CS218863B1 - Method of the controlled rafination by the sulphuric acid - Google Patents

Description

- 1 - 218 883

Ha3Bamie η300ρθτθηηη

Ciiocod ynpasjíneMoií cepHOKHCJioTHoíi pa ^ Hamm - 3 -

J ΗΘΗΜΗ Ρ Ο Ρ Ρ 3 3 3 3 3 3 3 3 3 3 c oc 3 3 3 3 3 3 K 3 io

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CodHpaioiiiHecH πρπ one hundred meters hjih πολο0ηημ cnocode KHCJiue cmojiu 218863 - 2 - The aqjdkhh Óhtb nepepaóOTanH b οπθιχειολβηϊιχ ycTSHOBKax mm seHanpaBjíeHH Ha xpanemie b de3onacnoQ jyifl OKpyataioiueií opejmΜβοτο mm aojishh óhtb odpadoTajm οοοτΒβτοτΒ ^ οΐφίΜΗ HeftTpajm-3yKiiíHMn BeniecTBaMH ancopdHpyroinHMH areHTaMH mm.

AND

Cnocoda papHHaimu c πομοπιβιο cepHOii khcjioth, ojieyiwa n / mmKHCJIHX CMOJI C ΠΟΒΗΠΙθΗΗΗΜ ΟΟββρΧΘΗΗΘΜ CepHOÍi KHCJIOTH flJLH ΠΟ-jiyHeHHH cneimajiBHux Mace h Julho pereHepapoBaima OTpadoTan-HHX Mace oóJiajxaíOT τβΜ He ^ ocTaTKOM, HTO ckopocth BKnejieraiHKHCJIHX (MY H3 peaKUHOHHOÍÍ ΟΜΘΟΗ HBJHWTCH ΟΗβΗΒ M3JIHMH HΟφορίΟΘΗΗΘ HX B 3βθ ΗΘΠρβρΗΒΗΗΧ ΠρΟΙξβΟΟΰΒ H3-3a BHOOKOÍÍnpOAOJDKHTeJILHOCTH ΒΗΑθΛβΗΗΗ CTaHOBHTCH ΗβΒΟ3ΜΟ3ΚΗΗΜ HJIH BO3-MOSHHM TOJIBKO IIpH yCJIOBHH dOJIE © BHCOKHX 3aTpaT.

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Pad o K 3 oj oj 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3

Bue MaTepnanu, Kas cepnaa KHOJioTa, cmojih h Macjia. *

Eme oahhm ηθαοοτητκομ cepHOKHCJioTHoli pa ^ HHaimu yrjieBo-flopojmux Máčejí hbjlíwtch Bucoime ποτθρκ Macjia - and about 25 ceB. $.

UejiB H3odpeTeHHg

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HaJioseHHe cyigHOOTH h3oópgt6hhh B οοηοβθ ΗβοόρβτβΗΗΗ jiesHT 3aAana pa3paČ0TKH cnocoda, κο-Topirií no3BOJiHT c πομοιηβιο cooTBeTCTByiouíHX AodasoK tokiim by-paaoM peryjmpoBaTB cepHOKHCJiOTnyio pa ^ Hnaumo, npeAHasHa ^ eH-Hyio rjir pereHepapoBaHUH OTpadoTaHHHX Wace h jym nojiyqeiiHHcneunaziBHUx Mace h hhcthx yimeBOAopoAOB, HTO b KORA ρθακ -ijhh pa4> HHaram odpa3yioTca onpejjejieHHue $ a3u Macjia, cmojih mkhcjioth, οκοροοτΒ ΒΐΐΛθΛβΗΗΗ $ a3 H3 peaKijKOHHofi CMecn dyjjeTnoBinneHa h oTiiajjaeT HeodxoAHMOCTB nepepadoTKH cmojih h khc-jioth. B οοοτΒβτοτΒΗΗ c H3odpeTeHueM κ peaKUHOHHoň CMecn, coctoh-meii H3 yrjteBOflopoaHHX Mace h khcjioth b 38βηοημοοτη otKQjnraecTBa cpejjCTBa ívlh pa ^ HHaijHH I ycTaHOBJíeraioro y ^ e H3 βθοτηημ cnocodoM, nocjie jjodaBneHHH ero hjih the nocjie οοοτβθτCTByromero OKOHHamia βρθμθηη pearajHH npn nepeMeiuHBaraiH h npnTeMnepaType ot 20 ° C and 60 ° C AodaBJímTT 0.01 o 3.0 nac-ΤΘΜ CMOJIHHOIO KOMHOHeHTa H OT 0.3 RO 1.5 HaCTH BOAH, peaKUJIOHHyio CMecB nepeBOAHT b annapaT-οτοτοΗΗΗΚ, b κοτοροΜ nocjie yuajunoTCH Macjio - khk BepxHaa, cwojia - kok cpeAmra Han KHCJiOTa - khk hhjkhhh $ aaa. nonyHaromascH 50-70% -a cepnaa KHCJiOTa h CMOJi MoryT óhtbHCn0JIB30BaHH Β KaHQCTBe ΒΤΟρΗΊΗΟΓΟ CUpBff ΠρΗ πρ0Η3Β0Α0ΤΒβMHHepajiBHux ysodperaiíi h npn cTpoHTejiBCTBe Aopor.

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50 B6C ·% CMOJIH

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Claims (1)

OBJECT OF THE INVENTION 218 863 A process for the controlled refining of sulfuric acid for the purpose of regenerating used oils and obtaining special oils and pure hydrocarbons, characterized in that for the refining of the reaction mixture from sulfuric acid and hydrocarbon oils, depending on the amount of refining agent provided by the known method, water is added after the addition, optionally after a certain reaction time, at a temperature of 20 to 60 ° C, preferably 20 to 40 ° C, of a resin component having a composition of 40 to 95 wt. % resin, 5 to 50 wt. % sulfite acids, 0.1 to 25 wt. % sulfuric acid, P, 1 to 25 wt. % of water obtained from the controlled refining of hydrocarbons with sulfuric acid in the addition of water, separately or in the form of a mixture of the refining agent to the resin component and to the water 1: 0.01: 0.3 to 1: 3.0: 1.5, with preferably 1: 0.02: 0.5 to 1: 2.5: 1.2, whereupon the refining reaction mixture is separated into a sulfuric acid phase, a resin phase and a refined oil phase, wherein the acidic and resin phases are predominantly in the period of sedimentation and / or heating up to 40 to 100 ° C and sulfuric acid, resin and refined oil are obtained in divided form. Recognized by the invention on the basis of the results of an expert review by the Office of Invention and Patenting, Berlin, DD. Printed by Moravian Printing Works, Operation 12, Leninova 21, Olomouc Price; 2,40 Kčs