CN114252334B - A method for testing the creep properties of high modulus polyethylene ropes - Google Patents

A method for testing the creep properties of high modulus polyethylene ropes Download PDF

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CN114252334B
CN114252334B CN202111563215.0A CN202111563215A CN114252334B CN 114252334 B CN114252334 B CN 114252334B CN 202111563215 A CN202111563215 A CN 202111563215A CN 114252334 B CN114252334 B CN 114252334B
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乐伟章
吴声龙
吴翔
吴�琳
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Jiangsu Shenyun Rope Co ltd
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    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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Abstract

一种测试高模量聚乙烯绳索蠕变性能的方法,属高分子纤维绳索性能检测领域。在常温条件下,由销柱固定绳索试样插接眼环的试验机用以进行绳索蠕变性能的测试;由试验机销柱的拉伸、停顿、往复循环运动,用以消除绳索的结构伸长;绳索试样在预选张力T紧张一段时间后由绳索试样中部两标记的位移用以计算得到绳索的蠕变伸长率、蠕变速率和比应力值;采用销柱固定插接眼环试样试验机的两销柱的间距不小于1800mm;张力T选择绳索断裂强力的50%至20%,其偏差范围为0.1~1﹪;两标记的间距不低于1000mm;在载荷恒定下进行高模量聚乙烯绳索蠕变性能的蠕变伸长率、蠕变速率及比应力的测定。可用于建立断裂强力不同的、各种线密度的高模量聚乙烯绳索蠕变性能的模型。A method for testing the creep performance of high modulus polyethylene ropes belongs to the field of polymer fiber rope performance testing. Under normal temperature conditions, a testing machine with a pin fixed to a rope sample and an eye ring is used to test the creep performance of the rope; the stretching, pausing, and reciprocating cyclic motion of the testing machine pin are used to eliminate the structural elongation of the rope; after the rope sample is tensed for a period of time under a preselected tension T, the displacement of two marks in the middle of the rope sample is used to calculate the creep elongation, creep rate and specific stress value of the rope; the spacing between the two pins of the testing machine with a pin fixed to the eye ring sample is not less than 1800mm; the tension T is selected to be 50% to 20% of the rope breaking strength, and its deviation range is 0.1 to 1%; the spacing between the two marks is not less than 1000mm; the creep elongation, creep rate and specific stress of the creep performance of the high modulus polyethylene rope are measured under constant load. It can be used to establish a model of creep performance of high modulus polyethylene ropes with different breaking strengths and various linear densities.

Description

一种测试高模量聚乙烯绳索蠕变性能的方法A method for testing the creep properties of high modulus polyethylene ropes

技术领域Technical Field

本发明属于高分子纤维绳索性能检测领域,具体涉及一种测试高模量聚乙烯绳索荷蠕变性能的方法。The invention belongs to the field of polymer fiber rope performance detection, and in particular relates to a method for testing the load creep performance of a high modulus polyethylene rope.

背景技术Background Art

高模量聚乙烯纤维是继碳纤维和芳纶之后出现的第三代高性能纤维,用其制造的绳索的断裂强度是最高的,为钢丝绳的8倍;在断裂强力相同时所需直径最细,为聚丙烯绳的50%;在相同直径时其断裂强力最大,为聚丙烯绳的3.8倍;其疲劳强度极高,在加速疲劳后测试的强力保持率>100%。High modulus polyethylene fiber is the third generation of high-performance fiber after carbon fiber and aramid. The rope made of it has the highest breaking strength, which is 8 times that of steel wire rope. When the breaking strength is the same, the required diameter is the thinnest, which is 50% of that of polypropylene rope. When the diameter is the same, its breaking strength is the largest, which is 3.8 times that of polypropylene rope. Its fatigue strength is extremely high, and the strength retention rate after accelerated fatigue test is >100%.

高模量聚乙烯纤维的高性能,决定了其在海洋平台锚缆定位系统中系泊缆的应用日益拓展,高模量聚乙烯系泊缆(亦称高模量聚乙烯绳索)发展为海洋油气资源开发的关键配套的高端装备之一。The high performance of high modulus polyethylene fiber determines its increasing application in mooring cables in offshore platform anchor cable positioning systems. High modulus polyethylene mooring cables (also known as high modulus polyethylene ropes) have developed into one of the key supporting high-end equipment for the development of offshore oil and gas resources.

蠕变是指在某温度和恒定应力下所发生的随时间缓慢而连续增大的塑性变形现象。Creep refers to the phenomenon of plastic deformation that occurs slowly and continuously over time under a certain temperature and constant stress.

高模量聚乙烯纤维由于分子链长、分子间作用力小,在恒定载荷长期作用下会产生分子链滑移现象,即不可逆转的变形—蠕变,这种现象强烈取决于负载、时间和温度。Due to the long molecular chain and small intermolecular force, high modulus polyethylene fiber will produce molecular chain slippage under long-term constant load, that is, irreversible deformation-creep. This phenomenon strongly depends on load, time and temperature.

高模量聚乙烯系泊缆在恒定载荷下长期工作,其蠕变性能关系到海洋平台的安全。因此,高模量聚乙烯纤维在用作海洋平台的系泊缆时,必须建立一个对应的蠕变性能文档模型。High modulus polyethylene mooring cables work for a long time under constant load, and their creep performance is related to the safety of offshore platforms. Therefore, when high modulus polyethylene fibers are used as mooring cables for offshore platforms, a corresponding creep performance document model must be established.

