CN116219742A - Antibacterial yarn and its production process and acetate fabric - Google Patents

Antibacterial yarn and its production process and acetate fabric Download PDF

Info

Publication number
CN116219742A
CN116219742A CN202310329423.7A CN202310329423A CN116219742A CN 116219742 A CN116219742 A CN 116219742A CN 202310329423 A CN202310329423 A CN 202310329423A CN 116219742 A CN116219742 A CN 116219742A
Authority
CN
China
Prior art keywords
antibacterial
extract
surfactant
polyester
fabric
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202310329423.7A
Other languages
Chinese (zh)
Inventor
黄振亚
陈海连
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Dingshang Textile Co ltd
Original Assignee
Shenzhen Dingshang Textile Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Dingshang Textile Co ltd filed Critical Shenzhen Dingshang Textile Co ltd
Priority to CN202310329423.7A priority Critical patent/CN116219742A/en
Publication of CN116219742A publication Critical patent/CN116219742A/en
Pending legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02GCRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/04Blended or other yarns or threads containing components made from different materials
    • D02G3/045Blended or other yarns or threads containing components made from different materials all components being made from artificial or synthetic material
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02GCRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/44Yarns or threads characterised by the purpose for which they are designed
    • D02G3/449Yarns or threads with antibacterial properties
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • D06M2101/08Esters or ethers of cellulose
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/20Cellulose-derived artificial fibres
    • D10B2201/28Cellulose esters or ethers, e.g. cellulose acetate
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/13Physical properties anti-allergenic or anti-bacterial
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention relates to the technical field of textile, and particularly discloses antibacterial yarns, a manufacturing process thereof and an acetate fabric. The manufacturing process of the antibacterial yarn comprises the following steps: step 1), blending acetate fiber and polyester fiber to obtain polyester blend; step 2), drying after the polyester blended soaking treatment liquid to obtain antibacterial yarns; the treatment fluid comprises the following components in parts by mass: 100 parts of water; 1-1.2 parts of plant composite extract; 5-6 parts of a surfactant; the plant compound extract is prepared by compounding herba Eichhorniae, cortex Cinnamomi Japonici and herba Houttuyniae and extracting. The invention has the advantage of enabling the fabric to have lasting antibacterial effect.

Description

抑菌纱线及其制作工艺及醋酸面料Antibacterial yarn and its production process and acetate fabric

技术领域technical field

本发明涉及纺织领域,尤其是涉及一种抑菌纱线及其制作工艺及醋酸面料。The invention relates to the field of textiles, in particular to an antibacterial yarn, a production process thereof and an acetate fabric.

背景技术Background technique

醋酸面料是由醋酸纤维纺织而成的面料,而醋酸纤维则是以醋酸和纤维素作为原料经酯化反应制得的人造纤维,具有良好的热塑性、酷似真丝的光泽、不易产生静电等优良性能,但醋酸纤维的拉伸强度较差,单纯用醋酸纤维纺织而成的面料较为容易破损。Acetate fabric is a fabric woven from acetate fiber, and acetate fiber is a man-made fiber made from acetate and cellulose through esterification reaction. It has good thermoplasticity, silk-like luster, and is not easy to generate static electricity. , but the tensile strength of acetate fiber is poor, and the fabric made of acetate fiber is more likely to be damaged.

涤纶纤维则是由聚对苯二甲酸(PTA)或对苯二甲酸二甲酯(DMT)和乙二醇(MEG)为原料,经酯化或酯交换和缩聚反应而制得的成纤高聚物——聚对苯二甲酸乙二醇酯(PET),经纺丝和后处理制成的纤维,涤纶纤维具有高强度、热稳定性好、耐皱、耐磨等优点,但是涤纶纤维由于低吸水性,容易产生静电。Polyester fiber is made of polyterephthalic acid (PTA) or dimethyl terephthalate (DMT) and ethylene glycol (MEG) as raw materials, through esterification or transesterification and polycondensation. Polymer——polyethylene terephthalate (PET), a fiber made by spinning and post-processing, polyester fiber has the advantages of high strength, good thermal stability, wrinkle resistance, wear resistance, etc., but polyester fiber Static electricity is easily generated due to low water absorption.

因此,通过将醋酸纤维和涤纶纤维混纺,能进行性能互补,但是醋酸纤维和涤纶纤维均缺乏抗菌抑菌的性能,混纺后制得的面料在抗菌性能上还有较大欠缺,难以满足消费者需求,因此还有改善空间。Therefore, by blending acetate fiber and polyester fiber, the performance can be complemented, but both acetate fiber and polyester fiber lack antibacterial and antibacterial properties, and the fabric obtained after blending still has a large lack of antibacterial performance, which is difficult to satisfy consumers. demand, so there is still room for improvement.

发明内容Contents of the invention

为了使面料具有持久的抑菌功效,本申请提供一种抑菌纱线及其制作工艺及醋酸面料。In order to make the fabric have a lasting antibacterial effect, the application provides an antibacterial yarn and its manufacturing process and acetate fabric.

第一方面,本申请提供一种抑菌纱线的制作工艺,采用如下的技术方案:In the first aspect, the application provides a manufacturing process of antibacterial yarn, adopting the following technical scheme:

一种抑菌纱线的制作工艺,包括以下步骤:A manufacturing process of antibacterial yarn, comprising the following steps:

步骤1),将醋酸纤维和涤纶纤维混纺,得涤纶混纺;Step 1), blending acetate fibers and polyester fibers to obtain polyester blends;

步骤2),涤纶混纺浸泡处理液后烘干,得抑菌纱线;Step 2), the polyester blended fabric is soaked in the treatment solution and then dried to obtain antibacterial yarn;

所述处理液包括以下质量份数的组分:The treatment liquid includes the following components in parts by mass:

水100份;100 parts of water;

植物复合提取物1-1.2份;Plant compound extract 1-1.2 parts;

表面活性剂5-6份;5-6 parts of surfactant;

所述植物复合提取物由凤眼草、桂皮、鱼腥草复配后提取所得。The plant compound extract is obtained by compounding water hyacinth, cassia bark and houttuynia cordata.

