CN115821588A - Fabric finishing agent for modal fabric and finishing method - Google Patents
Fabric finishing agent for modal fabric and finishing method Download PDFInfo
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Abstract
本发明涉及织物整理的技术领域，提供了一种莫代尔面料用织物整理剂及整理方法。本发明的织物整理剂是通过先制备以乙醇为溶剂的氨基硅溶胶，然后通过氨基与对醛基苯甲酸反应，再与Ag+络合而制得。利用该织物整理剂对莫代尔面料进行整理的步骤包括浸轧、烘干、烘焙，其中，烘焙的温度为200‑220℃。本发明的整理剂及整理方法可赋予莫代尔面料良好的抗起毛起球效果和抗菌性，并且具有良好的耐水洗性。The invention relates to the technical field of fabric finishing, and provides a fabric finishing agent for modal fabrics and a finishing method. The fabric finishing agent of the present invention is prepared by firstly preparing amino silica sol with ethanol as a solvent, then reacting amino groups with p-aldehyde benzoic acid, and then complexing with Ag + . The steps of using the fabric finishing agent to finish the modal fabric include padding, drying and baking, wherein the baking temperature is 200-220°C. The finishing agent and the finishing method of the invention can endow the modal fabric with good anti-pilling effect and antibacterial property, and has good washing resistance.
Description
技术领域technical field
本发明涉及织物整理的技术领域，提供了一种莫代尔面料用织物整理剂及整理方法。The invention relates to the technical field of fabric finishing, and provides a fabric finishing agent for modal fabrics and a finishing method.
背景技术Background technique
莫代尔面料是一种能够自然降解的环保性纺织品，其干强与涤纶接近，湿强高于普通胶粘纤维，吸湿性、染色性、柔软性、悬垂感等好于纯棉纤维，既具有天然纤维的优良质感，又具有合成纤维的实用性。莫代尔面料能够满足人们对服饰穿着舒适度的要求，越来越受到人们的喜爱。Modal fabric is an environmentally friendly textile that can be naturally degraded. Its dry strength is close to that of polyester, its wet strength is higher than that of ordinary adhesive fibers, and its hygroscopicity, dyeability, softness, and drape are better than pure cotton fibers. It has natural The fine texture of fiber has the practicality of synthetic fiber. Modal fabrics can meet people's requirements for clothing comfort, and are more and more popular.
莫代尔面料也有自身的缺点，比如容易起毛起球。起毛起球是指织物在加工和使用过程中，由于机械摩擦等作用，纤维头端滑出从而显露于织物表面（即起毛），相邻纤维进一步缠结在一起，形成小球（即起球）。由于莫代尔纤维内部的无定型区占比较高，并且其纤维截面为圆形，表面较为光滑，纵向无卷曲，导致纤维间的抱合力较小，因而纤维头更容易滑出并突出在纱线表面，即容易起毛起球，其起毛起球等级仅为1-2级。Modal fabrics also have their own disadvantages, such as easy pilling. Pilling refers to that during the processing and use of the fabric, due to mechanical friction and other effects, the fiber end slips out and is exposed on the surface of the fabric (that is, fluffing), and adjacent fibers are further entangled together to form small balls (that is, pilling). ). Due to the relatively high proportion of the amorphous area inside the modal fiber, and its fiber cross-section is round, the surface is relatively smooth, and there is no curl in the longitudinal direction, resulting in less cohesion between the fibers, so the fiber ends are easier to slide out and protrude on the surface of the yarn , that is, it is easy to pilling, and its pilling grade is only 1-2.
另外，从应用角度讲，莫代尔面料目前主要用于内衣、运动服饰、家纺用品中，由于内衣属于贴身衣物，运动衣经常接触大量汗液，家纺用品往往需要隔段时间更换，因而，与普通场合相比，用于这些场合的面料需要有更高的抗菌要求，也就是需要提高莫代尔面料的抗菌性能。In addition, from an application point of view, modal fabrics are currently mainly used in underwear, sportswear, and home textiles. Since underwear is close-fitting clothing, sportswear is often exposed to a lot of sweat, and home textiles often need to be replaced at regular intervals. Compared with that, the fabrics used in these occasions need to have higher antibacterial requirements, that is, the antibacterial properties of Modal fabrics need to be improved.
