CS241216B1 - Method of selective nickel catalyst preparation on carrier for hydrogenation - Google Patents

Method of selective nickel catalyst preparation on carrier for hydrogenation Download PDF

Info

Publication number: CS241216B1
Authority: CS; Czechoslovakia
Prior art keywords: nickel; hydrogenation; nickel hydroxide; catalyst; precipitate
Prior art date: 1983-12-01

Application number

CS896883A

Other languages

Czech (cs)

English (en)

Inventor

Vladimir Zapletal

Vladimir Prochazka

Jiri Cmolik

Frantisek Uhlir

Jaroslava Kudova

Jaroslav Prchlik

Jiri Ruzicka

Original Assignee

Vladimir Zapletal

Vladimir Prochazka

Jiri Cmolik

Frantisek Uhlir

Jaroslava Kudova

Jaroslav Prchlik

Jiri Ruzicka

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-12-01

Filing date

1983-12-01

Publication date

1986-03-13

1983-12-01 Application filed by Vladimir Zapletal, Vladimir Prochazka, Jiri Cmolik, Frantisek Uhlir, Jaroslava Kudova, Jaroslav Prchlik, Jiri Ruzicka filed Critical Vladimir Zapletal

1983-12-01 Priority to CS896883A priority Critical patent/CS241216B1/cs

1984-11-30 Priority to DD27013284A priority patent/DD245997A3/de

1984-12-04 Priority to BG6774084A priority patent/BG50070A1/xx

1984-12-05 Priority to SU847773677A priority patent/SU1447396A1/ru

1986-03-13 Publication of CS241216B1 publication Critical patent/CS241216B1/cs

Links

PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 20
238000005984 hydrogenation reaction Methods 0.000 title claims description 9
238000000034 method Methods 0.000 title description 8
238000002360 preparation method Methods 0.000 title description 2
239000002244 precipitate Substances 0.000 claims description 9
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 8
239000003513 alkali Substances 0.000 claims description 7
BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 claims description 7
239000000725 suspension Substances 0.000 claims description 7
150000001875 compounds Chemical class 0.000 claims description 5
229910052739 hydrogen Inorganic materials 0.000 claims description 5
239000001257 hydrogen Substances 0.000 claims description 5
238000004519 manufacturing process Methods 0.000 claims description 5
229910021529 ammonia Inorganic materials 0.000 claims description 4
239000003925 fat Substances 0.000 claims description 4
229910052751 metal Inorganic materials 0.000 claims description 4
239000002184 metal Substances 0.000 claims description 4
150000002815 nickel Chemical class 0.000 claims description 4
239000007787 solid Substances 0.000 claims description 4
239000000126 substance Substances 0.000 claims description 4
235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
239000008158 vegetable oil Substances 0.000 claims description 4
ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 claims description 3
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 3
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 3
229910052776 Thorium Inorganic materials 0.000 claims description 3
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 3
150000003863 ammonium salts Chemical class 0.000 claims description 3
229910052804 chromium Inorganic materials 0.000 claims description 3
239000011651 chromium Substances 0.000 claims description 3
229910052802 copper Inorganic materials 0.000 claims description 3
239000010949 copper Substances 0.000 claims description 3
150000002148 esters Chemical class 0.000 claims description 3
BBTOTXQDQDXXHB-UHFFFAOYSA-L nickel(2+) carbonate dihydrate Chemical compound [OH-].[OH-].[Ni++].OC(O)=O BBTOTXQDQDXXHB-UHFFFAOYSA-L 0.000 claims description 3
235000020777 polyunsaturated fatty acids Nutrition 0.000 claims description 3
229910052702 rhenium Inorganic materials 0.000 claims description 3
WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 claims description 3
229910052709 silver Inorganic materials 0.000 claims description 3
239000004332 silver Substances 0.000 claims description 3
229910052718 tin Inorganic materials 0.000 claims description 3
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 2
230000000737 periodic effect Effects 0.000 claims description 2
230000001376 precipitating effect Effects 0.000 claims description 2
229910052726 zirconium Inorganic materials 0.000 claims description 2
125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
239000000203 mixture Substances 0.000 claims 1
239000003054 catalyst Substances 0.000 description 15
230000000694 effects Effects 0.000 description 7
NVIFVTYDZMXWGX-UHFFFAOYSA-N sodium metaborate Chemical compound [Na+].[O-]B=O NVIFVTYDZMXWGX-UHFFFAOYSA-N 0.000 description 5
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 4
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
238000001035 drying Methods 0.000 description 4
229910052759 nickel Inorganic materials 0.000 description 4
ATYNVYNPWGEMMI-UHFFFAOYSA-H nickel(2+);carbonate;tetrahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[Ni+2].[Ni+2].[Ni+2].[O-]C([O-])=O ATYNVYNPWGEMMI-UHFFFAOYSA-H 0.000 description 4
238000001556 precipitation Methods 0.000 description 4
239000002002 slurry Substances 0.000 description 4
239000005909 Kieselgur Substances 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
238000001914 filtration Methods 0.000 description 3
238000005406 washing Methods 0.000 description 3
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
230000008901 benefit Effects 0.000 description 2
150000002431 hydrogen Chemical class 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
239000003607 modifier Substances 0.000 description 2
LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 2
229910000363 nickel(II) sulfate Inorganic materials 0.000 description 2
239000002245 particle Substances 0.000 description 2
239000002243 precursor Substances 0.000 description 2
229910000029 sodium carbonate Inorganic materials 0.000 description 2
239000011949 solid catalyst Substances 0.000 description 2
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical group [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
235000019484 Rapeseed oil Nutrition 0.000 description 1
206010040880 Skin irritation Diseases 0.000 description 1
239000004480 active ingredient Substances 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
150000001340 alkali metals Chemical class 0.000 description 1
235000019270 ammonium chloride Nutrition 0.000 description 1
BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
229910052921 ammonium sulfate Inorganic materials 0.000 description 1
235000011130 ammonium sulphate Nutrition 0.000 description 1
QDWJUBJKEHXSMT-UHFFFAOYSA-N boranylidynenickel Chemical compound [Ni]#B QDWJUBJKEHXSMT-UHFFFAOYSA-N 0.000 description 1
239000012018 catalyst precursor Substances 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
229910052740 iodine Inorganic materials 0.000 description 1
239000011630 iodine Substances 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
231100000614 poison Toxicity 0.000 description 1
238000006722 reduction reaction Methods 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000000741 silica gel Substances 0.000 description 1
229910002027 silica gel Inorganic materials 0.000 description 1
231100000075 skin burn Toxicity 0.000 description 1
230000036556 skin irritation Effects 0.000 description 1
231100000475 skin irritation Toxicity 0.000 description 1
235000012424 soybean oil Nutrition 0.000 description 1
239000003549 soybean oil Substances 0.000 description 1
239000003440 toxic substance Substances 0.000 description 1
150000003754 zirconium Chemical class 0.000 description 1

Landscapes

Catalysts (AREA)

CS896883A 1983-12-01 1983-12-01 Method of selective nickel catalyst preparation on carrier for hydrogenation CS241216B1 (en)

Priority Applications (4)

Application Number	Priority Date	Filing Date	Title
CS896883A CS241216B1 (en)	1983-12-01	1983-12-01	Method of selective nickel catalyst preparation on carrier for hydrogenation
DD27013284A DD245997A3 (de)	1983-12-01	1984-11-30	Verfahren zur herstellung von selektivem nickelkatalysator auf einem traeger fuer hydrierungsprozesse
BG6774084A BG50070A1 (en)	1983-12-01	1984-12-04	Method for preparing selective nickel catalyst on carrier for hydrogenation
SU847773677A SU1447396A1 (ru)	1983-12-01	1984-12-05	Способ приготовлени селективного никелевого катализатора на носителе дл процесса гидрировани

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS896883A CS241216B1 (en)	1983-12-01	1983-12-01	Method of selective nickel catalyst preparation on carrier for hydrogenation

Publications (1)

Publication Number	Publication Date
CS241216B1 true CS241216B1 (en)	1986-03-13

Family

ID=5440953

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS896883A CS241216B1 (en)	1983-12-01	1983-12-01	Method of selective nickel catalyst preparation on carrier for hydrogenation

Country Status (3)

Country	Link
BG (1)	BG50070A1 (de)
CS (1)	CS241216B1 (de)
DD (1)	DD245997A3 (de)

1983
- 1983-12-01 CS CS896883A patent/CS241216B1/cs unknown
1984
- 1984-11-30 DD DD27013284A patent/DD245997A3/de not_active IP Right Cessation
- 1984-12-04 BG BG6774084A patent/BG50070A1/xx unknown

Also Published As

Publication number	Publication date
DD245997A3 (de)	1987-05-27
BG50070A1 (en)	1992-05-15

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