通过采用上述技术方案,通过醋酸纤维和涤纶纤维混纺,制得的抑菌纱线具有较高的强度,耐高温染色,不易产生静电,染色效果较佳,从而使制得的面料质量较好。By adopting the above technical scheme, the antibacterial yarn prepared by blending acetate fiber and polyester fiber has high strength, high temperature dyeing resistance, is not easy to generate static electricity, and has better dyeing effect, so that the quality of the prepared fabric is better.

通过将涤纶混纺浸泡处理液后烘干,使得抑菌纱线通过处理液处理后能改善抑菌纱线的性能,由于处理液中含有植物复合提取物和表面活性剂,通过表面活性剂使得植物复合提取物中的抑菌成分能牢固地粘附在抑菌纱线表面,使得制得的面料在多次水洗后,仍能保持持久的抑菌功效。By soaking the polyester blend in the treatment solution and then drying, the antibacterial yarn can improve the performance of the antibacterial yarn after being treated with the treatment solution. Since the treatment solution contains plant compound extracts and surfactants, the surfactant can make the plants The antibacterial components in the composite extract can firmly adhere to the surface of the antibacterial yarn, so that the prepared fabric can still maintain a long-lasting antibacterial effect after repeated washing.

通过凤眼草、桂皮、鱼腥草复配,抑菌效果较佳,尤其适合与由醋酸纤维和涤纶纤维混纺而成的抑菌纱线,与抑菌纱线的相容性较好,且复配后的有效成分能更好地配合表面活性剂从而牢固地粘附在抑菌纱线表面,水洗时不易溶于水中而离开抑菌纱线,从而使得面料的抑菌效果更为持久,而且通过凤眼草、桂皮、鱼腥草复配后提取,提取物相互协同配合,不易产生异味,尤其是鱼腥草本身带有明显的异味,但经过复配后,能有效消除,使得面料带有持久抑菌功效的同时不易产生异味,减少因异味影响使用的情况。The combination of water hyacinth, cinnamon and houttuynia has better antibacterial effect, especially suitable for antibacterial yarn blended with acetate fiber and polyester fiber, and has better compatibility with antibacterial yarn, and The compounded active ingredients can better cooperate with the surfactant to firmly adhere to the surface of the antibacterial yarn. It is not easy to dissolve in water and leave the antibacterial yarn during washing, so that the antibacterial effect of the fabric is more durable. Moreover, through the compound extraction of water hyacinth, cinnamon, and houttuynia, the extracts cooperate with each other, and it is not easy to produce peculiar smell, especially the obvious peculiar smell of houttuynia itself, but after compounding, it can be effectively eliminated, making the fabric With long-lasting antibacterial effect, it is not easy to produce peculiar smell, reducing the situation that the use is affected by peculiar smell.

优选的,所述凤眼草、桂皮、鱼腥草的质量比例为1:4-5:0.5-1。Preferably, the mass ratio of the water hyacinth, cinnamon and houttuynia is 1:4-5:0.5-1.

通过采用上述技术方案,通过凤眼草、桂皮、鱼腥草以特定比例复配,抑菌效果更佳,无需在抑菌纱线上附着大量的提取物,具有更高的经济效益。By adopting the above-mentioned technical scheme, by compounding water hyacinth, cinnamon, and houttuynia in a specific ratio, the antibacterial effect is better, and there is no need to attach a large amount of extracts to the antibacterial yarn, which has higher economic benefits.

优选的,所述植物复合提取物的提取方法如下:Preferably, the extraction method of the plant compound extract is as follows:

步骤1),将凤眼草、桂皮、鱼腥草切碎,混匀,得复合药材;Step 1), chopping water hyacinth, cassia bark, and houttuynia cordata, and mixing them evenly to obtain compound medicinal materials;

步骤2),将复合药材投入浓度为35-45%的乙醇溶液中,乙醇溶液的质量为复合药材投入质量的2-3倍,常温搅拌1-2h,冷却至-30℃及以下,保持1-2h,升温并恒温70-75℃,搅拌8-10h,过滤,得提取液;Step 2), put the composite medicinal material into an ethanol solution with a concentration of 35-45%, the quality of the ethanol solution is 2-3 times the mass of the composite medicinal material, stir at room temperature for 1-2h, cool to -30°C or below, and keep for 1 -2h, heat up and keep the temperature at 70-75°C, stir for 8-10h, filter to obtain the extract;

步骤3),将提取液蒸发浓缩、干燥,得粉状的植物复合提取物。In step 3), the extract is evaporated, concentrated, and dried to obtain a powdered plant compound extract.

通过采用上述技术方案,通过采用乙醇溶液进行提取,使得凤眼草、桂皮、鱼腥草中亲水性和疏水性的物质均能被提取,从而使得提取物的抑菌效果更佳,同时由于醋酸纤维的亲水性更强而涤纶纤维的疏水性更强,从而使得提取物恰好能与抑菌纱线配合,相容性高,粘附牢固,抑菌功效得以持久保持。By adopting the above-mentioned technical scheme and extracting with ethanol solution, the hydrophilic and hydrophobic substances in water hyacinth, cinnamon, and houttuynia can be extracted, so that the antibacterial effect of the extract is better, and at the same time due to Acetate fiber is more hydrophilic and polyester fiber is more hydrophobic, so that the extract can be matched with antibacterial yarn, with high compatibility, strong adhesion, and long-lasting antibacterial effect.

优选的,所述表面活性剂为直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的复配。Preferably, the surfactant is a compound of sodium linear alkylbenzene sulfonate and nonylphenol polyoxyethylene ether.

通过采用上述技术方案,通过直链烷基苯磺酸钠、壬基酚聚氧乙烯醚复配,使得提高提取物与抑菌纱线粘附牢度的效果更佳,制得的面料的抑菌效果更为持久。By adopting the above-mentioned technical scheme, through the compounding of linear alkylbenzene sulfonate and nonylphenol polyoxyethylene ether, the effect of improving the adhesion fastness of the extract to the antibacterial yarn is better, and the antibacterial yarn of the prepared fabric is more effective. Bacteria are more durable.

