CS222962B1

CS222962B1 - Method of coating semiconductor devices with dip coating

Info

Publication number: CS222962B1
Application number: CS146879A
Authority: CS
Inventors: Georg Pfeil; Jurgen Henneberger; Peter Degenkolb; Wolf-Helge Lehman; Anita Voigt; Helga Meier; Peter Baumann
Original assignee: Georg Pfeil; Jurgen Henneberger; Peter Degenkolb; Lehman Wolf Helge; Anita Voigt; Helga Meier; Peter Baumann
Priority date: 1978-03-15
Filing date: 1979-03-05
Publication date: 1983-08-26
Also published as: PL214138A1; DD138490A3

Abstract

Cílem vynáleau je pokrývání polovodičových přístrojů hmotou, u níž se dosahuje hladký povrch, který nemá póry a trhliny a také vysoká odolnost vůči klimatickým účinkům při elektrickém zatížení a kromé toho, zajišiuje se vysoká životnost nevyužité hmoty pro povlaky. Úkol, vynálezu spočívá v tom, aby se vyloučilo použití hermetických těles a odstranily nedostatky již známých způsobů ponořování, a kromě toho, aby se zajistily nové provozní jakosti pro polovodičové přístroje zpracované ponořením s tím, že se musí najiti stejnorodý systém složek jako hmota pro pokrytí. V souladu s vynálezem, hmota pro pokrývání představuje jednotlivé složky: látku, zvyšující adhezi, prostředek pro vytváření příčných vazeb mezi makromolekulami a silikonový kaučuk. Složky se nanášejí na polovodičové přístroje v dané následnosti za sebou u několika ponořeních, po každém ponoření následuje sušení a tak nepřicházejí navzájem do styku. Po tomto polovodičové přístroje se nechají na výdrž při teplotě nad 100 °C, převážně při 120 °C. Je možné uskutečnit! cílevědomý nárůst vrstvy silikonového kaučuku o viskositě 70 000 ± 20 000 mPa.c.The aim of the invention is to cover semiconductor devices with a substance that achieves a smooth surface that is free from pores and cracks and also has high resistance to climatic effects under electrical load and, in addition, ensures a high service life of the unused coating substance. The task of the invention is to eliminate the use of hermetic bodies and eliminate the shortcomings of the already known dipping methods, and in addition, to ensure new operational qualities for semiconductor devices processed by dipping, with the need to find a homogeneous system of components as a coating substance. In accordance with the invention, the coating substance represents individual components: a substance that increases adhesion, a means for creating cross-links between macromolecules and silicone rubber. The components are applied to the semiconductor devices in a given sequence one after the other in several dippings, each dipping is followed by drying and thus do not come into contact with each other. After this, the semiconductor devices are left to stand at a temperature above 100 °C, mainly at 120 °C. It is possible to carry out a targeted growth of a layer of silicone rubber with a viscosity of 70,000 ± 20,000 mPa.c.

Description

Způsob pokrývání polovodičových přístrojů povlaky ponořovánímMethod of covering semiconductor devices by dip coating

Cílem vynáleau je pokrývání polovodičových přístrojů hmotou, u níž se dosahuje hladký povrch, který nemá póry a trhliny a také vysoká odolnost vůči klimatickým účinkům při elektrickém zatížení a kromé toho, zajišiuje se vysoká životnost nevyužité hmoty pro povlaky. Úkol, vynálezu spočívá v tom, aby se vyloučilo použití hermetických těles a odstranily nedostatky již známých způsobů ponořování, a kromě toho, aby se zajistily nové provozní jakosti pro polovodičové přístroje zpracované ponořením s tím, že se musí najiti stejnorodý systém složek jako hmota pro pokrytí.The aim of the invention is to coat the semiconductor devices with a material which provides a smooth surface that is free of pores and cracks, as well as high resistance to climatic effects under electrical load and, in addition, ensures a long service life of the unused coating material. SUMMARY OF THE INVENTION The object of the invention is to avoid the use of hermetic bodies and to eliminate the shortcomings of the already known immersion methods and, in addition, to ensure new operating qualities for immersion-treated semiconductor devices. .

V souladu s vynálezem, hmota pro pokrývání představuje jednotlivé složky: látku, zvyšující adhezi, prostředek pro vytváření příčných vazeb mezi makromolekulami a silikonový kaučuk.In accordance with the invention, the coating composition comprises the individual components: an adhesion promoter, a cross-linking agent between the macromolecules and a silicone rubber.

Složky se nanášejí na polovodičové přístroje v dané následnosti za sebou u několika ponořeních, po každém ponoření následuje sušení a tak nepřicházejí navzájem do styku. Po tomto polovodičové přístroje se nechají na výdrž při teplotě nad 100 °C, převážně při 120 °C.The components are applied to the semiconductor devices in succession for several immersions, each drying being followed by drying and thus do not come into contact with each other. After this, the semiconductor devices are allowed to withstand temperatures above 100 ° C, mainly at 120 ° C.

Je možné uskutečnit! cílevědomý nárůst vrstvy silikonového kaučuku o viskositě 70 000 ± 20 000 mPa.c.It is possible to realize! a purposeful increase in the layer of silicone rubber having a viscosity of 70,000 ± 20,000 mPa.c.

222 962222 962

Ha3B3HHe H3oópeTeHHaHa3B3HHe H3ooppeTeHHa

Cnocod ΠΟΚρΗΤΗΗ HOJiyiipOBOflHHKOBHX HpHÓOpOB OdOJIOHKQMH oKyHaHHeM * -Cnocod ΠΟΚρΗΤΗΗ HOJiyiipOBOflHHKOBHX HpHoOpOB OdOJIOHKQMH oKyHaHHeM * -

OdJiaCTL· HBHM6H6HHH HSOdpeTQHHH - ' 'OdJiaCTL · HBHM6H6HHH HSOdpeTQHHH - ''

H3odpeTemie KacaeTca cnocoda hokphthh οκτήηηηθμ nojiyupoBOflHHKOBHX HpHdopOB QÓQJÍQ^SSSSSÍ B HaCTHOCTH ΜΗΚρΟΟΧβΜ, KOTopae MoryT ιτρημθηητβοη irpu 3HaaiiTe^LHoS β>ι&κηοοτϊι oKpyxaDGieĚ cpesa h k Ha^exHocTH κοτορυχ npej^BBJBWTca ποβηοιθηHue TpedoBaHHH.H3odpeTemie KacaeTca cnocoda hokphthh οκτήηηηθμ nojiyupoBOflHHKOBHX HpHdopOB QÓQJÍQ ^ sssss B HaCTHOCTH ΜΗΚρΟΟΧβΜ, KOTopae Ballad ιτρημθηητβοη irpu 3HaaiiTe Lhoste ^ β> ι & κηοοτϊι oKpyxaDGieĚ CPEs to h ^ Ha ^ exHocTH κοτορυχ npej BBJBWTca ποβηοιθηHue TpedoBaHHH.

XapaKTepscToa %3bgcthhx TexigraeoKHx pemeHMXapaKTepscToa% 3bgcthhx TexigraeoKHx pemeHM

JUh 3auíHTH ot MexamreeeKHX Harpy30K h ot spejmax BO3#eĚctbhí oRpysaioinet cpe^a HoxyupoBOSHHKOBae npHdopHsaKxmaiDT B OdOJIOTOE. Tas KaK H60dX0#HM0CTL B 3WITe BHyTpHnpHdopHHX cxew, a Taxse ycjroBHH oicpyscamet epe#a ohchb paaoraHH, to h ancjio μθτο#οβ 3aKjnoaeffita noJiyiipoBOAHHKOBax BpadopoB b odOJTOHKH BeCLMa B6JE0KO.JUh 3auíHTH ot MexamreeeKHX Harpy30K h ot spejmax BO3 #Ectbhí oRpysaioinet cpe ^ a HoxyupoBOSHHKOBae npHdopHsaKxmaiDT B OdOJIOTOE. Tas KaK H60dX0 # HM0CTL B 3WITe BHyTpHnpHdopHHX cxew, and Taxse ycjroBHH oicpyscamet epe # and ohchb paaoraHH, it h ancjio μθτο # οβ 3aKjnoaeffita noJiyiipoBOAHHKBoToHoHoBoHoBoHoBoHoBoKoHoBoHoBoHoBoHoBoKoHoKoHoKoHoKoW

Pa3jmaioT repMeureHae h HerepMeTwme odoxoHKH. Γθρμθτϊηηημη odojio^Kaj® HasuBaiOT Taraie aopuyca, κοτορπβ ημθώτ τθήβ 1,33 . ΙΟ~θ Ha . ju c*“¹ /b pacaeTe Ha rejnrir npn pa3HHae xaBJíeHHĚ b I awí 3th aopuyca η3γοϊ3κώιβηκιτοη c πρημθηθhhsm MeTaooB, cTeoa h κθροκοεκΗ. Exaroflapa np^Menenz©Pa3jmaioT repMeureHae h HerepMeTwme odoxoHKH. Ojθρμθτϊηηημη odojio ^ Kaj® HasuBaiOT Taraie aopuyca, κοτορπβ ημθώτ τθήβ 1,33. Ha ~ θ Ha. ju c * ' ¹ / b pacaeTe Ha rejnrir npn pa3HHae xaBJíeHHe b I awi 3th aopuyca η3γοϊ3κώιβηκιτοη c πρημθηθhhsm MeTaooB, cTeoa h κθροκοεκΗ. Exaroflapa np ^ Menenz ©

3THX KOpnyCOB, 3£βΚΤρθΗΗΗβ ΒΛθΜΘΗΤΗ MOSHO npeflOXpaHHTB OT Bcex ΒΗβΠΕΗΗΧ B03&eScTBHŽ, ΚρΟΜΘ TOMHGpaTypií OKpy$aW& cpe#H. Jto 3τογο Kopnyca HanowwTCH ηηθρτηπμ h cyxHM ra3om. IIpoaeccH repMeTsaaijfflí npom^HTca b aTMOCpepe τθχηοjroraaecKHx ra30B. Kpowe τογο, nojiyupoBojcHESOBne npsdopa iiepe# repMeTH3anHet ode3ramasTCH b BaayyMHHX neaax, ySMeHHH aíícopdHpoBaHHot BaarH. Hocjie 3amHeH&s b oóojioh- 2 Ky HeoóxofíHMa npoBepKa Ha γθρμθτηηηοοτβ. ΙΪ3βθοτηη οομηθ pa3JnraHHe μθτο#η repMeTH3anHH. Tas, HanpHMep, πρκ óTKa3e ot opraHHHecKHX MaTepnajioB'_t H3Becrao MeTajuni3HpoBaHřie odpaTHOK CTOPOHH nOjyiOJKKH ΜΗΚρΟΟΧΘΜΗ Η ΠρΗΙΙ3ΗΒ3ΗΗΘ Θθ ΒΟΘΖ noBepxHocTLio κ ocHOBaimto Kopnyca mm KpenjieHHe c homodiko πρζηο^ίΗΟΓΟ cTeKJia. IÍ3-3a paoxoaóB na MeTaJum3amw npoine HpHKJieHBaTL ΒΗΥΤρίϊΠρΗόόρΗΗΘ ΘΛβΜβΗΤίΙ οποκοηληομ cmojioh.3THX COpnyCOB, 3 £ βΚΤρθΗΗΗβ ΒΛθΜΘΗΤΗ MOSHO npeflOXpaHHTB OT Bcex ΒΗβΠΕΗΗΧ B03 & eScTBHŽ, ΟΜΘρΟΜΘ TOMHGpaTypes OKpy $ aW & cpe # H. It is 3 years Kopnyca HanowwTCH h cyxHM ra3om. The βaeccH repMeTsaaijffli npom ^ HTca b aTMOCpepe τθχηοjroraaecKHx ra30B. Kpowe τογο, nojiyupoBojcHESOBne npsdopa iiepe # repMeTH3anHet ode3ramasTCH b BaayyMHHX neaax, ySMeHHH and moreopdHpoBaHHot BaarH. Hocjie 3 amHeH&s b ooojioh- 2 Ky HeooxophiHMa npoBepKa Ha γθρμθτηηηοοτβ. ΙΪ3βθοτηη οομηθ pa3JnraHHe μθτο # η repMeTH3anHH. Tas, HanpHMep, πρκ óTKa3e ot opraHHHecKHX MaTepnajioB ' _t H3Becrao MeTajuni3HpoBaHri odpaTHOK CTOPOHH nOjyiOJKKH ΟΟΧΘΜΗρΟΟΧΘΜΗ Π ΠρΗΙΙ3ΗΒ3ΗΗΘ ΘikoHHoHo cepoHoBepxHoc ocΘToHoBioPoHoHoBepxHoc. I3-3a paoxoaóB on MeTaJum3amw npoine HpHKJieHBaTL ΒΗΥΤρίϊΠρΗόόρΗΗΘ ΘΛβΜβΗΤίΙ οποκοηληομ cmojioh.

JUh repMeTH3ai#ní KopnycoB η3βθοτηη τθκηθ onocoda, ksk hmnyjiBCHaH KoímeHcaTopsas CBapKa, jia3epHaa cBapKa, θλθκτροηHO-Jiy^eBaH cBapica,. natóa c ctoocaMH mm de3 hhx, jmdo řep- * MeTH3anjra o noMoncbio nae^Horo CTe^Jia, irpu κοτοροδ: KpimiKa Kopnyca οοθεηηηθτοη o paMož Kopnyca ,ηη3κοππ3Βκημ cTemiOM.JUh repMeTH3aionni KopnycoB η3βθοτηη τθκηθ onocoda, ksk hmnyjiBCHaH KoemeHcaTopsas CBapKa, jia3epHaa cBapKa, θλθκτροηHO-Jiy ^ eBaH cBapica ,. natóa c ctoocaMH mm de3 hhx, namb- * MeTH3anjra o noMoncbio nae ^ Horo CTe ^ Jia, irp κοτοροδ: KpimiKa Kopnyca οοθεηηηθτοη o paMož Kopnyca, ηη3κοππ3Βκημ.

ΓβρΜΘΤΗ33ΙζΠΗ C ΙΙΟΜΟΙΜ ΟρΓβΗΗΗβΟΚΗΧ ΚΛθθΒ HecpaBHHMa C μθτολημη repMerasatwJXTMeTajraHsaniHeft mni ο ποΜοπξκο GTemia, t.k. Bce opramraecKue HCKyccTBeHHne MaTepnazni b pe3y3ii»Taτθ κορρο3ΗΗ nponycKaiOT BJiary.EcβρΜΘΤΗ33ΙζΠΗ C ΙΙΟΜΟΙΜρΓβΗΗΗβΟΚΗΧ ΚΛθθΒ HecpaBHHMa C μθτολημη repMerasatwJXTMeTajraHsaniHeft mni ο ποniοπξκο GTemia, t.k. Bce opramraecKue HCKyccTBeHHne MaTepnazni b pe3y3ii »Taτθ κορρο3ΗΗ nponycKaiOT BJiary.

BnaronapH repMeTH3anHH? nojiyirpoBonHHKOBHx πρπόοροΒ b othx Kopnyoax sogthtqjotch χοροιππθ 3KcmiyaTaiíH0HHiíe cBoiicTBa b TpedyeMoS TeMnepaTypHOH odjiacTH h npn padoTe bo bjis^hoS cpe^e. ΟΛΗΟΒρβΜΘΗΗΟ ΗΘΛΪ>3Η yiiyCKaTL H3 BH£a, OTHOCHTejILHO bhcokhs 3aTpara Ha repMeTH3auřw KopnycoB, KaK Hanpmep, npH ΜΘΤΗΟΗ3ζ3Ιξ0Η, ΠρΟΒβρΚβ Ha ΓβρΜΘΤΗΗΗΟΟΤΒ H Tifl.BnaronapH repMeTH3anHH? nojiyirpoBonHHKOBHx πρπόοροΒ b othx Kopnyoax sogthtqjotch χοροιππθ 3KcmiyaTaíH0HHiee cBoiicTBa b TpedyeMoS TeMnepaTypHOH departing th h npn ^ e psoTe bo cj e b e n e p b e. ΟΛΗΟΒρβΜΘΗΗΟ ΗΘΛΪ> 3Η yiiyCKaTL H3 BH £ a, OTHOCHTejILHO bhcokhs 3aTpara Ha repMeTH3aurw KopnycoB, KaK Hanpmep, npH ΜΘΤΗΟΗ3ζ3Ιξ0Η, ΠρΟΒβρΚβ Ha ΓβρΜΘΤΗΗΗΟΟΤΒ H Tifl.

Jlajiee η3Βθοτηη cnocoda 33κώοηθηηη b~ HerepMeTiPžHHe odojiomoa, TaK HanpHMep, πρηηητο, noKpuBaTB nojiynpoBojymKOBHe npadopu JUIH ΚΟρΟΤΚΟΒρβΜΘΗΗΟΗ 3ΗϋξΗΤΙί OT Β03£βΚ0ΤΕΗΗ BJI3PH ΟΛΟθΜ JiaKa. JUs opraHEraecKHx 3amnTHnx cjioeB, conepnamnx ro 3aTBepKeBaHHH peaKTHHHHe rpymm, Heodxojwo ynHTHBaTB βο3μο3κκοθ Η3ΜΘΗβΗΗΘ GOUpOTHBJíeHKH ΟΛΘΜΘΗΤΟΒ ΜΗΚρΟΟΧΘΜ. 3ΤΗ CJIOH JISKa HaHOCHTCH C ΠΟΜΟΙ3ΪΒΙΟ KHCTH, ρθΟΠΣϋΙΘΗΗΘΜ, ΟΚΥΉΗΗΗβΜ mm onpeocoBKoíi. Ohh He odecnenHBaioT AocTaTOHHot 3ainHTH οτ μθΧΗΗΗΉΘΟΚΗΧ B03fleĚCTBHS. ΠρΗ ΠΟΚρίΙΤΗΗ HOJiyiipOBOJlHHKOBHX npHdopOB THKCOTpOHHUMH CMGJIHMH, TOJICTKM CJIOH ΟΗΗΤΘΤΗΗβΟΚΟro MaTepnana odecnenHBaeT 3acpiTy ot κπημητηηθοκηχ B03fleSctbzh h μθχηηηηθοκηχ Harpy30K. OdojioHKa odpasyeTcn b pe3yjn>TaTe oKyHaHHH nojiynpoBo^HHKOBHX npsdopoB b thkcotpohHyio cMony, HanpHMep, ^eHOJio-ajiLserEmHyio mm onoKCHKHyraJlajiee η3odaθοτηη cnocoda 33kΒοηθηηη b ~ HerepMeTiPžHHe odojiomoa, TaK HanpHMep, πρηηητο, noKpuBaTB nojiynpoBojymKOBHe npadopu JUIH ΚΟΚΟΟΤΚΟΒΟΤΚΟΒ O OΚΚΚΗϋΗϋΗϋΗϋΗϋΗϋΗϋΗϋΗϋΗϋ JUs opraHEraecKHx 3amnTHnx cjioeB, conepnamnx ro 3aTBepKeBaHHH peaKTHHHH rpymm, Heodxojwo ynHTHBaTB βο3μο3κκοθ Η3ΜΘΗβΗΗΘ GOUpOTHBJíeeKH. 3ΤΗ CJIOH JISKa HaHOCHTCH C ΟΜΟΙΟΜΟΙΪΒΙΟΪΒΙΟ KHCTH, ρΟΟΣϋΙΘΗΗΘΜ, ΟΚΥΉΗΗΗβΜ mm onpeocoBKoíi. Ohh He is pricedHaBaioT AocTaTOHHot 3ainHTH οτ μθΧΗΗΗΉΘΟΚΗΧ B03fleĚCTBHS. ΠρΗ ΠΟΚρίΙΤΗΗ HOJiyiipOBOJlHHKOBHX npHdopOB THKCOTpOHHUMH CMGJIHMH TOJICTKM CJIOH ecβΟΚΟro MaTepnana odecnenHBaeT 3acpiTy ot κπημητηηθοκηχK03 h03f. OdojioHKa odpasyeTcn b p3yjn> TaTe oKyHaHHH nojiynpoBo ^ HHKOBHX npsdopoB b thkcotpohHyio cMony, HanpHMep, ^ eJJio-ajiLserEmHyio mm onoKCHKHyra

- 3 cmojih.- 3 cmojih.

J^ajiee η3βθοτθη cnocod βηχρθβογο ηοπηηθηκη, npn κοτοροΜ ΛΟΟΤΗΓΗΘΤΟΑ ΙΙΟΚρΗΤΗΟ ΟΗΗΤΟΤΗΊΟΟΚΗΜ MaTepHaJIOM TOJUipíHOH flO HeCKOJIBKHX fteCHTHX MHJUEHMCTpa. HaCTB nOJiyirpOBOflHHKOBHX npadopoB, nojvie^amaa hokphthh, HarpeBaeTCH ao I20°-I8Q° C, a 3aTeM noffBepraeTCH Βθ3Λβ2οτΒΗΚ) β3βηχρθηηογο H3MejiBneHHoro b hhjií rpaíiyjiHTa. 3aTBepaěBaiQniet upa KOMHaraoS TeMnepaType, HO eiHe peaJKTHBHOfi OjmOKOMHOHeHTHOS CMOJIH. CHHTeTHHeCKafl ' CMOJia npHKJieiíBaeTCH κ pasoipeToS nacTH, t.k. upa θτοη TeMnepaType OHa pasMamaeTca. 3aTeM CMona 3aTBep#eBaeT npn 3toě TeMnepaType OKOHnaTejiLHO.J ^ ajiee η3βθοτθη cnocod βηχρθβογο ηοπηηθηκη, npn κοτοροΜ ΛΟΟΤΗΓΗΘΤΟΑ ΙΙΟΚρΗΤΗΟ ΟΗΗΤΟΤΗΊΟΟΚΗΜ MaTepHaJIOM TOJUipíHOH flO HeCKOJIBKHX fteCHTHX MHJUEHMCTpa. HaCTB nOJiyirpOBOflHHKOBHX npadopoB, nojvie ^ amaa hokphthh, HarpeBaeTCH and I20 ° -18 ° C, and 3aTeM noffBepraeTCH Λθ3Λβ2οτΒΗΚ) β3βηχρθηηογο H3MejiBi hBi B ej ji ji ji ji ji ji. 3aTBepaiBaiQniet upa KOMHaraoS TeMnepaType, HO eiHe peaJKTHBHOfi OjmOKOMHOHeHTHOS CMOJIH. CHHTeTHHeCKafl 'CMOJia npHKJieiíBaeTCH and pasoipeToS nacTH, t.k. Upa θτοη TeMnepaType OHa pasMamaeTca. 3aTeM CMona 3aTBep # eBaeT npn 3toe TeMnepaType OKOHnaTejiLHO.

TeiuionpoBOAHOGTL TaKHX odojionen nojiynpoBojWKOBHX npiidopoB HefíocTaTOHHa. ΚροΜβ τογο, H3roToaBjmeMHe τθκημ odpa3OM odoJIOHKH ΕΕΜΘΙ0Τ HenpaBHJIBHyB) ΓΘΟΜΘΤρΗΗΘΟΚ^ΊΟ $opMy. JJpyTOH CHOcod 3amiKPieHHH nOJlynpOBOJÍHHKOBHX UpndopOB B odOJIOHKH sto 3ajiHBKa nx b ^opMax, HanpuMep, H3 imacTMaccH hjqí MeTanjia. IIojiyiipoBOAHHKOBHe npndopn 3aKjia#HBaioTCH b φορτ^Η. OcTasniHecH nycTodu sanojnunoTcn bhjíkoh cmojio®, KOTopaa 3aTeu 3aTBep£eBaeT. HeodxoflHMO πρημθηητβ npn stom xopoino ode’3raseHHHe cmojih, jyra τογο, HTodu ho odpa3OBHBajincL ny3upLKH. Bo3mohho TaKse norpynaTL nojiynpoBOflHHKOBHe npndopH b φορΜΗ, 3anojmeHHHe TpedyeMot nopnnen cmojih.TeiuionpoBOAHOGTL TaKHX odojionen nojiynpoBojWKOBHX npiidopoB HefiocTaTOHHa. 3ροΜβ τογο, H3roToaBjmeMHe θκκ odpaa a od od od od od od od od od od od JJpyTOH CHOcod 3amiKPieHHH nOJlynpOBĚHHKOBHX UpndopOB B odOJIOHKH one hundred 3ajiHBKa nx b ^ opMax, HanpuMep, H3 imacTMaccH hjqí MeTanjia. IIojiyiipoBOAHHKOBHe npndopn 3aKjia # HBaioTCH b φορτ ^ Η. TOTALNECODE OF SANYUNUNUNCTION BIOSYON®, KOTopaa 3aTeu 3aTBep £ eBaeT. HeodxoflHMO πρημθηητβ npn stom xopoino od'3raseHHH cmojih, jyra τογο, HTodu him odpa3OBHBajincL ny3upLKH. Bo3mohho TaKse norpynaTL nojiynpoBOflHHKOBHe npndopH b φορΜΗ, 3anojmeHHHe TpedyeMot nopnnen cmojih.

Enaro^apn dojininoK TOjnuHHe cjioh miacTMaccoBoro ποκρητηη, MOJKHO ΛΟΟΤΗΓΗΥΤΒ dOJiee jyniTejIBHOrO ΒρβΜβΗΗ 33ΰξΚΤΗ οτ aTΜΟύφθρΗΟΗ BJiarn. ΗθΟΜοτρη Ha sto, Bjiara npoHHKaeT bo BHy— TpnupiídopHyio nacTL (MHKpocxeMy) b MecTax βηβοήοβ ducTpee, H6M CKB03L IUláCTMaCCy.Enaro ^ apn dojininoK TOjnuHHe cjioh miacTMaccoBoro ποκρητηη, MOJKHO ΛΟΟΤΗΓΗΥΤΒ dOJiee jyniTejIBHOrO ΰρβΜβΗΗ 33ΰξΚΤΗ οτ aTΜΟύφθρΗΟΗ BJiarn. HaθΟΜοτρη Hsto, Bjiara npoHHKaeT or BHy-TpnupiídopHyio nacTL (MHKpocxeMy) b MecTax βηβοήοβ ducTpee, H6M CKB03L IUláCTMaCCy.

Upa tojicthx cjiohx imacTMaccH Β03ΗΗκαθτ TSKse spyran npodjieMa, a ΗΜθΗΗΟ npodjieMa, MexammecKHX HanpjBKenHH, H3-3a bhcoKoro κοθφφπΐίΗβΗΤΗ pacnrapeHEH cmojih ho cpaBHeHHK) c hojíJIOKKOH. JtM ΤΟΓΟ, HTOdH npeflOTBpaTHTB npn 3T0M ΜθΧ8ΗΗΗθ0Κ0β pa3pymeHae cmojih, πρημθηηιοτοη cmojih c KanojnniTejLHMH hjdi cMeca cmoji c jyníTejiBHog ynpyrocTBK). Upasna πρπ θτομ yxyn,UiaCTCH TepMOCTadHJILHOCTB. HCKJHOHeHHe COCTaBJIHKT ΗθΚΟΤΟρΗθUpa tojicthx cjiohx imacTMaccH Β03ΗΗκαθτ TSKis spyran npodjieMa, and ammθΗΗΟ npodjieMa, MexammecKHX HanpjBKenHH, H3-3a bhcoKoro κοθφφπΐίΗβΗΤΗ pojnrapeHEH (ciHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHeHe) JtM HT, HTOdH npeflOTBpaTHTB npn 3T0M ΜθΧ8ΗΗΗθ0Κ0β pa3pymeHae cmojih, πρημθηηιοτοη cmojih c KanojnniTejLHMH hjdi cMeca cmoji c elseTejiBHog ynpyrocTB. Upasna πρπ θτομ yxyn, UIACTCH TepMOCTadHJILHOCTB. HCKJHOHeHHe COCTaBJIHKT ΗθΚΟΤΟρΗθ

- 4 204 536 sajniBO^HHe Maccu Ha da3e ciunncoHa, κοτορκθ o^hsko odecneqJŠfeaioT He3HaHHTejii>Hyio 3auiHTy ot MexamnecKHx Harpy3OK. ·- 4 204 536 sajniBO ^ HHe Maccu Ha da3e ciunncoHa, κοτορκθ o ^hsko odecneqJŠfeaioT He3HaHHTejii> Hyio 3auiHTy ot MexamnecKHx Harpy3OK. ·

ΚρΟΜβ ΤΟΓΟ, Η3ΒΘ0ΤΘΗ CHOCOd TpaHC$epHOÉ OIipeCCOBKH HOJiyUPOBOJÍHHKOBHX HpHdopOB, KOTOpuS OCOdeHHO 3Κ0Η0ΜΗΗΘΗ ITpH 'η3Γοτοβλ:θηηη dojiLinoro Hncjia fleTajreg. OjmaKO npH npuMCHeHmi 9ΤΟΓΟ CHOCOda HeodXOJWH ΛΟρΟΓΟΟΤΟΑΙφΙθ npecc$opMH. B KaΗΘΟΤΒΘ Ο^ξΗΟΚΟΜΙΙΟΗΘΗΤΗΟΗ ΟΗΟΤβΜΗ ΠρΗΜΘΗΗΙΟΤΟΗ CMOJIH Ha CHJIHKOHOBOH m 3nOKCH£HOH ΟΟΗΟΒΘ, ΚΟΤΟρΗβ B ΗθΟΤΒθρ^θΗΗΟΜ coctohhhh npeACTaBJLHKT codoS irpx KOMHaTHoS TewmepaType noροιποκ, a npH padoneS TewnepaTypé ot 130° flo 180° C HaxoflHTCfl B Bfl3KOSCH#KOM COCTOHHHH. 3tH CMOJIU 3anpeCC0BHBa»TCH B $opwy, odBOJiaramaioT 3aparaee 3ajioHeHHHĚ Tyjia nojiyupoBosHHKObhS npadop h 3aTBepfleBaroT β τβπβιπιβ 1-5 mhhyt. Bo3HHKai0T EpOdjlCMH 33ΒξΗΤΗ OT ΜθΧΗΗίΓΊΘΟΚΗΧ Haj?py30K, B HaCTHOCTH,HpHΒΟΛΗΠξΗθ K HOBpeSfteHHIO 3JieKTpOAHHX BHBOflOB. B padOHHX ycjiobhhx dojr&nme nepenajm TeMnepaTypu itphbojvit κ MexamnecKHM HanpWKeHHHM H, BCJieflCTBHe 3ΤΟΓΟ, K HOBpeEfteHHflM HOJVIOHKH hjih paspuBy coejviHeHHH τοκοΒθ,ο^ιίξΗΧ fleTajien. BcjiejicTBHH θτοΓΟ, HeodXOflHMO. npeABapHTeJIBHpe. ΠΟϊφΗΤΗβ HyBCTBHTeJIBHHX Π0JQrnpOBOJXHHKOBHX. OJieMeHTOB 3JiaCTHHHOŽ CRHHKOHOBOH MaCCOH (Bce ΟΠΗΟΘΗΗΗΘ £0 CHX nop CHOCOdH B3HTH H3i H.Delfsí Hybridtechnik. Internationale Elektronische Rundschau 1971> Heft 12,OCρΟΜβ ΤΟΓΟ, Η3ΒΘ0ΤΘΗ CHOCOd TpaHC $ epHOE OIipeCCOBKH HOJiyUPOBOJÍHHKOBHX HpHdopOB, KOTOpuS OCOdeHHO 3Κ0Η0ΜΗΗΘΗ ITpH 'η3Γοτοβλ: θηηreg dojiLinoro Hnc. OjmaKO npH npuMCHeHmi 9 ΤΟΓΟ CHOCOda HeodXOJWH ΛΟρΟΓΟΟΤΟΑΙφΙθ npecc $ opMH. B KaΗΘΟΤΒΘ Ο ΗΟΚΟΜΙΙΟΗΘΗΤΗΟΗ ΜΗ OJ OJ OJ ΗΜΘΗΗΙΟΤΟΗ OJ OJ OJ OJ Ha Ha Ha Ha Ha Ha Ha Ha Ha pad pad pad pad pad pad pad pad pad pad pad pad pad pad pad 3tH CMOJIU 3anpeCC0BHBa TCH B $ opwy, odBOJiaramaioT 3aparaee 3ajioHeHHH Tyjia nojiyupoBosHHKObhS npadop h 3aTBepfleBaroT β τβπβιπιβ 1-5 mhhyt. Bo3HHKai0T EpOdjlCMH 33ΒξΗΤΗ OT ΜθΧΗΗίΓΊΘΟΚΗΧ Hajpypy30K, B HaCTHOCTH, HpHΒΟΛΗΠξΗθ K HOBpeSfteHHIO 3JieKTpOAHHX BHBOflOB. B padOHHX ycjiobhhx we do not hire TeMnepaTypu itphbojvit and MexamnecKHM HanpWKeHHHM H, BCJieflCTBHe 3ΤΟΓΟ, HOBpeEfteHHflM HOJVIOHKH hjih paspuBy ejviοοΒΒΗΧΗΧΗΧοοΒΗΧΗΧΗΧΗΧΗΧΗΧοοΗΧΒΗΧΗΧοοΒΗΧΗΧοοοΒΗΧΗΧοοοΒΒΗΧΗΧοΗΧοΒοΗΧΒΗΧΗΧοΗΧοΗΧΗΧΗΧΗΧο. BcjiejicTBHH θτοΓΟ, HeodXOflHMO. npeABapHTeJIBHpe. ΠΟϊφΗΤΗβ HyBCTBHTeJIBHHX Π0JQrnpOBOJXHHKOBHX. OJieMeHTOB 3JiaCTHHOHO CRHHKOHOBOH MaCCOH (Bce ΟΠΗΟΘΗΗΗΘ £ 0 CHX nop CHOCOdH B3HTH H3i H.Delfsi Hybridtechnik. Internationale Elektronische Rundschau 1971> Heft 12,

Epcžie ΤΟΓΟ, H3B0CTHH cnocodu 38ΚΕΕ)ΗΘΗΗΗ HOJiyiipOBOJXHHKOBHX npHdopOB B OdOJIOHKy HyTeM OKyHaHHH (DE-AS 1 221 324,Epcie ΤΟΓΟ, H3B0CTHH cnocodu 38ΚΕΕ) ΗΘΗΗΗ HOJiyiipOBOJXHHKOBHX npHdopOB B BONDS HyTeM OKyHaHHH (DE-AS 1 221 324,

DB-OS 1 540 408).DB-OS 1,540,408).

TaK, HanpHMep, Η3ΒΘ0ΤΗ0 ΗΟΚρΗΤΗβ HHTerpaJILHUX ΜΗΚρΟΟΧΘΜ jvlh 3aníHTH ot KJEHMaTHHecKHX BO3^oficTBHjí dyHa-uaynyKOM, a JVIH 3aHIHTH OT ΜΘΧΗΗΗΗΘΟΚΗΧ Harpy3OK $eHOJIO-aJL&JieiTHHOH cmojioh ( dd-ps 96 381). HeodxojwaH ropanan cyinua Φθηολβηοaju^ernsHot cmojih npn 160 °C npHBOjyíT ojvíhko κ Η3ΜΘηθηηημ CBOĚCTB pa3JfflHHHX CJIO&HHX ΟΚΟΤΘΜ, Κ£Κ HanpHMep, CJIOH CrNi · ΚρΟΜΘ ΤΟΓΟ, B OdOJIOHKe Β03ΗΗΚ3ΙΟΤ pa3pHBH CJIOH $eHOJIOajiBseiwmog cmojih, KOTopue nacTO hphbojiht k OTCJianBamiHM. JUh θτογο npodoBajm β KauecTBe epocjioekh πρημθηητβ chjihkohobuh KaynyK. Πρπ θτομ μηκροοχθμη norpyjsajia b chuhkohobhh KaynyK h nocjre βηοηχηηηη οτογο cjtoh b CMOJisHyra Maccy.TaK, HanpHMep, Η3ΒΘ0ΤΗ0 ΗΟΚρΗΤΗβ HHTerpaJILHUX ΜΗΚρΟΟΧΘΜ jvlh 3anHTH ot KJEHMaTHHecKHX BO3 ^ oficTBHji dyHa-uaynyKOM, and JVIH 3aHIHTH OT ΜΘΧΗΗΗΗΘΟΚΗΧ Harpy3OK $ eHOJiiiHiHiiHiiHiiHiiHi-iJiHi-eiJiHi-iJiHi-iJiHi-iJiHi-iJiHi-iJiHoi. HeodxojwaH ropanan cyinua Φθηολβηοaju ^ ernsHot cmojih npn 160C npHBOjyíT ojvíhko κ Η3ΜΘηθηηημ CBOĚCTB pa3JfflHHHX CJIO & HHX ΟΚΟΤΘΜ, Κ £ Κ HanpHMep, CJIOH CrNi · ΚρΟΜΘ ΤΟΓΟ B OdOJIOHKe Β03ΗΗΚ3ΙΟΤ pa3pHBH CJIOH $ eHOJIOajiBseiwmog cmojih, KOTopue retrieves hphbojiht to OTCJianBamiHM. JUh θτογο npodoBaym β KauecTBe epocjioekh πρημθηητβ chjihkohobuh KaynyK. Πρπ θτομ μηκροοχθμη norpyjsajia b chuhkohobhh KaynyK h nocjre βηοηχηηηη οτογο cjtoh b CMOJisHyra Maccy.

- 5 3Ta npoMeiKyTOHHaH npocaoHKa H3 cohkohoboio KayayKa BCJieflCTBHe cBoež ojiacTHHHOCTH xoth h irpenflTCTByeT noBpesAohhhm ctokjehhhoh nojyioJKKH, ho Bce-TaKH HapymaeT paBHOMepHÓcTLj ' TexHOJioranecKorcf riponecca, t.k. ghjihkohobhh KayayK paciqpěflěaaeTČjTnď^- GTeiuiy HepaBHOMepHO, τηηθτοη b hhth, λθγκο HaaHHaoT KanaTB η ημθθτ He3HaaHTejiBHoe KanejiBHoe BpeMH.- five 3TA npoMeiKyTOHHaH npocaoHKa H3 cohkohoboio KayayKa BCJieflCTBHe cBoež ojiacTHHHOCTH XOTH h irpenflTCTByeT noBpesAohhhm ctokjehhhoh nojyioJKKH him BCE-Takhte HapymaeT paBHOMepHÓcTLj 'TexHOJioranecKorcf riponecca, tk ghjihkohobhh KayayK paciqpěflěaaeTČjTnď ^- GTeiuiy HepaBHOMepHO, τηηθτοη b hhth, λθγκο HaaHHaoT KanaTB η ημθθτ He3HaaHTejiBHoe KanejiBHoe BpeMH.

Sto 3HaHHT, HTO 3JiaCTHHHOCTB BO BpGMH OdpadOTKH ÓHCTpO / H3MGHH6TCH, H HOBTOMy paCTBOp ftJIH ΟΚ^ΗΟΗΚΗ flOJKÍOH ΠΟΟΤΟΗΗ— ,Sto 3HaHHT, HTO 3JiaCTHHHOCTB BO BpGMH WasteOTKH ÓHCTpO / H3MGHH6TCH, H HOBTOMy paCTBOp ftJIH ΟΚ ^ ΗΟΗΚΗ flOJKÍOH ΠΟΟΤΟΗΗ—,

HO ΓΟΤΟΒΗΤΒΟΗ, ΠρΗΉθΜ, ΠΟΒΗΠΙΘΗΗΘ pnaCTHHHOCTH CHJIHKOHOBOro KaynyKa He Π03Β0ΗΗβτ λοοτηγηυτβ coxpaHHioiuyrocH TOjnmníy . CJIOH ΠΟΚρΗΤΕΗ. IÍ3 DB-OSl 540 408 Η3ΒΘ0ΤθΗ ClIOCOd OKyHaHHH, npa KOTOpOM HOJiynpOBO^HHKOBUS ITpíídop HOKpHBaeTCJI JWyMH BemecTBaMH. B nocjie#Hee BpeMH cTazio η3βθοτηο, hto jma noKpHTHH. nOJiynpOBOflHHKOBHX ITpHdopOB OdOJIOHKaMK ΠρΗΜβΗΗϊΟΤΟΗ CHJIHKOHOBHe MaOCH, KOTOpue npn COnpHKOCHOBeHHH c B03,nyX0M mm BaaroH, coftepacamenca b BO3jiyxe 3aTBepAeBaioT h, HanpnΜθρ, nocae C03£aHHH odojiOHKH nyTeM 3anHBKH odecneanBasT xoponme CBoficTBa noaynpoBo^HiiKOBHM irpudopaM. 3thJ cHJiHKOHOEHejMáccH HeVaBJíaiOTca κομποηθητηοη οηοτθμο2 h odpa3yK>T nocae oTBepwHHH odojioaKU c Henpa^uiBHOH γθομθτρη-Τ aecKOH φορΜοιι,. c Ha3BaHHHMH BLnne HeAocTaTKaMH jyia odpadoTKH.HO ΓΟΤΟΒΗΤΒΟΗ, ΠρΗΉθΜ, ΠΟΒΗΠΙΘΗΗΘ pnaCTHHHOCTH CHYIHKOHOBOro KaynyKa He Π03Β0ΗΗβτ λοοτηγηυτβ coxpaHHioiuyrocH TOjnmníy. CJIOH ΠΟΚρΗΤΕΗ. III DB-OSl 540 408 Η3ΒΘ0ΤθΗ ClIOCOd OKyHaHHH, npa KOTOpOM HOJiynpOBO ^ HHKOBUS ITipid HOKpHBaeTCJI JWyMH BemecTBaMH. B night # Hee BpeMH cTazio η3βθοτηο, hto jma noKpHTHH. nOJiynpOBOflHHKOBHX ITpHdopOB OdOJIOHKaMK ΠρΗΜβΗΗϊΟΤΟΗ CHJIHKOHOBHe MaOCH, KOTOpue npn COnpHKOCHOBeHHH c B03 nyX0M BaaroH mm, b coftepacamenca BO3jiyxe 3aTBepAeBaioT h HanpnΜθρ, nocą C03 £ AHHH odojiOHKH rivet 3anHBKH odecneanBasT xoponme CBoficTBa noaynpoBo ^ HiiKOBHM irpudopaM. 3thJ cHJiHKOHOEHejMáccH HeVaBJíaiOTca κομποηθητηοη οηοτθμο2 hr odpa3yK> T nocae oTBepwHHH odojioaKU c Henpa ^ uiBHOH γθομθτρη-Τ aecKOH φοΜΤ, c Ha3BaHHHMH BLnne HeAocTaTKaMH is yy waste.

UejiB H3odpeTeHHaUejiB H3odpeTeHHa

Ueju> H3odpeTeHua cogtoht b tom, HTodu nyTeM OKyHaHHa C03&aTL odoaoHKy nojiynpoBojnmKOBHM npndopaM, koTopas ημθθτ raauKyio, de3 TpenpiH h nop ποβθρχηοοτβ, ycTOHanByra κ khhMaTHaecKHM B03fteHCTB&HM πρπ ΘΛθκτρΗΗθοκοΗ Harpy3Ke, a κροΜθ τογο, HToda odecneaiiTB dojojnoĚ οροκ caysdH ηθηοποηβ30Β3ΗΗ0Η ftTIS OÓOJIOHKH MaCCH.Ueju> H3odpeTeHua cogtoht b that HTodu rivet OKyHaHHa C03 & ATL odoaoHKy nojiynpoBojnmKOBHM npndopaM, koTopas ημθθτ raauKyio, DE3 TpenpiH h nop ποβθρχηοοτβ, ycTOHanByra κ khhMaTHaecKHM B03fteHCTB & HM πρπ ΘΛθκτρΗΗθοκοΗ Harpy3Ke and κροΜθ τογο, HToda odecneaiiTB dojojnoĚ οροκ caysdH ηθηοποηβ30Β3ΗΗ0Η ftTIS OÓOJIOHKH Macchi.

IfejioateHHe cy-UHocTH H3odpeTeHHaIfejioateHHe cy-UHocTH H3odpeTeHHa

3a&aaa, pemaeMaa H3odpeTeHneM, coctoht b tom, STodu πρπΜβHHH H3B0CTHHH CHOCOd ΠΟΚρΗΤΗΗ nOJiyiipOBOflHHKOBHX HpHdopOB odojiosKaMH oKyHaHzeM, ycTpamíB npn stom h3jiokohhho Bimie ' - 6 **··- '.V3a & aaa, pemaeMaa H3odpeTeHneM, coctoht b tom, STodu πρπΜβHHH H3B0CTHHH CHOCOd ΠΟΚρΗΤΗΗ nOJiyiipOBOflHHKOBHX HpHdopOB odojiosKaMH oKyHaHieM, y3Tphhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh.

HeSOCTaTKH, HCKJDOHHTB ΠρΗΜΘΗβΗΗΘ ΓβρΜβΤΗδΗρΟΒΘΗΗΗΧKOpiyCOB,>. a κροΜθ τογο, odeoneHHTL jyra nojiynpoBOftHHKOBHX npndopoB ποκριιτηχ odoJKmaMH,· ηοβηθ SKcimyaTaiícioHHHe cBoficTBa, Ha . OCHOBe OflHOpOflHOŽ CHOTCMH K0MH0H6HT0B B ΚΟΊβΟΤΒβ MaOCH ποκριιτΗΗ. ·.·'··'..···· /1? -/; / 7^ - .HeSOCTaTKH, HCKJDOHHTB ΠρΗΜΘΗβΗΗΘ ΓβρΜβΤΗδΗρΟΒΘΗΗΗΧKOpiyCOB,>. a κροΜθ τογο, odoneHHTL jyra nojiynpoBOftHHKOBHX npndopoB ποκριιτηχ odoJKmaMH, · ηοβηθ SKcimyaTaiioHHHe cBoficTBa, Ha. OCHOBe OflHOpOflHOŽ CHOTCMH K0MH0H6HT0B B ΚΟΊβΟΤΒβ MaOCH ποκριιτΗΗ. ·. · '··' .. ···· / 1? - /; / 7 ^ -.

TexHHHecKHMH npiraHHaMH HeflocTaTKOB b y^e Η3ΒθάτΗΗΧ perneHHHX HBJIHeTCH,‘cpě^H HpOHerO, TO, ΗΤΟ Η3ΒβΟΤΗΗΘ OflHOpOflHHS οηοτθμη κομποηθητοβ H6 nojmaioTcn odpadoTKe mni ηθ odeone_^BaET TpedyeMHe SKerayaTaiíaoHHHe KanecTBa. >*., ' ' .·J'·/.··' j/Aíyví-'·’ ' ·TexHHHecKHMH npiraHHaMH HeflocTaTKOB b y ^ e Η3ΒθάτΗΗΧ perneHHHX HBJIHeTCH, 'CPE' H HpOHerO, TO, ΗΤΟ Η3ΒβΟΤΗΗΘ OflHOpOflHHS οηοτθμη κομποηθητοβ H6 nojmaioTcn odpadoTKe mni ηθ odeone_ ^ BaET TpedyeMHe SKerayaTaiíaoHHHe KanecTBa. > *., ''. · J '· /. ··' j / Aíyví- '· ’' ·

CoraacHO H3odpeTeHmo, sahana péigaeTca τθμ, hto ποκρκτιιβ odojióHKoS npoHcxoflHT tskhm odpa3OM,'3To Macca jwh OKynaHUH pa3Jioaeiia Ha οτββΛΒΗΗβ κομηοηθητη: BemecTBO, noBuniajouíee ajy?e3HíO, cpe^cTBO, odpasyramee nonepenHHe cbh3H : we^jy> MaKpoMOJieKyjiaMH h OTBep^naioinHlča^a' xoxofiy^» bhcokobh3khh chjihkohobhS KaynyK. Κομηοηθητη ηηηοοητοη Ha nojrynpoBOAHHkobhě npndop b flaiiHoS nocjie^oBaTejiBHOcTH ο#ηη 3a spyrHM b ηθοκολβκο oKynaHiít c noc^esytomen 3a whm oKyHaimeM cyiiikož h, TaicuM odpa3OM, He conpHKOcaiOTCH flo θτογο xpyr c Jípyγομ. B κοηηθ npoixecca HaHeceHHH ποκρητηη nojiynpoBOflHHKOBHe npndopH BLmepaoíBaioTCH npn 'ónpejiejieHHon j TeMnepaType. Iíejiecoodpa3Ho npHMeHHTL oTBepswaioiííHficH npn κομηθτηοη TeMnepaType BHCOKOBH3KHS CHJEHKOHOBHH KajKyK C BH3KOGTB 70 000+20 000 Míla. c.CoraacHO H3odpeTeHmo, Sahana péigaeTca τθμ, HTO ποκρκτιιβ odojióHKoS npoHcxoflHT tskhm odpa3OM, '3To Macca JWH OKynaHUH pa3Jioaeiia Ha οτββΛΒΗΗβ κομηοηθητη: BemecTBO, noBuniajouíee ajy? E3HíO CPE ^ cTBO, odpasyramee nonepenHHe cbh3H: we ^ jy> MaKpoMOJieKyjiaMH h OTBep ^ naioinHlča ^ and 'xoxofiy ^ »bhcokobh3khh chjihkohobhS KaynyK. Haομηοηθητη ηηηοοητοη Ha nojrynpoBOAHHkobeh npndop b flaiiHoS nocjie ^ oBaTejiBHOcTH ο # ηη 3a spyrHM b ηθοκολβκο oKynaHiM CH c ^ c ^ m ci m ci ic ci m ci ic ci ii ci u ci ic ci B κοηηθ npoixecca HaHeceHHH ποκρητηη nojiynpoBOflHHKOBHe npndopH BLmepaoíBaioTCH npn 'ónpejiejieHHon j TeMnepaType. Iiejiecoodpa3Ho npHMeHHTL oTBepswaioííHficH npn κομηθτηοη TeMnepaType BHCOKOBH3KHS CHJEHKOHOBHH KajKyK C BH3KOGTB 70,000 + 20,000 Miles. C.