发明内容Contents of the invention
本发明提出一种莫代尔面料用织物整理剂及整理方法，其目的在于赋予莫代尔面料良好的抗起毛起球效果和抗菌性。The invention proposes a fabric finishing agent and a finishing method for modal fabrics, the purpose of which is to endow modal fabrics with good anti-pilling effect and antibacterial properties.
为实现上述目的，本发明涉及的具体技术方案如下：To achieve the above object, the specific technical solutions involved in the present invention are as follows:
一种莫代尔面料用织物整理剂，所述织物整理剂的制备包括以下步骤：A fabric finishing agent for modal fabrics, the preparation of said fabric finishing agent may further comprise the steps:
（1）将氨丙基三甲氧基硅烷、乙醇、去离子水混合，搅拌均匀，静置至泡沫消失，加入氯化钠搅拌溶解，再将溶液调节至中性，在30℃搅拌60-90min，加入3A分子筛，密闭静置30-60min，过滤，得到硅溶胶；(1) Mix aminopropyltrimethoxysilane, ethanol, and deionized water, stir evenly, let it stand until the foam disappears, add sodium chloride and stir to dissolve, then adjust the solution to neutral, and stir at 30°C for 60-90min , add 3A molecular sieve, airtightly stand for 30-60min, filter to obtain silica sol;
（2）向步骤（1）制得的硅溶胶中加入乙酸，然后缓慢滴加对醛基苯甲酸的乙醇溶液，室温反应90-120min，再缓慢滴入醋酸银的乙醇分散液，加热到60℃反应120-150min，得到织物整理剂。(2) Add acetic acid to the silica sol prepared in step (1), then slowly drop the ethanol solution of p-aldehyde benzoic acid, react at room temperature for 90-120min, then slowly drop the ethanol dispersion of silver acetate, heat to 60 ℃ for 120-150min to obtain a fabric finishing agent.
步骤（1）是制备以乙醇为溶剂的硅溶胶的过程。该过程以氨丙基三甲氧基硅烷为前驱体，得到的硅溶胶为氨基硅溶胶。优选的，步骤（1）中的氨丙基三甲氧基硅烷、乙醇、去离子水、氯化钠的摩尔比为0.4-0.6：30：5：1。由于步骤（1）的硅烷水解缩合需要水的参与，而水的存在对步骤（2）的脱水反应不利，因此，先以乙醇、去离子水作为混合溶剂进行硅烷的水解缩合，再采用3A分子筛去除去离子水，得到以乙醇为溶剂的氨基硅溶胶。优选的，3A分子筛的用量为去离子水质量的6-8倍。Step (1) is the process of preparing silica sol with ethanol as solvent. The process uses aminopropyltrimethoxysilane as a precursor, and the obtained silica sol is amino silica sol. Preferably, the molar ratio of aminopropyltrimethoxysilane, ethanol, deionized water, and sodium chloride in step (1) is 0.4-0.6:30:5:1. Since the hydrolysis and condensation of silane in step (1) requires the participation of water, and the presence of water is unfavorable to the dehydration reaction in step (2), therefore, first use ethanol and deionized water as a mixed solvent for the hydrolysis and condensation of silane, and then use 3A molecular sieve Remove deionized water to obtain amino silica sol with ethanol as solvent. Preferably, the amount of 3A molecular sieve is 6-8 times the mass of deionized water.