优选的,所述直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的质量比例为1:2-3。Preferably, the mass ratio of linear alkylbenzene sulfonate to nonylphenol polyoxyethylene ether is 1:2-3.

通过采用上述技术方案,通过具体选择直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的比例,与提取物配合的效果更佳,抑菌纱线的抑菌效果更易保持。By adopting the above technical scheme, by specifically selecting the ratio of linear alkylbenzene sodium sulfonate and nonylphenol polyoxyethylene ether, the effect of combining with the extract is better, and the antibacterial effect of the antibacterial yarn is easier to maintain.

优选的,所述处理液的制备方法如下:Preferably, the preparation method of the treatment liquid is as follows:

步骤1),在水中投入表面活性剂,均质3-5min,停止均质,得表面活性剂溶液;Step 1), put surfactant into water, homogenize for 3-5 minutes, stop homogenization, and obtain surfactant solution;

步骤2),向表面活性剂溶液中投入植物复合提取物,搅拌60-90min,得处理液。In step 2), the plant compound extract is put into the surfactant solution and stirred for 60-90 minutes to obtain the treatment solution.

通过采用上述技术方案,通过均质,使得表面活性剂在水中分散均匀,在通过加入植物复合提取物后长时间搅拌,使得表面活性剂的亲水端或疏水段与对于的植物提取物充分接触,从而使得加强提取物在抑菌纱线中粘附牢度的效果更佳。By adopting the above-mentioned technical scheme, through homogenization, the surfactant is uniformly dispersed in water, and after adding the plant compound extract, it is stirred for a long time, so that the hydrophilic end or hydrophobic segment of the surfactant is fully in contact with the corresponding plant extract , so that the effect of strengthening the adhesion fastness of the extract in the antibacterial yarn is better.

优选的,所述步骤2)中,涤纶混纺浸泡处理液的时间为1分钟及以上。Preferably, in the step 2), the time for soaking the polyester blended fabric in the treatment solution is 1 minute or more.

通过采用上述技术方案,通过浸泡足够的时间,使得处理液中的提取物能牢固粘附在抑菌纱线上,使制得的面料的抑菌效果持久保持。By adopting the above technical scheme and soaking for a sufficient time, the extract in the treatment liquid can firmly adhere to the antibacterial yarn, so that the antibacterial effect of the prepared fabric can be maintained for a long time.

第二方面,本申请提供一种抑菌纱线,采用如下的技术方案:In the second aspect, the application provides a kind of antibacterial yarn, which adopts the following technical scheme:

一种抑菌纱线,由上述的抑菌纱线的制作工艺制得。An antibacterial yarn is prepared by the above-mentioned production process of the antibacterial yarn.

通过采用上述技术方案,抑菌纱线具有较高的强度,耐高温染色,不易产生静电,染色效果较佳,还具有持久的抑菌功效,用于制备面料时,面料的质量更佳。By adopting the above-mentioned technical solution, the antibacterial yarn has high strength, is resistant to high temperature dyeing, is not easy to generate static electricity, has better dyeing effect, and has long-lasting antibacterial effect. When used to prepare fabrics, the quality of fabrics is better.

第三方面,本申请提供一种醋酸面料,采用如下的技术方案:In the third aspect, the application provides an acetate fabric, which adopts the following technical solution:

一种醋酸面料,由上述的抑菌纱线纺织而成。An acetate fabric is woven from the antibacterial yarn mentioned above.

通过采用上述技术方案,醋酸面料具有较高的强度,耐高温染色,不易产生静电,染色效果较佳,还具有持久的抑菌功效,更好地满足消费者的使用需求。By adopting the above-mentioned technical solution, the acetate fabric has high strength, high temperature dyeing resistance, is not easy to generate static electricity, has better dyeing effect, and has a long-lasting antibacterial effect, which better meets the needs of consumers.

综上所述,本申请具有以下有益效果:In summary, the application has the following beneficial effects:

1、由于本申请通过将涤纶混纺浸泡处理液后烘干,使得抑菌纱线通过处理液处理后能改善抑菌纱线的性能,由于处理液中含有植物复合提取物和表面活性剂,通过表面活性剂使得植物复合提取物中的抑菌成分能牢固地粘附在抑菌纱线表面,使得制得的面料在多次水洗后,仍能保持持久的抑菌功效。1. Since this application soaks the polyester blend in the treatment solution and then dries it, the performance of the antibacterial yarn can be improved after the treatment solution is used to treat the antibacterial yarn. Since the treatment solution contains plant compound extracts and surfactants, it can be passed through The surfactant enables the antibacterial ingredients in the plant compound extract to firmly adhere to the surface of the antibacterial yarn, so that the prepared fabric can still maintain a long-lasting antibacterial effect after repeated washing.

2、本申请中优选通过凤眼草、桂皮、鱼腥草以特定比例复配,抑菌效果更佳,无需在抑菌纱线上附着大量的提取物,具有更高的经济效益。2. In this application, it is preferred to compound water hyacinth, cinnamon, and houttuynia in a specific ratio, which has better antibacterial effect and does not need to attach a large amount of extracts to the antibacterial yarn, which has higher economic benefits.

3、本申请中优选通过直链烷基苯磺酸钠、壬基酚聚氧乙烯醚复配,使得提高提取物与抑菌纱线粘附牢度的效果更佳,制得的面料的抑菌效果更为持久。3. In this application, it is preferable to compound linear alkylbenzene sulfonate and nonylphenol polyoxyethylene ether, so that the effect of improving the adhesion fastness of the extract to the antibacterial yarn is better, and the antibacterial yarn of the prepared fabric has a better antibacterial effect. Bacteria are more durable.

具体实施方式Detailed ways

以下结合实施例对本申请作进一步详细说明。The present application will be described in further detail below in conjunction with the examples.