HOJiynpOBOflHHKOBUe npHdOpH B OdOJIOHKaX BHflepHHKaiOTCH npH ΤΘΜnepaTypax βηιπθ 100 °C, npejxnonTHTejiLHo npn 120 °C. Upa θτομ HeosHnarao duna ycTanoBjíeHa npBMan 3ββηοημοοτέ> Mew hhcjiom jíHefi BtwepsKH npn onpejiejieHHoS TeMnepaType h hhcjiom ληθη, b TeneHKe κοτορπχ jyw nojiynpoBOflHHKOBHX npndopoB b odojionKax HadjntwaJiacB TpedyeMas ycToíhHBOCTL κ βο3αθκοτβιεκ) Bjiam.HOJiynpOBOflHHKOBUe npHdOpH B BONFLOW BHflepHHKaiOTCH npH epnepaTypax at 100 ° C, npejxnonTHTejiLHo npn 120 ° C. Upa θτομ HeosHnarao dune ycTanoBjíeHa npBMan 3ββηοημοοτέ> Mew hhcjiom jíHefi BtwepsKH npn onpejiejieHHoS TeMnepaType h hhcjiom ληθη b TeneHKe κοτορπχ jyw nojiynpoBOflHHKOBHX npndopoB b odojionKax HadjntwaJiacB TpedyeMas ycToíhHBOCTL κ βο3αθκοτβιεκ) Bjiam.

ípyraM npn3HaK0M H3odpeTeHHH ηβηηθτοη bo3Moshoctb ynpaBneHHH nexeHanpaBjíeHHHM HapaupiBaHHeM cJioeB oTBepnflaioiqerocH Ha xojiofty¹’ βηοοκοβη3κογο . cmíHKOHOBoro KaynyKa, b ηθοτηοοτη, na οοηοβθ Budopa ποοτοηηηογο 3anaHHoro KOjmnecTBa cpe^CTBa, odpa3yioinero nonepemme CBH3H Messy MaspoMOJieKyjiaMH, a TaKse onpe,nejieHHoro ββθμθηη npedimaHna nojiynpoBO£HHKOBoro npndopa b βηηηθ juh oKyHaHHH η οοοτΒθτοτΒγκιΐξθδ TeMnepaTypn pacTBopaípyraM npn3HaK0M H3odpeTeHHH ηβηηθτοη bo3Moshoctb ynpaBneHHH nexeHanpaBjíeHHHM HapaupiBaHHeM cJioeB oTBepnflaioiqerocH Ha xojiofty ¹ 'βοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοοο cmíHKOHOBoro KaynyKa b ηθοτηοοτη to οοηοβθ Budopa ποοτοηηηογο 3anaHHoro KOjmnecTBa CPE-CTAB, odpa3yioinero nonepemme CBH3H Messy MaspoMOJieKyjiaMH and taksa onpe, nejieHHoro ββθμθηη npedimaHna nojiynpoBO £ HHKOBoro npndopa b βηηηθ south oKyHaHHH η οοοτΒθτοτΒγκιΐξθδ TeMnepaTypn pacTBopa

- 7 πρκ SOCTaTOHHOM KOJDIHeCTBe CHJIHKOHOBOrO KSTOHa B BaHHe.- 7 πρκ SOCTaTOHHOM KOJDIHeCTBe CHHIHKOHOBOrO KSTOHa B BaHHe.

flpHMep OCymeCTBJíeHHfl Η3θύρθΤΘΗΗΗ 'flpHMep OCymeCTBJíeHHfl Η3θύρθΤΘΗΗΗ '

Η3θόρβΤΘΗΗβ Π0,Πρ00Ηθβ ΗΟΗΟΗΗβΤΟΗ HHJKe Ha ΠρΗΜβρθ ΘΓΟ ocymeoTBjíeHKH. . / . .H3θόρβΤΘΗΗβ Π0, Πρ00Ηθβ ΗΟΗΟΗΗβΤΟΗ HHJKe Ha ΠρΗΜβρθ ΘΓΟ ocymeoTBjíeHKH. . /. .

HOJiyirpÓBOAHHKOBHe irpHdopH, B HaCTHOCTH HHTeipaJIBHHe ΜΗΚρΟcxeMH, ýcTaHaBjíHBaioTCH Ha onpenejieHHae MecTa b Mara3HHe,' pacoHHTaHHOM, HanpHMep, Ha 100 inTyK. ’HOJiyirpÓBOAHHKOBHe irpHdopH, B HaCTHOCTH HHTeipaJIBHHe ΜΗΚρΟcxeMH, ýcTaHaBjíHBaioTCH Ha onpenejieHHae MecTa b Mara3HHe, 'pacoHHTaHHOM, HanpHMep, Ha inHMep. ’

OTJíeJIBHHe ΚΟΜΠΟΗΘΗΤΗ ftHH ΠΟΚρΗΤΗΗ ΗβΛΗΤΗ B ΟΤΑ&ΕΒΗΗΘ BaHHH. BHanajie HHTerpajt&HHe Kcncpocxem OKyHatoTcn b BemecTBO, no- . Bimaioinee a#re3ino, 'HanpHMep, οπηρτοβηζ pacTBop Giyoidoxypropyltriáthoxylan+Aminopropyltriathoxy^SaTeM CJIOÉ ΒβΙξβΟΤBa, noBíffliawdft ajy?e3mo 'cyniHTcn,· npn 70-100 °C. Hocjie θτογο HHTerpaELHne μηκροοχθμη OKyHaPTcn b BeinecTBo, odpasyromee nonepenHue cbh3H Mensy MaspoMOJieKyjiaMH, HanpHMep, cooTomqee H3 Dibutylzinndilaurat . B JiaKOBOM όθΗ3ΗΗΘ, CJIOH κοτοροΓο οπητβ-τθκη BHoyinHBaeTCH npH 70-100 °C. B τρβτπζ pa3 HHTerpajiLHue μηκροοχθμη OKyHa&TCH b BaHHy o chjihkohobhm KaynyKOM’. EaarosapH ηοοτοηηηομυ 3a#aHH0My KOjnmecTBy BenjecTBa, oópasysmero nonepemme cbh3H Mensy MaKpoMOJiexyJiaMH, HanpHMep, πρπ ΚΟΗΗβΗΤραφϊΗ Dibutylzinndilaurat b JiaKOBOM deH3HHe I : 15 h BpeMeHH οκτηθηηη μθηθθ I ceKyn^H, djiarosapn npedHBamw nojiynpoBosnnKOBnx npndopoB b BaHHe c chjehkohobhm KaynyKOM b Tenemie 3 MHHyT, πρπ τθμHepaType b BaHHe 50 °G, socTHraeTcn Tojniíraa cjioh chjihkoηοβογο KaynyKa, paBHan 0,6 mm.OTJíeJIBHHe ΚΟΜΠΟΗΘΗΤΗ ftHH ΠΟΚρΗΤΗΗ ΗβΛΗΤΗ B ΟΤΑ & ΕΒΗΗΘ BaHHH. BHanajie HHTpajt & HHe Kcncpocxem OKyHatoTcn b BemecTBO, no-. Bimaioinee a # re3ino, 'HanpHMep, οπηρτοβηζ pacTBop Giyoidoxypropyltriethoxylan + Aminopropyltriathoxy ^ SaTeM CJIOÉ ΒβΙξβΟΤBa, noBíffliawdft ajy? E3mo' cyniHT-100 ° Cpn 70 ° C. Hocjie θτογο HHTerpaELHne ηεκροοχθμη OKyHaPTcn b BeinecTBo, odpasyromee nonepenHue cbh3H Men's MaspoMOJieKyjiaMH, HanpHMep, cooTomqee H3 Dibutylzinndilaurat. B JiaKOBOM όθΗ3ΗΗΘ, CJIOH at BHoyinHBaeTCH npH 70-100 ° C. B τρβτπζ pa3 HHTerpajiLHue to OKyHa & TCH b BaHHy by chjihkohobhm KaynyKOM ´. EaarosapH ηοοτοηηηομυ 3a # aHH0My KOjnmecTBy BenjecTBa, oópasysmero nonepemme cbh3H Mensa MaKpoMOJiexyJiaMH, HanpHMep, πρπ ΚΟΗΗβΗΤραφϊΗ Dibutylzinndilaurat b JiaKOBOM deH3HHe I: 15h BpeMeHH οκτηθηηη μθηθθ I Čekyně ^ H djiarosapn npedHBamw nojiynpoBosnnKOBnx npndopoB b BaHHe c chjehkohobhm KaynyKOM b Tenemie 3 MHHyT, πρπ τθμHepaType b BaHHe 50 ° G, socTHraeTcn Tojniíraa cjioh chjihkoηοβογο KaynyKa, paBHan 0.6 mm.

Chjihkohobhh KaynyK ημθθτ doxBmyo bh3kocte, HanpHMep,Chjihkohobhh KaynyK ημθθτ doxBmyo bh3kocte, HanpHMep,

000 MHa. c, djiarosapn neMy oh xopoao npHjmnaeT κ ΜκκροcxeMaM h He μοηθτ cjihdikom όκοτρο οτθκητβ. HaHecenHoe βθmecTBO jyin odpaaoBaHHH nonepenHHx οβηθθη Mew ManpoMOJieKyjiaMH npoHHKaeT b chjihkohobhh KaynyK h npiiBojniT κ oTBepsΛθηηιο Ha BO3.nyxe, κοτοροβ 3aKaHHHBaeTCH μηκοημολβηο nocjie 16 nacoB.000 MHa. c, djiarosapn neMy oh xopoao npHjmnaeT κ κκκροcxeMaM h He μοηθτ cjihdikom όκοτρο οτθκητβ. HaHecenHoe βθmecTBO jyin odpaaoBaHHH nonepenHHx οβηθηη Mew ManpoMOJieKyjiaMH npoHHKaeT b chjihkohobhh KaynyK h npiiBojniT κ oTBepsΛθηκοHο BOBa3.nyxe.

HepBHe cTenaíoiííHe (no κθιηιημ) KOjnraecTBa οηπηκοηοβογο Kaynyxa HcnojEE>3yioTCH ποβτορηο. KaynyK, B03BpameHHUH TaKHM odpa- 8 30M, flQJI&eH ÓHTL HCH0JU>30BaH B ΤΘΗΘΗΗΘ ΟβΗΟΓΟ ftHH. IlOCJie 3Toro irponcxoAHT BTopoe cTeKasae b TeaeHae τρβχ aeTBepTea aaca c nocjieffyiouíHM TaMHOHupoBamieM HHTerpajiBHoS cx6mh Ha irpoKjiajtKe H3 ÓyMarH. Diaroiapa nocjiesyioineS, corjiacHO H3OόρθΤθΗΐοο, BHftepjKKe irpa 120 °C b TeaeHae 120 aacoB, οτ&ωΐΒHue BeiqecTBa coeflHHjwTCH b og^Hopo^Hyio Maccy ποκρκτΗΗ.HepBHe cTenaíoííHe (no κθιηιημ) KOjnraecTBa οηπηκοηοβογο Kaynyx HcnojEE> 3yioTCH ποβτορηο. KaynyK, B03BpameHHUH TaKHM odpa 8 30M, flQJI & eH HTHTH HCH0JU> 30BaH B ΤΘΗΘΗΗΘ ΟβΗΟΓΟ ftHH. IlOCJie 3Toro irponcxoAHT BTopoe cTeKasae b TeaeHae τρβχ aeTBepTea aaca c nocjieffyiouiHM TaMHOHupoBamieM HHTerpajiBHoS cx6mh Ha irpoKjiajtKe H3 ÓyMarH. Diaroiapa nocjiesyioineS, corjiacHO H3OlorρθΤθΗΐοο, BHftepjKKe irpa 120 ° C b TeaeHae 120 aacoB, Beτ τ Hue BeiqecTBa coeflHHjwTCH b b Hopo ^ Hyio Maccy ποκρκτΗΗ.

JUh stoé BHsepKKH upa onpeflejieHHoS TeMnepaType ηθοζηαθηηο duna ycTanoBjíeHa apaMaa cbh3L Me^ny KOjnaaecTBOM αηθη bhsepacKH a KOJnraecTBOM jyieS, b Tenegae κοτορυχ jyia nojiynpoBojvhhkobhx npaóopoB b odojionKax HadjnoflanacB TpedyeMáa ycTOÉHBBOCTB K B03£eSCTBHK> BJiaTH. T&K ΗΗΤΗβΗβΒΗΘΉ BH#epJKKa npanaeT' yOTOikHBOCTL K ΒΟ3βθΗ0ΤΒΗΧ) OKpyaíaEomero B03flyxa upa 96 % OTHOCHTSflLHOĚ BJiaHHOCTa H TeMnepaTyp&i-40-^OG B ΤβΗβΗΗβ 5 SHeS. C yBejnraeHHeM jyiaTejiLHocTa BtwepjKKa pacTeT TaK&e JWTejIBHOCTL yCTOifoHBOCTH K ΒΟ3£θ2θΤΒΗΚ) BJiara. IIojiynpoBOAHHKOBHe npadopn, ποκρκτΗβ a odpadoTamrie TaaaM odpasoM, ημθιοτ xopomae KaaecTBa ποβθρχηοοτκ upa flOCTaToahoS Tojnipme cjioh ποκρπτΗΗ a reoMeTpaaecKH iipaBajiLHoa φορΜθ odojioaicai TpeiííHHu a οτωιοβΗΗΗ ηθ βο3ηηκηιοτ. ΠροιχβΗΤ dpaaa MHKpoexeM, ΠΟΚΡΗΤΗΧ TSKHM Odpa3OM, MaJI, Τ.Κ. JHOdOH βθφθΚΤ odcwioaKH μοβηο λθγκο ycTpaHaTB sopadoTKoa.' TpedyeMaa Tepmoctohkoctl upa TeMnepaTypax flo 150 °C a ycToSnaBocTB κ B03£eScTBHK) BJiara, b οπηοβηηομ BHfle, odecneaeHH.South STOE BHsepKKH UPA onpeflejieHHoS TeMnepaType ηθοζηαθηηο dune ycTanoBjíeHa Apamate cbh3L Me ^ ny KOjnaaecTBOM αηθη bhsepacKH and KOJnraecTBOM jyieS b Tenegae κοτορυχ jyia nojiynpoBojvhhkobhx npaóopoB b odojionKax HadjnoflanacB TpedyeMáa ycTOÉHBBOCTB K £ B03 eSCTBHK> BJiaTH. T&K ΗΗΤΗβΗβΒΗΘΉ BH # epJKKa npanaeT 'yOTOikHBOCTL K ΒΟ3βθΗ0ΤΒΗΧ) OKpyaíaEomero B03flyxa upa 96% OTHOCHTSflLHO BJiaHHOCTa H TeMnepaType & i-40 40 ^O GB ΤβΗβ. C yBejnraeHHeM jyiaTejiLHocTa BtwepjKKa pacTeT TaK & e JWTejIBHOCTL yCTOifoHBOCTH K ΒΟ3 £ θ2θΤΒΗΚ) BJiara. IIojiynpoBOAHHKOBHe npadopn, ποκρκτΗβ and odpadoTamrie TAAA odpasoM, ημθιοτ xopomae KaaecTBa ποβθρχηοοτκ upa flOCTaToahoS Tojnipme cjioh ποκρπτΗΗ and reoMeTpaaecKH iipaBajiLHoa φορΜθ odojioaicai TpeiííHHu and οτωιοβΗΗΗ ηθ βο3ηηκηιοτ. ΠροιχβΗΤ dpaaa MHKpoexeM, ΠΟΚΡΗΤΗΧ TSKHM Odpa3OM, MaJI, Τ.Κ. JHOdOH βθφθΚΤ odcwioaKH μοβηο λθγκο ycTpaHaTB sopadoTKoa. ' TpedyeMaa Tepmoctohkoctl upa TeMnepaTypax flo 150 ° C and ycToSnaBocTB and B03 £ eScTBHK) BJiara, b οπηοβηηομ BHfle, odecneaeHH.

Diarofíapa HaneceHmo cjioeB ποκρΗτηη oKynaHaeM corjiacHO H3odpeTeHHKi, mosho socTamiyTL HeorpaHaaeHHoro cpoaa cxysdu caHHKOHOBoro Kayayaa b Batme, nponejKHBaa pas b Hesejm ocTaBinaaca b Hea KaynyK. Kayaya He μοηθτ CTaTL Henparo^HHM BCJieaoTBaa oTcyTCTBan κοητηκτβ c BenjecTBOM, odpaayiomero nonepeaHne cBS3a Mew MaapoMOJieKyjiaMK. Ebiarosapa 3TOMy, noTepa MaTepaana ΗβΒβχηκΗ.Diarophie HaneceHmo cjioeB oKynaHaeM corjiacHO H3odpeTeHHKi, mosho socTamiyTL HeorpaHaaeHHoro cpoaa cxysdu caHHKOHOBoro Kayayaa b Batme, nponejKHBaa pas b Hesej. Kayaya He CTaTL Henparo ^ HHM BCJieaoTBaa oTcyTCTBan an Benj Benj Benj Benj c BenjecTBOM, odpaayiomero nonepeaHne cBS3a Mew MaapoMOJieKyjiaMK. Ebiarosapa 3TOMy, noTep MaTepaan ΗβΒβχηκΗ.

$owjia H3oópeTeHHfl$ owjia H3ooppeTeHHfl

o r~.o r ~.

O'O'

ω.ω.

co what

oo ooo o

1. ClIOCOÓ nOKpHTHH nOJQ^OBOJpiKKOBHX ΠρΗόορΟΒ OÓOJIOHKaMH OKyηοηηθμ, οτπΗΉέκΐφώωϊ T6M, ^το Macca ποκρητμ, irpexcTaBJíeHHaa oT^ejnM® KOMnoHeHTaMH: ΒθπξβστΒΟ, noBHmaioinée ajp?e3HD, cpe^GTBO jvlh odpaaoBaHHa nonepe^Hax cBa3eií MejOT MaKpoMOjieKyjiaMH h OTBeps^aw^cfl πρκ KOMsaTHoS TermepaType, wemnpríí doomyio bhbkoctl chjqíkohobhS KayqyK, HanocHTca B^amoÉ nocaieAOBaTejiBHocTH no KomoHeHTaM οχο 3a spyrzM c nocjie;iyw& nocjce Kas^oro oKyuassa cymKoií, #o θτογο obh ηθ conpHKaca^oTca jjpyr cfjnpyroM, hhocjio ηοηοοθηκη ποκρΗτιω ποjrynpoBO^HHKOBue npHóopa bwpíkhbsjotch npa onpeA&JieííHOH τθμnepaType.First ClIOCOÓ nOKpHTHH nOJQ ^ OBOJpiKKOBHX ΠρΗόορΟΒ OÓOJIOHKaMH OKyηοηηθμ, οτπΗΉέκΐφώωϊ T6M, το Macca ποκρητμ ^, ^ oT irpexcTaBJíeHHaa ejnM® KOMnoHeHTaMH: ΒθπξβστΒΟ, noBHmaioinée AJP? E3HD CPE ^ GTBO jvlh odpaaoBaHHa nonepe-Hax cBa3eií MejOT MaKpoMOjieKyjiaMH OTBeps h ^ w ^ cfl πρκ KOMsaTHoS TermepaType, wemnpríí doomyio bhbkoctl chjqíkohobhS KayqyK, HanocHTca B ^ amoÉ nocaieAOBaTejiBHocTH well KomoHeHTaM οχο 3a spyrzM c nocjie; IYW & nocjce Kas ^ oro oKyuassa cymKoií, #O θτογο OBH ηθ conpHKaca ^ father jjpyr cfjnpyroM, hhocjio ηοηοοθηκη ποκρΗτιω ποjrynpoBO ^ HHKOBue npHóopa bwpíkhbsjotch npa onpeA & JieííHOH τθμnepaType.

2. Cnocod corjiacHO nynKTy I, oTJEHBaDirpďicH tgm, ητο bh3Kqctb OTBepwwroca npn KowaTHOK TewepaType, we^ero óojibmy© bb3Koctb CKzoiKOHOBoro Kayiýica οοοτοβ&ηθτ 70 000 20 000 Míla . c.2. Cnocod corjiacy nynKTy I, OTJEHBaDirpďicH tgm, ητο bh3Kqctb OTBepwwroca npn KowaTHOK TewepaType, we ero ojibmy © bb3Koctb CKzoiKOHOBoro Kayiýica οοοττος 000οοττος 000. C.

//

3. Gnocod coiviacHo nyHKTy I, oTjnmawf&on τθμ, ητο nojiyuposofíΗΗΚΟΒΗθ ΙφΗόορΗ C ΗΒΗΘΟβΗΗΗΜ HOKpHTHCM ΒΗίξ6ρ?ΕΗΒΗίΟΤΟΗ HpK TeMnepaType οβειπιθ 100 °G, ηρθχποητητθ^ίΒΗΟ npn 120 °G.3.

4. Gnocod corjiacHO nynKTy I, oTjmawďica τθμ, ητο bo3mosho yiTpasjíemie nejieHanpaBjíeHHHM HapaJnaBasaeM caoeB OTBepssaiamerocn Ha xo&ofly”, oeioinero dojitmys) bh3koctl ciuníKonoBoro KaynyKa, ocodenno, na οοηοβθ Budopa ποοτοηηηογο 3a$aHHoro KowiecTBa cpescTBa jw oópa3OBaHHH nonepewKx cbh3Gh,Fourth Gnocod corjiacHO nynKTy I oTjmawďica τθμ, ητο bo3mosho yiTpasjíemie nejieHanpaBjíeHHHM HapaJnaBasaeM caoeB OTBepssaiamerocn Ha xo & ofly "oeioinero dojitmys) bh3koctl ciuníKonoBoro KaynyKa, ocodenno to οοηοβθ Budopa ποοτοηηηογο 3a $ aHHoro KowiecTBa cpescTBa JW oópa3OBaHHH nonepewKx cbh3Gh,

Mensy MaKpoMoaeKyjíaMH onpesaaeHHon λπητβτιβηοοτη npeduBaHHH HOJiyHpOBOSHHKOBHX HpHÓOpOB B ΒΗΗΗΘ QKtflíaHSíH. H COOTBeTCTBywi TeamepaTyps npa socTaTonHOM KOJcmecTBe conκοηοβογο KayayKa b Banse.Mensy MaKpoMoaeKyjíaMH onpesaaeHHon λπητβτιβηοοτη npeduBaHHH HOJiyHpOBOSHHKOBHX HpHoOpOB B ΒΗΗΗΘ QKtflíaHSíH. H COOTBeTCTBywi TeamepaTyps npa socTaTonHOM KOJcmecTBe KayayKa b Banse.

AsHOTaiwAsHOTaiw

CnOCOÓ ΠΟΚΡΗΤ0Η KOJiyKpOBOflHHKOBHX DpUdopOB οόώΐΟΚΚδΜΚ ΟΚγΗΒΗΗθΜ ’ · - ΠβΛΚΟ ΗδΟόρβΤΘΗΙΙΗ KBJLS6TCH ΠΟΚρΗΤΗβ HOJiyBpOBOňHHKOBWC ' ; ; ; dopoB''Maccot, npa kotoooě floeTHraěŤca rjia^Kaa noBepxHÓcTB/’ , _; ř;' ;. , iíe, ngp h TpenpíH, a TaKse BacoKaa yoToírmocTB k’ '··-.. ' Kw^aTiBíeci™ βο3^θ0οτβηημ npa ‘ 3^θκτρκκθοκοί Harpy3Ke, a ^v , κροΜθ Toro, oóecneHKBaeTca óojilhioS οροκ'cayadH iíeHcnojiL3O’^: :^J BaHHoM jwa oóojiohkh MačciL· 3a&a^K3oďpěTeHHa coctoht b · _ \_Λ-ϊ-Js TOM, KTOdH HCKJGOHHTB ΚΡΗΜΘΗΘΗΗΘ''H yCTpá\ * hhtl ne^ocTam: ysce η3βθοτηηχ· cirocddoB OKyHaHEH, a κροΜβ < τογο, odecHeHHTB HOBue 3KCKnyaTaiíK0HHue KaaeeTBaJua odpadoTaHHHX nOrpyseiBieM nOaynpOBOXHHKOBHX npndopOB ΤβΜ, HTO ’ ňOJCKHa dHTB Ha%nena osHopoftHaa ,οηοτθμη κομποηθητοβ b KanecTΒθ MácOH JUH ΠΟΙφΗΤΗΗ.' . _; 'CnOCOÓ ΠΟΚΡΗΤ0Η KOJiyKpOBOflHHKOBHX DpUdopOB οόώΐΟΚΚδΜΚ ΟΚγΗΒΗΗθΜ '· - ΠβΛΚΟ ΗδΟόρβΤΘΗΙΙΗ KBJLS6TCH ΠΟΚρΗΤΗβ HOJiyBpOBOňHHKOBWC';;; dopoB '' Maccot, npa kotoooe floeTHraraca rjia ^ Kaa noBepxHÓcTB / ', _; ř; ';. IIE, NGP h TpenpíH and taksa BacoKaa yoToírmocTB to '·· - ..' ^ Kw aTiBíeci ™ βο3 θ0οτβηημ NPA ^ '^ 3 θκτρκκθοκοί Harpy3Ke, ^and, κροΜθ Toro, oóecneHKBaeTca óojilhioS οροκ'cayadH ^{iíeHcnojiL3O':} ^J BaHHoM JWA oóojiohkh MačciL · 3a & K3oďpěTeHHa coctoht a ^ b · _ \ _{Λ -ϊ} Js-TOM KTOdH HCKJGOHHTB ΚΡΗΜΘΗΘΗΗΘ''H yCTpá \ ^ * hhtl no vinegar: ysce η3βθοτηηχ · cirocddoB OKyHaHEH and κροΜβ <τογο, odecHeHHTB HOBUM 3KCKnyaTaiíK0HHue KaaeeTBaJua odpadoTaHHHX nOrpyseiBieM nOaynpOBOXHHKOBHX npndopOB ΤβΜ, HTO 'OJJJCKHa dHTB Ha% nen osHopoftHaa, οηοτθμη κομποηθητοβ b Boar SOUTH SOUTH ΠΟΙφΗΤΗΗ.' . _; '

CoraacHo Η3θόρβτβΗ03θ, Macca jyia ποκρπτΗΗ npe^cTaBJíeHa o^eaKM ΚΟΜΠΟΗβΗΤΜ: ΒδΙξβΟΤΒΟ,' ΚΟΒΗΙΠθΙΟΙξθθ ^ξΡθδΚΙΟ, OpeftCTBO jyia odpasoBaHKK nonepeKHHX cBK3eÉ Messy MaapoMoacKyaM h cohkohobhé KayayK.CoraacHo θ3θόρβτβΗ03θ, Macca jyia ποκρπτΗΗ npe ^ cTaBJíeHa o ^ eaKM ΚΟΜΠΙβΟΤΒΟ, ΚΟΒΗΙΠθΙΟΙξθθ ^ ξΡθδΚΙΟ, OpeftCTBO jyia odpasoBaHKX coheKaKeKeKeKyKeKeMeKeKeKeKeKeKeKeKeKeKeKeKeKeKeKeKeKeKeKeMe

ΚΟΜΠΟΗΘΗΤΗ H8HOCHTCH Ha KOJiynpOBOffHHKOBHe HpHdopu B flaHHOÉ nocjiesoBaTejiBHOCTH omh 3a spyrHM b ηθοκολβκο oKyHannS, c nocaejjywH nocae Ka^oro oKynaKKa cyinKoa η, τοκημ odpa3OM, χο stopo ηθ eonpHKacajoTca £pyr o japyroM. Hocae stopo noaynpoBo#κκκοΒΗβ npadopn BHsepsoíBaioTca irpa TeasiepaType cBHuie 100 °C, ΠρΘβΠΟΉΤΗΤ&ΜΟ ΙφΗ 120 °C<ΚΟΜΠΟΗΘΗΤΗ H8HOCHTCH Ha KOJiynpOBOffHHKOBHe HpHdopu B flaHHOÉ nocjiesoBaTejiBHOCTH omh 3a spyrHM b ηθοκολβκο oKyHannS, c nocaejjywH nocae Ka ^ oro oKynaKKa eo, oKonaKKa e3. Hocae stopo noaynpoBo # κκκοΒΗβ npadopn BHsepsoiBaioTca irpa TeasiepaType cBHuie 100 ° C, ΠρΘβΠΟΉΤΗΤ & ΜΟφΙ 120 ° C <

Bo3Mokho neaeHanpaBJíeHHoe HapamoaKiíe caoa chjihkohobopo Kaynysa c bh3koctho 70 000 i 20 000 MHa . c.Bo3Mokho neaeHanpaBJeeHHoe HapamoaKiae caoa chjihkohobopo Kaynysa c bh3koctho 70 000 and 20 000 MHa. C.

Claims

A method of coating semiconductor devices by dip coating, characterized in that the coating composition has individual components, namely an adhesion promoter, a crosslinking agent between the macromolecules and a room temperature curing agent, and a high viscosity silicone rubber which: The coating is applied sequentially according to the components one after the other and after each immersion the drying is carried out until these layers come into contact with each other and after application of the coating the semiconductor devices are left to stand at a certain temperature.

2. The method of claim 1, wherein the viscosity of the room temperature curing silicone rubber having a high viscosity is 70,000-20,000 mPa.c.

Method according to claim 1, characterized in that the coated semiconductor devices are held at a temperature above 100 ° C, preferably at 120 ° C.

4. A method according to claim 1, characterized in that it is possible to control a purposeful increase in cold-curing layers having a high viscosity of silicone rubber, in particular by selecting a fixed amount of means for forming cross-links between macromolecules of a certain residence time. apparatus in a dip bath and at an appropriate temperature with sufficient silicone rubber in the bath.

Recognized by the invention based on the results of expertise carried out by the Office of Invention and Patent, Berlin, DD