CN1621602A - Method for preparing antistatic fabric treatment liquid - Google Patents
Method for preparing antistatic fabric treatment liquid Download PDFInfo
- Publication number
- CN1621602A CN1621602A CN 200310105766 CN200310105766A CN1621602A CN 1621602 A CN1621602 A CN 1621602A CN 200310105766 CN200310105766 CN 200310105766 CN 200310105766 A CN200310105766 A CN 200310105766A CN 1621602 A CN1621602 A CN 1621602A
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- Prior art keywords
- liquid
- rare earth
- water
- kilogram
- rare
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000007788 liquid Substances 0.000 title claims abstract description 30
- 239000004744 fabric Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000002360 preparation method Methods 0.000 claims abstract description 13
- 239000012153 distilled water Substances 0.000 claims abstract description 11
- 239000008234 soft water Substances 0.000 claims abstract description 11
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 4
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims abstract description 3
- WIVXEZIMDUGYRW-UHFFFAOYSA-L copper(i) sulfate Chemical compound [Cu+].[Cu+].[O-]S([O-])(=O)=O WIVXEZIMDUGYRW-UHFFFAOYSA-L 0.000 claims abstract description 3
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 claims abstract description 3
- 235000019345 sodium thiosulphate Nutrition 0.000 claims abstract description 3
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 23
- -1 rare-earth compound Chemical class 0.000 claims description 17
- 239000012530 fluid Substances 0.000 claims description 7
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 239000004094 surface-active agent Substances 0.000 claims description 6
- 238000004043 dyeing Methods 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 4
- 230000008595 infiltration Effects 0.000 claims description 4
- 238000001764 infiltration Methods 0.000 claims description 4
- 150000002910 rare earth metals Chemical class 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 claims description 2
- 229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 2
- 239000003651 drinking water Substances 0.000 claims description 2
- 235000020188 drinking water Nutrition 0.000 claims description 2
- 229910052747 lanthanoid Inorganic materials 0.000 claims description 2
- 150000002602 lanthanoids Chemical class 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 150000002739 metals Chemical class 0.000 claims description 2
- 229910001404 rare earth metal oxide Inorganic materials 0.000 claims description 2
- 229910052706 scandium Inorganic materials 0.000 claims description 2
- SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 claims description 2
- 235000011150 stannous chloride Nutrition 0.000 claims description 2
- 239000001119 stannous chloride Substances 0.000 claims description 2
- 229910052727 yttrium Inorganic materials 0.000 claims description 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 2
- 239000000126 substance Substances 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 230000007797 corrosion Effects 0.000 abstract description 2
- 238000005260 corrosion Methods 0.000 abstract description 2
- 230000002045 lasting effect Effects 0.000 abstract description 2
- 229910021591 Copper(I) chloride Inorganic materials 0.000 abstract 1
- 229910000365 copper sulfate Inorganic materials 0.000 abstract 1
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 abstract 1
- 229940045803 cuprous chloride Drugs 0.000 abstract 1
- 239000002736 nonionic surfactant Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 230000003068 static effect Effects 0.000 description 4
- 238000005303 weighing Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000000149 penetrating effect Effects 0.000 description 3
- 208000013016 Hypoglycemia Diseases 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 238000005108 dry cleaning Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000191 poly(N-vinyl pyrrolidone) Polymers 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000009958 sewing Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention is the preparation process of antistatic fabric treating liquid for the direct treatment of fabric. The antistatic fabric treating liquid consists of liquid An and liquid B. The liquid An includes copper sulfate, copper chloride, cuprous sulfate and cuprous chloride 0.01-10 kg; RE element and RE compound 0.002-2.5 kg; non-ionic surfactant 0.01-10 kg; soft water or distilled water 0.005-5.0 kg; and water 5-5000 kg. The liquid B includes sodium thiosulfate 0.01-15 kg and water 5-500 kg. The present invention has lasting and stable antistatic performance, stable chemical performance, high corrosion resistance, good weather adaptability and other advantages.