步骤（2）包括两个过程：一是以乙酸为催化剂，硅溶胶中的氨基与对醛基苯甲酸的醛基发生醛胺缩合反应，公知的，醛基与氨基容易反应（室温下即可）脱除水，并生成-CH=N-（希夫碱）；二是-CH=N-中的N与Ag+发生配位络合的过程。优选的，步骤（2）中的对醛基苯甲酸、醋酸银、乙酸与步骤（1）中的氨丙基三甲氧基硅烷的摩尔比为1：0.5：0.02：1。优选的，对醛基苯甲酸的乙醇溶液中，对醛基苯甲酸、乙醇的摩尔比为1：15-20。优选的，醋酸银的乙醇分散液中，醋酸银、乙醇的摩尔比为1：15-20。Step (2) includes two processes: one is using acetic acid as a catalyst, and the amino group in the silica sol reacts with the aldehyde group of p-formylbenzoic acid to undergo an aldehyde-amine condensation reaction. It is known that the aldehyde group and the amino group are easy to react (it can be ) to remove water and generate -CH=N- (Schiff base); the second is the process of coordination complexation between N in -CH=N- and Ag + . Preferably, the molar ratio of p-formylbenzoic acid, silver acetate, acetic acid in step (2) to aminopropyltrimethoxysilane in step (1) is 1:0.5:0.02:1. Preferably, in the ethanol solution of p-aldehyde benzoic acid, the molar ratio of p-aldehyde benzoic acid to ethanol is 1:15-20. Preferably, in the ethanol dispersion of silver acetate, the molar ratio of silver acetate to ethanol is 1:15-20.
一种莫代尔面料用织物整理方法，步骤包括浸轧、烘干、烘焙。A fabric finishing method for modal fabrics, the steps of which include padding, drying and baking.
其中，所述浸轧采用上述织物整理剂，浴比为1：20-30，时间为20-30min，带液率为70-75%。Wherein, the above-mentioned fabric finishing agent is used in the padding, the bath ratio is 1:20-30, the time is 20-30min, and the liquid carrying rate is 70-75%.
优选的，所述烘干的温度为65-70℃，时间为3-5min。Preferably, the drying temperature is 65-70° C. and the drying time is 3-5 minutes.
所述烘焙的温度为200-220℃，时间为2-4min。The temperature of the baking is 200-220° C., and the time is 2-4 minutes.
采用上述织物整理剂对莫代尔面料进行整理，具有以下效果：第一，由于聚硅氧烷具有良好的成膜性，随着溶剂蒸发，聚硅氧烷在面料表面形成网络状膜层，可降低面料表面摩擦系数，减小面料与物体之间的摩擦，从而防止纤维头端滑出外露，再加上通过对醛基苯甲酸引入了苯环，可提高膜层硬度，使膜层更为耐磨，可更好地防止纤维头端滑出，起到良好的抗起毛起球效果；第二，由于-CH=N-与Ag+的络合物具有良好的抗菌性能，可赋予莫代尔面料良好的抗菌性，使其更适合用于内衣、运动服饰、家纺用品等场合；第三，在氨基聚硅氧烷与对醛基苯甲酸的醛基反应后，在结构上引入了羧基，在烘焙过程中，羧基与莫代尔面料上的羟基（纤维素的羟基）可发生一定程度的缩合，有利于聚硅氧烷膜层在面料表面牢固附着，因而具有良好的耐水洗性。Using the above-mentioned fabric finishing agent to finish Modal fabrics has the following effects: First, because polysiloxane has good film-forming properties, as the solvent evaporates, polysiloxane forms a network-like film on the surface of the fabric, which can reduce The surface friction coefficient of the fabric reduces the friction between the fabric and the object, thereby preventing the fiber end from slipping out and exposing. In addition, the benzene ring is introduced through p-aldehyde benzoic acid, which can increase the hardness of the film layer and make the film layer more durable. Grinding can better prevent the fiber head from slipping out and play a good anti-pilling effect; second, because the complex of -CH=N- and Ag + has good antibacterial properties, it can endow Modal fabrics with good antibacterial properties. The antibacterial properties make it more suitable for underwear, sportswear, home textiles and other occasions; third, after the reaction of amino polysiloxane with the aldehyde group of p-aldehyde benzoic acid, a carboxyl group is introduced in the structure, and it is baked During the process, the carboxyl group and the hydroxyl group on the modal fabric (the hydroxyl group of cellulose) can condense to a certain extent, which is conducive to the firm attachment of the polysiloxane film layer on the surface of the fabric, so it has good washing resistance.
本发明提供了一种莫代尔面料用织物整理剂及整理方法，与现有技术相比，其突出的特点和优异的效果在于：本发明先制备了以乙醇为溶剂的氨基硅溶胶，然后通过氨基与对醛基苯甲酸反应，再与Ag+络合，制得织物整理剂。通过聚硅氧烷在面料表面成膜，可防止纤维头端滑出外露，起到抗起毛起球的效果。通过-CH=N-与Ag+的络合赋予面料良好的抗菌性。并且，由于整理剂聚硅氧烷的结构上含有羧基，可通过羧基与纤维素羟基的缩合实现聚硅氧烷膜层在面料表面牢固附着，具有良好的耐水洗性。The invention provides a fabric finishing agent and a finishing method for Modal fabrics. Compared with the prior art, its outstanding features and excellent effects are: the invention firstly prepares amino silica sol with ethanol as a solvent, and then passes amino React with p-aldehyde benzoic acid, and then complex with Ag + to prepare fabric finishing agent. The polysiloxane is used to form a film on the surface of the fabric, which can prevent the fiber end from slipping out and have an anti-pilling effect. The complexation of -CH=N- with Ag + endows the fabric with good antibacterial properties. Moreover, since the structure of the finishing agent polysiloxane contains carboxyl groups, the polysiloxane film layer can be firmly attached to the surface of the fabric through the condensation of carboxyl groups and cellulose hydroxyl groups, and has good washing resistance.
具体实施方式Detailed ways
以下通过具体实施方式对本发明作进一步的详细说明，但不应将此理解为本发明的范围仅限于以下的实例。在不脱离本发明上述方法思想的情况下，根据本领域普通技术知识和惯用手段做出的各种替换或变更，均应包含在本发明的范围内。The present invention will be further described in detail through specific embodiments below, but it should not be understood that the scope of the present invention is limited to the following examples. Without departing from the above-mentioned method idea of the present invention, various replacements or changes made according to common technical knowledge and customary means in this field shall be included in the scope of the present invention.
实施例1Example 1
整理剂制备：（1）将0.05mol氨丙基三甲氧基硅烷、3mol乙醇、0.5mol去离子水混合，搅拌均匀，静置至泡沫消失，加入0.1mol氯化钠搅拌溶解，再将溶液调节至中性，在30℃搅拌90min，加入54g3A分子筛，密闭静置30min，过滤，得到硅溶胶；（2）向步骤（1）制得的硅溶胶中加入0.001mol乙酸，然后缓慢滴加含0.05mol对醛基苯甲酸的乙醇溶液（乙醇为1mol），室温反应90min，再缓慢滴入含0.025mol醋酸银的乙醇分散液（乙醇为0.5mol），加热到60℃反应150min，得到织物整理剂。Finishing agent preparation: (1) Mix 0.05mol aminopropyltrimethoxysilane, 3mol ethanol, and 0.5mol deionized water, stir evenly, let stand until the foam disappears, add 0.1mol sodium chloride and stir to dissolve, then adjust the solution To neutrality, stir at 30°C for 90 minutes, add 54g of 3A molecular sieves, seal and stand for 30 minutes, and filter to obtain silica sol; (2) Add 0.001mol acetic acid to the silica sol prepared in step (1), and then slowly add 0.05 1mol ethanol solution of p-aldehyde benzoic acid (1mol ethanol), react at room temperature for 90min, then slowly drop into ethanol dispersion containing 0.025mol silver acetate (0.5mol ethanol), heat to 60°C and react for 150min to obtain fabric finishing agent .
整理过程：（1）浸轧，剪取16cm×16cm的莫代尔面料（40s拉架平纹布），以上述整理剂进行浸轧，浴比为1：25，时间为30min，带液率为75%；（2）烘干，温度为65℃，时间为3min；（3）烘焙，温度为200℃，时间为2min。Finishing process: (1) padding, cut 16cm×16cm modal fabric (40s frame plain weave), padding with the above finishing agent, the bath ratio is 1:25, the time is 30min, and the liquid retention rate is 75%; (2) drying at a temperature of 65°C for 3 minutes; (3) baking at a temperature of 200°C for 2 minutes.