实施例1Example 1

一种抑菌纱线,抑菌纱线的制作工艺包括以下步骤:A kind of antibacterial yarn, the manufacture technology of antibacterial yarn comprises the following steps:

步骤1),将醋酸纤维和涤纶纤维通过集聚纺纱工艺进行混纺,得涤纶混纺,涤纶混纺的支数为48英支,捻度为90捻/10cm,醋酸纤维和涤纶纤维的质量比例为1:1。Step 1), the acetate fiber and the polyester fiber are blended through a compact spinning process to obtain a polyester blend, the count of the polyester blend is 48 pounds, the twist is 90 twists/10cm, and the mass ratio of the acetate fiber to the polyester fiber is 1: 1.

步骤2),涤纶混纺通过辊筒带动经过处理液槽并在处理液槽中浸泡处理液,处理液槽的长度为15m,涤纶混纺沿处理液槽的长度方向运行,涤纶混纺在处理液槽中的运行速度为15m/min,涤纶混纺离开处理液槽后进入烘干机中烘干,收卷得抑菌纱线。Step 2), the polyester blend is driven by the roller through the treatment liquid tank and soaked in the treatment liquid in the treatment liquid tank, the length of the treatment liquid tank is 15m, the polyester blend runs along the length direction of the treatment liquid tank, and the polyester blend is in the treatment liquid tank The running speed is 15m/min. After the polyester blend leaves the treatment liquid tank, it enters the dryer for drying, and the antibacterial yarn is wound up.

其中,醋酸纤维的细度为1.5D,长度41-42mm,为二型醋酯纤维。Among them, the fineness of acetate fiber is 1.5D, the length is 41-42mm, and it is type II acetate fiber.

其中,涤纶纤维的细度为2.5D,长度38-39mm,为聚对苯二甲酸乙二醇纤维。Among them, the fineness of polyester fiber is 2.5D, and the length is 38-39mm, which is polyethylene terephthalate fiber.

其中,处理液为水、植物复合提取物、表面活性剂的复配。Wherein, the treatment solution is a compound of water, plant compound extract and surfactant.

处理液的制备方法如下:The preparation method of the treatment liquid is as follows:

步骤1),在100kg水中投入5kg表面活性剂,均质3min,停止均质,得表面活性剂溶液。In step 1), 5 kg of surfactant is put into 100 kg of water, homogenized for 3 minutes, and the homogenization is stopped to obtain a surfactant solution.

步骤2),向表面活性剂溶液中投入1kg植物复合提取物,搅拌60min,得处理液。In step 2), 1 kg of plant compound extract was put into the surfactant solution, and stirred for 60 minutes to obtain a treatment solution.

其中,植物复合提取物为凤眼草、桂皮、鱼腥草复配后提取所得。Among them, the plant compound extract is extracted from water hyacinth, cinnamon and houttuynia after compounding.

植物复合提取物的提取方法如下:The extraction method of plant compound extract is as follows:

步骤1),将1kg凤眼草、4kg桂皮、0.5kg鱼腥草切碎,混匀,得复合药材。Step 1): Mince 1kg water hyacinth, 4kg cassia bark, and 0.5kg houttuynia cordata, and mix them evenly to obtain a compound medicinal material.

步骤2),将复合药材投入浓度为45%的乙醇溶液中,乙醇溶液的质量为复合药材投入质量的2倍,常温搅拌1h,冷却至-30℃,保持1h,升温并恒温70℃,搅拌10h,通过200目滤布过滤,得提取液。Step 2), put the composite medicinal material into an ethanol solution with a concentration of 45%, the quality of the ethanol solution is twice the mass of the composite medicinal material, stir at room temperature for 1 hour, cool to -30°C, keep for 1 hour, heat up and keep the temperature at 70°C, and stir After 10 hours, filter through a 200-mesh filter cloth to obtain an extract.

步骤3),将提取液旋蒸浓缩,旋蒸温度60℃,压力0.01Mpa,浓缩至膏状,将膏状物在烘箱中加热干燥,得粉状的植物复合提取物。Step 3) Concentrate the extract by rotary steaming at a temperature of 60°C and a pressure of 0.01Mpa, and concentrate to a paste, and heat and dry the paste in an oven to obtain a powdery plant compound extract.

其中,表面活性剂为直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的复配,直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的质量比例为1:2。Among them, the surfactant is a compound of linear alkylbenzene sulfonate sodium and nonylphenol polyoxyethylene ether, and the mass ratio of linear alkylbenzene sodium sulfonate and nonylphenol polyoxyethylene ether is 1:2.

实施例2Example 2

一种抑菌纱线,抑菌纱线的制作工艺包括以下步骤:A kind of antibacterial yarn, the manufacture technology of antibacterial yarn comprises the following steps:

步骤1),将醋酸纤维和涤纶纤维通过集聚纺纱工艺进行混纺,得涤纶混纺,涤纶混纺的支数为48英支,捻度为90捻/10cm,醋酸纤维和涤纶纤维的质量比例为1:1。Step 1), the acetate fiber and the polyester fiber are blended through a compact spinning process to obtain a polyester blend, the count of the polyester blend is 48 pounds, the twist is 90 twists/10cm, and the mass ratio of the acetate fiber to the polyester fiber is 1: 1.

步骤2),涤纶混纺通过辊筒带动经过处理液槽并在处理液槽中浸泡处理液,处理液槽的长度为15m,涤纶混纺沿处理液槽的长度方向运行,涤纶混纺在处理液槽中的运行速度为15m/min,涤纶混纺离开处理液槽后进入烘干机中烘干,收卷得抑菌纱线。Step 2), the polyester blend is driven by the roller through the treatment liquid tank and soaked in the treatment liquid in the treatment liquid tank, the length of the treatment liquid tank is 15m, the polyester blend runs along the length direction of the treatment liquid tank, and the polyester blend is in the treatment liquid tank The running speed is 15m/min. After the polyester blend leaves the treatment liquid tank, it enters the dryer for drying, and the antibacterial yarn is wound up.

其中,醋酸纤维的细度为1.5D,长度41-42mm,为二型醋酯纤维。Among them, the fineness of acetate fiber is 1.5D, the length is 41-42mm, and it is type II acetate fiber.