授权公告号为CN 103234841 B,授权公告日为2016年2月10日的中国发明专利,公开了一种测试超高分子量聚乙烯纤维拉伸蠕变性能的方法,其采用纤维拉伸试验机在常温下以蠕变载荷、拉伸速度、蠕变时间、纤维测试长度为自变量,进行纤维蠕变伸长率的测定。该方法是将纤维试样二端分别夹入上、下夹持器中,在设定拉伸速度下逐渐施加载荷,从初负荷至蠕变载荷后维持一定的蠕变时间,记录的试样伸长率即为蠕变伸长率。该方法的蠕变时间为10~100min、测试长度为100~500mm,这不符合高模量聚乙烯绳索蠕变性能的测试需要以小时为单位的蠕变时间、试样有效长度最少为1800mm的要求。该方法以纤维拉伸试验机机的上、下夹持器间距为试样测试长度,由夹持器的位移值计算得到伸长率,由于高模量聚乙烯纤维在测试中易从夹持器内滑行出部分长度而造成伸长率测试旳偏差。该方法所述的定载荷伸长率为到达蠕变载荷后在蠕变时间内纤维的伸长率,在蠕变时间内试验机停止拉伸后虽然伸长率不变,但是纤维所受的拉应力随着时间的延续而递减,因此测定的是拉伸的伸长率,不是恒定载荷的蠕变伸长率。。The Chinese invention patent with the authorization announcement number CN 103234841 B and the authorization announcement date of February 10, 2016 discloses a method for testing the tensile creep properties of ultra-high molecular weight polyethylene fibers, which uses a fiber tensile testing machine at room temperature with creep load, tensile speed, creep time, and fiber test length as independent variables to measure the creep elongation of the fiber. The method is to clamp the two ends of the fiber sample into the upper and lower clamps respectively, gradually apply the load at a set tensile speed, maintain a certain creep time from the initial load to the creep load, and the recorded sample elongation is the creep elongation. The creep time of this method is 10 to 100 minutes and the test length is 100 to 500 mm, which does not meet the requirements of the creep performance test of high modulus polyethylene ropes, which requires a creep time in hours and a minimum effective length of 1800 mm. This method uses the distance between the upper and lower clamps of the fiber tensile tester as the test length of the specimen, and calculates the elongation from the displacement value of the clamp. Since high modulus polyethylene fibers are prone to slide out of the clamp part of the length during the test, the elongation test will be biased. The constant load elongation described in this method is the elongation of the fiber during the creep time after reaching the creep load. Although the elongation remains unchanged after the tester stops stretching during the creep time, the tensile stress on the fiber decreases with time. Therefore, the elongation of the stretch is measured, not the creep elongation under constant load.

高模量聚乙烯(超高分子量聚乙烯)绳索的标准GB/T30668-2014《超高分子量聚乙烯纤维8股、12股编绳和复编绳索》规定了物理性能的线密度和断裂强力的要求,其依据GB/T 8834《绳索有关物理和机械性能的测定》指定的试验方法和试验条件下测得。GB/T30668无绳索伸长与蠕变性能的要求,但也指出“不同等级超高分子量聚乙烯长丝应注意有不同的蠕变性能”。The standard GB/T30668-2014 for high modulus polyethylene (UHMWPE) ropes, "UHMWPE fiber 8-strand, 12-strand braided ropes and double braided ropes", specifies the requirements for the linear density and breaking strength of physical properties, which are measured under the test methods and test conditions specified in GB/T 8834 "Determination of physical and mechanical properties of ropes". GB/T30668 does not have requirements for rope elongation and creep properties, but also points out that "different grades of UHMWPE filaments should pay attention to different creep properties".

纤维绳索测试方法的标准GB/T 8834《绳索有关物理和机械性能的测定》规定了绳索线密度、捻距、伸长、断裂强力特性的测试方法,但未列入绳索蠕变性能的测试方法。其绳索伸长的测量步骤:在预加张力下测量试样中部两标记间的距离;通过试验机的往复运动部件以匀速拉伸逐渐增加张力,当张力达到断裂强力的75﹪时停机,尽快测量两标记间的距离,由拉伸前后两标距计算得到绳索伸长率。该方法在停止拉伸后绳索所受的拉应力随着时间的延续而递减,故其测定的是拉伸的伸长率不是恒定载荷的蠕变伸长率。The standard GB/T 8834 "Determination of Physical and Mechanical Properties of Ropes" for fiber rope testing methods specifies the test methods for rope linear density, lay length, elongation, and breaking strength, but does not include the test method for rope creep performance. The steps for measuring rope elongation are: measure the distance between the two marks in the middle of the sample under pre-tension; gradually increase the tension by stretching at a uniform speed through the reciprocating parts of the testing machine, stop the machine when the tension reaches 75% of the breaking strength, measure the distance between the two marks as soon as possible, and calculate the rope elongation from the two gauge lengths before and after stretching. This method determines the tensile stress of the rope as time goes on after the stretching stops, so it measures the elongation of the stretching, not the creep elongation under constant load.

如何才能正确地测量高模量聚乙烯纤维的恒定载荷蠕变参数和相关性能,是实际测量工作中急待解决的关键技术问题。How to correctly measure the constant load creep parameters and related properties of high modulus polyethylene fibers is a key technical problem that needs to be solved urgently in actual measurement work.

发明内容Summary of the invention

为了克服现有技术存在着测定的是拉伸伸长率而不是恒定载荷蠕变伸长率的缺陷,本发明的技术方案提供了一种测试高模量聚乙烯绳索蠕变性能的方法。该技术方案的实施,可以建立断裂强力不同的、各种线密度的高模量聚乙烯绳索的蠕变性能的文档模型;从这个模型中,可以获得蠕变性能数据(蠕变速率、容许蠕变伸长和时间),预测每年的蠕变预期、整条绳索设计寿命的累积蠕变伸长,在同等特定比应力和温度条件下的对比可以得知绳索蠕变速率与纤维蠕变的比例。In order to overcome the defect of the prior art that the tensile elongation is measured instead of the constant load creep elongation, the technical solution of the present invention provides a method for testing the creep performance of high modulus polyethylene ropes. The implementation of the technical solution can establish a document model of the creep performance of high modulus polyethylene ropes with different breaking strengths and various linear densities; from this model, creep performance data (creep rate, allowable creep elongation and time) can be obtained, and the annual creep expectation and the cumulative creep elongation of the entire rope design life can be predicted. The comparison under the same specific stress and temperature conditions can know the ratio of the rope creep rate to the fiber creep.

本发明的技术方案是:提供一种测试高模量聚乙烯绳索蠕变性能的方法,其所测试的绳索蠕变性能,至少包括绳索蠕变伸长率、绳索蠕变速率以及绳索比应力;其特征是所述测试高模量聚乙烯绳索蠕变性能的方法,在以下模式和条件下进行:The technical solution of the present invention is to provide a method for testing the creep performance of a high modulus polyethylene rope, wherein the tested creep performance of the rope at least includes the creep elongation of the rope, the creep rate of the rope and the specific stress of the rope; the method is characterized in that the method for testing the creep performance of the high modulus polyethylene rope is carried out under the following modes and conditions:

在常温条件下,由销柱固定绳索试样插接眼环的试验机用以进行绳索蠕变性能的测试;Under normal temperature conditions, the testing machine with a pin fixing the rope sample and inserting the eye ring is used to test the creep performance of the rope;

由试验机销柱的拉伸、停顿、往复循环运动,用以消除绳索的结构伸长;The stretching, pausing, and reciprocating motion of the testing machine pin are used to eliminate the structural elongation of the rope;

绳索试样在预选张力T紧张一段时间后由绳索试样中部两标记的位移用以计算得到绳索的蠕变伸长率、蠕变速率和比应力值;After the rope sample is subjected to the preselected tension T for a period of time, the displacement of the two marks in the middle of the rope sample is used to calculate the creep elongation, creep rate and specific stress value of the rope;

其中,所述的绳索蠕变试验,应在控制温度的条件下执行,温度不超过25℃和温差在5℃范围内;The creep test of the rope shall be carried out under temperature control, with the temperature not exceeding 25°C and the temperature difference within 5°C;

采用销柱固定插接眼环试样试验机的两销柱的间距不小于1800mm;The distance between the two pins of the eye ring specimen testing machine fixed with pins shall not be less than 1800mm;

张力T选择绳索断裂强力的50%至20%,其偏差范围为0.1~1﹪;The tension T is selected to be 50% to 20% of the rope breaking strength, with a deviation range of 0.1 to 1%;

两标记的间距不低于1000mm;The distance between two marks shall not be less than 1000mm;

所述测试高模量聚乙烯绳索蠕变性能的方法,在载荷恒定下进行高模量聚乙烯绳索蠕变性能的蠕变伸长率、蠕变速率及比应力的测定。The method for testing the creep performance of the high modulus polyethylene rope is to measure the creep elongation, creep rate and specific stress of the creep performance of the high modulus polyethylene rope under a constant load.

所述测试高模量聚乙烯绳索蠕变性能的方法,用于建立断裂强力不同的、各种线密度的高模量聚乙烯绳索的蠕变性能的文档模型;从这个模型中,能够获得绳索试样的蠕变数据,预测每年的蠕变预期、整条绳索设计寿命的累积蠕变伸长,在同等特定比应力和温度条件下对比,获得绳索试样的绳索蠕变速率与纤维蠕变的比例。The method for testing the creep performance of a high modulus polyethylene rope is used to establish a document model of the creep performance of high modulus polyethylene ropes with different breaking strengths and various linear densities; from this model, the creep data of the rope sample can be obtained, the annual creep expectation and the cumulative creep elongation of the entire rope design life can be predicted, and the ratio of the rope creep rate to the fiber creep of the rope sample can be obtained by comparison under the same specific specific stress and temperature conditions.

具体的,所述的蠕变数据至少包括蠕变速率、容许蠕变伸长和时间。Specifically, the creep data at least includes creep rate, allowable creep elongation and time.

进一步的,所述测试高模量聚乙烯绳索蠕变性能的方法,包括以下步骤:Furthermore, the method for testing the creep performance of high modulus polyethylene rope comprises the following steps:

步骤1:试样安装在试验机;Step 1: Install the specimen in the testing machine;

步骤2:施加绳索断裂强力的2﹪的负载;Step 2: Apply a load equal to 2% of the rope’s breaking strength;

步骤3:伸长计应安装设置在绳索两标记之间;Step 3: The extensometer should be installed between the two marks on the rope;

步骤4:张力以每分钟加载绳索断裂强力的10﹪的速度到绳索断裂强力的50﹪后保持30分钟;Step 4: The tension is increased at a rate of 10% of the rope's breaking strength per minute to 50% of the rope's breaking strength and then maintained for 30 minutes;

步骤5:张力以每分钟减少绳索断裂强力的10﹪的速度到绳索断裂强力20﹪;Step 5: The tension is reduced at a rate of 10% of the rope breaking strength per minute to 20% of the rope breaking strength;

步骤6:张力以0.03赫兹至0.1赫兹的频率在绳索断裂强力的10﹪和30﹪之间循环300次;Step 6: The tension is cycled 300 times between 10% and 30% of the rope breaking strength at a frequency of 0.03 Hz to 0.1 Hz;

步骤7:须在预定控制温度、预选张力T的紧张下至少7天,应在这个时间连续测量标距长度,采样率最低每小时一次;Step 7: The sample must be kept at the predetermined controlled temperature and pre-selected tension T for at least 7 days. The gauge length should be measured continuously during this time, with a sampling rate of at least once per hour.

