CN117191237A - Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature - Google Patents

Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature Download PDF

Info

Publication number
CN117191237A
CN117191237A CN202310900177.6A CN202310900177A CN117191237A CN 117191237 A CN117191237 A CN 117191237A CN 202310900177 A CN202310900177 A CN 202310900177A CN 117191237 A CN117191237 A CN 117191237A
Authority
CN
China
Prior art keywords
epoxy resin
residual stress
simulation device
heat shield
curing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202310900177.6A
Other languages
Chinese (zh)
Inventor
陈荣
何金
李进
赵琦
张弛
李松原
宋晓博
张黎明
方琼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
State Grid Tianjin Electric Power Co Ltd
Electric Power Research Institute of State Grid Tianjin Electric Power Co Ltd
State Grid Corp of China SGCC
Original Assignee
State Grid Tianjin Electric Power Co Ltd
Electric Power Research Institute of State Grid Tianjin Electric Power Co Ltd
State Grid Corp of China SGCC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by State Grid Tianjin Electric Power Co Ltd, Electric Power Research Institute of State Grid Tianjin Electric Power Co Ltd, State Grid Corp of China SGCC filed Critical State Grid Tianjin Electric Power Co Ltd
Priority to CN202310900177.6A priority Critical patent/CN117191237A/en
Publication of CN117191237A publication Critical patent/CN117191237A/en
Pending legal-status Critical Current

Links

Landscapes

  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)

Abstract

本发明涉及基于非均匀温度固化环氧绝缘件残余应力模拟装置及方法,本发明通过环氧树脂浇注部分以及隔热罩构建了基于非均匀温度固化的环氧树脂绝缘件残余应力模拟装置,并且对无隔热罩区域以及隔热罩覆盖区域分别测试试样残余应力最大值,可以实现同一试样两端应力出现较大差值,并且可对不同固化温度下环氧树脂固化产物的应力分布情况进行控制,量化固化温度对环氧树脂绝缘件残余应力的影响。本发明通过隔热棉覆被在块状试样模具的外表面,可以有效改变并检测环氧树脂固化产物的残余应力,为研究固化温度不均条件下环氧树脂绝缘件的残余应力集中情况提供了试验方法。

The present invention relates to a residual stress simulation device and method for epoxy insulation parts based on non-uniform temperature curing. The invention constructs a residual stress simulation device for epoxy resin insulation parts based on non-uniform temperature curing through an epoxy resin pouring part and a heat shield, and The maximum residual stress of the sample is measured separately in the area without the heat shield and the area covered by the heat shield, which can achieve a large difference in stress at both ends of the same sample, and can also analyze the stress distribution of epoxy resin cured products at different curing temperatures. The situation was controlled to quantify the effect of curing temperature on the residual stress of epoxy resin insulation parts. The present invention covers the outer surface of the block sample mold with thermal insulation cotton, which can effectively change and detect the residual stress of the cured epoxy resin product, in order to study the residual stress concentration of the epoxy resin insulation parts under the condition of uneven curing temperature. Test methods are provided.

