CS240116B1 - Method of flexible quartz chromatographic columns production and equipment for performance of this method - Google Patents

Method of flexible quartz chromatographic columns production and equipment for performance of this method Download PDF

Info

Publication number: CS240116B1
Authority: CS; Czechoslovakia
Prior art keywords: capillary; tube; quartz; temperature; quartz tube
Prior art date: 1983-07-14

Application number

CS835309A

Other languages

Czech (cs)

English (en)

Other versions

CS530983A1 (en

Inventor

Ludek Vodicka

Jan Triska

Jiri Mostecky

Jiri Goetz

Milos Hayer

Gabriela Kuncova

Original Assignee

Ludek Vodicka

Jan Triska

Jiri Mostecky

Jiri Goetz

Milos Hayer

Gabriela Kuncova

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-07-14

Filing date

1983-07-14

Publication date

1986-02-13

1983-07-14 Application filed by Ludek Vodicka, Jan Triska, Jiri Mostecky, Jiri Goetz, Milos Hayer, Gabriela Kuncova filed Critical Ludek Vodicka

1983-07-14 Priority to CS835309A priority Critical patent/CS240116B1/cs

1984-05-14 Publication of CS530983A1 publication Critical patent/CS530983A1/cs

1984-07-03 Priority to DD26486484A priority patent/DD244049A3/de

1984-07-13 Priority to DE19843425924 priority patent/DE3425924A1/de

1984-07-16 Priority to FR8411246A priority patent/FR2549228B3/fr

1984-07-16 Priority to NL8402248A priority patent/NL8402248A/nl

1984-07-16 Priority to GB08417997A priority patent/GB2143442B/en

1986-02-13 Publication of CS240116B1 publication Critical patent/CS240116B1/cs

Links

VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 46
239000010453 quartz Substances 0.000 title claims description 32
238000000034 method Methods 0.000 title claims description 22
238000004519 manufacturing process Methods 0.000 title claims description 3
230000005526 G1 to G0 transition Effects 0.000 claims abstract description 18
229920003055 poly(ester-imide) Polymers 0.000 claims abstract description 12
239000004642 Polyimide Substances 0.000 claims abstract description 11
229920001721 polyimide Polymers 0.000 claims abstract description 11
239000004922 lacquer Substances 0.000 claims abstract description 7
239000011248 coating agent Substances 0.000 claims abstract description 3
238000000576 coating method Methods 0.000 claims abstract description 3
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 10
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 10
239000001257 hydrogen Substances 0.000 claims description 10
229910052739 hydrogen Inorganic materials 0.000 claims description 10
238000001035 drying Methods 0.000 claims description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
229910052786 argon Inorganic materials 0.000 claims description 5
238000004587 chromatography analysis Methods 0.000 claims description 5
239000000203 mixture Substances 0.000 claims description 5
229920002312 polyamide-imide Polymers 0.000 claims description 5
229920000642 polymer Polymers 0.000 claims description 5
238000006073 displacement reaction Methods 0.000 claims description 4
239000012153 distilled water Substances 0.000 claims description 4
230000008569 process Effects 0.000 claims description 4
229920002379 silicone rubber Polymers 0.000 claims description 4
239000004945 silicone rubber Substances 0.000 claims description 4
238000004804 winding Methods 0.000 claims description 4
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 3
238000010438 heat treatment Methods 0.000 claims description 3
229910017604 nitric acid Inorganic materials 0.000 claims description 3
238000005498 polishing Methods 0.000 claims description 3
239000002966 varnish Substances 0.000 claims description 3
238000005406 washing Methods 0.000 claims description 3
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
229910052799 carbon Inorganic materials 0.000 claims description 2
239000000460 chlorine Substances 0.000 claims description 2
229910052801 chlorine Inorganic materials 0.000 claims description 2
230000001419 dependent effect Effects 0.000 claims description 2
238000000605 extraction Methods 0.000 claims description 2
239000007789 gas Substances 0.000 claims description 2
239000001307 helium Substances 0.000 claims description 2
229910052734 helium Inorganic materials 0.000 claims description 2
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 2
239000001301 oxygen Substances 0.000 claims description 2
229910052760 oxygen Inorganic materials 0.000 claims description 2
230000001681 protective effect Effects 0.000 claims description 2
239000004952 Polyamide Substances 0.000 claims 1
229920002647 polyamide Polymers 0.000 claims 1
239000010410 layer Substances 0.000 description 13
239000011521 glass Substances 0.000 description 9
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
230000008021 deposition Effects 0.000 description 7
229910002804 graphite Inorganic materials 0.000 description 7
239000010439 graphite Substances 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
239000000377 silicon dioxide Substances 0.000 description 6
229910044991 metal oxide Inorganic materials 0.000 description 4
150000004706 metal oxides Chemical class 0.000 description 4
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
230000008901 benefit Effects 0.000 description 3
239000012535 impurity Substances 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
125000005372 silanol group Chemical group 0.000 description 3
239000002904 solvent Substances 0.000 description 3
238000009736 wetting Methods 0.000 description 3
239000004962 Polyamide-imide Substances 0.000 description 2
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
229910052782 aluminium Inorganic materials 0.000 description 2
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 2
FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
238000011144 upstream manufacturing Methods 0.000 description 2
229910000838 Al alloy Inorganic materials 0.000 description 1
108010010803 Gelatin Proteins 0.000 description 1
229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
229910052581 Si3N4 Inorganic materials 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
ATRMIFNAYHCLJR-UHFFFAOYSA-N [O].CCC Chemical compound [O].CCC ATRMIFNAYHCLJR-UHFFFAOYSA-N 0.000 description 1
230000002411 adverse Effects 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
238000004873 anchoring Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
230000001143 conditioned effect Effects 0.000 description 1
238000005336 cracking Methods 0.000 description 1
230000009849 deactivation Effects 0.000 description 1
239000004205 dimethyl polysiloxane Substances 0.000 description 1
235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 description 1
238000011049 filling Methods 0.000 description 1
239000011888 foil Substances 0.000 description 1
238000004817 gas chromatography Methods 0.000 description 1
229920000159 gelatin Polymers 0.000 description 1
239000008273 gelatin Substances 0.000 description 1
235000019322 gelatine Nutrition 0.000 description 1
235000011852 gelatine desserts Nutrition 0.000 description 1
230000006872 improvement Effects 0.000 description 1
230000002779 inactivation Effects 0.000 description 1
230000006698 induction Effects 0.000 description 1
230000007246 mechanism Effects 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
QPJSUIGXIBEQAC-UHFFFAOYSA-N n-(2,4-dichloro-5-propan-2-yloxyphenyl)acetamide Chemical compound CC(C)OC1=CC(NC(C)=O)=C(Cl)C=C1Cl QPJSUIGXIBEQAC-UHFFFAOYSA-N 0.000 description 1
239000003921 oil Substances 0.000 description 1
239000003973 paint Substances 0.000 description 1
229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
239000013047 polymeric layer Substances 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 description 1
229910001950 potassium oxide Inorganic materials 0.000 description 1
238000010926 purge Methods 0.000 description 1
230000009467 reduction Effects 0.000 description 1
238000000926 separation method Methods 0.000 description 1
HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 1
KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
229910001948 sodium oxide Inorganic materials 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
239000007858 starting material Substances 0.000 description 1
230000003068 static effect Effects 0.000 description 1
239000004408 titanium dioxide Substances 0.000 description 1
239000005051 trimethylchlorosilane Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/24—Coatings containing organic materials
- C03C25/26—Macromolecular compounds or prepolymers
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B23/00—Re-forming shaped glass
- C03B23/04—Re-forming tubes or rods
- C03B23/047—Re-forming tubes or rods by drawing

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Geochemistry & Mineralogy (AREA)
General Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
General Life Sciences & Earth Sciences (AREA)
Application Of Or Painting With Fluid Materials (AREA)
Moulding By Coating Moulds (AREA)
Treatment Of Liquids With Adsorbents In General (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Physical Or Chemical Processes And Apparatus (AREA)

CS835309A 1983-07-14 1983-07-14 Method of flexible quartz chromatographic columns production and equipment for performance of this method CS240116B1 (en)

Priority Applications (6)

Application Number	Priority Date	Filing Date	Title
CS835309A CS240116B1 (en)	1983-07-14	1983-07-14	Method of flexible quartz chromatographic columns production and equipment for performance of this method
DD26486484A DD244049A3 (de)	1983-07-14	1984-07-03	Verfahren zur herstellung biegsamer chromatografischer quarz-kapillarsaeulen und vorrichtung zur realisierung des verfahrens
DE19843425924 DE3425924A1 (de)	1983-07-14	1984-07-13	Verfahren zur herstellung von biegsamen, kapillaren, chromatographischen kolonnen auf der basis von kieselsaeure und vorrichtung zur durchfuehrung dieses verfahrens
FR8411246A FR2549228B3 (fr)	1983-07-14	1984-07-16	Procede pour la production de colonnes capillaires chromatographiques siliceuses flexibles et appareillage pour sa mise en oeuvre
NL8402248A NL8402248A (nl)	1983-07-14	1984-07-16	Werkwijze voor de vervaardiging van buigzame, capillaire, chromatografische kwartskolommen en een inrichting voor de uitvoering van deze werkwijze.
GB08417997A GB2143442B (en)	1983-07-14	1984-07-16	Method of manufacturing pliable quartz capillary chromatographic columns and arrangement for execution of this method

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS835309A CS240116B1 (en)	1983-07-14	1983-07-14	Method of flexible quartz chromatographic columns production and equipment for performance of this method

Publications (2)

Publication Number	Publication Date
CS530983A1 CS530983A1 (en)	1984-05-14
CS240116B1 true CS240116B1 (en)	1986-02-13

Family

ID=5397745

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS835309A CS240116B1 (en)	1983-07-14	1983-07-14	Method of flexible quartz chromatographic columns production and equipment for performance of this method

Country Status (6)

Country	Link
CS (1)	CS240116B1 (de)
DD (1)	DD244049A3 (de)
DE (1)	DE3425924A1 (de)
FR (1)	FR2549228B3 (de)
GB (1)	GB2143442B (de)
NL (1)	NL8402248A (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP0192204A1 (de) *	1985-02-19	1986-08-27	The Perkin-Elmer Corporation	Flexible kapillare Chromatographiesäule
DE19649335C1 (de) *	1996-11-28	1998-06-18	Schott Geraete	Glaskapillarrohr mit angeformter Einengung seines Innendurchmessers, Verfahren zum Herstellen eines derartigen Glaskapillarrohres und Vorrichtung zur Durchführung des Verfahrens

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1139243B (de) *	1959-04-09	1962-11-08	British Petroleum Co	Vorrichtung zur Herstellung einer Glas- oder Quarzwendel
FR1590632A (de) *	1968-06-21	1970-04-20
US4293415A (en) *	1979-04-27	1981-10-06	Hewlett-Packard Company	Silica chromatographic column
JPS599502B2 (ja) *	1980-06-03	1984-03-02	古河電気工業株式会社	ガスクロマトグラフイ−用石英製分離管の製造方法

1983
- 1983-07-14 CS CS835309A patent/CS240116B1/cs unknown
1984
- 1984-07-03 DD DD26486484A patent/DD244049A3/de not_active IP Right Cessation
- 1984-07-13 DE DE19843425924 patent/DE3425924A1/de not_active Withdrawn
- 1984-07-16 GB GB08417997A patent/GB2143442B/en not_active Expired
- 1984-07-16 FR FR8411246A patent/FR2549228B3/fr not_active Expired
- 1984-07-16 NL NL8402248A patent/NL8402248A/nl not_active Application Discontinuation

Also Published As

Publication number	Publication date
GB2143442B (en)	1987-03-25
NL8402248A (nl)	1985-02-01
CS530983A1 (en)	1984-05-14
DE3425924A1 (de)	1985-01-24
FR2549228A1 (fr)	1985-01-18
GB2143442A (en)	1985-02-13
GB8417997D0 (en)	1984-08-22
FR2549228B3 (fr)	1985-11-22
DD244049A3 (de)	1987-03-25

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US4293415A (en)	1981-10-06	Silica chromatographic column
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EP0809108A1 (de)	1997-11-26	Kapillarsaüle für chromatographische Trennungen und Verfahren zur Herstellung
Ilkova et al.	1971	A simple versatile method for coating of glass capillary columns
Bartle	1973	Film thickness of dynamically coated open-tubular glass columns for gas chromatography
US3182394A (en)	1965-05-11	Method of making capillary columns
GB993322A (en)	1965-05-26	Method and apparatus for making optic devices
JPS6138561A (ja)	1986-02-24	可撓性石英毛管クロマトグラフイ−カラムの製法及び製造装置
JPS599502B2 (ja)	1984-03-02	ガスクロマトグラフイ−用石英製分離管の製造方法
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GB2143442A (en)	1985-02-13	Method of manufacturing pliable quartz capillary chromatographic columns
Sumpter et al.	1991	Enhanced radial dispersion in open tubular column chromatography
Blomberg	1977	Measurement of the average thickness of the film of stationary phase in dynamically coated glass capillary columns for gas chromatography
EP0101982B1 (de)	1988-11-30	Chromatographische Säule
RU2090497C1 (ru)	1997-09-20	Способ получения углерод-углеродного композита, стойкого к окислению
Tata et al.	1960	An apparatus for centrifugal acceleration of paper chromatography
US4732714A (en)	1988-03-22	Method and apparatus for centrifugal casting of contact lenses in open molds
SU1408364A1 (ru)	1988-07-07	Способ изготовлени стекл нных капилл рных хроматографических колонок и устройство дл его осуществлени
JPS60186431A (ja)	1985-09-21	光フアイバ母材の延伸装置
JP2682603B2 (ja)	1997-11-26	無機コート光ファイバの製造装置及び製造方法
JPS6120494B2 (de)	1986-05-22