步骤8:样品被卸载。Step 8: The sample is unloaded.

更进一步的,所述高模量聚乙烯绳索蠕变性能的测量和计算方法包括:Furthermore, the method for measuring and calculating the creep performance of the high modulus polyethylene rope includes:

对下述3种标距长度进行测量:The following three gauge lengths are measured:

5.1)在步骤3–5中,测量拉伸负载的标距;5.1) In steps 3–5, measure the gauge length of the tensile load;

5.2)在步骤6中,测量循环载荷的标距;5.2) In step 6, measure the gauge length of the cyclic load;

5.3)在步骤7中,预选张力T紧张下的标距与完成时间;5.3) In step 7, preselect the gauge length and completion time under tension T;

具体的,在步骤7中,连续测量的采样率为最低每小时一次。Specifically, in step 7, the sampling rate of the continuous measurement is at least once per hour.

进一步的,待测绳缆的蠕变性能使用下述公式进行计算:Furthermore, the creep performance of the tested cable is calculated using the following formula:

A、蠕变伸长率:A. Creep elongation:

G=[(l-l2)/l2]×100%G = [(ll 2 )/l 2 ] × 100%

式中:Where:

G为蠕变伸长率,%;l为步骤7中预选张力T紧张下的标距,单位为毫米;l2为步骤2中断裂强力2﹪时的标距,单位为毫米;G is creep elongation, %; l is the gauge length under the preselected tension T in step 7, in millimeters; l2 is the gauge length at the breaking strength of 2% in step 2, in millimeters;

B、蠕变速率:B. Creep rate:

Gt=G/h Gt =G/h

式中:Gt为蠕变速率,﹪/h;G为蠕变伸长率,﹪;h为蠕变时间,单位为小时;Where: Gt is the creep rate, ﹪/h; G is the creep elongation, ﹪; h is the creep time, in hours;

C、比应力:C. Specific stress:

SC=T/ρS C =T/ρ

式中:Sc为绳索的比应力,单位为牛顿/特克斯;T为步骤7中预选的张力,单位为千[牛顿];ρ为绳索的线性密度,单位为千[特克斯]。Where: Sc is the specific stress of the rope, in Newton/tex; T is the tension preselected in step 7, in kilonewtons; ρ is the linear density of the rope, in kilotex.

更进一步的,所述测试高模量聚乙烯绳索蠕变性能的方法,包括以下内容或步骤:Furthermore, the method for testing the creep performance of high modulus polyethylene rope comprises the following contents or steps:

8.1)温度控制;8.1) Temperature control;

8.2)样品制备与初始测量;8.2) Sample preparation and initial measurement;

8.3)试验机调控;8.3) Testing machine control;

8.4)试验准备;8.4) Experimental preparation;

8.5)蠕变性能测试;8.5) Creep performance test;

8.6)绳索蠕变性能的计算;8.6) Calculation of rope creep properties;

8.7)记录应记录的数据。8.7) Record the data that should be recorded.

进一步的,在所述的测试高模量聚乙烯绳索蠕变性能的方法中:Further, in the method for testing the creep properties of high modulus polyethylene rope:

A、所述的温度控制包括控制试验室温度,使温度不超过25℃和温差在5℃范围内;A. The temperature control includes controlling the temperature of the test chamber so that the temperature does not exceed 25°C and the temperature difference is within 5°C;

B、所述的样品制备与初始测量包括截取绳索2米加10个捻距长度的样品,测量初始长度L0和称量质量m,在中部作间距不小于1米的两个r标记,测量初始标距l0B. The sample preparation and initial measurement include cutting a sample of 2 meters of rope plus 10 lay lengths, measuring the initial length L 0 and weighing the mass m, making two r marks with a spacing of not less than 1 meter in the middle, and measuring the initial gauge length l 0 ;

C、所述的试验机调控包括采用销柱固定绳索试样插接眼环的试验机,两销柱的间距不小于1800mm;其中,试验机的拉伸速度;在预选张力T对试样紧张之前为常速级,由电机调速达到加载速率的要求;在预选张力T对试样紧张时为低速级,电机调速的微速或停运使预选张力T在其0.1~1﹪范围内波动,以达到载荷恆定的作用;C. The control of the testing machine includes a testing machine that uses a pin to fix the rope sample and insert the eye ring, and the distance between the two pins is not less than 1800mm; wherein, the stretching speed of the testing machine; before the pre-selected tension T is tightened on the sample, it is a normal speed level, and the motor speed is adjusted to meet the requirements of the loading rate; when the pre-selected tension T is tightened on the sample, it is a low speed level, and the motor speed adjustment is slow or stopped to make the pre-selected tension T fluctuate within the range of 0.1 to 1% to achieve the effect of load stability;

D、所述的试验准备包括:D. The test preparation includes:

D1)试样安装在试验机上;D1) The specimen is installed on the testing machine;

D2)伸长计应安装在绳索标记之间,调节摄像机焦距和光圈;D2) The extensometer should be installed between the rope marks and the camera focus and aperture should be adjusted;

D3)施加绳索断裂强力的2﹪的负载,测量标距l2D3) Apply a load of 2% of the rope breaking strength and measure the gauge length l 2 ;

E、所述的蠕变性能测试包括:E. The creep performance test includes:

E1)消除绳索的结构伸长;E1) Eliminate the structural elongation of the rope;

E2)在恒定张力下对稳态蠕变进行测定;E2) Determination of steady-state creep under constant tension;

E3)测试结束后样品应被卸载。E3) The sample should be unloaded after the test.

在本发明的技术方案中,所述的绳索蠕变伸长率为在某温度和恒定张力下所发生的随时间缓慢而连续增大的塑性伸长率;所述的绳索蠕变速率为单位时间的蠕变伸长率;所述的绳索比应力为单位线密度的张力。In the technical solution of the present invention, the creep elongation of the rope is the plastic elongation that increases slowly and continuously with time under a certain temperature and constant tension; the creep rate of the rope is the creep elongation per unit time; and the specific stress of the rope is the tension per unit linear density.

与现有技术比较,本发明的优点是:Compared with the prior art, the advantages of the present invention are:

1.本发明技术方案所提供的测试高模量聚乙烯绳索蠕变性能的方法,克服了现有技术存在着因拉伸速度较大而无法对绳索施加恒定载荷、测定的是拉伸的伸长率而不是恒定载荷的蠕变伸长率的缺陷;1. The method for testing the creep performance of high modulus polyethylene rope provided by the technical solution of the present invention overcomes the defects of the prior art that a constant load cannot be applied to the rope due to a high tensile speed, and what is measured is the tensile elongation rather than the creep elongation under a constant load;

2.本发明的技术方案,在载荷恒定下进行高模量聚乙烯绳索蠕变性能的蠕变伸长率、蠕变速率及比应力的测定;2. The technical solution of the present invention is to measure the creep elongation, creep rate and specific stress of the creep properties of high modulus polyethylene rope under constant load;

3.本发明技术方案的实施,可以建立断裂强力不同的、各种线密度的高模量聚乙烯绳索的蠕变性能的文档模型;从这个模型中,可以获得蠕变数据(蠕变速率、容许蠕变伸长和时间),预测每年的蠕变预期、整条绳索设计寿命的累积蠕变伸长,在同等特定比应力和温度条件下对比,可以得知绳索试样的绳索蠕变速率与纤维蠕变的比例。3. The implementation of the technical solution of the present invention can establish a document model of the creep performance of high modulus polyethylene ropes with different breaking strengths and various linear densities; from this model, creep data (creep rate, allowable creep elongation and time) can be obtained, and the annual creep expectation and the cumulative creep elongation of the entire rope design life can be predicted. By comparing under the same specific specific stress and temperature conditions, the ratio of the rope creep rate to the fiber creep of the rope sample can be obtained.

具体实施方式DETAILED DESCRIPTION

下面对本发明做进一步说明。The present invention is further described below.

本发明所测试的绳索蠕变性能,包括绳索蠕变伸长率—在某温度和恒定张力下所发生的随时间缓慢而连续增大的塑性伸长率;绳索蠕变速率—单位时间的蠕变伸长率;以及绳索比应力—单位线密度的张力。The creep properties of the rope tested by the present invention include the creep elongation of the rope - the plastic elongation that increases slowly and continuously with time under a certain temperature and constant tension; the creep rate of the rope - the creep elongation per unit time; and the specific stress of the rope - the tension per unit linear density.

本发明的技术方案,通过以下方式来实现绳索蠕变性能的测试:The technical solution of the present invention realizes the test of the creep performance of the rope by the following methods:

在常温条件下由销柱固定绳索试样插接眼环的试验机用以进行绳索蠕变性能的测试;The testing machine, which uses pins to fix rope specimens and insert eyelets under normal temperature conditions, is used to test the creep performance of ropes.

由试验机销柱的拉伸、停顿、往复循环运动,用以消除绳索的结构伸长;The stretching, pausing, and reciprocating motion of the testing machine pin are used to eliminate the structural elongation of the rope;

绳索试样在预选张力T紧张一段时间后由绳索试样中部两标记的位移用以计算得到绳索的蠕变伸长率、蠕变速率和比应力值。After the rope sample is subjected to the preselected tension T for a period of time, the displacement of the two marks in the middle of the rope sample is used to calculate the creep elongation, creep rate and specific stress value of the rope.

本技术方案中的绳索蠕变试验,应在控制温度的条件下执行,温度不超过25℃和温差在5℃范围内。The creep test of the rope in this technical solution should be carried out under temperature controlled conditions, with the temperature not exceeding 25°C and the temperature difference within 5°C.

采用销柱固定插接眼环试样试验机的两销柱的间距不小于1800mm。The distance between the two pins of the eye ring specimen testing machine fixed with pins shall not be less than 1800mm.

张力T应当选择绳索断裂强力的50%至20%,其偏差范围为0.1~1﹪。The tension T should be selected to be 50% to 20% of the rope breaking strength, with a deviation range of 0.1 to 1%.

两标记的间距不低于1000mm。The distance between two marks shall not be less than 1000mm.

本发明还提供了一种测试高模量聚乙烯绳索蠕变性能的方法,包括以下步骤:The present invention also provides a method for testing the creep performance of a high modulus polyethylene rope, comprising the following steps:

步骤1:试样安装在试验机;Step 1: Install the specimen in the testing machine;

步骤2:施加绳索断裂强力的2﹪的负载;Step 2: Apply a load equal to 2% of the rope’s breaking strength;

步骤3:伸长计应安装在绳索两标记之间;Step 3: The extensometer should be installed between the two marks on the rope;

步骤4:张力以每分钟加载绳索断裂强力的10﹪的速度到绳索断裂强力的50﹪后保持30分钟;Step 4: The tension is increased at a rate of 10% of the rope's breaking strength per minute to 50% of the rope's breaking strength and then maintained for 30 minutes;

步骤5:张力以每分钟减少绳索断裂强力的10﹪的速度到绳索断裂强力20﹪;Step 5: The tension is reduced at a rate of 10% of the rope breaking strength per minute to 20% of the rope breaking strength;

步骤6:张力以0.03赫兹至0.1赫兹的频率在绳索断裂强力的10﹪和30﹪之间循环300次;Step 6: The tension is cycled 300 times between 10% and 30% of the rope breaking strength at a frequency of 0.03 Hz to 0.1 Hz;

步骤7:须在预定控制温度、预选张力T的紧张下至少7天,应在这个时间连续测量标距长度,采样率最低每小时一次;Step 7: The sample must be kept at the predetermined controlled temperature and pre-selected tension T for at least 7 days. The gauge length should be measured continuously during this time, with a sampling rate of at least once per hour.

步骤8:样品应被卸载。Step 8: The sample should be unloaded.

本发明还提供了一种测试高模量聚乙烯绳索蠕变性能的测量和计算方法:The present invention also provides a method for measuring and calculating the creep performance of high modulus polyethylene ropes:

对下述3种标距长度进行测量:The following three gauge lengths are measured:

1)步骤3-5,拉伸负载的标距;1) Steps 3-5, gauge length of tensile load;

2)步骤6,循环载荷的标距;2) Step 6, gauge length of cyclic load;

3)步骤7,预选张力T紧张下的标距与完成时间(连续测量采样率:最低每小时一次)。3) Step 7, pre-select the gauge length and completion time under tension T (continuous measurement sampling rate: minimum once per hour).

待测绳缆的蠕变性能使用下述公式进行计算:The creep performance of the tested rope is calculated using the following formula:

A、蠕变伸长率:A. Creep elongation:

G=[(l-l2)/l2]×100%G = [(ll 2 )/l 2 ] × 100%

式中:Where:

G—蠕变伸长率,%;G—creep elongation, %;

l—步骤7中预选张力T紧张下的标距,单位为毫米,(mm);l—the gauge length under the preselected tension T in step 7, in millimeters (mm);

l2—步骤2中断裂强力2﹪时的标距,单位为毫米,(m)。l 2 — gauge length when the breaking strength is 2﹪ in step 2, in millimeters (m).

B、蠕变速率:B. Creep rate:

Gt=G/h Gt =G/h

式中:Where:

Gt—蠕变速率,﹪/h; Gt — creep rate, ﹪/h;

G—蠕变伸长率,﹪;G—creep elongation, ﹪;

h—蠕变时间,单位为小时(h)。h—creep time, in hours (h).

C、比应力:C. Specific stress:

SC=T/ρS C =T/ρ

式中:Where:

Sc—绳索的比应力,单位为牛顿/特克斯(N/tex);Sc—specific stress of the rope, in Newton/tex (N/tex);

T—步骤7预选的张力,单位为千[牛顿](kN);T—the tension preselected in step 7, in kilonewtons (kN);

ρ—绳索的线性密度,单位为千[特克斯](ktex)。ρ—Linear density of the rope, in ktex.

最佳实施方式:Best Practice:

1、温度控制:1. Temperature control:

控制试验室温度,使温度不超过25℃和温差在5℃范围内;记录测试蠕变期间的温度;Control the test room temperature so that it does not exceed 25°C and the temperature difference is within 5°C; record the temperature during the creep test;

2、样品制备与初始测量:2. Sample preparation and initial measurement:

截取绳索2米加10个捻距长度的样品,测量初始长度L0(精确至0.5﹪)和称量质量m(精确至0.5﹪),在中部作间距不低于1米的两个r标记,测量初始标距l0(精确至0.5﹪);Cut a sample of 2 meters plus 10 lay lengths of rope, measure the initial length L 0 (accurate to 0.5%) and weigh the mass m (accurate to 0.5%), make two r marks with a spacing of not less than 1 meter in the middle, and measure the initial gauge length l 0 (accurate to 0.5%);

3、试验机调控:3. Testing machine control:

采用销柱固定绳索试样插接眼环的试验机,两销柱的间距不小于1800mm;其中,试验机的拉伸速度;在预选张力T对试样紧张之前为常速级,由电机调速达到加载速率的要求;在预选张力T对试样紧张时为低速级,电机调速的微速或停运使预选张力T在其0.1~1﹪范围内波动,能达到载荷恆定的作用;The testing machine adopts pins to fix the rope specimen and insert the eye ring. The distance between the two pins is not less than 1800mm. Among them, the tensile speed of the testing machine is normal speed before the pre-selected tension T is applied to the specimen, and the motor speed is adjusted to meet the requirements of the loading rate. When the pre-selected tension T is applied to the specimen, it is low speed. The slow speed or stop of the motor speed adjustment makes the pre-selected tension T fluctuate within the range of 0.1~1﹪, which can achieve the effect of load stability.

4、试验准备:4. Test preparation:

1)试样安装在试验机上;1) The sample is installed on the testing machine;

2)伸长计应安装在绳索标记之间,调节摄像机焦距和光圈;2) The extensometer should be installed between the rope marks and the camera focus and aperture should be adjusted;

3)施加绳索断裂强力的2﹪的负载,测量标距l2(精确至0.5﹪);3) Apply a load of 2% of the rope breaking strength and measure the gauge length l 2 (accurate to 0.5%);

5、蠕变性能测试:5. Creep performance test:

1)消除绳索的结构伸长;1) Eliminate the structural elongation of the rope;

由试验机销柱的拉伸、停顿、往复循环运动,用以消除绳索的结构伸长:The stretching, pausing, and reciprocating motion of the testing machine pin are used to eliminate the structural elongation of the rope:

a)张力以每分钟加载绳索断裂强力的10﹪的速度到绳索断裂强力的50﹪后保持30分钟;a) The tension is applied at a rate of 10% of the rope's breaking strength per minute to 50% of the rope's breaking strength and then maintained for 30 minutes;

b)张力以每分钟减少绳索断裂强力的10﹪的速度到绳索断裂强力20﹪;b) The tension is reduced at a rate of 10% of the rope breaking strength per minute to 20% of the rope breaking strength;

c)张力以0.03赫兹至0.1赫兹的频率在绳索断裂强力的10﹪和30﹪之间循环300次;c) The tension is cycled 300 times at a frequency of 0.03 Hz to 0.1 Hz between 10% and 30% of the rope breaking strength;

2)在恒定张力下对稳态蠕变进行测定:2) Determination of steady-state creep under constant tension:

恒定张力T为绳索断裂强力的50%至20%;须在在预定控制温度、预选张力T的紧张下至少7天,应在这个时间连续测量标距长度l(精确至0.5﹪),采样率最低每小时一次;The constant tension T is 50% to 20% of the rope breaking strength; it must be at a predetermined controlled temperature and pre-selected tension T for at least 7 days, during which the gauge length l should be measured continuously (accurate to 0.5%), with a sampling rate of at least once per hour;

3)测试结束后样品应被卸载;3) The sample should be unloaded after the test;

6、绳索蠕变性能的计算:6. Calculation of rope creep performance:

1)线密度:1) Linear density:

ρ=m/L1 ρ=m/L 1

L1=l2×L0/l0 L 1 = l 2 × L 0 / l 0

式中:Where:

ρ—绳索线密度,单位为千[特克斯](ktex);ρ—rope linear density, in ktex;

m—试样的质量,单位为克(g);m—mass of the sample, in grams (g);

L1—断裂强力2﹪张力时的试样长度,单位为米(m);L 1 — length of the sample when the breaking strength is 2% tension, in meters (m);

l2—断裂强力2﹪时的标距,度单位为米(m);l 2 — gauge length when the breaking strength is 2%, in meters (m);

L0—初始长度,单位为米(m);L 0 —initial length, in meters (m);

l0—初始标距,单位为米(m)。l 0 —initial scale length, in meters (m).

2)蠕变伸长率:2) Creep elongation:

G=[(l-l2)/l2]×100G = [(ll 2 )/l 2 ] × 100

式中:Where:

G—蠕变伸长率,%;G—creep elongation, %;

l—预选张力T紧张下的标距,单位为毫米,(mm);l—gauge length under pre-selected tension T, in millimeters (mm);

l2—断裂强力2﹪时的标距,单位为毫米,(m)。l 2 — gauge length when the breaking strength is 2%, in millimeters (m).

3)蠕变速率:3) Creep rate:

Gt=G/h Gt =G/h

式中:Where:

Gt—蠕变速率,﹪/h; Gt — creep rate, ﹪/h;

G—蠕变伸长率,﹪;G—creep elongation, ﹪;

h—蠕变时间,单位为小时(h)。h—creep time, in hours (h).

4)比应力:4) Specific stress:

SC=T/ρS C =T/ρ

T=t×FMBS T=t×F MBS

式中:Where:

Sc—绳索的比应力,单位为牛顿/特克斯(N/tex);Sc—specific stress of the rope, in Newton/tex (N/tex);

T—预选的张力,单位为千[牛顿](kN);T—preselected tension, in kilonewtons (kN);

ρ—绳索的线性密度,单位为千[特克斯](ktex);ρ—linear density of the rope, in ktex;

t—应力比,﹪;t—stress ratio, ﹪;

FMBS—特定的最低绳索断裂强力,单位为牛顿(N)。F MBS — Specific minimum rope breaking strength in Newtons (N).

7、以下为应记录的数据:7. The following data should be recorded:

—样本类型和线性密度;— Sample type and linear density;

—应力比τ和比应力Sc;—stress ratio τ and specific stress Sc;

—测试蠕变期间的温度;— temperature during creep testing;

—蠕变伸长率和蠕变速率。—Creep elongation and creep rate.

本发明的技术方案,在载荷恒定条件下,进行高模量聚乙烯绳索蠕变性能的蠕变伸长率、蠕变速率及比应力的测定;采用本发明的技术方案,可以建立断裂强力不同的、各种线密度的高模量聚乙烯绳索的蠕变性能的文档模型;从这个模型中,可以获得蠕变数据(蠕变速率、容许蠕变伸长和时间),预测每年的蠕变预期、整条绳索设计寿命的累积蠕变伸长,在同等特定比应力和温度条件下对比可以得知绳索蠕变速率与纤维蠕变的比例。The technical solution of the present invention measures the creep elongation, creep rate and specific stress of the creep performance of a high modulus polyethylene rope under constant load conditions; by adopting the technical solution of the present invention, a document model of the creep performance of high modulus polyethylene ropes with different breaking strengths and various linear densities can be established; from this model, creep data (creep rate, allowable creep elongation and time) can be obtained, and the annual creep expectation and the cumulative creep elongation of the entire rope design life can be predicted. By comparison under the same specific specific stress and temperature conditions, the ratio of the rope creep rate to the fiber creep can be obtained.

本发明可广泛用于高模量聚乙烯纤维的恒定载荷蠕变测试领域。The invention can be widely used in the field of constant load creep test of high modulus polyethylene fibers.