其中,涤纶纤维的细度为2.5D,长度38-39mm,为聚对苯二甲酸乙二醇纤维。Among them, the fineness of polyester fiber is 2.5D, and the length is 38-39mm, which is polyethylene terephthalate fiber.

其中,处理液为水、植物复合提取物、表面活性剂的复配。Wherein, the treatment solution is a compound of water, plant compound extract and surfactant.

处理液的制备方法如下:The preparation method of the treatment liquid is as follows:

步骤1),在100kg水中投入5.5kg表面活性剂,均质4min,停止均质,得表面活性剂溶液。In step 1), 5.5 kg of surfactant was put into 100 kg of water, homogenized for 4 minutes, and the homogenization was stopped to obtain a surfactant solution.

步骤2),向表面活性剂溶液中投入1.1kg植物复合提取物,搅拌75min,得处理液。In step 2), 1.1 kg of plant compound extract was put into the surfactant solution, and stirred for 75 minutes to obtain a treatment solution.

其中,植物复合提取物为凤眼草、桂皮、鱼腥草复配后提取所得。Among them, the plant compound extract is extracted from water hyacinth, cinnamon and houttuynia after compounding.

植物复合提取物的提取方法如下:The extraction method of plant compound extract is as follows:

步骤1),将1kg凤眼草、4.5kg桂皮、0.75kg鱼腥草切碎,混匀,得复合药材。In step 1), chop 1kg water hyacinth, 4.5kg cassia bark, and 0.75kg houttuynia cordata, and mix them uniformly to obtain a compound medicinal material.

步骤2),将复合药材投入浓度为40%的乙醇溶液中,乙醇溶液的质量为复合药材投入质量的2.5倍,常温搅拌1.5h,冷却至-30℃,保持1.5h,升温并恒温73℃,搅拌9h,通过200目滤布过滤,得提取液。Step 2), put the compound medicinal material into the ethanol solution with a concentration of 40%, the quality of the ethanol solution is 2.5 times of the mass of the compound medicinal material, stir at room temperature for 1.5h, cool to -30°C, keep for 1.5h, heat up and keep the temperature at 73°C , Stir for 9h, and filter through a 200-mesh filter cloth to obtain an extract.

步骤3),将提取液旋蒸浓缩,旋蒸温度60℃,压力0.01Mpa,浓缩至膏状,将膏状物在烘箱中加热干燥,得粉状的植物复合提取物。Step 3) Concentrate the extract by rotary steaming at a temperature of 60°C and a pressure of 0.01Mpa, and concentrate to a paste, and heat and dry the paste in an oven to obtain a powdery plant compound extract.

其中,表面活性剂为直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的复配,直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的质量比例为1:2.5。Among them, the surfactant is a compound of linear alkylbenzene sulfonate sodium and nonylphenol polyoxyethylene ether, and the mass ratio of linear alkylbenzene sodium sulfonate and nonylphenol polyoxyethylene ether is 1:2.5.

实施例3Example 3

一种抑菌纱线,抑菌纱线的制作工艺包括以下步骤:A kind of antibacterial yarn, the manufacture technology of antibacterial yarn comprises the following steps:

步骤1),将醋酸纤维和涤纶纤维通过集聚纺纱工艺进行混纺,得涤纶混纺,涤纶混纺的支数为48英支,捻度为90捻/10cm,醋酸纤维和涤纶纤维的质量比例为1:1。Step 1), the acetate fiber and the polyester fiber are blended through a compact spinning process to obtain a polyester blend, the count of the polyester blend is 48 pounds, the twist is 90 twists/10cm, and the mass ratio of the acetate fiber to the polyester fiber is 1: 1.

步骤2),涤纶混纺通过辊筒带动经过处理液槽并在处理液槽中浸泡处理液,处理液槽的长度为15m,涤纶混纺沿处理液槽的长度方向运行,涤纶混纺在处理液槽中的运行速度为15m/min,涤纶混纺离开处理液槽后进入烘干机中烘干,收卷得抑菌纱线。Step 2), the polyester blend is driven by the roller through the treatment liquid tank and soaked in the treatment liquid in the treatment liquid tank, the length of the treatment liquid tank is 15m, the polyester blend runs along the length direction of the treatment liquid tank, and the polyester blend is in the treatment liquid tank The running speed is 15m/min. After the polyester blend leaves the treatment liquid tank, it enters the dryer for drying, and the antibacterial yarn is wound up.

其中,醋酸纤维的细度为1.5D,长度41-42mm,为二型醋酯纤维。Among them, the fineness of acetate fiber is 1.5D, the length is 41-42mm, and it is type II acetate fiber.

其中,涤纶纤维的细度为2.5D,长度38-39mm,为聚对苯二甲酸乙二醇纤维。Among them, the fineness of polyester fiber is 2.5D, and the length is 38-39mm, which is polyethylene terephthalate fiber.

其中,处理液为水、植物复合提取物、表面活性剂的复配。Wherein, the treatment solution is a compound of water, plant compound extract and surfactant.

处理液的制备方法如下:The preparation method of the treatment liquid is as follows:

步骤1),在100kg水中投入6kg表面活性剂,均质5min,停止均质,得表面活性剂溶液。In step 1), 6 kg of surfactant is put into 100 kg of water, homogenized for 5 minutes, and the homogenization is stopped to obtain a surfactant solution.

步骤2),向表面活性剂溶液中投入1.2kg植物复合提取物,搅拌90min,得处理液。In step 2), 1.2 kg of plant compound extract was put into the surfactant solution, and stirred for 90 minutes to obtain a treatment solution.

其中,植物复合提取物为凤眼草、桂皮、鱼腥草复配后提取所得。Among them, the plant compound extract is extracted from water hyacinth, cinnamon and houttuynia after compounding.

植物复合提取物的提取方法如下:The extraction method of plant compound extract is as follows:

步骤1),将1kg凤眼草、5kg桂皮、1kg鱼腥草切碎,混匀,得复合药材。Step 1): Mince 1kg water hyacinth, 5kg cassia bark, and 1kg houttuynia cordata, and mix them evenly to obtain a compound medicinal material.