Description

Device and method for simulating residual stress of epoxy insulating part based on non-uniform temperature curing
Technical Field
The invention belongs to the technical field of high-voltage electricity, and particularly relates to a device and a method for simulating residual stress of an epoxy insulating part based on non-uniform temperature curing.
Background
Along with the gradual expansion of the application scale of the ultra-high voltage transmission line in the electric power system of China, the sizes of the epoxy resin insulators in the GIS and the GIL are continuously increased, and the reliability requirement of the insulators is greatly improved. The epoxy resin insulating part is a key part for bearing electric insulation and mechanical support in GIS/GIL equipment, receives the comprehensive effect of multiple physical fields such as electricity, heat, magnetism and the like in the operation process, the working reliability of the epoxy resin insulating part directly influences the stability of an electric power system, and the epoxy resin insulating part is extremely complex in internal stress distribution condition, breaks and bursts and happens at the moment, so that the epoxy resin insulating part is widely focused by researchers.
The residual stress is a local stress concentration phenomenon caused by the influence of a process in the preparation process of the workpiece, and after coupling external stress application, the residual stress is extremely likely to cause the initiation or brittle failure of microcracks of the insulating part, so that serious accidents such as partial discharge, explosion and the like are caused. The insulating part inevitably contains residual stress before being put into operation, but the related factory inspection standard is not implemented by the current manufacturers, so that the operation reliability of the epoxy resin insulating part is greatly restricted. The reaction of epoxy and anhydride in the epoxy resin insulating part casting material is exothermic reaction, and the difference of the local crosslinking reaction degree is increased along with the increase of the volume of the die; and the temperature difference is extremely large in the production process, and large residual stress is likely to occur in the epoxy resin insulating part due to the fact that the thermal expansion coefficients of the metal insert, the guide rod and the epoxy composite insulating material are not matched.
Disclosure of Invention
The invention aims to overcome the defects of the prior art, provides a device and a method for simulating the residual stress of an epoxy insulating part based on non-uniform temperature curing, can effectively change and detect the residual stress of an epoxy resin cured product by coating the outer surface of a block-shaped sample die with heat insulation cotton, and provides a test method for researching the concentration condition of the residual stress of the epoxy resin insulating part under the condition of non-uniform curing temperature.
The invention solves the technical problems by adopting the following technical scheme:
the utility model provides an epoxy insulator residual stress analogue means based on inhomogeneous temperature solidification, including epoxy pouring part and heat exchanger, wherein, epoxy pouring part suit is inside the heat exchanger, and epoxy pouring part top includes mould backplate and mould roof, and the setting of mould roof carries out threaded connection through the screw hole that sets up in the four corners at the mould backplate, and the top of mould backplate and mould roof is equipped with pouring mouth and observation mouth simultaneously, and the observation mouth is cylindrical, and the pouring mouth is round platform shape, round platform shape top diameter is greater than round platform bottom diameter.
And moreover, the heat shield is a cuboid with a hollow inside, the inner surface layer is filled with heat insulation cotton and sleeved on the outer side of the epoxy resin pouring part, so that the tightness of the simulation device is improved.
A simulation method of an epoxy resin insulator residual stress simulation device based on non-uniform temperature curing comprises the following steps:
step 1, pouring CT-5531 epoxy resin, TF-1 curing agent and micrometer alumina into a clean beaker according to the mass ratio of 100:44:306;
step 2, placing the mixture into a magnetic stirrer, and stirring for 10 minutes to uniformly mix the mixture;
step 3, after the mixture is uniformly mixed, placing the mixture into a vacuum drying oven at 50 ℃, continuously vacuumizing for 15 minutes, and fully removing air in the mixture;
step 4, pouring the mixture into an epoxy resin pouring part;
step 5, sleeving the heat insulation cover with the heat insulation cotton plugged inside on the outer surface of the epoxy resin pouring part, and completing assembly;
step 6, placing the assembled simulation device into a constant-temperature oven at 130 ℃ for curing for 10 hours;
step 7, after the preset time is reached, taking out the assembled simulation device, cooling to room temperature, and demolding to obtain an epoxy resin insulating part sample;
and 8, performing stress detection by using ultrasonic stress detection equipment, and respectively testing the maximum value of the residual stress of the sample in the heat shield-free area and the heat shield coverage area.
The invention has the advantages and positive effects that:
according to the invention, the epoxy resin insulation part residual stress simulation device based on non-uniform temperature curing is constructed through the epoxy resin pouring part and the heat shield, and the maximum value of the residual stress of the sample is tested for the non-heat shield area and the heat shield coverage area respectively, so that a larger difference value of stress at two ends of the same sample can be realized, the stress distribution condition of an epoxy resin cured product at different curing temperatures can be controlled, and the influence of the curing temperature on the residual stress of the epoxy resin insulation part is quantized. According to the invention, the thermal insulation cotton is coated on the outer surface of the block sample mold, so that the residual stress of the epoxy resin cured product can be effectively changed and detected, and a test method is provided for researching the concentration condition of the residual stress of the epoxy resin insulating part under the condition of uneven curing temperature.
Drawings
FIG. 1 is a diagram of a casting portion of an epoxy resin according to the present invention;
FIG. 2 is a cross-sectional view of a casting portion of an epoxy resin according to the present invention;
fig. 3 is a structural view of the heat shield of the present invention.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings.
The utility model provides an epoxy insulator residual stress analogue means based on heterogeneous temperature solidification, as shown in fig. 1, including containing epoxy pouring part and heat exchanger, wherein, epoxy pouring part suit is inside the heat exchanger, as shown in fig. 2 and 3, epoxy pouring part top includes mould backplate and mould roof, the setting of mould roof carries out threaded connection through the screw hole that sets up in the four corners at the mould backplate, the top of mould backplate and mould roof is equipped with pouring mouth and observation mouth simultaneously, the observation mouth is cylindrical, the pouring mouth is round platform shape, round platform shape top diameter is greater than round platform bottom diameter. The bottom radius of the pouring opening is 0.5cm, the top radius is 1cm, and the height is 1cm. Meanwhile, a cuboid cavity of 10 multiplied by 2cm is dug in the die back plate and the die top plate to serve as a pouring cavity.
The heat shield is a cuboid with a hollow inside, the inner surface layer is filled with heat insulation cotton and sleeved on the outer side of the epoxy resin pouring part, and the heat shield is used for improving the tightness of the simulation device. The radius of the observation port is 0.5cm, the height of the observation port is 1cm, the effective discharge of internal bubbles can be realized through the observation port, and meanwhile, the effective inflow of the castable can be realized through the circular truncated cone design of the pouring port.
A simulation method of an epoxy resin insulator residual stress simulation device based on non-uniform temperature curing comprises the following steps:
step 1, pouring CT-5531 epoxy resin, TF-1 curing agent and micrometer alumina into a clean beaker according to the mass ratio of 100:44:306;
step 2, placing the mixture into a magnetic stirrer, and stirring for 10 minutes to uniformly mix the mixture;
step 3, after the mixture is uniformly mixed, placing the mixture into a vacuum drying oven at 50 ℃, continuously vacuumizing for 15 minutes, and fully removing air in the mixture;
step 4, pouring the mixture into an epoxy resin pouring part;
step 5, sleeving the heat insulation cover with the heat insulation cotton plugged inside on the outer surface of the epoxy resin pouring part, and completing assembly;
step 6, placing the assembled simulation device into a constant-temperature oven at 130 ℃ for curing for 10 hours;
step 7, after the preset time is reached, taking out the assembled simulation device, cooling to room temperature, and demolding to obtain an epoxy resin insulating part sample;
and 8, performing stress detection by using ultrasonic stress detection equipment, and respectively testing the maximum value of the residual stress of the sample in the heat shield-free area and the heat shield coverage area.
Performing stress detection by using ultrasonic stress detection equipment, wherein the maximum value of the residual stress of the sample is 1.03MPa in the region without the heat shield; in the heat shield coverage area, the maximum value of the residual stress of the test sample is 17.87MPa. The method has the advantages that the residual stress of the epoxy resin cured product can be effectively changed and detected by covering the outer surface of the block sample mold with the heat insulation cotton, and a test method is provided for researching the concentration condition of the residual stress of the epoxy resin insulating part under the condition of uneven curing temperature.
It should be emphasized that the examples described herein are illustrative rather than limiting, and therefore the invention includes, but is not limited to, the examples described in the detailed description, as other embodiments derived from the technical solutions of the invention by a person skilled in the art are equally within the scope of the invention.