实施例2Example 2
整理剂制备：（1）将0.05mol氨丙基三甲氧基硅烷、3mol乙醇、0.5mol去离子水混合，搅拌均匀，静置至泡沫消失，加入0.1mol氯化钠搅拌溶解，再将溶液调节至中性，在30℃搅拌80min，加入54g3A分子筛，密闭静置30min，过滤，得到硅溶胶；（2）向步骤（1）制得的硅溶胶中加入0.001mol乙酸，然后缓慢滴加含0.05mol对醛基苯甲酸的乙醇溶液（乙醇为1mol），室温反应100min，再缓慢滴入含0.025mol醋酸银的乙醇分散液（乙醇为0.5mol），加热到60℃反应140min，得到织物整理剂。Finishing agent preparation: (1) Mix 0.05mol aminopropyltrimethoxysilane, 3mol ethanol, and 0.5mol deionized water, stir evenly, let stand until the foam disappears, add 0.1mol sodium chloride and stir to dissolve, then adjust the solution To neutrality, stir at 30°C for 80 minutes, add 54g of 3A molecular sieves, seal and stand for 30 minutes, and filter to obtain silica sol; (2) Add 0.001mol acetic acid to the silica sol prepared in step (1), and then slowly add 0.05 1mol ethanol solution of p-formylbenzoic acid (1mol ethanol), react at room temperature for 100min, then slowly drop into ethanol dispersion containing 0.025mol silver acetate (0.5mol ethanol), heat to 60°C and react for 140min to obtain fabric finishing agent .
整理过程：（1）浸轧，剪取同上的莫代尔面料，以上述整理剂进行浸轧，浴比为1：25，时间为27min，带液率为73%；（2）烘干，温度为65℃，时间为3min；（3）烘焙，温度为210℃，时间为2min。Finishing process: (1) padding, cut the modal fabric as above, and padding with the above finishing agent, the liquor ratio is 1:25, the time is 27min, and the liquid retention rate is 73%; (2) drying, the temperature is 65°C for 3 minutes; (3) Baking at 210°C for 2 minutes.
实施例3Example 3
整理剂制备：（1）将0.05mol氨丙基三甲氧基硅烷、3mol乙醇、0.5mol去离子水混合，搅拌均匀，静置至泡沫消失，加入0.1mol氯化钠搅拌溶解，再将溶液调节至中性，在30℃搅拌70min，加入54g3A分子筛，密闭静置30min，过滤，得到硅溶胶；（2）向步骤（1）制得的硅溶胶中加入0.001mol乙酸，然后缓慢滴加含0.05mol对醛基苯甲酸的乙醇溶液（乙醇为1mol），室温反应110min，再缓慢滴入含0.025mol醋酸银的乙醇分散液（乙醇为0.5mol），加热到60℃反应130min，得到织物整理剂。Finishing agent preparation: (1) Mix 0.05mol aminopropyltrimethoxysilane, 3mol ethanol, and 0.5mol deionized water, stir evenly, let stand until the foam disappears, add 0.1mol sodium chloride and stir to dissolve, then adjust the solution To neutrality, stir at 30°C for 70 minutes, add 54g of 3A molecular sieves, seal and stand for 30 minutes, and filter to obtain silica sol; (2) Add 0.001mol acetic acid to the silica sol prepared in step (1), and then slowly add 0.05 1mol ethanol solution of p-aldehyde benzoic acid (1mol ethanol), react at room temperature for 110min, then slowly drop into ethanol dispersion containing 0.025mol silver acetate (0.5mol ethanol), heat to 60°C and react for 130min, to obtain fabric finishing agent .
整理过程：（1）浸轧，剪取同上的莫代尔面料，以上述整理剂进行浸轧，浴比为1：25，时间为24min，带液率为72%；（2）烘干，温度为65℃，时间为3min；（3）烘焙，温度为210℃，时间为4min。Finishing process: (1) padding, cut the modal fabric as above, and padding with the above finishing agent, the liquor ratio is 1:25, the time is 24min, and the liquid retention rate is 72%; (2) drying, the temperature is 65°C for 3 minutes; (3) Baking at 210°C for 4 minutes.
实施例4Example 4
整理剂制备：（1）将0.05mol氨丙基三甲氧基硅烷、3mol乙醇、0.5mol去离子水混合，搅拌均匀，静置至泡沫消失，加入0.1mol氯化钠搅拌溶解，再将溶液调节至中性，在30℃搅拌60min，加入54g3A分子筛，密闭静置30min，过滤，得到硅溶胶；（2）向步骤（1）制得的硅溶胶中加入0.001mol乙酸，然后缓慢滴加含0.05mol对醛基苯甲酸的乙醇溶液（乙醇为1mol），室温反应120min，再缓慢滴入含0.025mol醋酸银的乙醇分散液（乙醇为0.5mol），加热到60℃反应120min，得到织物整理剂。Finishing agent preparation: (1) Mix 0.05mol aminopropyltrimethoxysilane, 3mol ethanol, and 0.5mol deionized water, stir evenly, let stand until the foam disappears, add 0.1mol sodium chloride and stir to dissolve, then adjust the solution To neutrality, stir at 30°C for 60 minutes, add 54g of 3A molecular sieves, airtightly stand for 30 minutes, and filter to obtain silica sol; (2) Add 0.001mol acetic acid to the silica sol prepared in step (1), and then slowly dropwise add 1mol ethanol solution of p-aldehyde benzoic acid (1mol ethanol), react at room temperature for 120min, then slowly drop into ethanol dispersion containing 0.025mol silver acetate (0.5mol ethanol), heat to 60°C and react for 120min to obtain fabric finishing agent .
整理过程：（1）浸轧，剪取同上的莫代尔面料，以上述整理剂进行浸轧，浴比为1：25，时间为20min，带液率为70%；（2）烘干，温度为65℃，时间为3min；（3）烘焙，温度为220℃，时间为4min。Finishing process: (1) padding, cutting the same modal fabric as above, and padding with the above finishing agent, the bath ratio is 1:25, the time is 20min, and the liquid retention rate is 70%; (2) drying, the temperature is 65°C for 3 minutes; (3) Baking at 220°C for 4 minutes.
性能测试：Performance Testing:
（1）按照GB/T 4802.1-2008《纺织品 织物起毛起球性能的测定 第1部分：圆轨迹法》的方法测试面料的起毛起球等级，按GB/T 8629-2017 中的家庭洗涤及干燥程序对面料分别进行20次、50次水洗，再测试起毛起球等级；（2）按照GB/T 20944.3-2008《纺织品 抗菌性能的评价 第3部分：振荡法》的方法测试面料对金黄色葡萄球菌的抑菌率，并在水洗20次、50次后再次测试抑菌率。所得数据如表1所示。(1) According to the method of GB/T 4802.1-2008 "Determination of the Pilling Properties of Textile Fabrics Part 1: Circular Track Method", the pilling level of the fabric is tested, according to the domestic washing and drying in GB/T 8629-2017 The program washes the fabric 20 times and 50 times respectively, and then tests the pilling level; (2) According to the method of GB/T 20944.3-2008 "Evaluation of Antibacterial Properties of Textiles Part 3: Oscillating Method", the fabric is tested for golden yellow grape The antibacterial rate of the coccus, and the antibacterial rate was tested again after washing 20 times and 50 times. The obtained data are shown in Table 1.
表1：Table 1:
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| CN104480696A (en) * | 2014-12-01 | 2015-04-01 | 江苏金太阳纺织科技有限公司 | Anti-sliding finishing agent for regenerated cellulose fiber fabric, working fluid and anti-sliding finishing process |
| CN105926275A (en) * | 2016-05-18 | 2016-09-07 | 江苏阳光集团有限公司 | Antibacterial and mildew-resistant finishing method of wool cotton fabric |
| CN110306340A (en) * | 2019-05-16 | 2019-10-08 | 北京化工大学 | Antibacterial natural textile material with surface modified borneol and its preparation method and application |
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| CN104480696A (en) * | 2014-12-01 | 2015-04-01 | 江苏金太阳纺织科技有限公司 | Anti-sliding finishing agent for regenerated cellulose fiber fabric, working fluid and anti-sliding finishing process |
| CN105926275A (en) * | 2016-05-18 | 2016-09-07 | 江苏阳光集团有限公司 | Antibacterial and mildew-resistant finishing method of wool cotton fabric |
| CN110306340A (en) * | 2019-05-16 | 2019-10-08 | 北京化工大学 | Antibacterial natural textile material with surface modified borneol and its preparation method and application |
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