the first two times, changing water for 6 hours in the last four times, centrifuging for 2 times at a rotating speed of 10000r/min and 10 minutes each time, separating impurities to obtain purified protein solution which is solution a, and controlling the dosage ratio of degummed silk and lithium bromide to be 25g to 80g;
adding sodium carbonate into boiling water, stirring at uniform speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring every 15min, fishing out the steamed silk, rubbing with deionized water for three times, removing residual sericin, and obtaining degummed silk, wherein the dosage ratio of the sodium carbonate, the boiling water and the silk is controlled to be 24.65 g/10L/30 g.
S2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, stirring at a constant speed, adding tween-80, stirring for 2 hours at a rotating speed of 350r/min to obtain a suspension, controlling the dosage ratio of the bergamot oil to the rose alcohol to the alpha-ionone to the deionized water to be 5 mg/10 mL, wherein the dosage of the tween-80 is 1.5% of the dosage of the bergamot oil;
and S3, adding the suspension into the solution a, uniformly stirring for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing for 1h in an ammonium sulfate saturated aqueous solution, uniformly stirring in the dialysis process to form microspheres, and preparing the perfume composition for textiles, wherein the volume ratio of the suspension to the solution a is controlled to be 1:15.
Comparative example 1
This comparative example is compared to example 1, the textile is sprayed directly with bergamot oil, rosol and alpha-ionone.
Comparative example 2
The comparative example is a commercial rose fragrance.
The perfume compositions prepared in examples 1-4 and comparative examples 1 and 2 were added to water in a weight ratio of 1:1000, after stirring uniformly, the fabrics were soaked in water for 30min, after which the fabrics were washed with clear water, dried in the air, and 10 smellers were found to test the retention time of fragrance on the fabrics, and the data were recorded for 2h, 10h and 24h, respectively, with the results shown in table 1 below, wherein the scores were according to table 2 below:
TABLE 1
TABLE 2 scoring basis
Standard of Rank and score
The fragrance is similar or not at 20cm, and the fragrance is smelled at 10cm Level 1
The fragrance at 10cm is similar or not, and 5cm smells the fragrance Level 2
The 5cm part has the fragrance, and the nose smells the fragrance 3 grade
The smell at the nose end is similar to that of the nose Grade 4
Fragrance-free Grade 5
From Table 1 above, it can be seen that the fragrance compositions of examples 1-4 have a longer fragrance-preserving effect.
In the description of the present specification, the descriptions of the terms "one embodiment," "example," "specific example," and the like, mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiments or examples. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing is merely illustrative and explanatory of the invention, as various modifications and additions may be made to the particular embodiments described, or in a similar manner, by those skilled in the art, without departing from the scope of the invention or exceeding the scope of the invention as defined in the claims.

Claims (5)

1. A fragrance composition for textiles, characterized in that: the method comprises the following steps of:
step S1, adding degummed silk into 80% lithium bromide solution by mass fraction, completely immersing, placing in a 50-60 ℃ oven for dissolution, oscillating for 1 time every 1 hour to obtain protein solution, dialyzing, centrifuging for 2 times at 10000r/min for 10min each time, and separating out impurities to obtain purified protein solution, namely solution a;
s2, respectively adding bergamot oil, rose alcohol and alpha-ionone into deionized water, uniformly stirring, adding tween-80, and stirring at a rotating speed of 350r/min for 2 hours to prepare a suspension;
s3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing for 1h in an ammonium sulfate saturated aqueous solution, stirring at a constant speed in the dialysis process to form microspheres, and preparing a spice composition for textiles, wherein the volume ratio of the suspension to the solution a is controlled to be 1:10-15;
the degummed silk comprises the following steps:
adding sodium carbonate into boiling water, stirring at uniform speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring every 15min, fishing out the steamed silk, rubbing with deionized water for three times, removing residual sericin, and obtaining degummed silk, wherein the dosage ratio of the sodium carbonate, the boiling water and the silk is controlled to be 24.65 g/10L/30 g.
2. A perfume composition for textile products according to claim 1, characterized in that: in the step S1, the dosage ratio of the degummed silk to the lithium bromide is controlled to be 25g to 80g.
3. A perfume composition for textile products according to claim 1, characterized in that: in the step S2, the dosage ratio of bergamot oil, rose alcohol, alpha-ionone and deionized water is controlled to be 5 mg:5:5 mg:10 mL, and the dosage of tween-80 is 1-1.5% of the dosage of bergamot oil.
4. A perfume composition for textile products according to claim 1, characterized in that: the duration of the dialysis in step S1 was 36h, the total water was changed 6 times during the dialysis, the first two times each 3h, and the last four times each 6 h.
5. A perfume composition for textile products according to claim 1, characterized in that: the perfume composition is orange and rose type.
CN202111130096.XA 2021-09-26 2021-09-26 Perfume composition for textiles Active CN113756104B (en)

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Publication number Priority date Publication date Assignee Title
CN115887730B (en) * 2022-03-22 2024-03-12 德晟康(苏州)生物科技有限公司 Microsphere suitable for hydrocolloid dressing, preparation method thereof and compound protein slow-release hydrocolloid dressing

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104822366A (en) * 2012-07-13 2015-08-05 塔夫茨大学 Encapsulation of fragrances and/or flavoring agents in silk fibroin biomaterials
CN105544210A (en) * 2016-01-21 2016-05-04 苏州印丝特纺织数码科技有限公司 Fabric post-finishing agent based on modified silk fibroin solution and preparation method of fabric post-finishing agent
CN107405277A (en) * 2014-12-02 2017-11-28 丝绸医疗公司 Silk performance garments and products and methods of making the same
CN108316018A (en) * 2018-03-15 2018-07-24 南通纺织丝绸产业技术研究院 A kind of preparation method of fibroin albumen/chitosan functional solution

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104822366A (en) * 2012-07-13 2015-08-05 塔夫茨大学 Encapsulation of fragrances and/or flavoring agents in silk fibroin biomaterials
CN107405277A (en) * 2014-12-02 2017-11-28 丝绸医疗公司 Silk performance garments and products and methods of making the same
CN105544210A (en) * 2016-01-21 2016-05-04 苏州印丝特纺织数码科技有限公司 Fabric post-finishing agent based on modified silk fibroin solution and preparation method of fabric post-finishing agent
CN108316018A (en) * 2018-03-15 2018-07-24 南通纺织丝绸产业技术研究院 A kind of preparation method of fibroin albumen/chitosan functional solution

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