Claims (3)

1.基于非均匀温度固化环氧绝缘件残余应力模拟装置,其特征在于:包括含环氧树脂浇注部分以及隔热罩,其中,环氧树脂浇注部分套装在隔热罩内部,环氧树脂浇注部分顶部包括模具背板和模具顶板,模具顶板设置在模具背板通过设置在四角的螺纹孔进行螺纹连接,同时模具背板和模具顶板的顶部设有浇筑口和观测口,观测口为圆柱形,浇筑口为圆台形,圆台形顶部直径大于圆台底部直径。1. A residual stress simulation device based on non-uniform temperature curing epoxy insulation parts, characterized by: including an epoxy resin pouring part and a heat shield, wherein the epoxy resin pouring part is set inside the heat shield, and the epoxy resin pouring part is Part of the top part includes a mold back plate and a mold top plate. The mold top plate is set on the mold back plate and is threaded through threaded holes provided at the four corners. At the same time, the tops of the mold back plate and the mold top plate are provided with a pouring port and an observation port. The observation port is cylindrical. , the pouring opening is in the shape of a truncated cone, and the diameter of the top of the truncated cone is larger than the diameter of the bottom of the truncated cone. 2.根据权利要求1所述的基于非均匀温度固化环氧绝缘件残余应力模拟装置,其特征在于:所述隔热罩为内部中空的长方体,内部表层填充隔热棉,套装在环氧树脂浇注部分外侧,用于提高模拟装置的密封性。2. The residual stress simulation device for curing epoxy insulation parts based on non-uniform temperature according to claim 1, characterized in that: the heat shield is a hollow rectangular parallelepiped, the inner surface is filled with heat insulation cotton, and is covered with epoxy resin. The outside of the pouring part is used to improve the sealing of the simulation device. 3.一种如权利要求1和2任一项所述的基于非均匀温度固化环氧绝缘件残余应力模拟装置的模拟方法,其特征在于:包括以下步骤:3. A simulation method based on the residual stress simulation device of non-uniform temperature cured epoxy insulation parts according to any one of claims 1 and 2, characterized in that: it includes the following steps: 步骤1、将CT-5531环氧树脂、TF-1固化剂、微米氧化铝按照100:44:306的质量比,倒入干净的烧杯中;Step 1. Pour CT-5531 epoxy resin, TF-1 curing agent, and micron alumina into a clean beaker according to the mass ratio of 100:44:306; 步骤2、将混合物放入磁力搅拌器中,搅拌10分钟,使其均匀混合;Step 2. Put the mixture into a magnetic stirrer and stir for 10 minutes to mix evenly; 步骤3、混合物均匀混合后,放入50℃的真空干燥箱中,连续抽真空15分钟,充分去除混合物体中的空气;Step 3. After the mixture is evenly mixed, place it in a vacuum drying oven at 50°C and vacuum continuously for 15 minutes to fully remove the air in the mixture; 步骤4、将混合物浇筑到环氧树脂浇注部分中;Step 4. Pour the mixture into the epoxy resin pouring part; 步骤5、将内部塞有隔热棉的隔热罩套在环氧树脂浇注部分外表面,完成组装;Step 5. Place the heat shield with insulation cotton inside on the outer surface of the epoxy resin pouring part to complete the assembly; 步骤6、将组装好的模拟装置放入130℃的恒温烤箱中固化10h;Step 6. Place the assembled simulation device into a constant temperature oven at 130°C for curing for 10 hours; 步骤7、到达预定时间后,将组装好的模拟装置取出冷却至室温,脱模得到环氧树脂绝缘件试样;Step 7. After reaching the predetermined time, take out the assembled simulation device, cool it to room temperature, and demould to obtain the epoxy resin insulation sample; 步骤8、使用超声应力检测设备进行应力检测,在无隔热罩区域以及隔热罩覆盖区域分别测试试样残余应力最大值。Step 8. Use ultrasonic stress testing equipment to conduct stress testing, and test the maximum residual stress of the sample in the area without the heat shield and the area covered by the heat shield.
CN202310900177.6A 2023-07-21 2023-07-21 Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature Pending CN117191237A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310900177.6A CN117191237A (en) 2023-07-21 2023-07-21 Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310900177.6A CN117191237A (en) 2023-07-21 2023-07-21 Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature

Publications (1)

Publication Number Publication Date
CN117191237A true CN117191237A (en) 2023-12-08

Family

ID=88987580

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202310900177.6A Pending CN117191237A (en) 2023-07-21 2023-07-21 Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature

Country Status (1)

Country Link
CN (1) CN117191237A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN120064345A (en) * 2025-03-21 2025-05-30 中国科学院武汉岩土力学研究所 Device and method for measuring residual stress of rock mass at non-uniform temperature

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN120064345A (en) * 2025-03-21 2025-05-30 中国科学院武汉岩土力学研究所 Device and method for measuring residual stress of rock mass at non-uniform temperature
CN120064345B (en) * 2025-03-21 2025-12-02 中国科学院武汉岩土力学研究所 Apparatus and method for measuring residual stress in rock masses under non-uniform temperatures

Similar Documents

Publication Publication Date Title
CN102096032B (en) Experimental facility and method for electric heating combined stress aging with oil-paper insulation of transformer
CN112130041B (en) GIL post insulator burst fault simulation test platform and measurement method
CN108267484B (en) Measurement device for transport properties at high temperature and high pressure based on diamond anvil
CN117191237A (en) Residual stress simulation device and method for curing epoxy insulation parts based on non-uniform temperature
CN109633430B (en) Abnormal temperature rise fault monitoring experimental device for real GIS equipment
CN102628819B (en) Test method for evaluating the oxidation stability of transformer oil under high voltage AC or DC electric field
CN203929897U (en) A kind of experimental provision that accelerates heat ageing for paper oil insulation
CN108931715A (en) A kind of test method that reactor turn-to-turn insulation is influenced by temperature changing stress and device
CN101834062B (en) Sealed pouring method of bushing insulator and conducting rod
CN111948253B (en) A device and method for measuring thermal insulation temperature rise of concrete
CN111037819B (en) Preparation method of epoxy insulation composite material with improved static dissipation characteristic
CN113092962A (en) Electric-thermal-gas multi-stress combined aging experiment platform and method for insulating material
CN206096193U (en) A environment case for electronic components electrical property in situ test
WO2023098141A1 (en) Measurement sample and measurement method for tensile strength of interface surface between epoxy composite material and aluminium
Zhang et al. Partial discharge characteristics of cavities with different appearances and positions in solid insulation
CN106885977A (en) A kind of adjustable paper oil insulation discharge test device of temperature
CN118067290B (en) Residual stress distribution detection method of epoxy insulation parts based on infrared
CN113414914A (en) Preparation mold for epoxy resin plate for insulation in power industry
CN111398708B (en) Electromagnetic material comprehensive test microwave heating equipment and method
CN110646297B (en) A high temperature water environment fracture toughness test device
CN219715457U (en) Temperature-control type mortar concrete ring constraint shrinkage test device
CN110349716A (en) Hollow porcelain composite insulator and its processing method
CN216621497U (en) A portable constant temperature heating and temperature measuring device for proton exchange membrane coating process
CN206030354U (en) A mould for pouring epoxy resin nanocomposite disc sample
CN204065335U (en) The pick-up unit of impregnating resin material breakdown intensity in a kind of low temperature environment

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination