CR20220188A - Proceso para la preparación de cloruro de tiofosforilo y acefato. - Google Patents

Proceso para la preparación de cloruro de tiofosforilo y acefato.

Info

Publication number
CR20220188A
CR20220188A CR20220188A CR20220188A CR20220188A CR 20220188 A CR20220188 A CR 20220188A CR 20220188 A CR20220188 A CR 20220188A CR 20220188 A CR20220188 A CR 20220188A CR 20220188 A CR20220188 A CR 20220188A
Authority
CR
Costa Rica
Prior art keywords
preparation
acephate
thiophosphoryl chloride
present
thiophosphoryl
Prior art date
Application number
CR20220188A
Other languages
English (en)
Inventor
Gopalrao Atul Wankhade
Rajju Devidas Shroff
Raj Kumar ARORA
Lilaram Kamal Kataria
Raj Kumar Tiwari
Amul Manubhai Desai
Vic Prasad
Original Assignee
Upl Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Upl Ltd filed Critical Upl Ltd
Publication of CR20220188A publication Critical patent/CR20220188A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/22—Amides of acids of phosphorus
    • C07F9/26—Amides of acids of phosphorus containing P-halide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/22—Amides of acids of phosphorus
    • C07F9/24—Esteramides
    • C07F9/2454—Esteramides the amide moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/2479—Compounds containing the structure P(=X)n-N-acyl, P(=X)n-N-heteroatom, P(=X)n-N-CN (X = O, S, Se; n = 0, 1)
    • C07F9/2487—Compounds containing the structure P(=X)n-N-acyl, P(=X)n-N-heteroatom, P(=X)n-N-CN (X = O, S, Se; n = 0, 1) containing the structure P(=X)n-N-C(=X) (X = O, S, Se; n = 0, 1)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/14—Sulfur, selenium, or tellurium compounds of phosphorus
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/22—Amides of acids of phosphorus
    • C07F9/24—Esteramides
    • C07F9/2454—Esteramides the amide moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/2479—Compounds containing the structure P(=X)n-N-acyl, P(=X)n-N-heteroatom, P(=X)n-N-CN (X = O, S, Se; n = 0, 1)
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/26—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-nitrogen bonds
    • A01N57/28—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-nitrogen bonds containing acyclic or cycloaliphatic radicals
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Compression, Expansion, Code Conversion, And Decoders (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invención describe un proceso mejorado para la preparación de acefato e intermedios de este. Más particularmente, la presente invención se refiere a un proceso para la preparación de cloruro de tiofosforilo útil para la producción comercial de pesticidas y compuestos farmacéuticamente activos.
CR20220188A 2019-10-19 2020-10-13 Proceso para la preparación de cloruro de tiofosforilo y acefato. CR20220188A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IN201921042520 2019-10-19
PCT/IB2020/059584 WO2021074775A1 (en) 2019-10-19 2020-10-13 Process for preparation of thiophosphoryl chloride and acephate

Publications (1)

Publication Number Publication Date
CR20220188A true CR20220188A (es) 2022-06-21

Family

ID=75538629

Family Applications (1)

Application Number Title Priority Date Filing Date
CR20220188A CR20220188A (es) 2019-10-19 2020-10-13 Proceso para la preparación de cloruro de tiofosforilo y acefato.

Country Status (12)

Country Link
US (1) US12281131B2 (es)
JP (1) JP7773462B2 (es)
KR (1) KR20220086617A (es)
CN (1) CN114728791A (es)
AR (1) AR120238A1 (es)
AU (1) AU2020366145A1 (es)
BR (1) BR112022007515A2 (es)
CA (1) CA3158017A1 (es)
CR (1) CR20220188A (es)
MX (1) MX2022004691A (es)
PY (1) PY2065741A (es)
WO (1) WO2021074775A1 (es)

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE834243C (de) * 1948-11-17 1952-03-17 Bayer Ag Verfahren zur Herstellung von Phosphorsulfochlorid
US2850354A (en) 1953-07-22 1958-09-02 Monsanto Chemicals Manufacture of thiophosphoryl chloride
US2715561A (en) 1953-10-02 1955-08-16 Florian F Knotz Method of preparing thiophosphorylchloride
DE1145589B (de) 1959-06-06 1963-03-21 Ministerul Ind Petrolului Verfahren zur Herstellung von Phosphorsulfochlorid
DE2032832A1 (en) * 1969-08-04 1971-02-18 Bitterfeld Chemie Catalytic preparation of phosphorus sulpho- - chloride
JPS53116295A (en) * 1977-03-22 1978-10-11 Sumitomo Chem Co Ltd Production of thiophosphoryl trichloride
JPS6475494A (en) * 1987-09-17 1989-03-22 Nippon Soda Co Production of n-acyl, o,s-dimethylphosphoroamidethioate
JP3291987B2 (ja) * 1995-08-07 2002-06-17 住友化学工業株式会社 Ｏ，ｓ−ジメチル−ｎ−アセチルホスホルアミドチオエートの精製法
US5464600A (en) * 1994-12-27 1995-11-07 Bayer Corporation Amine catalyzed reaction in the production of thiophosphoryl chloride
JP3409590B2 (ja) * 1996-06-20 2003-05-26 住友化学工業株式会社 Ｏ，ｏ−ジメチルホスホロアミドチオエートの製造法
US6251350B1 (en) * 1999-06-21 2001-06-26 Bayer Corporation Process for the manufacture of thiophosphoryl chloride
CN102603795A (zh) * 2011-01-22 2012-07-25 李坚 以磷酰氯为原料一步反应合成乙酰甲胺磷
CN208151245U (zh) 2018-03-13 2018-11-27 吴德华 一种半连续生产o,o-二甲基硫代磷酰氯的系统

Also Published As

Publication number Publication date
AR120238A1 (es) 2022-02-09
US20230002424A1 (en) 2023-01-05
US12281131B2 (en) 2025-04-22
CA3158017A1 (en) 2021-04-22
CN114728791A (zh) 2022-07-08
BR112022007515A2 (pt) 2022-07-12
WO2021074775A1 (en) 2021-04-22
KR20220086617A (ko) 2022-06-23
JP7773462B2 (ja) 2025-11-19
JP2022553239A (ja) 2022-12-22
PY2065741A (es) 2021-08-13
AU2020366145A1 (en) 2022-05-19
MX2022004691A (es) 2022-05-10

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