Claims (6)

1. A method of testing the creep performance of a high modulus polyethylene rope, the tested rope creep performance comprising at least rope creep elongation, rope creep rate and rope specific stress; the method is characterized in that the method for testing the creep property of the high-modulus polyethylene rope is carried out under the following modes and conditions:
Under the normal temperature condition, the testing machine for fixing the rope sample by the pin column and inserting the eye ring is used for testing the creep performance of the rope; the tensile, pause and reciprocating cyclic motion of the pin of the tester is used for eliminating the structural elongation of the rope, and comprises the following steps:
step 1: applying a load of 2% of the rope breaking strength;
step 2: the extensometer is arranged between the two marks of the rope;
Step 3: the tension is maintained for 30 minutes after loading the speed of 10% of the rope breaking strength to 50% of the rope breaking strength;
Step 4: the tension is reduced by 10% of the rope breaking strength per minute to 20% of the rope breaking strength;
Step 5: the tension circulates 300 times between 10% and 30% of the rope breaking strength at a frequency of 0.03 hz to 0.1 hz;
Step 6: at least 7 days under tension of a preselected tension T at a predetermined control temperature, the gauge length should be measured continuously at this time, with the sampling rate being at least once per hour;
After the pre-selected tension T is tensed for a period of time, the creep elongation, creep rate and specific stress value of the rope are calculated by the displacement of the two marks in the middle of the rope sample;
The rope creep test is carried out under the condition of controlling the temperature, the temperature is not more than 25 ℃ and the temperature difference is within the range of 5 ℃;
The distance between two pins of the pin fixing plug-in eye ring sample testing machine is not less than 1800mm;
The tension T is 50 to 20 percent of the breaking strength of the rope, and the deviation range is 0.1 to 1 percent;
the distance between the two marks is not less than 1000mm;
the method for testing the creep performance of the high-modulus polyethylene rope comprises the steps of measuring the creep elongation, the creep rate and the specific stress of the creep performance of the high-modulus polyethylene rope under constant load;
the creep performance of the cable to be tested is calculated by using the following formula:
A. creep elongation:
G=[(l-l2)/l2]×100%
Wherein:
G is creep elongation,%; l is the gauge length under the pre-selected tension T tension in the step 6, and the unit is millimeter; l 2 is the gauge length in millimeters when breaking the strength 2% in the step 1;
B. Creep rate:
Gt=G/h
Wherein: g t is creep rate,%/h; g is creep elongation; h is creep time in hours;
C. specific stress:
SC=T/ρ
Wherein: sc is the specific stress of the rope in Newton/tex; t is a preselected tension in kilonewtons; ρ is the linear density of the rope in kilo [ tex ].
2. The method for testing the creep property of the high-modulus polyethylene rope according to claim 1, wherein the method for testing the creep property of the high-modulus polyethylene rope is used for establishing a document model of the creep property of the high-modulus polyethylene rope with different breaking strength and various linear densities; from this model, creep data of the rope sample can be obtained, creep expectation per year, cumulative creep elongation of the whole rope design life can be predicted, and the ratio of the rope creep rate to the fiber creep of the rope sample can be obtained by comparison under the same specific stress and temperature conditions.
3. The method of testing the creep properties of a high modulus polyethylene rope according to claim 2, wherein said creep data comprises at least creep rate, allowable creep elongation and time.
4. The method for testing creep properties of a high modulus polyethylene rope according to claim 1, wherein said method for measuring and calculating creep properties of a high modulus polyethylene rope comprises:
the following 3 gauge lengths were measured:
4.1 Step 2-4), measuring the gauge length of the tensile load;
4.2 In step 5), measuring the gauge length of the cyclic load;
4.3 In step 6), the gauge length and the completion time under tension T are preselected.
5. The method for testing creep properties of a high modulus polyethylene rope according to claim 1, wherein said method for testing creep properties of a high modulus polyethylene rope comprises the following contents or steps:
5.1 Temperature control;
5.2 Sample preparation and initial measurement;
5.3 A testing machine regulates and controls;
5.4 Test preparation;
5.5 Creep performance test;
5.6 Calculation of the creep properties of the rope;
5.7 Record the data that should be recorded.
6. The method for testing creep properties of a high modulus polyethylene rope according to claim 5, wherein
A. The temperature control comprises controlling the temperature of a laboratory to ensure that the temperature is not more than 25 ℃ and the temperature difference is within the range of 5 ℃;
B. The sample preparation and initial measurement comprises the steps of intercepting a sample with the length of 2 meters and 10 lay lengths of a rope, measuring the initial length L 0 and the weighing mass m, marking two r marks with the distance of not less than 1 meter at the middle part, and measuring the initial gauge length L 0;
C. the regulation and control of the testing machine comprise a testing machine for fixing rope samples to be inserted into eye rings by adopting pins, wherein the distance between the two pins is not less than 1800mm; wherein, the stretching speed of the tester; the speed is regulated by a motor to meet the requirement of loading speed when the preselected tension T is constant before tensioning the sample; when the preselected tension T is in tension on the sample, the speed is low, and the preselected tension T fluctuates within the 0.1-1% range due to the micro speed or the shutdown of the motor speed regulation so as to achieve the effect of constant load;
D. the test preparation comprises:
d1 A test sample is arranged on a testing machine;
D2 An extensometer is arranged between the rope marks, and the focal length and the aperture of the camera are adjusted;
d3 2% of the rope breaking strength is applied, and the gauge length l 2 is measured;
E. the creep performance test comprises the following steps:
e1 Eliminating structural elongation of the rope;
E2 Measuring steady state creep at constant tension;
E3 The sample should be unloaded after the test is completed.
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Denomination of invention: A method for testing the creep performance of high modulus polyethylene ropes

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