步骤2),将复合药材投入浓度为35%的乙醇溶液中,乙醇溶液的质量为复合药材投入质量的3倍,常温搅拌2h,冷却至-30℃,保持2h,升温并恒温75℃,搅拌8h,通过200目滤布过滤,得提取液。Step 2), put the compound medicinal material into an ethanol solution with a concentration of 35%, the quality of the ethanol solution is 3 times the mass of the compound medicinal material, stir at room temperature for 2 hours, cool to -30°C, keep for 2h, heat up and keep the temperature at 75°C, and stir After 8 hours, filter through a 200-mesh filter cloth to obtain an extract.

步骤3),将提取液旋蒸浓缩,旋蒸温度60℃,压力0.01Mpa,浓缩至膏状,将膏状物在烘箱中加热干燥,得粉状的植物复合提取物。Step 3) Concentrate the extract by rotary steaming at a temperature of 60°C and a pressure of 0.01Mpa, and concentrate to a paste, and heat and dry the paste in an oven to obtain a powdery plant compound extract.

其中,表面活性剂为直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的复配,直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的质量比例为1:3。Among them, the surfactant is a compound of linear alkylbenzene sulfonate sodium and nonylphenol polyoxyethylene ether, and the mass ratio of linear alkylbenzene sulfonate sodium and nonylphenol polyoxyethylene ether is 1:3.

实施例4Example 4

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

植物复合提取物的提取方法中:In the extraction method of plant compound extract:

步骤1),将1kg凤眼草、3.5kg桂皮、1.75kg鱼腥草切碎,混匀,得复合药材。Step 1): Mince 1kg water hyacinth, 3.5kg cassia bark, and 1.75kg houttuynia cordata, and mix them evenly to obtain a compound medicinal material.

实施例5Example 5

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

植物复合提取物的提取方法中:In the extraction method of plant compound extract:

步骤1),将0.5kg凤眼草、5.5kg桂皮、0.25kg鱼腥草切碎,混匀,得复合药材。Step 1): Mince 0.5kg water hyacinth, 5.5kg cassia bark, and 0.25kg houttuynia cordata, mix well to obtain a compound medicinal material.

实施例6Example 6

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

表面活性剂为直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的复配,直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的质量比例为1:1。The surfactant is a compound of linear alkylbenzene sulfonate sodium and nonylphenol polyoxyethylene ether, and the mass ratio of linear alkylbenzene sodium sulfonate and nonylphenol polyoxyethylene ether is 1:1.

实施例7Example 7

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

表面活性剂为直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的复配,直链烷基苯磺酸钠、壬基酚聚氧乙烯醚的质量比例为1:4。The surfactant is a compound of linear alkylbenzene sulfonate sodium and nonylphenol polyoxyethylene ether, and the mass ratio of linear alkylbenzene sodium sulfonate and nonylphenol polyoxyethylene ether is 1:4.

对比例1Comparative example 1

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用金银花等量替换凤眼草。Replace water hyacinth with the same amount of honeysuckle.

对比例2Comparative example 2

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用艾叶等量替换凤眼草。Replace water hyacinth with the same amount of mugwort leaves.

对比例3Comparative example 3

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用金银花等量替换桂皮。Replace the cinnamon with an equal amount of honeysuckle.

对比例4Comparative example 4

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用艾叶等量替换桂皮。Replace the cinnamon with the same amount of mugwort leaves.

对比例5Comparative example 5

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用金银花等量替换鱼腥草。Use the same amount of honeysuckle to replace Houttuynia cordata.

对比例6Comparative example 6

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用艾叶等量替换鱼腥草。Replace Houttuynia cordata with the same amount of mugwort leaves.

对比例7Comparative example 7

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用月桂醇硫酸钠等量替换直链烷基苯磺酸钠。Sodium lauryl sulfate is used to replace sodium linear alkylbenzene sulfonate.

对比例8Comparative example 8

一种抑菌纱线,与实施例2相比,区别仅在于:A kind of antibacterial yarn, compared with embodiment 2, difference only lies in:

采用月桂醇硫酸钠等量替换壬基酚聚氧乙烯醚。The nonylphenol ethoxylate was replaced by an equivalent amount of sodium lauryl sulfate.

应用例1Application example 1

一种醋酸面料,由实施例1的抑菌纱线经纬编织造工艺而成。A kind of acetic acid fabric is formed by the antibacterial yarn warp and weft knitting process of embodiment 1.

应用例2Application example 2

一种醋酸面料,由实施例2的抑菌纱线经纬编织造工艺而成。A kind of acetic acid fabric is formed by the antibacterial yarn warp and weft knitting process of embodiment 2.

应用例3Application example 3

一种醋酸面料,由实施例3的抑菌纱线经纬编织造工艺而成。A kind of acetic acid fabric is formed by the antibacterial yarn warp and weft knitting process of embodiment 3.

应用例4Application example 4

一种醋酸面料,由实施例4的抑菌纱线经纬编织造工艺而成。A kind of acetic acid fabric, is formed by the antibacterial yarn warp and weft knitting process of embodiment 4.

应用例5Application example 5

一种醋酸面料,由实施例5的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by the antibacterial yarn warp and weft knitting process of embodiment 5.

应用例6Application example 6

一种醋酸面料,由实施例6的抑菌纱线经纬编织造工艺而成。A kind of acetic acid fabric is formed by the antibacterial yarn warp and weft knitting process of embodiment 6.

应用例7Application example 7

一种醋酸面料,由实施例7的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by the antibacterial yarn warp and weft knitting process of embodiment 7.

应用例8Application example 8

一种醋酸面料,由对比例1的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 1.

应用例9Application example 9

一种醋酸面料,由对比例2的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 2.

应用例10Application Example 10

一种醋酸面料,由对比例3的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 3.

应用例11Application Example 11

一种醋酸面料,由对比例4的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 4.

应用例12Application example 12

一种醋酸面料,由对比例5的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 5.

应用例13Application Example 13

一种醋酸面料,由对比例6的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 6.

应用例14Application Example 14

一种醋酸面料,由对比例7的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 7.

应用例15Application Example 15

一种醋酸面料,由对比例8的抑菌纱线经纬编织造工艺而成。A kind of acetate fabric, is formed by warp and weft knitting process of antibacterial yarn of comparative example 8.

实验1Experiment 1

根据20944.1-2007《纺织品抗菌性能的评价第1部分:琼脂平皿扩散法》检测各应用例的醋酸面料的抗菌效果,对照页采用100%棉织物。According to 20944.1-2007 "Evaluation of Antibacterial Performance of Textiles Part 1: Agar Plate Diffusion Method", the antibacterial effect of the acetic acid fabrics in each application example was tested, and the control page used 100% cotton fabrics.

将醋酸面料清洗1次后进行测试,记为清洗1次的抑菌效果。After washing the acetic acid fabric once, test it, and record it as the antibacterial effect of washing once.

将醋酸面料清洗100次后进行测试,记为清洗100次的抑菌效果。After washing the acetic acid fabric 100 times, test it, and record it as the antibacterial effect of washing 100 times.

清洗时,将长1m、宽1m的醋酸面料投入洗衣机中,洗衣机中注入1L水,添加1ml洗衣液(蓝月亮深层洁净护理洗衣液),在洗衣机中搅拌清洗30min,过两遍清水,晾干,即完成1次清洗。When cleaning, put the acetic acid fabric with a length of 1m and a width of 1m into the washing machine, inject 1L of water into the washing machine, add 1ml of laundry detergent (Blue Moon Deep Cleansing Care Laundry Liquid), stir and wash in the washing machine for 30 minutes, rinse with clean water twice, and dry in the air , which completes 1 wash.

清洗100次时,每次清洗间隔30min。When cleaning 100 times, the interval between each cleaning is 30 minutes.

实验1的具体检测数据详见表1。The specific detection data of Experiment 1 are shown in Table 1.

表1Table 1

Figure BDA0004154412010000081
Figure BDA0004154412010000081

Figure BDA0004154412010000091
Figure BDA0004154412010000091

根据表1的数据对比可得,通过凤眼草、桂皮、鱼腥草复配后提取所得的植物复合提取物与涤纶混纺的相容性较好,能牢固粘附在纺纱线表面,起到持久的抑菌效果,在多次水洗后仍能保持较好的抑菌功效,而当凤眼草、桂皮、鱼腥草中的任一一种被替换成其他抑菌药材后,即便替换成抑菌效果更好的药材,也仅能使刚制得的面料能具有很好的抑菌功效,但在多次水洗后,抑菌功效显著下降,抑菌持久性不佳。According to the comparison of the data in Table 1, it can be concluded that the composite plant extract obtained by compounding water hyacinth, cassia bark, and houttuynia cordata has good compatibility with polyester blends, and can firmly adhere to the surface of spinning yarns to play a role. To achieve a long-lasting antibacterial effect, it can still maintain a good antibacterial effect after repeated washing, and when any one of water hyacinth, cinnamon, and houttuynia is replaced by other antibacterial medicinal materials, even if it is replaced The medicinal material with better antibacterial effect can only make the newly prepared fabric have good antibacterial effect, but after repeated washing, the antibacterial effect decreases significantly, and the antibacterial persistence is not good.

通过直链烷基苯磺酸钠、壬基酚聚氧乙烯醚复配,能更好的提高植物复合提取物的有效成分粘附在纱线表面的牢度,更耐水洗,抑菌效果能更为持久地保持,而当直链烷基苯磺酸钠、壬基酚聚氧乙烯醚中的任一一种被替换成其他表面活性剂后,辅助提高植物复合提取物的有效成分粘附在纱线表面的牢度的效果出现下降。Through the combination of linear alkylbenzene sulfonate and nonylphenol polyoxyethylene ether, it can better improve the fastness of the active ingredients of the plant compound extract to the surface of the yarn, and it is more washable and antibacterial. It is maintained more permanently, and when any one of linear alkylbenzene sulfonate and nonylphenol polyoxyethylene ether is replaced by other surfactants, it can help improve the adhesion of the active ingredients of the plant compound extract to the The effect on the fastness of the yarn surface appears to decrease.

本具体实施例仅仅是对本申请的解释,其并不是对本申请的限制,本领域技术人员在阅读完本说明书后可以根据需要对本实施例做出没有创造性贡献的修改,但只要在本申请的权利要求范围内都受到专利法的保护。This specific embodiment is only an explanation of this application, and it is not a limitation of this application. Those skilled in the art can make modifications to this embodiment without creative contribution according to needs after reading this specification, but as long as the rights of this application All claims are protected by patent law.

Claims (9)

1. A manufacturing process of antibacterial yarn is characterized in that: the method comprises the following steps:
step 1), blending acetate fiber and polyester fiber to obtain polyester blend;
step 2), drying after the polyester blended soaking treatment liquid to obtain antibacterial yarns;
the treatment fluid comprises the following components in parts by mass:
100 parts of water;
1-1.2 parts of plant composite extract;
5-6 parts of a surfactant;
the plant compound extract is obtained by compounding and extracting Eichhornia crassipes, cinnamon and houttuynia cordata.
2. The process for producing bacteriostatic yarn according to claim 1, wherein: the mass ratio of the ailanthus altissima to the cassia bark to the cordate houttuynia is 1:4-5:0.5-1.
3. The process for producing bacteriostatic yarn according to claim 2, characterized in that: the extraction method of the plant composite extract comprises the following steps:
step 1), cutting the ailanthus altissima, the cinnamon and the cordate houttuynia into pieces, and uniformly mixing to obtain a compound medicinal material;
step 2), putting the composite medicinal material into an ethanol solution with the concentration of 35-45%, stirring for 1-2 hours at normal temperature, cooling to-30 ℃ and below, keeping for 1-2 hours, heating and keeping the temperature at 70-75 ℃, stirring for 8-10 hours, and filtering to obtain an extract, wherein the mass of the ethanol solution is 2-3 times of the mass of the composite medicinal material;
and 3) evaporating, concentrating and drying the extracting solution to obtain the powdery plant composite extract.
4. A process for producing a bacteriostatic yarn according to any one of claims 1-3, characterized in that: the surfactant is the compound of straight-chain sodium alkylbenzenesulfonate and nonylphenol polyoxyethylene ether.
5. The process for producing bacteriostatic yarn according to claim 4, wherein: the mass ratio of the linear sodium alkylbenzenesulfonate to the nonylphenol polyoxyethylene ether is 1:2-3.
6. The process for producing bacteriostatic yarn according to claim 5, wherein: the preparation method of the treatment fluid comprises the following steps:
step 1), adding a surfactant into water, homogenizing for 3-5min, and stopping homogenizing to obtain a surfactant solution;
and 2) adding the plant composite extract into the surfactant solution, and stirring for 60-90min to obtain the treatment liquid.
7. The process for producing bacteriostatic yarn according to claim 6, wherein: in the step 2), the time of soaking the polyester blended spinning treatment fluid is 1 minute or more.
8. A bacteriostatic yarn, characterized in that: a process for the production of a bacteriostatic yarn according to any one of claims 1 to 7.
9. An acetic acid fabric, which is characterized in that: a woven from the bacteriostatic yarn of claim 8.
CN202310329423.7A 2023-03-30 2023-03-30 Antibacterial yarn and its production process and acetate fabric Pending CN116219742A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310329423.7A CN116219742A (en) 2023-03-30 2023-03-30 Antibacterial yarn and its production process and acetate fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310329423.7A CN116219742A (en) 2023-03-30 2023-03-30 Antibacterial yarn and its production process and acetate fabric

Publications (1)

Publication Number Publication Date
CN116219742A true CN116219742A (en) 2023-06-06

Family

ID=86573200

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202310329423.7A Pending CN116219742A (en) 2023-03-30 2023-03-30 Antibacterial yarn and its production process and acetate fabric

Country Status (1)

Country Link
CN (1) CN116219742A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117090043A (en) * 2023-08-23 2023-11-21 浙江菲摩斯纺织有限公司 Decorative fabric and production process thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107397386A (en) * 2017-08-12 2017-11-28 安徽楚艾农业科技有限公司 A kind of moxa quilt and preparation method thereof
CN110685148A (en) * 2019-10-23 2020-01-14 成工业制衣(苏州)有限公司 Novel antibacterial textile fabric
CN114468416A (en) * 2020-10-23 2022-05-13 亿利新材料有限公司 Prevent antibacterial cool type gauze mask of haze
US20220333278A1 (en) * 2021-04-07 2022-10-20 LUOLAI LIFESTYLE TECHNOLOGY Co.,Ltd. Antibacterial textile and preparation method thereof
CN115852670A (en) * 2022-11-26 2023-03-28 杭州邦球纺织有限公司 Mildew-proof antibacterial fabric and production process thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107397386A (en) * 2017-08-12 2017-11-28 安徽楚艾农业科技有限公司 A kind of moxa quilt and preparation method thereof
CN110685148A (en) * 2019-10-23 2020-01-14 成工业制衣(苏州)有限公司 Novel antibacterial textile fabric
CN114468416A (en) * 2020-10-23 2022-05-13 亿利新材料有限公司 Prevent antibacterial cool type gauze mask of haze
US20220333278A1 (en) * 2021-04-07 2022-10-20 LUOLAI LIFESTYLE TECHNOLOGY Co.,Ltd. Antibacterial textile and preparation method thereof
CN115852670A (en) * 2022-11-26 2023-03-28 杭州邦球纺织有限公司 Mildew-proof antibacterial fabric and production process thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117090043A (en) * 2023-08-23 2023-11-21 浙江菲摩斯纺织有限公司 Decorative fabric and production process thereof

Similar Documents

Publication Publication Date Title
CN102041680A (en) Finishing agent for polyester imitation silk fabric and its preparation and post-treatment method
CN101177810B (en) Preparation method of health preserving jute blended yarn
CN103498273B (en) Shell fabric of blending bamboo fibers and polyesters
CN104389099A (en) Ultraviolet resisting and static preventing textile fabric and preparation method thereof
WO2022166136A1 (en) Preparation method for antibacterial, antiviral and mildewproof polyester spunlace non-woven fabric containing phbv material
CN101307502A (en) The preparation method of pineapple leaf fiber
CN103255488A (en) Preparation method of high-strength viscose fiber
CN103859615A (en) Preparation method of anti-microbial and healthcare modal and milk blending underwear by adopting traditional Chinese medicine rheum officinale
CN101851803A (en) A kind of viscose fiber with health care function and preparation method thereof
CN116219742A (en) Antibacterial yarn and its production process and acetate fabric
CN105133135B (en) Bamboo fiber and fibrilia fiber blending cloth
CN103361850B (en) Pineapple fiber, copper ammonia fiber and dacron blended fabric
CN110656503B (en) A kind of water-absorbing composite silk fabric and processing method thereof
WO2024119615A1 (en) Preparation method for antibacterial and anti-mite intelligent constant-temperature fiber
JP5646572B2 (en) Modified fiber and method for producing the same
CN104695075A (en) Banana, linen and wool fiber blended yarn and application thereof
JP2004360163A (en) Towel cloth
CN114734689A (en) Fabric based on zinc ion antibacterial and heating and weaving method thereof
WO2021243934A1 (en) Tencel fiber and silver ion composite fiber fabric and manufacturing method therefor
CN105755826A (en) Preparation method for electrostatic elimination in high-performance fiber spinning process
CN117984634A (en) A kind of stretch-resistant folded cloth and preparation method thereof
CN112342654A (en) Bamboo fiber and cotton fabric and production process thereof
CN116556043A (en) A skin-toning fabric with hanging silk properties and its preparation method
CN114575141A (en) Nano sea-island fibre/terylene composite material and its preparing method
CN108277641A (en) A method of preventing pure cotton textile pilling

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20230606