Description
One, technical field: the present invention relates to a kind of preparation method who eliminates the treatment fluid of static of the fabric.Be applicable to department and industries such as oil, instrument, weaving, printing, plastics, communication, medical treatment, to eliminate the influence and the harm of static.
Two, background technology: static is well-known to the various influences of human society, the main method of handling static of the fabric at present has: the 1st, apply anion or CATION or both sexes or non-ionic surface active agent at fiber surface, this method is easy to use, but its defective is not durable, and process is soaped or the dry-cleaning meeting was lost efficacy because of coming off; The 2nd, sneak into surfactant at fibrous inside, this only is adapted at using on the film; The 3rd, by RESIN FINISH, will there be the resin of electric conductivity to be added in the fiber the inside, perhaps by chemical graft, the macromolecule of electric conductivity is connected on fiber surface, these class methods are bigger to the physical property influence of fiber, and the expense costliness.Simultaneously, ubiquity the manufacturing technique complexity, and cost height, feel are soft inadequately, designs and varieties are few, and conductive compound is to weak points such as the influence of human body and serviceability are relatively poor.
Three, summary of the invention: the purpose of this invention is to provide a kind of have permanent antistatic performance and stable chemical performance, harmless, soft and the good preparation method that can directly carry out the anti-static fabric treatment fluid of antistatic treatment to fabric arranged.
The preparation method of anti-static fabric treatment fluid is under certain temperature and pressure, and the composition and the consumption of each material are in the used antistatic treatment liquid of being made up of A liquid and B liquid of 50 kilograms of fabrics of every processing:
A liquid: a, copper sulphate, copper chloride, cuprous sulfate and stannous chloride, the consumption of above-mentioned single or mixing cpd is the 0.01-10 kilogram; The consumption sum of b, rare earth elemental metals and rare-earth compound is the 0.002-2.5 kilogram; C, have the infiltration and the non-ionic surface active agent 0.01-10 kilogram of level dyeing effect; D, reagent soft water or distilled water 0.005-5.0 kilogram; E, water or soft water or distilled water 5-5000 kilogram.B liquid: a, sodium thiosulfate 0.01-15 kilogram; B, water or drinking-water or distilled water 5-500 liter.Described rare earth element is meant the whole elements of scandium, yttrium and group of the lanthanides; Rare-earth compound is meant rare-earth hydroxide, rare earth peroxide, rare earth oxide, rare earth halide, rare earth nitrades, rare earth sulfate and rare earth carbonate.The non-ionic surface active agent with infiltration and level dyeing effect described in the A liquid can be the non-ionic surface active agent that penetrating agent JFC or peregal etc. have infiltration and level dyeing effect.The pressure of fabric when carrying out antistatic treatment is normal pressure.The temperature of fabric when carrying out antistatic treatment is 20-100 ℃.
Preparation method of the present invention compared with prior art has lasting and stable antistatic property; Stable chemical performance, good corrosion resistance have adaptability preferably to various weathers; Soft, intensity good, serviceability is good; Have good dyeability, can dye the multiple color and luster of system according to different needs; And processing characteristics, as: cutting, sewing, making etc.
Four, description of drawings: do not have
Five, the specific embodiment:
Embodiment 1:A liquid preparation: in capacity is 500 liters stainless steel charging basket, it is better with glass or enamel to change the charging basket inner-wall material, pour into through 10 kilograms of the pure cupric sulfate pentahydrates of reagent of weighing, add 300 liters of soft water, after stirring makes dissolving, add successively again by 25 liters of formulated 1% (concentration) sulfuric acid solutions of the acid of 0.25 kilogram of reagent bright sulfur and 25 liters of distilled water, adding is by 10 liters of formulated 2% (concentration) mixed rare earth chlorides solution of 0.2 kilogram of mixed rare earth chlorides and 10 liters of distilled water, add 1.5 kilograms of penetrating agent JFCs, add soft water to 500 liter, stir, form A liquid.B liquid preparation: in the change charging basket of 250 liters of capacity, pour into, add 250 liters of soft water, stir and make dissolving be B liquid through 11 kilograms of the hypos of weighing.
The preparation of antistatic treatment liquid is to adopt solution mixture, and A liquid and B liquid are uniformly mixed into the antistatic treatment treatment fluid, the use antistatic treatment liquid while mixing with 2: 1 volume ratio.
Embodiment 2:A liquid preparation: change in the charging basket at No. 1, pour into through 2 kilograms of the pure Salzburg vitriols of reagent of weighing, add 90 liters of 60 ℃ of soft water, after stirring makes dissolving, pour in Q113 ~ 28 type rope impregnating mangle grooves, add 1200 liters of soft water, add successively again by 10 liters of the sulfuric acid solutions of the acid of 0.1 kilogram of reagent bright sulfur and 10 liters of distilled water formulated 1% (concentration), adding is by 5 liters of formulated 2% (concentration) mishmetal chlorinated solutions of 0.1 kilogram of mixed rare earth chlorides and 5 liters of distilled water, add 3 kilograms of penetrating agent JFCs, stir, form A liquid.B liquid preparation: change in the charging basket at No. 2, pour into, add 50 liters of soft water, stir and make dissolving be B liquid through 2.4 kilograms of the hypos of weighing.
Claims (2)
1, the preparation method of anti-static fabric treatment fluid is characterized in that under certain temperature and pressure, and the composition and the consumption of each material are in the used antistatic treatment liquid of being made up of A liquid and B liquid of 50 kilograms of fabrics of every processing:
A liquid: a, copper sulphate, copper chloride, cuprous sulfate and stannous chloride, the consumption of above-mentioned single or mixing cpd is the 0.01-10 kilogram; The consumption sum of b, rare earth elemental metals and rare-earth compound is the 0.002-2.5 kilogram; C, have the infiltration and the non-ionic surface active agent 0.01-10 kilogram of level dyeing effect; D, reagent soft water or distilled water 0.005-5.0 kilogram; E, water or soft water or distilled water 5-5000 kilogram.
B liquid: a, sodium thiosulfate 0.01-15 kilogram; B, water or drinking-water or distilled water 5-500 liter.
2, by the preparation method of the described anti-static fabric treatment fluid of claim 1, it is characterized in that rare earth element is meant the whole elements of scandium, yttrium and group of the lanthanides; Rare-earth compound is meant rare-earth hydroxide, rare earth peroxide, rare earth oxide, rare earth halide, rare earth nitrades, rare earth sulfate and rare earth carbonate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310105766 CN1621602A (en) | 2003-11-30 | 2003-11-30 | Method for preparing antistatic fabric treatment liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310105766 CN1621602A (en) | 2003-11-30 | 2003-11-30 | Method for preparing antistatic fabric treatment liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1621602A true CN1621602A (en) | 2005-06-01 |
Family
ID=34757402
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200310105766 Pending CN1621602A (en) | 2003-11-30 | 2003-11-30 | Method for preparing antistatic fabric treatment liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1621602A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103334294A (en) * | 2013-07-04 | 2013-10-02 | 郭立新 | A kind of preparation method of flame-retardant conductive fiber |
| CN106436277A (en) * | 2016-09-21 | 2017-02-22 | 东莞市联洲知识产权运营管理有限公司 | Finishing agent based on rare earth element and nanogold as well as preparing and finishing method thereof |
-
2003
- 2003-11-30 CN CN 200310105766 patent/CN1621602A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103334294A (en) * | 2013-07-04 | 2013-10-02 | 郭立新 | A kind of preparation method of flame-retardant conductive fiber |
| CN103334294B (en) * | 2013-07-04 | 2015-07-08 | 郭立新 | Preparation method of flame-retardant conductive fiber |
| CN106436277A (en) * | 2016-09-21 | 2017-02-22 | 东莞市联洲知识产权运营管理有限公司 | Finishing agent based on rare earth element and nanogold as well as preparing and finishing method thereof |
| CN106436277B (en) * | 2016-09-21 | 2018-10-23 | 管家依 | A kind of finishing agent and its preparation and method for sorting based on rare earth element and nanogold |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |