CS266351B1 - Apparatus using exhaust heat of low temperature or electric energy for producing mechanic energy and cooling - Google Patents

Apparatus using exhaust heat of low temperature or electric energy for producing mechanic energy and cooling Download PDF

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Publication number
CS266351B1
CS266351B1 CS811828A CS182881A CS266351B1 CS 266351 B1 CS266351 B1 CS 266351B1 CS 811828 A CS811828 A CS 811828A CS 182881 A CS182881 A CS 182881A CS 266351 B1 CS266351 B1 CS 266351B1
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CS
Czechoslovakia
Prior art keywords
absorber
desorber
solution
stage
pressure
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CS811828A
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Czech (cs)
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CS182881A1 (en
Inventor
Hans Dipl Ing Foerster
Original Assignee
Foerster Hans
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Application filed by Foerster Hans filed Critical Foerster Hans
Publication of CS182881A1 publication Critical patent/CS182881A1/en
Publication of CS266351B1 publication Critical patent/CS266351B1/en

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01K—STEAM ENGINE PLANTS; STEAM ACCUMULATORS; ENGINE PLANTS NOT OTHERWISE PROVIDED FOR; ENGINES USING SPECIAL WORKING FLUIDS OR CYCLES
    • F01K25/00—Plants or engines characterised by use of special working fluids, not otherwise provided for; Plants operating in closed cycles and not otherwise provided for
    • F01K25/06—Plants or engines characterised by use of special working fluids, not otherwise provided for; Plants operating in closed cycles and not otherwise provided for using mixtures of different fluids
    • F01K25/065—Plants or engines characterised by use of special working fluids, not otherwise provided for; Plants operating in closed cycles and not otherwise provided for using mixtures of different fluids with an absorption fluid remaining at least partly in the liquid state, e.g. water for ammonia
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
    • F25B15/00—Sorption machines, plants or systems, operating continuously, e.g. absorption type
    • F25B15/02—Sorption machines, plants or systems, operating continuously, e.g. absorption type without inert gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
    • F25B29/00—Combined heating and refrigeration systems, e.g. operating alternately or simultaneously
    • F25B29/006—Combined heating and refrigeration systems, e.g. operating alternately or simultaneously of the sorption type system
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A30/00—Adapting or protecting infrastructure or their operation
    • Y02A30/27—Relating to heating, ventilation or air conditioning [HVAC] technologies
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
    • Y02B30/00—Energy efficient heating, ventilation or air conditioning [HVAC]
    • Y02B30/62—Absorption based systems

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Engine Equipment That Uses Special Cycles (AREA)
  • Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Description

266 361 F0XK/220267266 361 F0XK / 220267

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ΚΟΤΟρβΜ «3/100 Γ1ΟΙΙ0Χ3ΟΤ «aO/IUII0U rilKUMotipaaoM πο/iyMennoro aoraToro pacTBOpa ot CTynen0 κ cTyneMM aecopeepa, pacsonan cpe«a npkl btomtíojibuiePi nacTbo onsrrb ocBOdoxxaeTcn 0 stmm npenwrcTByeT «ocT0*eH0p npe«noMT0Te/ibHbix <so/ibui0xU10POT narpy3K0 (uihpot xerasaiwi). Ηβ«οοτβτκοΜ βτογο MHorocTyneHMaToro cnocoda no ορθβμθημ» cnponeccoM c TojibKO o«hoň CTyneHb» pacui0peH09 0 aacopeu00 ae/iaeTca bo3H0khoooh0o noTepb.I>aciii0pon0o paooHBfl oponu npQ0cxo«0T πρμ btom τα/ibKO ao mbctb sadopa MaMaucuieH ατ.νηοιΐ0««0/101100. MaxepxxM «a/ibnefluiero aaaopa mmbpt tskmm odpasoM ηβλοοτ«τκμ, kotopho ho Moryr «monpaBaaHW. B xpyroM cnocodB «ocopdep ββκβΗηβτβη ycTpotteTBOM TeruionepeAaMM o npucoaxMMeMHMMpoacpoyapoM αλρ οτ«θ/ιομ0« raaa or xmakoctm. B/iaroxapn κοητβκτυ Mexxy psctbopom cpexHeMKoiiueinpaii00 0 padOMeft cpaAoM mmctotb napa padonaM cpaxu HabiadexHO χολχηβ <«Tk M«/ioft, cc/10««3/101100 napa aďcopdUMOHHofl xmakoctm ne npeHedpexMMo Ma/10. 3το πρ0βολητ k ηοτβρβ aTonxonepanaxe TypduiHu 0 nperwrcTByaT TpedyeMOHy cuxbHOMy oxxaxxeHMo τβηχαΗοοΜτβχη. KpomoΤ01Ό. nap pacíOMiafl cpaxu daa AonoAH0Te/ibHoH ommgtkm Ha Μοχβτ πρ0μοιι$ιτi>csi «/in nprí03oo«ciiiaXI.1/10/1«. ΗβχουτβτκοΜ e btom cnocoda wo/meTc*! Taxxe OTxaa ot paroHepaTMBHoro τβη/ιοοΡΜβκα Mexxytsu/diuM 0 óoraTbiM pacTBOpOH. BoraTuPl ρβοτοορ npo«oap0Ta/ibHO HarpenaoTCíi γορρμμμ xumobum raaoM,adcopdU00. ΑβΒΛβΗ0βΜ napa. κατοροΛ a odJiacTu paeoMeH TOMnopaTypu ne / iban npeHBdperaTb. Tpe «syeT ΟΒ033ΤβΛ bHOB ΟΓρβΗ0ΜΒΗ0βοτχοΑΜψΒΓο Ten / ia, το ecTb 266 351 2 pu He 3 3» »3 3 3 3 K 3 3 3 3 3 3 3 3 3 3 «A / i0TN / ibMyp κα / ioMwy e ΜβρατοροΜ pen0pKy / 10000 <« βΦ / ιοΐ'Μ <ιτορ), Ho <: ι.! 3ΐ: ι; ν 0/10 ΚραΤΚΟβρβΜΒΜΗΒΒ KO / ie «í / l» ma »TC« nOTPOdHOCTb B XOMW ΟΓρβΗΜΜΜΒββΤ ρβΒΗΟΜΒΡΜΟΒ0cno / i b3ooa »i0o cyuiecTBypuiero ηρο« / ιοχβΗ00 OTXo «sn ero ren / ia. 03 naTUMTMj · ΡΓ No. 940466 m No, 942515 msbbcthu cnoooau npaopamwnHH τοπ / ia uMexanM'tecKep meprkip c μοπο / ιι> 3οβ3ημβμ mhoí'0x eeutecTB. κ τ ο / / / 10 10 10 10 10 10 10 10 10 n n n n n n eň eň eň eň eň eň T T T T T T T T T T T T T T T T T or or or or or or or or or or NPH btom Typei4HoK oTBHpaeTcp padosan CPE "and yxw riepex ιιολημμplti! HI0piil I0UM 143 ipOMUMy lOMHOPI I 0T> THM4M M nOOTyTUMT B BdOOpdSP CO CTynBMMBVUM ypOBHBM ΧΒΒΛΒΗΜΒ.Ho NPH Hap.yuiBH00 npuiHuma ηρατ0θοτοκβ to« worse (pacTaop ζadcopdU0OHHa «cpe / TA) pacuiuppoTCPl II 1/1 H IC 1 B 1 C 2 O 2 CO 2 O 2 O C 1 H 2 O 2 W 1 O 2 CT 1 H 2 O 5 K 1 O / 10110 * 1. ΚΟΤΟρβΜ «3/100 Γ1ΟΙΙ0Χ3ΟΤ« AO / IUII0U rilKUMotipaaoM πο / iyMennoro aoraToro pacTBOpa rpm CTynen0 κ cTyneMM aecopeepa, pacsonan CPE "and npkl btomtíojibuiePi nacTbo onsrrb ocBOdoxxaeTcn 0 stmm npenwrcTByeT« ocT0 eH0p NPE * «noMT0Te / ibHbix <Sa / ibui0xU10POT narpy3K0 (uihpot xerasaiwi). Ηβ «οοτβτκοΜ βτογο MHorocTyneHMaToro cnocoda well ορθβμθημ» cnponeccoM c TojibKO the "follow after CTyneHb» pacui0peH09 0 aacopeu00 ae / iaeTca bo3H0khoooh0o noTepb.I> aciii0pon0o paooHBfl curtain npQ0cxo «0T πρμ btom τα / ibKO and mbctb sadopa MaMaucuieH ατ.νηοιΐ0« «0 / 101100. MaxepxxM «a / ibnefluiero aaaopa mmbpt tskmm odpasoM ηβλοοτ« τκμ, kotopho ho Moryr «monpaBaaHW. B xpyroM cnocodB «ocopdep ββκβΗηβτβη ycTpotteTBOM TeruionepeAaMM by npucoaxMMeMHMMpoacpoyapoM αλρ οτ« θ / ιομ0 «raaa or xmakoctm. B / iaroxapn κοητβκτυ Mexxy psctbopom cpexHeMKoiiueinpaii00 0 padOMeft cpaAoM mmctotb napa padonaM cpaxu HabiadexHO χολχηβ <«Tk M« / ioft, cc / 10 «3/101100 napa adcopdUMOHHofl xmakoctm no npeHedpexMMo Ma / 10. 3το πρ0βολητ to ηοτβρβ andTonxonepanaxe TypduiHu 0 nperwrcTByaT TpedyeMOHy cuxbHOMy oxxaxxeHMo τβηχαΗοοΜτβχη. KpomoΤ01Ό. nap paciOMiafl cpaxu daa AonoAH0Te / ibHoH ommgtkm Ha χοχβτ πρ0μοιι $ ιτi> csi / / in npri03oo «ciiiaXI.1 / 10/1«. ΧβχουτβτκοΜ e btom cnocoda wo / meTc *! Taxxe OTxaa ot paroHepaTMBHoro τβη / ιοοΡΜβκα Mexxytsu / diuM 0 óoraTbiM pacTBOpOH. BoraTuPl ρβοτοορ npo «oap0Ta / ibHO HarpenaoTCíi γορρμμμ xumobum raaoM

KpyroBoM < saMKHyTufl) npouecc dxaroxapsi aiOMy Tpadyer cx0uikom μηογο τβη/ia, κατοραο ποτομ/ii i/ixi ιο au ( i, o 1 oe/ioi 10 03 diitxiioro pacTBOpa onwtb b OKpyxaumye cpaný 0 omocto ι οπ/ιοορμοιιο mi/x/ívmmctumm npo«yKT»M0, to ecTb Mexxy doraTUM 0 dexnuM pacTeopoM, npo0cxox*rr «Ba npoueccaT«n/ionepe«aM0 o 3arp03H*iioiiiefl cpexofl CxypHa/ι Energie 26/1974/, 3 οτρ.83-87 ΜΛ0 nu/ioxennaíi oaíiBKa ΦΡΓ No. 2342263). lle/ib 03QdpeTeH00 ,KpyroBoM <saMKHyTufl) npouecc dxaroxapsi aiOMy tpadyer cx0uikom ηογο τα, κατοραο ποτομ / ii i / ixi ιο au (i, 1 oe / ioi 10 03 diitxiioro pacTBOpa onwtb b OKpyxaumye cpaný 0 omocto ι οπ / ιοορμοιιο mi / x / ívmmctumm npo «yKT» M0, to ecTb Mexxy doraTUM 0 dexnuM pacTeopoM, npo0cxox * rr «Ba npoueccaT« n / ionepe «aM0 o 3arp03H * iioiiiefl cxypHa / ι Energy 26/1974 /, 3 οτρ.83-87 ΜΛ0 nu / ioxennaíi and BKa a No. 2342263). lle / ib 03QdpeTeH00

Lle/ib» 03ο<5ρβτβκ0ϊ( wb/iwjtcw ycTpottcToo TepMO«0HaM0MecKoro Kpyroeoro npouecca, np0 kotopomnpO03BO/(0TC0 ΟΧΗΟΒρΟΜΟΗΗΟ MOXaH0MeCKa*1 0/10 3/IOKTP0HOCKa0 ΠΟ/1β3ΗβΡ ΒΗβΡΓ0Α 0, Β «βΗΜΟΜ C/iyMae,ΧΟ/ΙΟ/Ι Ο 0'JMOHS1OMblM0 ΚΟΜηθΗβΗΤ3Μ0 ΦΟΡΜ ΘΗ6ΡΓ00, 03 ΟΤΧΟΛΡψβΓΟ ΤβΠΛβ He3HaM0Te/lbHOPOTeMnepaTypHoro υροβηρ. np0MeM Ten/ioHoc0Te/ib ox/iax«aeTcsi β ιιΐ0ροκοΡί TeMnepaTypHofl o<s/iacT0 «orermepaTyp 3HaM0Te/ibHO H0*e 10ÍJ“C.Lle / ib »03ο <5ρβτβκ0ϊ (wb / iwjtcw ycTpottcToo TepMO) 0HaM0MecKoro Kpyroeoro npouecca, np0 kotopomnpO03BO / (0TC0 XρΟΜΟΗΗΟ MOXaH0MeCKa * 1 0/10 3 / IOKTP0HOCKa0 ΠΟ / 1β3ΗβΡ ΒΗβΡΓ0Α 0,« βΗΜΟΜ C / iyMae, ΧΟ / ΙΟ / Ι Ο 0'JMOHS1OMblM0 ΚΟΜηθΗβΗΤ3Μ0 ΦΟΡΜ ΘΗ6ΡΓ00, 03 ΟΤΧΟΛΡψβΓΟ ΤβΠΛβ He3HaM0Te / lbHOPOTeMnepaTypHoro υροβηρ. np0MeM He / ioHoc0Te / ib ox / IAX "aeTcsi β ιιΐ0ροκοΡί TeMnepaTypHofl of <s / iacT0« orermepaTyp 3HaM0Te / ibHO H0 * e 10ÍJ "C.

Ifei49iiren0<? .cymtiog.TH 0?odpexstinyt. B ocHoey M3OdpeTBH0p no,noxeHa τβχΗΜΜββκβΒ aarnsa «οβαβτβ ycTpoitoTBO αλ« kicnoabsoeaHMnOTxoAPwaro τβπ/ia HMaxoro TeMnepaTypHoro ypoBMfl a xaMecTae npouecca, xonoAH«x>iitaro npoueccciipou00 i ttpMMMecKuro cnocoda np0 πρηχθηβημμ napu pa«OMero eaatecTBa o xopouio MacopeMpynuaMcnPDriiniííl epe/ioPí. naxo/ivimePlcu nox bucok0M χαο/ιβΗ0θΜ 0 K0n«mett np0 «aB/iaH00 OKpyxaioinett cpe/iu. 0no/xxo/c;iiU0M adcopdUHOHHUM cpeacTBOM - αλ« npo03Bo«cTBa MexaH0MacxoM 0/10 ΒΛβκτρΜΜβοκαΜ sHepruuO OAHOBpeMBHHUM npO03BO/(CTBOM XO/IO/(a . (lF'0 3tom padonan cpaxa o bmcok0m «ao/ien0eM n/iaro«apíi «acopdU00 «ο/ixna np0 bmcokom ««0/101100 ror>M0'iooK0 oN/ie/iíiTbcn 10 pacTaopa, neperpaaaTbcn, pacwMpwrbcn βμβκτμβηο b TypdMHa ο οτλορομ napa 0 d/iaroxapn cTyneuMaToří adcopdU00 - οοοτββτοτΒβΗΗα CTynoHííM «aB/ien0p sadopa Typd0niii - np0 oahuopbmbhhom οτοοΑβ τβπΛβ onwTb nonacTb b X0«K0W pacTBOp. to ecTb a adcopdU0OHMy» cpexy, ΠΡ0ΜΟΜ cs/iaro«apyi bucokomy naobimeH0K> poraToro pacTBOpa 0, c/ie«ooaTO/ibna, hmskoR naMa/ibnoři 266 asi TOMnepaType Aecopeuwi4, bosmomho οχΑβιΚΑβΗΜβ τβΠΑΟΗΟΟΜΤβΑΡ b uiiapokoH TeMnepaTypMofl opabcth nWCnOAbOOBaMIAe ΟΤΧΟΑ«ΚβΓΟ ΤΘΠΛβ C HedOAblUHH ΤβΜΠβρβΤΥρΗΗΜ ypQBHBM.Ifei49iiren0 <? .cymtiog.TH 0? odpexstinyt. B ocHoey M3OdpeTBH0p Well noxeHa τβχΗΜΜββκβΒ aarnsa «οβαβτβ ycTpoitoTBO αλ« kicnoabsoeaHMnOTxoAPwaro τβπ / i HMaxoro TeMnepaTypHoro ypoBMfl and xaMecTae npouecca, xonoAH «x> iitaro npoueccciipou00 and ttpMMMecKuro cnocoda NP0 πρηχθηβημμ napu PA« Omer eaatecTBa of xopouio MacopeMpynuaMcnPDriiniííl EPE / ioPí. naxo / ivimePlcu nox bucok0M χαο / ιβΗ0θΜ 0 K0n «mett np0« aB / iaH00 OKpyxaioinett cpe / iu. 0no / xxo / c; iiU0M adcopdUHOHHUM cpeacTBOM - αλ n npo03Bo c cTBa MexaH0MacxoM 0/10 ΒΛβκτρΜΜβοκαΜ sHepruuO OAHOBpeMBHHUM npO03BO / (CTBOM XO / IO / (a. (Ien0eM n / iaro) apII «acopdU00« ο / Ixnay NP0 bmcokom «« 0/101100 ror> M0'iooK0 oN / IE / iíiTbcn 10 pacTaopa, neperpaaaTbcn, pacwMpwrbcn βμβκτμβηο b TypdMHa ο οτλορομ Napa 0 d / iaroxapn cTyneuMaToří adcopdU00 - οοοτββτοτΒβΗΗα CTynoHííM «aB / ien0p sadopa Typd0niii - np0 oahuopbmbhhom οτοοΑβ τβπΛβ onwTb nonacTb b X0 «K0W pacTBOp. To ecTb and adcopdU0OHMy» cpexy, ΠΡ0ΜΟΜ cs / iaro , bosmomho οχΑβιΚΑβΗΜβ τβΠΑΟΗΟΟΜΤβΑΡ b uiiapokoH TeMnepaTypMofl opabcth nWCnOAbOOBaMIAe ΟΤΧΟΑ ΚβΓΟ ΤΘΠΛβ C HedOAblUHH ΤβΜΠβρβΤΥρΗΗΜ ypQBHBM.

Coorue tct nranno ΜβοοροτβκΜ» »τ« aaxaM· pauiaaTCP tbm, mto obamuM pootbop, πολυμλκμιιμΜοη naMI4AHBM ΚΟΜΜΟ AOCOpOOPa, ΟΤΑββΤ CBOO "OUtyTMMOe" ΤΟΠΛΟ ΟΗβΜβΛβ ΠρβμίΜΧΙΜΒΟΤΒΘΗΗΟ ΡΘΓβΜβΡαΤΜΒΗΟ ΒAecopeepe μοοτκμηογο ποτοκβ MacTui AeraayeMoro pacTBopa μαία b πβρβμμηομ neperpeoareAe - napanpddOHoM CPWAW. ΠΟΛΟΟΛΙ4ΜΜΜ K TypdMHO Ο OTdOPOM Π«Ρ· Μ nOA.yM«K)l«l4MC*l (((» ΝΟΡΧΗΟΜ ΚιιΠΙ,ΙΠ «Μιιι,ιροπρη,14 ΙΙΟΠΙΊΙIpWAGI BOHHO ΠΟΟΑΒ ΡΤΟΓΟ ΠρΟΙΑΟΧΟΑΙΑΤ ΜβΑΜΗβΛΗΙΑΡ ρΟΓΟΜΟΡΛΤΜΒΜβΡ ΟΤΑΑΜβ Τ«ΠΛΛ 11 .VRTpOflOTBMηαρβΑβΜίΑ τθπλο doraroMy pacTBOpy, ποαβοαιαηομυ β AecopdBp, Μ Β αοηηομ CAyMae, CAeA.yuMnaw οταβμο Τ«ΠΛΑ ΠΡΟΙ4ΟΧ0ΧΙ4Τ Μ XOAOAMAbMMX ΥΟΤροΜβΤΒΛΧ β BHOIUHI4M ΟΤΒΟΑΟΜ TWWM 14 ««AHUM ρβΟΤΟΟΡ dOAWOCTbPpacuinpweTCM β acjcopóunoHHoW cTyneHU ημοκογο aobaokiap, Πρια ®τομ κοκαοηοιαρυοτοη napoodpasnap paduMae cpeAa, noAyMaomapce Ha bbpxhbhMHorocTyneHMaTofl TypdiAMu c otpopom napaTypaviHU c οτρορομ napa, a mbctiaMhoCoorue stranded nranno ΜβοοροτβκΜ »» τ «· AAXA pauiaaTCP TBM to these obamuM pootbop, πολυμλκμιιμΜοη naMI4AHBM ΚΟΜΜΟ AOCOpOOPa, ΟΤΑββΤ CBOO" OUtyTMMOe "ΤΟΠΛΟ ΟΗβΜβΛβ ΠρβμίΜΧΙΜΒΟΤΒΘΗΗΟ ΡΘΓβΜβΡαΤΜΒΗΟ ΒAecopeepe μοοτκμηογο ποτοκβ MacTui AeraayeMoro pacTBopa μαία b πβρβμμηομ neperpeoareAe - napanpddOHoM CPWAW. The ΠΟΛΟΟΛΙ4ΜΜΜ TypdMHO OTdOPOM Ο Π «· Ρ Μ nOA.yM« K) l «l4MC L * (((» ΝΟΡΧΗΟΜ ΚιιΠΙ, ΙΠ «Μιιι, ιροπρη 14 ΙΙΟΠΙΊΙIpWAGI BOHHO ΠΟΟΑΒ ΡΤΟΓΟ ΠρΟΙΑΟΧΟΑΙΑΤ ΜβΑΜΗβΛΗΙΑΡ ρΟΓΟΜΟΡΛΤΜΒΜβΡ ΟΤΑΑΜβ Τ« ΠΛΛ 11 .VRTpOflOTBMηαρβΑβΜίΑ τθπλο doraroMy pacTBOpy, AecopdBp ποαβοαιαηομυ β, Μ β αοηηομ CAyMae, CAeA.yuMnaw οταβμο Τ «ΠΛΑ ΠΡΟΙ4ΟΧ0ΧΙ4Τ Μ XOAOAMAbMMX ΥΟΤροΜβΤΒΛΧ β BHOIUHI4M ΟΤΒΟΑΟΜ TWWM 14« «AHUM ρβΟΤΟΟΡ dOAWOCTbPpacuinpweTCM β acjcopóunoHHoW cTyneHU ημοκογο aobaokiap, Πρια ®τομ κοκαοηοιαρυοτοη napoodpasnap paduMae CPEA, noAyMaomapce Ha bbpxhbhMHorocTyneHMaTofl TypdiAMu c otpopom napaTypaviHU c οτρορομ napa, a mbctiaMho

MacTMMHoro ποτοκβMacTMMHoro ποτοκβ

T enAOOdHBHHI4K (4, B komus ABcopaepa, mam ηοΑΗοοτωο Mepea neperpoBareAbI4A14 ΜβΟΤΙΑΜΜΟ MBpB3 ΠβρβΓρβΒβΤβΑύ HHOrOCΤΥΠβΗΜβΤΟΛ KOHABHCMpyBTCH 14 ΠΟΑΒΟΑΙ4ΤΟΡ Μβρβ3 adCOpdllUOHH.yK) xoAOAHAbHy» ycTanooKy ηθποορβαοτβθηηο k aaeopaiwoHHofl CTyneHM ηιαβκογο aobabhiap. PadoMap cpe«a®«·βΚΤΙ4ΒΗΟ paCUHAPPOTCP Β TypdlAHO C OTdOPOM Πβρβ ΜΗΟΓΟΟΤΥΠβΗΜβΤΟ 14 dOAMuM ρβΟΤΒΟΡ 0 ΟΤ,ΥΠβΜΙΑaacopauHH ηι43κογο αββαβμιαρ HeperyAiApyeMO nor/iomaer (43 nepuott cr,yneni4 (ημοκογο αββλβημη)TypdMHM oToopa napa 14, b αβηηοη CAyMae, 143 aacaptsuHOHHoC xoAOAiAAbHOd υοτθηοβκια - nap padoneflcpoau ao KOHueHTpauHM paBHOBecHH. Ποοαβ sToro Hacocon ΗβΓΗβτββτορ pacTBop <aescopdBHT) aoAaBABHMP CABAy»U|eM, dOABB BUCQKOtt CTynBHM adCOPdUlAIA 14 ΠΟΓΛΟΙΚββΤ T3M BHOBb (lap padOMBtf CpBAUi43 βτοροΛ CTynewi4 TypdiAHM OTdopa napa ao κοημβητρακιαια peBHOBBCMP, ποοαβ μβγο ocyutecTBAPBTCPAaAbHB«IUGB CTynBHMaTOB HaCMWBHI4B paCTBOpa 143-33 ΟΤΥΠΒΗΜβΤΟΓΟ nOBUlUBHlAP ΑβΒΑΒΗΙΑΡ pACTBOpa ΠΡΙ4cooTBBTGTBy»maM oTdope napoe paaoMeM cpbau (43 οοοτββτοτβυριιιιαχ οτ,νηβΗβΜ τ,υρριαηη g ατβοροπnapa, τβκ mto ποοαβ ποοαβαηβΗ crynaHui aacopaiwi (CTyneHb aacopouuvt eucoKoro αββαοηιαρ) cmauhoHacumenHuř, paeoMefl cpbaoM doraTuM pacTBop c hvokoM HaMaAbHofl TeHneparypofl αβοορρμιαια -dAarOAapH OrpaHMMBHH» ΤΒΠΛΟΠΒΡΒΑβΜΙΑ OT dBAHOPO paCTBOpa K ΡΟΓβΤΟΗΥ paCTBOpy B ΤΒΠΛΟΟΡΗΒΗΚΙΑΚβBdAI43l4 COCTOPHI4P ΚΙ4ΠΘΗΙ4Ρ, ΠΡΒΑΠΟΜΤΙΑΤΒΛΜ-ΙΟ, C ΟΠΡΒΑΒΛΒΗΗΗΗ ΠΒΡΒΟΧΛβΧΑΒΗΙΑΒΗ - ΠΟΟΤΥΠββΤ 14 BABCOpdBP. Πρ(4 STOH TBnAOMOCIATBAb, ?'hoABOAI4HHR Β ΠΡΟΤΜΒΟΤΟΚΒ K ΑΒΓ33ΥβΗΟΗ.Υ paCTBOpy BAecopdepe, oXAaxxaeTcp siiaMHTBAbHO hiaxb KXFC (4 oahobpbhbhho AocTwaeTCp Bucoxap miaciotu napapadOMBfl CpBAU B ABCOpdBpB, Θ OCOdOft Ι4ΟΠΟΑΗβΗΙ414 l43OdPBTBHI4P npBAyCMOTpBHO, MTO KOAMMBCTUOHacuiueHHoro paCTBOpa nepeA ποοαβαηθΜ (eucoKoro asbashiap) CTyneHb» adcopdUMiA paíJABAPBTCp,aaTBH oAHa MacTb ποαβοαιατορ k CTyneHH a<scop<3ui4(4 BucoKoro αββαβηιαρ, a Apyrap MacTb - eABCOpdBP CpBAHero ΑβΒΛβΗΙΑΡ. KOTOPUft ΡβΒΟΤββΤ ΠΡΗΡβΒΗΟΜ ΑβΒΛβΗΜΜ,. ΒΚΛΒΜβΗ ΠαρβΑΑΒΑϋΗΟ 14OdOrpBBaBTCH OTXOAPUIHM ΤΒΠΑΟΗ ewe HB3HaMI4TBAbHOrO ΤβΜΠβρβΤΥΡΗΟΓΟ ypOBHíl. (lap paaOMeřl CpBAUstopo Aecopoepa ορβαηβγο αββαβημα ηρόχοΑΚΤ β CTyneHb aacopdUHH BucoKoro αββαβηηη, wa-aa MerooTdop napa paeoMett cpbam CTyneHia . βμοοκογο αββαβημη ' TyptsuiHw oTcsopa napa cootbbtctbbhhoyMonhuiaeTcp, r,pn stoh koahmbctbo pa«soMeM cpbau. pacuiupouHoW ao do/iae huiskoM ούυποηη aiibanhihhb TypduiHB oTdopa napa noBUwaeTcn b pasHoW napě.T enAOOdHBHHI4K (4, B whom have ABcopaepa, MAM ηοΑΗοοτωο MEPE neperpoBareAbI4A14 ΜβΟΤΙΑΜΜΟ MBpB3 ΠβρβΓρβΒβΤβΑύ HHOrOCΤΥΠβΗΜβΤΟΛ KOHABHCMpyBTCH 14 ΠΟΑΒΟΑΙ4ΤΟΡ Μβρβ3 adCOpdllUOHH.yK) xoAOAHAbHy »ycTanooKy ηθποορβαοτβθηηο to aaeopaiwoHHofl CTyneHM ηιαβκογο aobabhiap. PadoMap CPE «A®« · βΚΤΙ4ΒΗΟ paCUHAPPOTCP Β TypdlAHO C OTdOPOM Πβρβ ΜΗΟΓΟΟΤΥΠβΗΜβΤΟ 14 dOAMuM ρβΟΤΒΟΡ 0 ΟΤ, ΥΠβΜΙΑaacopauHH ηι43κογο αββαβμιαρ HeperyAiApyeMO Nor / iomaer (43 nepuott cr, yneni4 (ημοκογο αββλβημη) TypdMHM oToopa hood 14 b αβηηοη CAyMae 143 aacaptsuHOHHoC xoAOAiAAbHOd υοτθηοβκια - for padoneflcpoau and KOHueHTpauHM paBHOBecHH. Ποοαβ Stora Hacocon ΗβΓΗβτββτορ pacTBop <aescopdBHT) aoAaBABHMP CABA »U | eM dOABB BUCQKOtt CTynBHM adCOPdUlAIA 14 ΠΟΓΛΟΙΚββΤ T3M BHOBb (LAP padOMBtf CpBAUi43 βτοροΛ CTynewi4 TypdiAHM OTdopa hood and κοημβητρακιαια peBHOBBCMP, ποοαβ μβγο ocyutecTBAPBTCPAaAbHB« IUGB CTynBHMaTOB HaCMWBHI4B paCTBOpa 143-33 ΟΤΥΠΒΗΜβΤΟΓΟ nOBUlUBHlAP ΑβΒΑΒΗΙΑΡ pACTBOpa ΠΡΙ4cooTBBTGTBy »m oTdope napoe paaoMeM cpbau g , Τβκ MTO ποοαβ ποοαβαηβΗ crynaHui aacopaiwi (CTyneHb aacopouuvt eucoKoro αββαοηιαρ) cmauhoHacumenHuř, paeoMefl cpbaoM doraTuM pacTBop c hvokoM HaMaAbHofl TeHneparypofl αβοορρμιαια -dAarOAapH OrpaHMMBHH »ΤΒΠΛΟΠΒΡΒΑβΜΙΑ OT dBAHOPO paCTBOpa K ΡΟΓβΤΟΗΥ paCTBOpy B ΤΒΠΛΟΟΡΗΒΗΚΙΑΚβBdAI43l4 COCTOPHI4P ΚΙ4ΠΘΗΙ4Ρ, ΠΡΒΑΠΟΜΤΙΑΤΒΛΜ-ΙΟ C ΟΠΡΒΑΒΛΒΗΗΗΗ ΠΒΡΒΟΧΛβΧΑΒΗΙΑΒΗ - ΠΟΟΤΥΠββΤ 14 BABCOpdBP. Πρ (4 STOH TBnAOMOCIATBAb,? 'HoABOAI4HHR Β ΠΡΟΤΜΒΟΤΟΚΒ K ΑΒΓ33ΥβΗΟΗ.Υ paCTBOpy BAecopdepe, oXAaxxaeTcp siiaMHTBAbHO hiaxb KXFC (4 oahobpbhbhho AocTwaeTCp Bucoxap miaciotu napapadOMBfl CPBA ABCOpdBpB B, Θ OCOdOft Ι4ΟΠΟΑΗβΗΙ414 l43OdPBTBHI4P npBAyCMOTpBHO MTO KOAMMBCTUOHacuiueHHoro paCTBOpa NEP ποοαβαηθΜ (eucoKoro asbashiap) CTyneHb » adcopdUMiA paíJABAPBTCp, aaTBH oAHa MacTb ποαβοαιατορ to CTyneHH and <SCOP <3ui4 (4 BucoKoro αββαβηιαρ and Apyrap MacTb - eABCOpdBP CpBAHero ΑβΒΛβΗΙΑΡ. KOTOPUft ΡβΒΟΤββΤ ΠΡΗΡβΒΗΟΜ ΑβΒΛβΗΜΜ ,. ΒΚΛΒΜβΗ ΠαρβΑΑΒΑϋΗΟ 14OdOrpBBaBTCH OTXOAPUIHM ΤΒΠΑΟΗ ewe HB3HaMI4TBAbHOrO ΤβΜΠβρβΤΥΡΗΟΓΟ ypOBHíl. (LAP paaOMeřl CpBAUstopo Aecopoepa ορβαηβγο αββαβημα ηρόχοΑΚΤ β CTyneHb aacopdUHH BucoKoro αββαβηηη, wa-aaMoooTdop napa paeoMett cpbam CTyneHia. βμοοκογο αββαβημη 'TyptsuiHw oTcsopa napa coot bbtctbbhhoyMonhuiaeTcp, r, pn stoh koahmbctbo pa «soMeM cpbau. pacuiupouHoW and do / iae huiskoM ούυποηη aiibanhihhb TypduiHB oTdopa napa noBUwaeTcn b pasHoW nape.

AeraaoBaHHufl b Aecopdepe cpeAHero αββαβηηρ psctbop ποοαβ pereHepaTMBHotf οταβμη TenAa bABCOpdBpe MaCTHMHOrO ΠΟΤΟΚΒ 14A14 Β ΤβΠΛΟΟΡΜΒΗΗΙ4Κβ paCTBOpa COBAHHHBTCP C dBAHUM paCTBOPOH 143ABCOpdBpa. B CABAyioujeH BapuaHTB κοποληβημη ι43οβρβτβηιαρ πρβαυομοτρβηο, mto odpaTHoe οχβτνιβ padOMeflCPBAU npOIACXOAlAT Β ΤβρΜΙ4ΜΒΟΚΟΜ ΑΒΥΧΟΤΥΠβΗΜβΤΟΜ ΚΟΜΠΡΘΟΟΟΡβ, Πρΐ4ΜΕΜ HaCUUtBHHU^ pacTBOP OTcTyneHH adcopdUHH eucoKoro αββαβηιαρ ppoxoamt MBpea τβπαοοβμβηηηκ b abcoppop cpeAHeroAaBABHHH, ABCOPdHPOBaHHUM Πβρ padOMBft CpBAU ΚΟΤΟΡΟΓΟ ΠΟΓΑΟΜ3βΤΟΡ B CTynSHH peCOpdBHH dBAHHHpaCTBQpOM (43 ABCOpdepa, PBCOdBHT ΗβΓΗβΤββΤΟΗ HOCPCOM AO dOABB BUCOKOrO ΑΒΒΑβΜΙ4Ρ,npBABapHTBAbHO ΗβΓρβΒββΤΟΡ Β ΤβΠΑΟΟΡΗΒΗΗΙ4Κβ, padOMaP CpBAA OnPTb OCBOdOXAaBTCP Β AOCOpdBPB,neperpesaeTCp (4 pacuiiApswTCP β TypdMHe OTdopa napa, Tsm bpbmbhbm noAyMawuinflCH o Aecop«sepecpeAHero αββαβηηρ «sbahuA pacTBop hocab pereHepaTHBHofl otabmia τβηΑβ προχοαητ b abcoppop(4A(4 b npeABapMTBAbHutt neperpesaTBAb, αβηηοη CAyMae. b ýcTpottcTBO oxAaxABHiAp aap pacuii4peM(4P 14 norAOiHBHHp napa padOMefl cpbau.AeraaoBaHHufl b Aecopdepe cpeAHero αββαβηηρ psctbop ποοαβ pereHepaTMBHotf TenAa bABCOpdBpe MaCTHMHOrO ΠΟΤΟΚΒ 14A14 ΒβΠΛΟΟΡΜΒΗΗΙ4Κβ paCTBOpa COBAHHHBTCP C dBAHUM paCTBOPOH 143ABCOpdBpa. B CABAyioujeH BapuaHTB κοποληβημη ι43οβρβτβηιαρ πρβαυομοτρβηο MTO odpaTHoe οχβτνιβ padOMeflCPBAU npOIACXOAlAT Β ΤβρΜΙ4ΜΒΟΚΟΜ ΑΒΥΧΟΤΥΠβΗΜβΤΟΜ ΚΟΜΠΡΘΟΟΟΡβ, Πρΐ4ΜΕΜ HaCUUtBHHU ^ pacTBOP OTcTyneHH adcopdUHH eucoKoro αββαβηιαρ ppoxoamt MBpea τβπαοοβμβηηηκ b abcoppop cpeAHeroAaBABHHH, ABCOPdHPOBaHHUM Πβρ padOMBft CPBA ΚΟΤΟΡΟΓΟ ΠΟΓΑΟΜ3βΤΟΡ B CTynSHH peCOpdBHH dBAHHHpaCTBQpOM (43 ABCOpdepa, PBCOdBHT ΗβΓΗβΤββΤΟΗ HOCPCOM AO dOABB BUCOKOrO ΑΒΒΑβΜΙ4Ρ, npBABapHTBAbHO ΗβΓρβΒββΤΟΡ Β ΤβΠΑΟΟΡΗΒΗΗΙ4Κβ, padOMaP CPBA OnPTb OCBOdOXAaBTCP Β AOCOpdBPB, neperpesaeTCp (4 pacuiiApswTCP β TypdMHe OTdopa Napa, Tsm bpbmbhbm noAyMawuinflCH of Aecop «sepecpeAHero αββαβηηρ« sbahuA pacTBop hocab pereHepaTHBHofl otabmia τβηΑβ προχοαητ b abcoppop (4A (4 b npeABapMTBAbHutt neperpesaTBAb , αβηηοη CAyMae. b ýcTpottcTBO oxAaxAB HiAp aap pacuii4peM (4P 14 norAOiHBHHp napa padOMefl cpbau)

B xaMecTBe dAaronpi4PTHoro ΒβρΐιβΗΤβ eunoAHeHiAP (43OdpeTeHi4P nocpeACTBOM KOMdMHauiAiA napaAAeAbMoft μ ποοΑβΑΟΒβτβΑόΗοΛ Aecopduwt npBAycMOTpeHO, μτο ηοτοκ nacumeMHoro pacTBopa nocAe erynOHM adCOpdU(4(4, npBAnOMTHTBAbHO nOCAB CTynBHI4 adCOPdUI4(4 BUCOKOrO ΑβΒΑβ(((4Ρ paaABAPBTCP (4 nocAe AaAbHettweM ογαβμμ τβπαα βCTyneHI4 adCOpdUMH ηηβκοπο α.ίοαβηηρ 266 351 4 OA0H MaCTMMHMtt ΠΟΤΟΚ ΠΡΟΧΟΧ0Τ Μβρβ3 ΤβΠΧΟΟΡΜβΚΜ0Κ Β Aecopdep ορβΧΗΟΓΟ ΑαΒΧ6Η0·Α 0AecapdMpoeaHHbiW ταμ nap padoneft cpexu ποαβοαι/itcs, κ cTynenu pecopdunn, β κοτοροΗ αρ.υγοΛMacTMMMuW ποτοκ pacTBOpa na cryneHM adcopdU00 eucoKoro Α3ΒΧβΜ0η πρ0Μβηηβτοη β KanecToeaescoprtonra 0 norxanaer napu padonefl apexu apexnera xecapeepa.B xaMecTBe dAaronpi4PTHoro ΒβρΐιβΗΤβ eunoAHeHiAP (43OdpeTeHi4P nocpeACTBOM KOMdMHauiAiA napaAAeAbMoft μ ποοΑβΑΟΒβτβΑόΗοΛ Aecopduwt npBAycMOTpeHO, μτο ηοτοκ nacumeMHoro pacTBopa nocą erynOHM adCOpdU (4 (4 npBAnOMTHTBAbHO nOCAB CTynBHI4 adCOPdUI4 (4 BUCOKOrO ΑβΒΑβ (((4Ρ paaABAPBTCP (4 nocą AaAbHettweM ογαβμμ τβπαα βCTyneHI4 adCOpdUMH ηηβκοπο α .ίοαβηηρ 266351 4 OA0H MaCTMMHMtt ΠΟΤΟΚ ΠΡΟΧΟΧ0Τ Μβρβ3 ΤβΠΧΟΟΡΜβΚΜ0Κ Β Aecopdep ορβΧΗΟΓΟ ΑαΒΧ6Η0 · Α 0AecapdMpoeaHHbiW ταμ voltage padoneft CPEx ποαβοαι / ITCS, κ cTynenu pecopdunn, β κοτοροΗ αρ.υγοΛMacTMMMuW ποτοκ pacTBOpa to cryneHM adcopdU00 eucoKoro Α3ΒΧβΜ0η πρ0Μβηηβτοη β KanecToeaescoprtonra 0 norxanaer napu padonefl apex apexnera xecapeepa.

PecoptfaT npoxoAMT nenocpeACToenno nocxe οτογο nepea τβηχοοΒΜβΗΜΜΧ pacTeopa β xecopdep βkambctub doraroro pacTBOpa. BsxhmM pacTBoff M9 xecopdepa cpexHero xaexaHvm pacuiupneTcn nocxeperewepaTMBHOřl OTxann Tenxa b xecopdepe nacTMnworo ηοτοκβ κ β τοπλοολμοκηυικβ 0, β cxynaeΠρ0ΜβΜβΗ00 ΛΟΠΟΧΗ0ΤβΧΙ>ΗΟΓΟ yCTPOWcTBa ΟΧΧΘΧΛβΗ0ϊ1 - Β ΟΤΥΠΒΗΙΛ adCOpdU00 Η03ΚΟΓΟ ΑβΒΧ6Η0« ΑΧ·ΧnorxoutctHHn napa padoneft cpexu. BexHuM. ρββτβορ M9 xecopdepa προχοχμτ nocxe ρβτβΗβρβΤΜΒΜοαnTTOMii Tenxa β τβηΑοοόΗβΗΗΜΚ pacTBOpa μ. b AaHHOM cxynae, β ycTpoňcTBe uxxaMewsi cTynenHadCOPdll00 O nP0dX030TOXbHO ΟΧ0ΗβΚΟΒΟ0 KOHUBHTPaUHeft pacTBOpa. (! npoAricriTiiroAbnoM oapnaMTO 0οηοχΗβΗ0β 03θβρβτβη0« npexycMOTpeHO. mto Aau-nenne cmctomu.noWc i oyBinoe o Aracopnrape cpexnero eauxonun μ Β CTyn«H0 adCOPdU00 0x0 cT,ynaiH0 pecopdL'00.CBmattMoPI c Aocop«sepaM cpexHero χβΒχβΜΜη, β ρβΜ0Μβ paaoTw na cxoxbonuieM xaoxennn Axn(iMpnihi0t)tui0«i KOJtwoattMPI TOMnepaiyp oxxaxxaioweM cpexu 0 xx« peryxupoeaHMfl KonuwnTpaunn rtoraioropacTBOpa. nocrynaewero b Aecopdep, peryxupyeTcn. H ripei/iM.yuiecTOCHHOM eapuanTe BunoxHenun 03OdpeTeH00 AXít 9kokom00 oxxaxxaiQUieft cpexu1 ipexycMorpeMO. mto nnpisx bxoxom pacruopa b CTynen0 adcopdU00 pacnaxoxen axMadíiTMMecKHttaacoprfep. a κ euxoxy oryneHM adcopdUMM hmskoto mtMMH-wm ποακαβμβη βχβ axMadaTMMecxMffadcopdep. b kotopom pacTeop, buxox«wiH 03 cTyneHM aacopcsepa η03κογο αββχοημβ, nacuutaeTcnpadoneft cpeMoW 03 cT.yneH0 H03Koro xaBxenun Typd0HU c οτΰοροΜ napa, npuneM nap padoneft cpexu,ι»μχολ»«ι(00 b ιόχοβηυο nacTb axuada-rwiecKoro adcopdepa, ηροχοΛ0τ ποτομ b cTynenb adcopdi»00Μ03ΚΟΓΟ AaBXeH0í1. AXSl 03ΟΰΡβΤβΗ0ϊ, Πρ0ΜβΜβΗ0β Π3ρΜ. padOU0X BeUÍBCTB βΜΜ03Κ—BOA3 CO3XaeT OCOdOe npB0MyUieCTBO.Ποχοτ nafíTw Taxxe πρ0Μβηβη0Β xpyran padonaa cpexa BucoKoro α3βαβη0«, κοτορβί, κμπμι πρμAaBXOH00 OKpyxaKJlUKftt CpOAU dOXOe H03KOM, UOM AXW βΜΜ0βΚβ, , ΗβΠΡ0Μθρ, CO», F 13, F 23 -0X0 BTaH 0COOX0H0H00 C noAXOAÍWBfl X0XKOCTbK) adCOpdU00.PecoptfaT npoxoAMT nenocpe o nep τ τ o o o o o o ac ac ac ac ac ac pacTeopa β xecopdep βkambctub doraroro pacTBOpa. BsxhmM pacTBoff M9 xecopdepa cpexHero xaexaHvm pacuiupneTcn nocxeperewepaTMBHOřl OTxann Tenxa b xecopdepe nacTMnworo ηοτοκβ κ β τοπλοολμοκηυικβ 0, β cxynaeΠρ0ΜβΜβΗ00 ΛΟΠΟΧΗ0ΤβΧΙ> ΗΟΓΟ yCTPOWcTBa ΟΧΧΘΧΛβΗ0ϊ1 - Β ΟΤΥΠΒΗΙΛ adCOpdU00 Η03ΚΟΓΟ ΑβΒΧ6Η0 «ΑΧ · ΧnorxoutctHHn Napa padoneft CPEx. BexHuM. ρββτβορ M9 xecopdepa προχοχμτ nocxe ρβτβΗβρβΤΜΒΜοαnTTOMii Tenxa β τβηΑοοόΗβΗΗΜΚ pacTBOpa μ. b AaHHOM cxynae, β ycT leastcTBe uxxaMewsi cTynenHadCOPdll00 O nP0dX030TOXbHO ΟΧ0ΗβΚΟΒΟ0 KOHUBHTPaUHeft pacTBOpa. (! NpoAricriTiiroAbnoM oapnaMTO 0οηοχΗβΗ0β 03θβρβτβη0 «npexycMOTpeHO. MTO Aau-Nenni cmctomu.noWc and oyBinoe of Aracopnrape cpexnero eauxonun μ Β CTyn« H0 adCOPdU00 0x0 CT ynaiH0 pecopdL'00.CBmattMoPI c Aocop "Sepa cpexHero χβΒχβΜΜη, β ρβΜ0Μβ paaoTw to cxoxbonuieM xaoxennn AXN (iMpnihi0t) tui0 «i KOJtwoattMPI TOMnepaiyp oxxaxxaioweM CPEx 0 xx« peryxupoeaHMfl KonuwnTpaunn rtoraioropacTBOpa. nocrynaewero b Aecopdep, peryxupyeTcn. Ripe H / iM.yuiecTOCHHOM eapuanTe BunoxHenun 03OdpeTeH00 Axit 9kokom00 oxxaxxaiQUieft cpexu1 ipexycMorpeMO. MTO nnpisx bxoxom pacruopa b CTynen0 adcopdU00 pacnaxoxen axMadíiTMMecKHttaacoprfep. and κ euxoxy oryneHM adcopdUMM hmskoto mtMMH-wm ποακαβμβη βχβ axMadaTMMecxMffadcopdep. b kotopom pacTeop, buxox «wih 03 cTyneHM aacopcsepa η03κογο αββχοημβ, nacuutaeTcnpadoneft cpeMoW 03 cT.yneH0 H03Koro xaBxenun Typd0HU c οτΰοροΜ Napa npuneM padoneft CPEx example, ι» μχολ »« ι ( 00 b ι χ β β ac T T T T T u u u u u u axu ada-rwiecKoro adcopdepa, ηροχοΛ0τ ποτομ b cTynenb adcopdi »00Μ03ΚΟΓΟ AaBXeH0í1 AXSl 03ΟΰΡβΤβΗ0ϊ, Πρ0ΜβΜβΗ0β Π3ρΜ. padOU0X BeUÍBCTB βΜΜ03Κ-Boa3 CO3XaeT OCOdOe npB0MyUieCTBO.Ποχοτ nafíTw taxxi πρ0Μβηβη0Β xpyran padonaa CPEx BucoKoro α3βαβη0 «κοτορβί, κμπμι πρμAaBXOH00 OKpyxaKJlUKftt CpOAU H03KOM doxorubicin, UOM AXW βΜΜ0βΚβ,, ΗβΠΡ0Μθρ CO», F 13, F 23 C -0X0 BTaH 0COOX0H0H00 noAXOAÍWBfl X0XKOCTbK) adCOpdU00.

Maoaperenue noxpodnee nowcnmeTC*, M0xecxexyiou(0M np0MepoM BunoxHen0«,. Ha np0xoxennuxMopioxax noKaaawo> na «ne. 1 - np0Hi*0n0aAbHan cxeMa npouecca copdU00 axí, noxynevww, MexanunecKofl<3ΧΟΚΤΡ0ΜβΟΚθϋ) 3ΗΒΡΓ00 03 ΟΤΧΟΑίΒΙΘΓΟ ΤβΠΧβ C ΠβρΒΡΜ ρβΓΌΗβρ3Τ0ΒΜηΜ0cnoAb3OBan0eM «usunecKoro Tenxa dexHoro pacTBOpa b xecopdepe nacT0MHoroηοτοκβ corxacHo 03θΰρβτβΗ0Ρ ítur. 2 - np0HU0n0axbHaR cxeMa npouecca copaunn corxacwo 03οορβτβη0» noxodno «nr.l cnopBMH perenepaTnsHbíM ucnoxbsoeaHueM Tenxa e npexBapuTexbHOM neperpeeaTexe 0pacui0peH0eM npouecca dxaroxape nacTunHoft KOHxeHcau00 0 oxxaxxeHuo. ®0r. 3 - np0HU0n0a/ibHaa cxeMa npouecca copdU00 corAacno 03θβρβτβΗ0» ποχαΰκο «0Γ.1 0x02 c AecopesepoM cpexHero xaBxeH0a, BKX»MeHHUM napaxxexbHO CTyneH0 a«scopdU00EiucoKoro xaexeH0«, xxn BUTecHeH0« paaoHeM cpexu b HanpaexeH00 H03K0XA3BxeH00 οτΰορβ b Typ<50ne c oTtsopoM napa. Φ0Γ. 4 - np0HU0n0axbnap cxeMa npouecca copcsu00 corxacHo 03θΒρβτβΗ0κ> ποχοβηο eur.l 0x02 ax« xonoxHMTexbHoro ucnoxbsoeaHua otxoawwo Tenxa c oněmi ημοκμμTeMnepaTypKUM ypoBneM nocpeACTBOM AByxcTyneHnaToro TepMunecKoro c*aT0«padoneM cpexu. «0Γ. 5 - np0HU0nnaxbMa« cxeMa npouecca copdtwi corxacno 03θΰρβτβΗ0κ> cnocxexoBaTexbHWM 0 napaxxexbHbíM βκχ»ηβΗ0βΜ xecopdepoB b B0Ae cneuHaxbnoříKOMd0Hau00 npoueccos no «0Γ. 3 0 «0Γ. 4. «0Γ. 6 - paopea nacTM aacopeepa xxn npouecca copdU00 corxacHo ηοοβροτομη», b kotopom nepeA 0X0 3a cTyneníwi adcopdepa xonoxH0TexbHO BKxonenu ax0adaT0necK0e adcopdepu. B xecopdep 1 nocTynaeT BBepxy doraruCI pacTBop m nonaxaeT nepes ycTpo«CTBO pacnpexexen0« 5 296-361 x «eia/ib rjdMena bbiubctb e QdorpeeaeMy» MacTb Aecopdepa 2. β xotopoH on ηροτοκββτ bhxb o bxabηββΗχχ no BepTHKa/ibHWM TpyaaM χ npx stoh οτλββτ padOMy» cpeAy, xoTopaw u προτχβατοχβ κneraaoBaHHOMy pacTeopy tbmbt βββρχ. ΠοαοβηηΜ npoueco ηροτνκββτ τβκχβ o Aeoopdepe μβοτχμμογοηοτοκβ 22. ΤβπΛΟΗοΟχτβΛβ aax odorpeea moctx Aecopdepa 2, nocxOAbxy oh οτΑββτ Tfsn.no odorpeeaÓO3 ΧΒΜΒΗβΗΧΆ ·β3Μ, ΠΟΟΤνΠββΤ ΒΗΧ3Ϋ V BXOAB ΑΛί, ΤβΠΑβ ΟβΟΓρβΒβ 7 Β MaCTb ABCOpdepa 2 ηποκχΑββτ ero ΜβρβΒ βμχοα μλχ τβπαβ odorpeea Q. lípu odorpBBB napou ρβ3ΑβΑβΗχβ odorpeisaeMoW MacTX Aecopdepa wbaw«tc»i npeAnoMTxreAbHMM,πρχμβμ β ββρχηθΛ mbotm xcnoAbsyeTcx nap ηβομιιιθηηχ βοαββ Hxaxoro αββαβηχη. a b μηχηοΗ Μβοτχ -dOABB ΒΜΟΟΧΟΓΟ ΑβΒΑΒΗΧΧ. ΒβΑΗΗΜ PBOTBOP, nOAyMaOlUXWCfl Β OTCTOMHXXB ABCOpdepa 1, ΟΤΑββΤ CBOO«XBHMeCKOB ΤβΠΛΟ ΧΛΧ B ABCOpdepB ΜβΟΤΧΜΗΟΓΟ ΠΟΤΟΚβ 22 - MaCTX ΡΟΓβΤΟΓΟ paCTBOpU, ΠΡΟΤβΚβΧ cxxay HaBQpx, <®nr.l> xax B npeABapMTOAbHOM neperpeeaTaAe 10 - napooepaaHOtt ΑβοορβχροΒβΗΗοΜ paeoMeH cpefle (Φι/ιγ.2). JlasibHefluian οτββΜβ τβΠΑβ ββαηογο pacTBOpa «soraTOny pacTBopy προχοχοΑχτΒ ΤΒΠΛΟΟΒΜβΗΗΧΚβ 9. ΒβΑΗΜΛ paCTBOP ΠΟΠβΑββΤ ΗβΠΟΟΡβΑΟΤΒΘΗΗΟ 3β 3ΤΜΜ ΜβρβΒ yCTpOptCTBO ΑΛΗ ρβΟΒΧΡΘΗΧΧ 13,ycTpoflcTBO αχΑβχΑβΗΧΧ 14 κ CTyneHX adcopdepa ηχοκογο ΛββΑβκχη. Β yoTpoHcTBe οχΛβχΑβΗχχ 14προχοχοαχτ οτΑβΜβ τβΠΑβ οχΛβ*Αβιοι«βί1 ορβΑβ. napoodpaaHan padOMan ορβΑβ. BWXOA«uan y γολοβηοΛ Μβοτχ Aecopdepa 1, MarpooaeTcn AaAbiue. Β ΛβΗΗΟΜ C/iyMae, Β ΠΡβΑΒβΡΗΤβΛβΗΟΜ ΠβρβΓρβΒβΤβΛΘ 1(1 HO B AOdOM CAyMaC - B nOCTOPOHWBOdOrpeaaeMOM ΠβρβΓρΟΒβΤβΛβ 3, ΟΗββΜβΗΗΟΜ BXOAOM ΤβΠΛΟΗΟΟΧΤΒΛΗ 11 M BWXOAOM ΤΒΠΛΟΗΟΟΜΤβΛΗ 12.χ ποηοΑββτ ποτομ β ΜΜΟΓΟοτί/πβΗΜβτύηο TypdMHy οτβορβ napo 4, β χοτοροΜ napoodpasíHan paeoMawορβΑβ cTyneHMaTO pacwxpweTcx. Οτ oTABAbHux CTynenefl Typdxnw οτβορβ napa paeoMan cpeAa nonaAaeT x οοοτββτοτβυιοχημCTyneHPH aecopdepa 6.6', 6", 6"’ x BcacwBaeTcx tbm eeAHWM pacTBOPOH xax cryneMMOTO ceortimeniiMMpaCTBOpOH Β XaMBCTBB MXAKOfl adCOpdUXOHHOW ΟρβΑΜ <ΒβΟΟρββΗΤβ), ΟΤΑΒΒΒΗ adCOpdUXOHHOe ΤβΠΛΟoxAaMAaumett ορβΑβ. B cooTBeTCTByBUieft CTyneHX aecopdepa 6,6', 6", 6"' λβαημΛ ρβοτβορnarpyxaeTca xax y*e ηρβΑΒβρχτβΛβΗο odorameHHbíM ρβοτβορ πομτχ ao coctoxhxx MacMtueHxn aaw βτοΛΟΤΥΠβΗΧ C padOHOtf CPBAOtt, ΠΡΧΜΒΜ' ΚΟΑΧΜβΟΤΒΟ ββΟΟρββΗΤβ (ΰβΑΗΜΛ ρβοτβορ XAM ΟβΟΓΘΙ«ΒΗΗΜ{<ρβοτβορ) οηρβΑβΑηβτ κοαχμθοτβο pacuixpaoutettcx padOMeft ορβΑΜ cooTBeTCTBy»wefl cTynenx rypdxnu cuTdupoM napa x, ΟΑΗβκο. koaxmbctbo pacuixpxBiueMcx ρμομβΜ opoau oo raerovi HoporyAxpyexiiiM.PaCTBOP, ΜΘΟΜΙΙΙβΗΗΜΗ B CTynBHX SdCOpdepa ΗΧ3ΚΟΓΟ ΑβΒΛβΗΧΗ 6, ΗβΓΗβΤββΤΟΧ HacOCOM 6 AO dOABBBMcoxoro ΑβΒΑβκχη x. dAarOAapx BTO^y. b CABAyomeM CTynenx adcopdepa 6’ npx dOAee bmcoxomΑβΒΛΒΗΧΧ OnPTb ΜΟΜβΤ ΠΟΓΛΟίμβΤβ padOMyio CPBAy. npx STOH ΜβΟΤΟΜ OTdOpa_TyPdXHW O OTdOpOM napa,npBAnaaHaMeHHUM αλη btoB cTyneHX aecopdepa, sadxpaeTcn τβκ μηογο ραβΟΜβΧ ορβΑΜ, μτο ρβοτβορanpTb πομτχ ΛΟΟτχΓββτ οοοτοχΗχβ HaCMlueHxx (xoHueHTpauxn paBHOBecxsú. 3txm οηρβΑβΑχβτοη οτβορpadoneM cpbam X3 TypdXHM c OTdOpOM napa 4 b saoxcxHOCTX οτ boshomhoctx HarpyxeHxia pacTtsopa ticooTBBTcTByiomett CTyneHX adcopdepa. ()Tdop hb peryaxpy»T, oh peryAxpyeTcx ooh. Ot crynrsHx xCTyneHX HarHBTaeTcn odorauieHHMfl ρβοτβορ HacocoM 6.6*. 6", 6"' ao' cooTBBTCTByomero do/iee BMcoxoro AaejieHxn x ποαβοαχτοβ Ha KOHue Aecopdepa 1 β κβΜβοτΒβ doraToro pacTBOpa. npx otomCTyneHMaTO odorauiaeTcx pbctbop paeoMetf cpeAoft Tax CxAbHo, μτο oh ΑοβχβΗ xMGTb oMeHb Hxexy»TennepaTypy HaMajia ABcopeuxx aab doraToro pacTBOpa npx bxoab b Aecopdep li nocTynanutxft xexoAy τβΠΑβ odorpeea 7 s MacTb Aecopdepa 2 τβηΑΟΗΟοχτβΑβ aa« xcnoAbSOBaHxn οτχοαημβγο τβπαβΟΧΑβΑΑββΤΟΧ OMeHb CAydOKO X ΒΟ3ΜΟΜβΗ TOAbXO ΟΓρβΗΧΜβΗΗΜΛ npBAnapXTBAbHMX OdOrpBB ΡΟΓβΤΟΓΟpacTBOpa aah pereHepaTXBHoro ποΓΑΟίκβΗχβ τβπΛβ β τβΠΑοοβΜθΗΗΧκβ 9, τβχ μτο β οοοβμχ cAVMaíixΜΟΜΗΟ OTXaaaTbCH ΟΤ ΤβΠΛΟΟβΜβΗΜΧΚβ 9,Maoaperenue noxpodnee nowcnmeTC * M0xecxexyiou (0M np0MepoM BunoxHen0 «Ha ,. np0xoxennuxMopioxax noKaaawo> for" Sun 1 - np0Hi * 0n0aAbHan cxeMa npouecca copdU00 Axi, noxynevww, MexanunecKofl <3ΧΟΚΤΡ0ΜβΟΚθϋ) 3ΗΒΡΓ00 03 ΟΤΧΟΑίΒΙΘΓΟ ΤβΠΧβ C ΠβρΒΡΜ ρβΓΌΗβρ3Τ0ΒΜηΜ0cnoAb3OBan0eM «usunecKoro Tenxa dexHoro pacTBOpa b xecopdepe nacT0MHoroηοτοκβ corxacHo 03θΰρβτβΗ0Ρ ítur. 2 - np0HU0n0axbHaR cxeMa npouecca copaunn corxacwo 03οορβτβη0 »noxodno« nr.l cnopBMH perenepaTnsHbiM ucnoxbsoeaHueM Tenxa e npexBapuTexbHOM 0pacui0peH0eM npouecca dxaroxape nacTunHoft KOHxeHcau00 0 oxxaxxeHuo. ®0r. 3 - np0HU0n0a / ibha cxeMa npouecca copdU00 corAacno 03θβρβτβΗ0 »ποχαΰκο« 0Γ.1 0x02 c AecopesepoM cpexHero xaBxeH0a, BKX »MeHHUM napaxxexbHO CTyneH0 and« scopdU00EiucoKoro xaexeH0 «xxn BUTecHeH0« paaoHeM CPEx b HanpaexeH00 H03K0XA3BxeH00 οτΰορβ type b <c 50ne oTtsopoM Napa. Φ0Γ. 4 - np0HU0n0axbnap cxeMa npouecca copcsu00 corxacHo 03θΒρβτβΗ0κ> ποχοβηο eur.l 0x02 ax x xonoxHMTexbHoro ucnoxbsoeaHua otxoawwo Tenxa c oněmi ημοκμμTeMnepaTypKUM ypoBneM nocpeACTBOM AByxcTyneHnaToro TepMunecKoro c * aT0 «padoneM cpexu. «0Γ. 5 - np0HU0nnaxbMa «cxeMa npouecca copdtwi corxacno 03θΰρβτβΗ0κ> cnocxexoBaTexbHWM 0 napaxxexbHbíM βκχ» ηβΗ0βΜ xecopdepoB b B0Ae cneuHaxbnoKOMd0Hau00 npoueccos no «0Γ. 3 0 «0Γ. 4. «0Γ. 6 - paopea nacTM aacopeepa xxn npouecca copdU00 corxacHo ηοοβροτομη », b kotopom nepeA 0X0 3a cTyneniwi adcopdepa xonoxH0TexbHO BKxonen ax0adaT0necK0e adcopdepu. B 1 xecopdep nocTynaeT BBepxy doraruCI pacTBop m nonaxaeT nepes ycTpo «CTBO pacnpexexen0« 5 x 296 to 361 "EIA / IB rjdMena bbiubctb e QdorpeeaeMy» MacTb Aecopdepa second β xotopoH he ηροτοκββτ bhxb of bxabηββΗχχ no BepTHKa / ibHWM TpyaaM χ npx stack οτλββτ padOMy »CpeAy, xoTopaw u προτχβατοχβ κneraaoBaHHOMy pacTeopy tbmbt βββρχ. ΠοαοβηηΜ npoueco ηροτνκββτ τβκχβ of Aeoopdepe μβοτχμμογοηοτοκβ 22nd ΤβπΛΟΗοΟχτβΛβ AAX odorpeea moctx Aecopdepa 2 nocxOAbxy oh οτΑββτ Tfsn.no odorpeeaÓO3 ΧΒΜΒΗβΗΧΆ · β3Μ, ΠΟΟΤνΠββΤ ΒΗΧ3Ϋ In BXOAB ΑΛί, ΤβΠΑβ ΟβΟΓρβΒβ 7 Β MaCTb ABCOpdepa 2 ηποκχΑββτ Night ΜβρβΒ βμχοα μλχ τβπαβ odorpeea Q. lime orp orp orp orp Α orp orp orp orp orp orp orp orp orp orp orp ba orp orp orp orp orp orp orp T T T T T T T T T T T x x x x x x x. and b μηχηοΗ Μβοτχ -dOABB ΒΜΟΟΧΟΓΟ ΑβΒΑΒΗΧΧ. ΒβΑΗΗΜ PBOTBOP, nOAyMaOlUXWCfl Β OTCTOMHXXB ABCOpdepa 1 ΟΤΑββΤ CBOO «XBHMeCKOB ΤβΠΛΟ ΧΛΧ B ABCOpdepB ΜβΟΤΧΜΗΟΓΟ ΠΟΤΟΚβ 22 - MaCTX ΡΟΓβΤΟΓΟ paCTBOpU, ΠΡΟΤβΚβΧ cxxay HaBQpx <®nr.l> XAX B npeABapMTOAbHOM neperpeeaTaAe 10 - napooepaaHOtt ΑβοορβχροΒβΗΗοΜ paeoMeH cpefle (Φι / ιγ. 2). JlasibHefluian οτββΜβ τβΠΑβ ββαηογο pacTBOpa «soraTOny pacTBopy προχοχοΑχτΒ ΤΒΠΛΟΟΒΜβΗΗΧΚβ ninth ΒβΑΗΜΛ paCTBOP ΠΟΠβΑββΤ ΗβΠΟΟΡβΑΟΤΒΘΗΗΟ 3β 3ΤΜΜ ΜβρβΒ yCTpOptCTBO ΑΛΗ ρβΟΒΧΡΘΗΧΧ 13 ycTpoflcTBO αχΑβχΑβΗΧΧ 14 κ CTyneHX adcopdepa ηχοκογο ΛββΑβκχη. O yoTpoHcTBe οχΛβχΑβΗχχ 14προχοχοαχτ οτΑβΜβ τβΠΑβ οχΛβ * Αβιοι «βί1 ορβΑβ. napoodpaaHan padOMan ορβΑβ. BWXOA 'uan y γολοβηοΛ Μβοτχ Aecopdepa 1, MarpooaeTcn AaAbiue. Β ΛβΗΗΟΜ C / iyMae, Β ΠΡβΑΒβΡΗΤβΛβΗΟΜ ΠβρβΓρβΒβΤβΛΘ 1 (1 HO AOdOM CAyMaC B - B nOCTOPOHWBOdOrpeaaeMOM ΠβρβΓρΟΒβΤβΛβ 3 ΟΗββΜβΗΗΟΜ BXOAOM ΤβΠΛΟΗΟΟΧΤΒΛΗ 11 M BWXOAOM ΤΒΠΛΟΗΟΟΜΤβΛΗ 12.χ ποηοΑββτ ποτομ β ΜΜΟΓΟοτί / πβΗΜβτύηο TypdMHy οτβορβ Napo 4 β χοτοροΜ napoodpasíHan paeoMawορβΑβ cTyneHMaTO pacwxpweTcx. Οτ oTABAbHux CTynenefl Typdxnw οτβορβ Napa paeoMan CPEA nonaAaeT οοοτββτοτβυιοχημCTyneHPH aecopdepa x 6.6 ', 6 ", 6"' x BcacwBaeTcx TBM eeAHWM pacTBOPOH XAX cryneMMOTO ceortimeniiMMpaCTBOpOH Β XaMBCTBB MXAKOfl adCOpdUXOHHOW ΟρβΑΜ <ΒβΟΟρββΗΤβ) ΟΤΑΒΒΒΗ adCOpdUXOHHOe ΤβΠΛΟoxAaMAaumett ορβΑβ. B cooTBeTCTByBUieft CTyneHX aecopdepa 6,6 ', 6 ", 6"' λβαημΛ ρβοτβορnarpyxaeTca XAX e * y ηρβΑΒβρχτβΛβΗο odorameHHbíM ρβοτβορ πομτχ and coctoxhxx MacMtueHxn AAW βτοΛΟΤΥΠβΗΧ C padOHOtf CPBAOtt, ΠΡΧΜΒΜ 'ΚΟΑΧΜβΟΤΒΟ ββΟΟρββΗΤβ (ΰβΑΗΜΛ ρβοτβορ XAM ΟβΟΓΘΙ «ΒΗΗΜ {<ρβοτβορ) οηρβΑβΑηβτ κοαχμθοτβο pacuixpaoutettcx padOMeft ορβΑΜ cooTBeTCTBy »wefl cTynenx rypdxnu cuTdupoM napa x, ΟΑΗβκο. koaxmbctbo pacuixpxBiueMcx ρμομβΜ opoau oo raer HopxAxpyexiiiM.PaCTBOP, ΜΘΟΜΙΙΙβΗΗΜΗB CTynBHX SdCOpdepa ΗΧ3ΚΟΓΟ ΑβΒΛβΗΧΗ 6, ΓΗβΓΗβΤββΤΟΧ HacOCOM 6 AO dOABBBMcoxoro ΑβΒΑβκχη x. dAarOAapx BTO ^ y. b CABAyomeM CTynenx adcopdepa 6 ’npx dOAee bmcoxomΑβΒΛΒΗΧΧ OnPTb ΜΟΜβΤ ΠΟΓΛΟίμβΤβ padOMyio CPBAy. npx STOH ΜβΟΤΟΜ OTdOpa_TyPdXHW O OTdOpOM Napa npBAnaaHaMeHHUM αλη Engine cTyneHX aecopdepa, sadxpaeTcn τβκ μηογο ραβΟΜβΧ ορβΑΜ, μτο ρβοτβορanpTb πομτχ ΛΟΟτχΓββτ οοοτοχΗχβ HaCMlueHxx (xoHueHTpauxn paBHOBecxsú. 3txm οηρβΑβΑχβτοη οτβορpadoneM CPBA X3 TypdXHM c OTdOpOM Napa 4 b saoxcxHOCTX οτ boshomhoctx HarpyxeHxia pacTtsopa ticooTBBTcTByiomett CTyneHX adcopdepa. () TDOPO HB peryaxpy »T oh peryAxpyeTcx ooh. Ot crynrsHx xCTyneHX HarHBTaeTcn odorauieHHMfl ρβοτβορ HacocoM 6.6. * 6", 6 " ', and' cooTBBTCTByomero to / IEE BMcoxoro AaejieHxn x ποαβοαχτοβ Ha KOHue Aecopdepa 1 β κβΜβοτΒβ doraToro pacTBOpa. npx otomCTyneHMaTO odorauiaeTcx pbctbop paeoMetf cpeAoft Tax CxAbHo, μτο oh ΑοβχβΗ xMGTb oMeHb Hxexy »Tennepa HaMajia types ABcopeuxx aab doraToro pacTBOpa npx bxoab b Aecopdep li nocTynanutxft xexoAy τβΠΑβ odorpeea 7 with MacTb Aecopdepa 2 τβηΑΟΗΟοχτβΑβ aa« xcnoAbSOBaHxn ο τχοαημβγο τβπαβΟΧΑβΑΑββΤΟΧ OMeHb CAydOKO X ΒΟ3ΜΟΜβΗ TOAbXO ΟΓρβΗΧΜβΗΗΜΛ npBAnapXTBAbHMX OdOrpBB ΡΟΓβΤΟΓΟpacTBOpa aah pereHepaTXBHoro ποΓΑΟίκβΗχβ τβπΛβ β τβΠΑοοβΜθΗΗΧκβ 9 τβχ μτο β οοοβμχ cAVMaíixΜΟΜΗΟ OTXaaaTbCH ΟΤ ΤβΠΛΟΟβΜβΗΜΧΚβ 9

Μχοτοτβ napoodpasHoro padonerocpoACTBa Taxaw BMCOxax. μτο nap ρββοΜβϋ cpbam momot dMTbOAHOBpBMBHHO XCnOAb3OBaTbC$) AAÍ1 Πρ'θΧ3ΒΟΑΟΤΒβ ΧΟΑΟΑβ <ΦΧΓ.2>. ΠΡΧ BTOM CXXXaCTCM MaCTHMHWflηοτοκ napa padOMett cpeAM Μβρβ3 apnaTypy 21 b BO3AyuiHOM ΠΒρβοχΑβχΑαβτοχ b xoAOAXAbHXKe 16 x HaxanAXBaeTcw b cocyAe 17. ycTpoMcTBe paciuxpenxn IQ ao ΑβΒΑβκχχ χοπαρχτβΛπ 19 x btxm οτβχρββτοη τοπαο xa xsiawareHTa 20.Μχοτοτβ napoodpasHoro padonerocpoACTBa Taxaw BMCOxax. μτο nap ρββοΜβϋ cpbam momot dMTbOAHOBpBMBHHO XCnOAb3OBaTbC $) AAI1 Πρ'θΧ3ΒΟΑΟΤΒβ ΧΟΑΟΑβ <ΦΧΓ.2>. ΠΡΧ BTOM CXXXaCTCM MaCTHMHWflηοτοκ Napa padOMett CPEA Μβρβ3 apnaTypy 21b BO3AyuiHOM ΠΒρβοχΑβχΑαβτοχ b xoAOAXAbHXKe 16 x HaxanAXBaeTcw b cocyAe 17th ycTpoMcTBe paciuxpenxn IQ and ΑβΒΑβκχχ χοπαρχτβΛπ x 19 x btxm οτβχρββτοη τοπαο xsiawareHTa 20th

(lap padOMeM ορβΑΜ npOXOAXT OT XCnapXTBAX 19 AAX ηΟΓΑΟΙΙΙβΗΧη ΤβΠΑβ ΜΒΡΒΒ XOAOAXAbHXK 19 X dAxxaMuieH no αοβαβηχο οτυπβηχ adcopoepa (ηχ3Κογο ΑβΒΑβΗχχ) Β χ cAyxxT ταη β cobaxhbhxx c(lap padOMeM ορβΑΜ npOXOAXT OT XCnapXTBAX 19 AAX ηΟΓΑΟΙΙΙβΗΧη ΤβΠΑβ ΜΒΡΒΒ XOAOAXAbHXK 19 X dAxxaMuieH no αοβαβηχο οτυπβηχ adcopoepa

οτβοροΜ napa paeaMett ορβΑΜ Χ3 ηοοΛβΑΗβΜ CTyneHX TypdXHM ο οτβορομ napa 4 aasi odorauieHXH deAHoro pacTBOpa onxcaHHMH cnocodon.'οτβοροΜ napa paeaMett ορβΑΜ Χ3 ηοοΛβΑΗβΜ CTyneHX TypdXHM ο οτβορομ napa 4 aasi odorauieHXH deAHoro pacTBOpa onxcaHHMH cnocodon. '

PacuixpBHxe οοηοβηογο ycTpoMcTBa corAacHO xaodpeTeMX» ΑοοτχΓββτοη daaroAapn napaAAeabHOMyPacuixpBHxe οοηοβηογο ycTpoMcTBa corAacHO xaodpeTeMX »ΑοοτχΓββτοη daaroAapn napaAAeabHOMy

ΧΟΗΑβΗΟβΤΟΡΒ, XOHAOHcaTΚΟΗΑβΗΟβΤ paClUXpnBTCÍl B 266 351 6 ΒΚΛβΜβΗΡΙ» AUCOPrtCpa ΟρβΑΗΒΓυ ΛβΒΛβΗΜί, 1' B CfMiy ΜΒΓΟ paCWMpeHMB paáOMBft CPBXM O T.ypeSMHC cot<mpoh napa 4 CMetqaeTcn b ctopohv hmskmx μομμμΜ OTeopa. «μμμτ k cuxnee bucukmmTCnnepaTypHMM nepenaAaM. lípu stoh ποτοκ Hacumennoro pacTBopa pa3«i:jp,ieTc$i nepeA nocxeAHefó(bucokoto Aanjienníi> cTynenb» aacopaepa 5"'. MacTMMHuíí ποτοκ pacToopa προχοβητ HenocpeacieeHHOui cTyrioub aacoptiepa ducokoto Ano/iennsi 5"'. flpyrod MacTMMHuW ποτοκ orforamennoro pacTBopa nocjienorAomem/iíi rerixa β τβηκχΜΜβΗΜΜΚβ 9' ηροχοχΗΤ β Aecopaep cpemero xaexera«i 1‘. bkapmoiihhňnapaMexbHO c xecopdepOH 1. o kotopom AecopenpyeTca HaeecTMM cnococsoM paaonaB cpexa. 1'lapuparfOMctf cpexa, noxyMnownecn b roxoBHoň msctm xecopdepa cpeBHero nao-nenníi 1'. npoxoxsrr bcrynenb aacopesepa bucokoto AaBAennm 5"'. BjiaroAapm 3TOMy moxbt esuTb b pasnioň mcpo yMBHbuieHοτλορ napa paaoHeň cpexu na TypesnHbt c ot<sopom napa 4 xxa stoh CTyneHM xaexeHMP, a pacuinpennepaíoneB cpexu b Typňwie c ot<sopom napa 4 y/iyMuiaeTcsi exaroAapsi oraný b noxbay doxee HH3KHxAaBxennří oirfopa. ΒβαηριΛ psctbop H3 Aecopaepa cpeAHero AaBxennsi 1 ηροχοΛητ nocxe οτμμμ oτοπχοοόΜβΗΗΜΚβ pacToopa 9' Tenxa aoraTOMy pacTsopy. npoxoxsxueMy Mepe3 xecoptsep cpexuoroxaBxeHMP 1’. Mepea ycTpoňcTBO paeuinpeHnsi 13' cobmbctho c eexnuM pacTBopon na xecoppepa J(4>nr .3) . Μοφηαηκθιιηη ycTpoPtcTBa corxacHO Μ3θ<5ρβτβΗΐχο peaxn3yioTCia «sxaroAapsi πρμμοιμιηο pacsoTaoiueroΠΟΧ CpeXHMM XaBXOHMeM ΒΤΟΡΟΓΟ xecopdepa 1'. ΑΟΠΟΧΗηΤβΧΡΗΟΓΟ ΤΒΠΛΟΟΟΗβΗΗΜΚΒ pacTBopa 9' Hrt/iarcuiapp ΑΟΠΟΛΗητβχΡΗΟΛ ycranoBKe cxexyninero a<scoptsepa b enxe CTynenn pecopóunn 26.ClΑβΗΟβΤΟΡΒ B 266 351 6 UCβΜβΗΡΙ »AUCOPrtCpa ΟρβΑΗΒΓυ ΛβΒΛβΗΜί, 1 'B CfMiy ΜΒΓΟ paCWMpeHMB paMOMBft CPBXM About T.ypeSMHC cot <mpoh napa 4 CMetqaeTcn b ctopohv hmskmx μομμμΜ OTeopa. «Μμμτ to cuxnee bucukmmTCnnepaTypHMM nepenaAaM. lime stack ποτοκ Hacumennoro pacTBopa PA3 «i: jp, ieTc $ i do not wish nocxeAHefó (bucokoto Aanjienníi> cTynenb» aacopaepa 5 ''. MacTMMHuíí ποτοκ pacToopa προχοβητ HenocpeacieeHHOui cTyrioub aacoptiepa ducokoto Yes / iennsi 5 ''. flpyrod MacTMMHuW ποτοκ orforamennoro pacTBopa nocjienorAomem / Class III rerixa β τβηκχΜΜβΗΜΜΚβ 9 'ηροχοχΗΤ β Aecopaep cpemero xaexera «i 1'. bkapmoiihhňnapaMexbHO c xecopdepOH the first kotopom AecopenpyeTca HaeecTMM cnococsoM paaonaB CPEx. 1'lapuparfOMctf CPEx, noxyMnownecn b roxoBHoň MSCT xecopdepa cpeBHero versa nenníi 1 '. npoxoxsrr bcrynenb aacopesepa bucokoto AaBAennm 5 " '. BjiaroAapm 3TOMy moxbt esuTb b pasnioň mcpo yMBHbuieHοτλορ napa paaoHeň CPEx to TypesnHbt c ot <SOPO Napa 4 XXa stack CTyneHM xaexeHMP and pacuinpennepaíoneB CPEx b Typňwie c ot <SOPO Napa 4 y / iyMuiaeTcsi exaroAapsi trihalides b noxbay Doxey HH3KHxAaBxennří oirfopa. CtβαηριΛ psctbop H3 Aecopaepa cpeAHero AaBxennsi 1 ηροχοΛητ nocxe ο μμμ oτοπχοοόΜβΗΗΜΚβ pacToopa 9 'Tenxa aoraTOMy pacTsopy. npoxoxsxueMy Mepe3 xecoptsep cpexuoroxaBxeHMP 1'. Mepea ycT leastcBO paeuinpeHnsi 13 'cobmbctho c eexnuM pacTBopon on xecoppepa J (4> nr .3). Cοφηαηκθιιηη ycTpoPtcTBa corxacHO θ3θ <5ρβτβΗΐχο peaxn3yioTCia «sxaroAapsi πρμμοιμιηο pacsoTaoiueroΠΟΧ CpeXHMM XaBXOHMeM ΒΤΟΡΟΓΟ xecopdepa 1 '. ΑΟΠΟΧΗηΤβΧΡΗΟΓΟ ΤΒΠΛΟΟΟΗβΗΗΜΚΒ pacTBopa 9 'Hrt / iarcuiapp ΑΟΠΟΛΗητβχΡΗΟΛ ycranoBKe cxexyninero a <scoptsepa b enxe CTynenn pecopóunn 26.

Bxaroxapsi Taxoň Moxn«MKaui« ycTpoňCTBa moxho nxn nooucMTb buxox Mexann^iecKOři aiepruu mxmnpncrioeoeíMTb npouecc κ μηογμη ncnoxb3yeMWM TenxoHocnTexpM. sacTi/iMHO c csoxee hh3khm ,υροβηβμTGMnepaTypM, meh .TpeeyeTcn npn ochobhom npouecce. K-nn ncnoxb30BaHnsi OTxoAsxuero Tenxa c ομβηι»ΗΙΛ3ΚΜΜ ypooHOM TeMnepaTypH μχμ axíi noxyHeHnn OMeHb bucokmx xaoxeHMň paooneif cpexunpe»yCMOTpeno XByxeTynemaToe TepMnnecKoe cxaTne. ikífi cTyneHM οκατηη cxeAypuine 1 riepctan Aecopaunn npn cpexHeH xaBjíeHwa m pecopaunsi paaoMeři cpexu npn cpeanen xatuiaimi nxaxce BTopan Aecoprfunn npn bucokom xaBxeHww. npn stoh aoraTbtrt pacTBop. κοτορηΗ βηχοχμτ H3CTyneHM aacopaepa bucokoto xaBxeHim 5' n xaoxeHMe κοτορογο noetuueno Hacocon 6" προχοχμτ Mepe3τβπχοοόΜβΗΐΐΜΧ 9 b xecopcsep 1’ cpeAHero xaBxeHníi. PaesoMap cpexa. AecopanpoBaHHaH b xecop<sepecpexwero AaBxennsi 1'. πραχοχητ b CTynenb pecopaunn 26. Β KanecTBe aacopaeHTa b cTynenbpecopaunn 26 προχοχμτ «sexHbiň pacTBop, ouxoAPinnň M3 OTcToňnnKa xecopesepa 4, oxxaxAeHHBiži aτβΜηχοοΡΜβιίΗΜΚβ, pacTBopa 9' n paciunpeHHuň b ycTpoňcTee pacuinpeHna 13'. Kpone toto ohoóoramaBTcn napoM pa<sovieň cpexu na xecoptsepa cpeAHero AaBxenníi 1’ . nocxe noeuuieHníi Aanxennsihbcocúm 24 n nocxe norxomeHnfl Tenxa b TenxoocsMeHHHKe pacTBopa 9’ odorauieHnuň pacTBop προχοχμτb aecopesep .1’ . Bexnuří pacTBop n3 xecopaepa cpexnero xaexenníi 1' ιιροχοχητ n3oecTnuM oapa3OMnepea npeABapnTexbHuří neperpeeaTexb 10. τβηχοοβΜβΗΗηκ 9. ycTpoňcTBO pacuinpennp 13 nycTpoňcTBO oxxaxAenns? 14 CTyneHn aacopeepa hhskoto xaBxeHMSi 5<$nr.4>. B paciunpenHOM ochobhom ycTpořicTBe xecopesep 1 paaoTaeT κβκ xecoptsep βηοοκογο χ,ιηχοιιμλ.Bxaroxapsi Taxon Moxn «MKaui« ytTBBa moxho nxn nooucMTb buxox Mexann ^ iecKOr aiepru mxmnpncrioeoeiMTb npouecc κ μηογμη ncnoxb3yeMWM TenxoHocnTexpM. sacTi / iMHO c csoxee hh3khm, υροβηβμTGMnepaTypM, meh .TpeeyeTcn npn ochobhom npouecce. K-nn ncnoxb30BaHnsi OTxoAsxuero Tenxa c ομβηι »ΚΜΜ3ΚΜΜ ypooHOM TeMnepaTypH μχμ axi noxyHeHnn OMeHb bucokmx xaoxeHMo paooneif cpexunpe» yCMOTpeno XByxeTynemaToe TepMnnecKoe cxaTne. ikífi cTyneHM cxeAypuine 1 riepctan Aecopaunn npn cpexHeH xaBjíeHwa m pecopaunsi paaoMers cpexu npn cpeanen xatuiaimi nxaxce BTopan Aecoprfunn npn bucokom xaBxeHww. npn stack aoraTbtrt pacTBop. κοτορηΗ βηχοχμτ H3CTyneHM aacopaepa bucokoto xaBxeHim 5 'n xaoxeHMe κοτορογο noetuueno Hacocon 6 "προχοχμτ Mepe3τβπχοοόΜβΗΐΐΜΧ xecopcsep 9 b 1' cpeAHero xaBxeHníi. PaesoMap CPEx. AecopanpoBaHHaH b xecop <sepecpexwero AaBxennsi 1 '. πραχοχητ b CTynenb pecopaunn 26th Β KanecTBe aacopaeHTa b cTynenbpecopaunn 26 προχοχμτ «sexHbiň pacTBop, ouxoAPinnň M3 OTcToňnnKa xecopesepa 4 oxxaxAeHHBiži aτβΜηχοοΡΜβιίΗΜΚβ, pacTBopa 9 'n paciunpeHHuň b ycTpoňcTee pacuinpeHna 13'. Kpone this ohoóoramaBTcn beverages pa <sovieň CPEx to xecoptsepa cpeAHero AaBxenníi 1 '. nocxe noeuuieHníi Aanxennsihbcocúm 24 n nocxe norxomeHnfl Tenxa b TenxoocsMeHHHKe pacTBopa 9 'odorauieHnuň pacTBop n3 xecopaepa cpexnero xaexennii 1' ιιροχοχητ n3oecTnuM oapa3OMnepea npeABapnTexb hiero neperpeeaTexb 10. oxxaxAenns? 14 CTyneHn aacopeepa hhskoto xaBxeHMSi 5 <$ nr.4> .B paciunpenHOM ochobhom ycTpořicTBe xecopesep 1 paaoTaeT κβκ xecoptsep βηοοκογο χ, ιηχοιιμλ.

Cxe«yni«a'/T ΜοχηΦηκηιιη'Χ noxy-taeTCí) csxaroAapf, Tony. mto tsoraTHíí pacTBop, HMewmnň noBwuieHHoexaexeHMe d/iaroxapíi nacocy 6" n BUXOAviinnň npn HaneuciueM xaBxennn acscopaepa e CTyrieHb adcopdepa5". paaxexmeTCíi Ha xea nacTnMHux ηοτοκβ. Oauh MacTnHHwň ποτοκ προχοχητ nocxe noBuuiennnTBMnepaTypu β τβπχοοώΜβΗΗηκβ 9 b xecopeep cpeAHero xaBxeHna 1’. TtecopůnpoBaHHuřt tsm nappatíOMePí cpeAW onsn b ncacuBaeTCfl ( pecop<snpyeTcsú b CTyneHn pecoptsunn 26 nocpeACTBOM xpyroroH3CTMHHOTO ΠΟΤΟΚβ ΰΟΓβΤΟΓΟ paCTBOpa. Ba3HHKai0lHHH ΤβΚΗΜ O«Spa3OM eoraTblň paCTBOp <pecop«saT>nocxe noDMUiennm xaBxenns) nocpeACTBOM Hacoca 24 n noBuiueHns, TeMnepaTypu β τβηχοοΰΜΒΗΗηκοpacTBopa 9' BuxaeTcsi na Aecop«sep 1.Cxe «yni« a '/ T ΜοχηΦηκηιιη'Χ noxy-taeTCí) csxaroAapf, Tony. mto tsoraTHíí pacTBop, HMewmnň noBwuieHHoexaexeHMe d / iaroxapi nacocy 6 "n BUXOAviinnnpn HaneuciueM xaBxennn acscopaepa e CTyrieHb adcopdepa5". paaxexmeTCíi Ha xea nacTnMHux ηοτοκβ. Oauh MacTnHHwn ποτοκ προχοχητ nocxe noBuuiennnTBMnepaTypu β τβπχοοώΜβΗΗηκβ 9 b xecopeep cpeAHero xaBxeHna 1 ’. TtecopůnpoBaHHuřt TSM nappatíOMePí cpeAW onsn b ncacuBaeTCfl (pecop <snpyeTcsú b CTyneHn pecoptsunn 26 nocpeACTBOM xpyroroH3CTMHHOTO ΠΟΤΟΚβ ΰΟΓβΤΟΓΟ paCTBOpa. Ba3HHKai0lHHH ΤβΚΗΜ O «Spa3OM eoraTblň paCTBOp <pecop" SAT> nocxe noDMUiennm xaBxenns) nocpeACTBOM Hacoca 24 n noBuiueHns, TeMnepaTypu β τβηχοοΰΜΒΗΗηκοpacTBopa 9 'BuxaeTcsi to Aecop «Sep 1.

BoahuPí pacTBop n3 xecopeepa cpeAHero xaexeHMíi 1' προχοχητ nseecTHUM cnocoeoM Mepc3τβηχοοΡΜβΗΗΜΚ 9. ycTpoňcTBO pacujHpeHHS, 13 n ycTpoňCTBO oxxaxAennsi 14 CTyneHM a<scop<sepaHMUKoro xaexeHMP 5. β to BpeMA KaK aeAHbiPi pacTBop. buxoxswiH ns xecopdepa 1. οηπαογμηιιηι-ιotspasoM προχοχητ nepea τοηχοοΰΜβΗπηκ pacTBopa 9'. ycTpoňcTBO pacuinpeHnn 13' n yCTpoWcTBOoxjiaxACHHíi 14' . HenocpeACToeHHO nocxe θτογο θτοτ aeAHHtf pacTBop CTyneHn adcopesepa CMeuinoacTcac npWdxn3MTexbHO OAnnaKOBoň KonueHTpaunefl pacTBopa. nanpnMep, CTynenn aacopaepa 5".BoahuPí pacTBop n3 xecopeepa cpeAHero xaexeHMii 1 'ntecsum cnocoeoM Mepc3τβηχοοΡΜβΗΗΜΚ 9. ycT leastcBO pacujHpeHHS; buxoxswiH ns xecopdepa 1. οηπαογμηιιηι-ιotspasoM προχοχητ nepea τοηχοοΰΜβΗπηκ pacTBopa 9 '. at least tBO pacuinpHnn 13 'n yTpoWcTBOoxjiaxACHHi 14'. HenocpeACToeHHO nocxe θτογο θτοτ aeAHHtf pacTBop CTyneHn adcopesepa CMeuinoacTcac npWdxn3MTexbHO OAnnaKOBoon KonueHTpaunefl pacTBopa. nanpnMep, CTynenn aacopaepa 5 ".

MraK. Happwy c onncannuM bosmoxhm pa3Hooespa3Hbie KOMesnnaunn n pacuinpenna ycTpoftcTiia,παχουλή kotopux peaxňayoTcn cneunaxbHbie npncnocodxeHnst κ KoxnMecTBy n KanecTBy hochtc-íiíiOTXOAíiuiero Tenxa. HanppiKep. ecxn ηΜββτοίΐ b pacnopíixennn TenxoHocnTexb c onenb HC3HaHnTCAbiiuM 7 266 361 ΤβΜΠβρβΤ,νρΗΜΜ ypOBHeM. ΒΟ3ΜΟΜΗΟ npMMBHflTb ΑΟΠΟΛΗΜΤΒΛ bHUp) ΑβΟΟΡΟβρ ΒΗΤΒΟΗΒΗΗΗ «Λ») CTynCHklÍlrtCOPrfGpa HI4XB CTynOHM ορβΑΗΒΓΟ ΑββΛβΗΜΗ ΜΛΜ BK?l»MMTb ΟΓΟ napa/ifle/tbHo ΟΤΥΠΟΗΜ ΟΡΟΛΗΟΓΟΛβΒΛβΗΜΗ. ΠρΗΜβΗ OH ΠβρβΓργχββΤ TO/IbKO CTynBHb ΑβΒ-ΛΘΗΜΗ, HO αΛΒΓΟΛΛΡ» βΗΥ ΛΟΟΤΜΓββΤΟΗAajibHeMuiee BUTecneHuie paeoMeM cpeaw b rypeuiHB c OTdOpOM napa 4 B CTopoHy hmskuix AaoaennCOTOOpa 14 3THM - <SO/IBB BblCOKHO ΤβΠ^ΙΟηβρβηβΑΗ . 266 3S1 8Cloud. Happwy c onncannuM bosmoxhm pa3Hooespa3Hbie KOMesnnaunn n pacuinpenna ycTpoftcTiia, παχουλή kotopux peaxnayoTcn cneunaxbHbie npncnocodxeHnst κ KoxnMecTBy n KanecTBy hochtc-iiOTXOAiiuiero Tenxa. HanppiKep. ecxn ηΜββτοίΐ b pacnopíixennn TenxoHocnTexb c onenb HC3HaHnTCAbiiuM 7 266 361 ΤβΜΠβρβΤ, νρΗΜΜ ypOBHeM. Yn3ΜΟΜΗΟ npMMBHflTb ΑΟΠΟΛΗΜΤΒΛ bHUp) ΑβΟΟΡΟβρ ΒΗΤΒΟΗΒΗΗΗ «Λ») CTynCHklIlrtCOPrfGpa HI4XB CTynOHM ορβΑΗΒΓΟ ΑββΛβΗΜΗ ΜΛΜ BK? L »MMTb ΟΓΟ napa / ifle / tbHo ΟΤΥΠΟΗΜ ΟΡΟΛΗΟΓΟΛβΒΛβΗΜΗ. ΠρΗΜβΗ OH ΠβρβΓργχββΤ TO / IbKO CTynBHb ΑβΒ-ΛΘΗΜΗ, HO αΛΒΓΟΛΛΡ »βΗΥ ββΤΟΗAajibHeMuiee BUTecneHuie paeoMeM cpeaw b rypeuiHB c OTdOpOM napa 4 B CTopoHy hmskuix AaoaennCOTOOpa 14 3THM - <SO / IBB BblCOKHO ΤβΠ ^ ΙΟηβρβηβΑΗ. 266 3S1 8

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MaotípeTeHne Kacaarcí, nponaBOACTBa MexaHi/iMBCKoft βηβργι/μ H3 OTxoAfiutero Teruia b KaMecToeripouecca, Aono/iHswmoro ΤΒΡΜΟΑΜΗβΜΜΗβοκΜβ cnocoau, npoM3BOA«wti/ie ciTXci«»wje τβπ/ιο, μ κρ,τγοβμβnpuuBccM. npviMBM npn 3TOM ηοΛβ3Ηθβ npaoapaaoBaMvie τβπΛβ HaxoAMTcn e oa/,aoTM HBanaMUTo/ibnoro-reMnapaTypHoro ypOBKfl t £ 260°C)· ljeai> naotípeTenHíi - τβκ npeoepaaciBaTb TepMOAMHaMUMecKuň KpyroBoft npouecc, mtocsuMcnojit>3ooaTb OTxoaflwee τβπ/ιο He3HaHMT«JibHOro ypoenst a/i« npoi/i3BOACTBa βηβρρμμ ú7iaro«ap$iox^ax/<enMK> 3naMMTe/ibHO ημχθ 100°C.Ot ΜΗ aca aca, aca aca ACT aca a aca i aca aca μ 3 3 3 3 je je je je je je je je je je je je je je je je je je je je je je je je je je je je je je je je je je npviMBM npn 3TOM ηοΛβ3Ηθβ npaoapaaoBaMvie τβπΛβ HaxoAMTcn e oa /, aoTM HBanaMUTo / ibnoro-reMnapaTypHoro ypOBKfl t £ 260 ° C) · ljeai> naotípeTenHíi - τβκ npeoepaaciBaTb TepMOAMHaMUMecKuň KpyroBoft npouecc, mtocsuMcnojit> 3ooaTb OTxoaflwee τβπ / ιο He3HaHMT «JibHOro ypoenst and / i« npoi / i3BOACTBa βηβρρμμ ú7iaro «ap $ ix ^ ax / <enMK> 3naMMTe / ibHO ημχθ 100 ° C.

CymeCTDO MSOBPBTBMMfl GQOTOMT B TOM, MTO B KpyrOBOM npouecco nOCpBACTBOM «BCOprtUMM ΠΡΜbuciikom /KaojieHMH pcBOdoxAaeTCB pacsoMaa cpeAa BwcoKoro AasjíeHkia. ee neperpeeaoT. βφφβκτιίβηοpacuJMpíiuT b MHorocTyneMMaToň Typautne c otpopom napa μ ποορβαοτβομ CTyneMMaToW aescopeuun cnooapacTi:iop<;w)T u χμλκομ pacTBOpe. to ecTb e aacopounoHHOí, cpene,CymeCTDO MSOBPBTBMMff GQOTOMT B TOM, MTO B KpyrOBOM npouecco nOCpBACTBOM «BCOprtUMM ΠΡΜbuciikom / KaojieHMH pcBOdoxAaeTCB pacsoMaa cpeAa BwcoKoro AasjieHkia. ee neperpeeaoT. β p φ M M M b b b b b b b y y y y y y y y y y y y y u u u u u ac ac ac ac ac ac ac ac ac ac ac ecTb e aacopounoHHO, cpene,

Ori/iaCTM ΠΡΜΜβΗβΗΜΡ Μ3Ο«5ρβΤΟΗΜί11 - ΥΟΤβΗΟΒΚΜ SUiepHOfl ΒΗβρΓβΤΜΚΜ C ΒΜΟΟΚΟΤβΜΠβρβΤΙ/ρΗΜΜ DPOUBCCOM B ΓΟΛ0Ι/1 TyptíMHbl. -- Χμμμμβοκμβ ycTanooKM, - npoueccbt cyuiKM. - npoueccu. npon3BOAwmne aumoboH ra3. Φΐ/ir. 2 266 351 «ΟΡΙΊΧΛΑ M3GBPETEHI49 1. ycTpotfcTuo ζιζιρ ncnozib3ODannsi oTxoamuero τβηζια ηκοκογο TeMnepaTypHoro ypotiHsi aasi npoMSBQACTBa ΜβχβΗΜΜβεκοΜ μλμ aaexTpMMecxoří sneprwM c no omaopy e*nx>wenni»i ifomuuukctuomxoaoaa u Bkiae ycTpoňcTBa zionoziHuTezibHoro ox/ioMeHHn copauwoHHHX ycTaHOBOK na ochubbtbphmmbckmx cnocoaoo npui ηρΜΜβΗβΗΜΜ napu paaoMero aeutecTBa c χοροοιο aacopaHpyeMoři papOMeftcpeaoft bucokoto naujienwsi p c xnaxoft aacopaunonnoň cpeaoft. b xotopom paaOMan cpuaa eucuKoroaaBzíeHura poasiercp ocaodoxBaeMOň riyTen aecopauHH npi4 ducokom zxauziennn h, noczie neperpeua,paciuuippenoft nozi coBepuieHueM paaoTU b MHorocTyneHMaToň Typamie c oTaopoM napa, OTAHMaowoecmtom, mto nozuioH aecopaepa (1) comosh c BXoaoM b nar peaaTezibH.yio cbkuiw aecopaepa μβοτμμηογοnoroxa (22) mžím c npeaBapMTeabHUM neperpeeaTeaeM <10) mra oTaaMM renzia na caaaoro pacTBopa,Buxoau kotopux coeaMHeHu c BxozxoM pacTBopa b cTyneHb ΗΜ3ΚΟΓΟ raBjíeura aacopaepa <5) μβρββTenzioortMeHHMK <9) μ. πρμ HeoaxoaMMocTM, mbp©3 oxaaxaaioinMe ycTpoftCTBa <14> mra aaabMeftuieHοτλβμμ Tenzia na caaaoro pacTBopa. b to βρβμη κβκ npeaycMorpeno εοοιμηβημβ οτ roaoBKMaecopaepa <1> aan ποΛΗΟίΙ ujím MacTMMuoří noaaMM napooapaai-ioM paaoMeíf cpeau Mepea neperpaaaTeaM<10. 3) κ Bnycxy napa e MHorocTyneHMaTyn TypaMHy c οτβορβΜ <4), nptweM o cziynae ToabxoOri / iaCTM ΠΜβΜβΗΜΡ Μ3Ο «5ρβΤΟΗΜί11 - ΗΟΒΚΜβΗΟΒΚΜ SUiepHOfl ΒΗβρΓβΤΜΚΜC ΒΜΟΟΚΟΤβΜΠβρβΤΙ / ρΗΜΜ DPOUBCCOM B ΓΟΛ0Ι / 1 TyptíMHbl. - Χμμμμβοκμβ ycTanooKM, - npoueccbt cyuiKM. - npoueccu. npon3BOAwmne aumoboH ra3. Φΐ / ir. 2266351 «ΟΡΙΊΧΛΑ M3GBPETEHI49 first ycTpotfcTuo ζιζιρ ncnozib3ODannsi oTxoamuero τβηζια ηκοκογο TeMnepaTypHoro ypotiHsi AASI npoMSBQACTBa ΜβχβΗΜΜβεκοΜ μλμ aaexTpMMecxoří sneprwM C NO omaopy e * nx> wenn» i ifomuuukctuomxoaoaa at Bkiae ycTpoňcTBa zionoziHuTezibHoro ox / ioMeHHn copauwoHHHX ycTaHOBOK to ochubbtbphmmbckmx cnocoaoo npui ηρΜΜβΗβΗΜΜ napu paaoMero aeutecTBa c χοροοιο aacopaHpyeMoors papOMeftcpeaoft bucokoto naujienwsi pc xnaxoft aacopaunonnoň cpeaoft. b xotopom paaOMan cpuaa eucuKoroaaBzíeHura poasiercp ocaodoxBaeMOň riyTen aecopauHH npi4 ducokom zxauziennn h noczie neperpeua, paciuuippenoft NOZI coBepuieHueM paaoTU b MHorocTyneHMaToň Typamie c oTaopoM Napa OTAHMaowoecmtom MTO nozuioH aecopaepa (1) c comosh BXoaoM b born peaaTezibH.yio cbkuiw aecopaepa μβοτμμηογοnoroxa (22) I can c npeaBapMTeabHUM neperpeeaTeaeM <10) mra oTaaMM renzia to ca pacTBopa, Buxoau kotopux coeaMHeH c BxozxoM pacTBopa b cTyneHb ΗΜ3ΚΟΓΟ raBjíeura aacopaepa <5) μβρβTenzioortMeHHMK <9) μ. πρμ HeoaxoaMMocTM, mbp © 3 oxaaxaaioinMe ycTpoftCTBa <14> mra aaabMeftuieHοτλβμμ Tenzia na caaaoro pacTBopa. b to βρβμη κβκ npeaycMorpeno εοοιμηβημβ οτ roaoBKMaecopaepa <1> aan ποΛΗΟίΙ ujím MacTMMuoří noaaMM napooapaai-ioM paaoMeíf cpeau Mepea neperpaaaTeaM <10. 3) κ Bnycxy napa e MHorocTyneHMaTyn TypaMHy c οτβορβΜ <4), nptweM o cziynae Toabxo

MacTMMHOiS noaaMM napooapasHoft paaoMei* cpeau b TypaMHy c OTaopoM <4) cyinecTByeT aonoauMTeabHoeοοβαμηβημβ οτ roaooxM aecopaepa <1) Mepe3 aacopauMoHHy» xoaoaMabny» yciaHOBKy iippmo k anycK.ynapa b CTyneHb ημβχογο aaBaeHMH aacopaepa <5). κ xaxaoít CTyneiiM ziaoaeHM?, TypaMHU c othopoh<4> othocmtcp cooTBBTCToyomaíi CTyneHb aacopaepa <5. 5’ ', 5' ’ ) o Lieaiax ποβικιιιοημμ xbbzbiwa mcytuecTByeT neperyziMpyeMoe coeaMHeHMe οτ nepBoH CTyneHM (ημβκογο aaozieHMSi) TypaMHU o otpopom<4) azísi OTBoaa paaoMeW cpeau. pacuíMpenHoW noa coBepuieHMeM paaoTU Ha οτοίή CTyneHM ztaBzíeuMíi. κBnycxy napa b CTyneHb ημοκογο aanzieHMw aacopaepa <5>. b to bpibmíi k.ik npeaycMOTpew no oanncocauiHUTeabHbiH TpyeonpOBoa aap OTBoaa pacuíMpennoW paaoweH cpeau cooTueTCTBywiueW CTyneHMaaezietiMn οτ apyrux cTyneHeW aaBaeHMn TypauHu c OTaopoM <4> κ enycxy napa b othochuiviocp k HenyCTyneHb aacopaepa <5', 5''. 5'''> m Buxoa pacTBopa 143 nocaeaHeň CTyneHM (bucokoto zoBaeHHp) aacopaepa <5* ' ' ) coeaMHen c opoci4Tezien b aecopaepe <1) m. πρμ HeoaxoaMMocTM. 14 c opocMTeaewaecopaepa MacTMwnoro ηοτοχβ (22) Mepe3 nacoc <6''*) 14 aa« norzioineHMsi renzia 143 cnaooro paCTBOpa Μβρβ3 ΤεΠΛΟΟΰΗβΗΗΙΙΚ < 9). 2. ΥοτροΛοτβο no nyHXTy 1, oTJiMwaDineecn τβΜ, mto noaeoaxa pacTBopa paaaeaena Ha aoe οβτβμ aoBxoaa pacTBopa o nocaeaHoo CTyneHb <Bucoxoro aasaeHMfi) aacopaepa <5’’*>, oana eeTBb nakotopux coeauHeHa c BxoaoM pacTBopa b CTyneHb bucokoto aaeaeHuin aacopaepa <5’ ' ‘ ), a οτ apyroCíbotou McxoaMT coeauHeHue Mepe3 aecopaep MacTUWHoro ποτοχβ uziu Mepea TenjiooaMenHux pacTBopa<9’> mra noTJiouieHira Tenaa 143 oaeaHeHHoro pacTBopa aecopaepa cpeanero aasaeiinsi <1‘>, xopoci4Teao βτογο aecopaepa cpeaHero aao/ieHUM <1’), roaoaxa χοτορογο coeaHHena c unycxoM napa bCTyneHb bucokoto aaeaeHMíi aacopaepa <5*'’), b to BpeMíi xax pacnoaoxeH Tpyaonpoaoa οτ noaaonaaecopaepa cpeaHero aaeaeHkip <1‘> Mepea τβπλοορμβηηηχ pacTBopa <9') x eoeziunuTezibHOMyTpyaonpoBoay Mexay ποζοτοηομ aecopaepa <1) 14 BxoaoM pacTBopa b aacopaep HM3xoro ziatiziennw <5). 3. ycTpoWcTBO no nyHXTy 1, oTauMapuieecsi tbm, mto aa« βτορμμηογο cxaTHp paaoMečt cpearanpeaycMOTpeH aeyxcTyneHMaTbiW TepMHMecxnň xoMnpeccop, πριηΜβΜ ohixoa pacTBopa 143 cTyneuMbucokoto aaBzíeHMH aacopaepa <5''> coeauHeH Mepe3 τι2πζιοοομοηηι4Χ <9) c opocMTeaeM aecopaepacpeaHero aaBaeHUP <1’). roaoBxa nocaeaHero coeauiHeHa c enycxoM napa b pecopamnoHHyw CTyneHb<26), a caaauft pacTBop obzsbtcb noaaBaeMUM b pecopauun 143 noaaoHa aecopaepa <1> aan OTaaMinTenaa Mepe3 TenaooaMeHHMX pacTBopa <9’> na exoae pacTBopa a pecopauMOHHyp cTynent» <26). hBbixoa pacTBopa 143 pecopauHOHHOft CTynenw <26) cepaan c opocuiTeaeM aecopaepa <1> Mepes Hacoc<24) 14 aasr noraouieHMSi Ten/ia Mepes TenaooaneHHHx pacTBopa <9‘>. opumch roaooxa aecopaepa <1)coe«MH8HB c enycxoM napa 0 Typautny c OTaopow (4) Mepeo neperpeBaTeaui <10, 3) 14 rioaaonaecopaepa cpeaHero aaeaeHinp <1’> coeauiHen c bxoaom pacTBopa b CTyneHb Hinaxoro aanziem4íiaacopaepa <5) Mepea npeaoapHTeabHbiň neperpeeaTeab <10). TenaooaMenHkix <9) azra οταβμμ renzia 143caaaoro pacTBopa 14, npi4 Heoaxoai4MOCTH, Mepe3 oxaaaaaniUHe ycTprjflcTBa <14). 10 266 351MacTMMHOiS noaaMM napooapasHoft paaoMei CPEA b * c TypaMHy OTaopoM <4) cyinecTByeT aonoauMTeabHoeοοβαμηβημβ οτ roaooxM aecopaepa <1) Mepe3 aacopauMoHHy »xoaoaMabny» yciaHOBKy iippmo to anycK.ynapa b CTyneHb ημβχογο aaBaeHMH aacopaepa <5). κ xaxaoít CTyneiiM ziaoaeHM ?, TypaMHU c othopoh <4> othocmtcp cooTBBTCToyomai CTyneHb aacopaepa <5. 5 '', 5 '') about Lieaiax ποβικιιιοημμ xbbzbiwa mcytuecTByeT neperyziMpyeMoe coeaMHeHMe οτ nepBoH CTyneHM (ημβκογο aaozieHMSi) TypaMHU about otpop <4) and OTBoaa paaoMeW cpeau. pacuíMpenHoW noa coBepuieHMeM paaoTU Ha οτοίή CTyneHM ztaBzíeuMíi. κBnycxy napa b CTyneHb ημοκογο aanzieHMw aacopaepa <5>. b it bpibmíi k.ik npeaycMOTpew well oanncocauiHUTeabHbiH TpyeonpOBoa AAP OTBoaa pacuíMpennoW paaoweH CPEA cooTueTCTBywiueW CTyneHMaaezietiMn οτ apyrux cTyneHeW aaBaeHMn TypauHu OTaopoM c <4> b κ enycxy nappa othochuiviocp to HenyCTyneHb aacopaepa <5 ', 5' '. 5 '' Buxoa pacTopa 143 nocaeaHM CTyneHM (bucokoto zoBaeHHp) aacopaepa <5 * '') coeaMHen c opoci4Tezien b aecopaepe <1) m. Πρμ HeoaxoaMMocTM. 14 c opocMTeaewaecopaepa MacTMwnoro ηοτοχβ (22) Mepe3 nacoc <6 '' *) 14 aa «norzioineHMsi renzia 143 cnaooro paCTBOpa Μβρβ3 ΤεΠΛΟΟΰΗβΗΗΙΙΚ <9). Second ΥοτροΛοτβο well nyHXTy 1 oTJiMwaDineecn τβΜ MTO noaeoaxa pacTBopa paaaeaena Ha aoe οβτβμ aoBxoaa pacTBopa of nocaeaHoo CTyneHb <Bucoxoro aasaeHMfi) aacopaepa <5 '>, Oana eeTBb nakotopux coeauHeHa c BxoaoM pacTBopa b CTyneHb bucokoto aaeaeHuin aacopaepa <5' ') and οτ apyroCíbotou McxoaMT coeauHeHue Mepe3 aecopaep MacTUWHoro ποτοχβ uziu MEPE TenjiooaMenHux pacTBopa <9'> MRA noTJiouieHira Tena 143 oaeaHeHHoro pacTBopa aecopaepa cpeanero aasaeiinsi <1 '>, xopoci4Teao βτογο aecopaepa cpeaHero AAO / ieHUM <1') roaoaxa χοτορογο coeaHHena C unycxoM Napa bCTyneHb bucokoto aaeaeHMíi aacopaepa <5 * '), b it BpeMíi XAX pacnoaoxeH Tpyaonpoaoa οτ noaaonaaecopaepa cpeaHero aaeaeHkip <1'> MEPE τβπλοορμβηηηχ pacTBopa <9 ') x eoeziunuTezibHOMyTpyaonpoBoay Mexa ποζοτοηομ aecopaepa <1) 14 BxoaoM pacTBopa b aacopaep HM3xoro ziatiziennw < 5). Third ycTpoWcTBO well nyHXTy 1 oTauMapuieecsi TBM MTO aa «βτορμμηογο cxaTHp paaoMečt cpearanpeaycMOTpeH aeyxcTyneHMaTbiW TepMHMecxnň xoMnpeccop, πριηΜβΜ ohixoa pacTBopa 143 cTyneuMbucokoto aaBzíeHMH aacopaepa <5 '> coeauHeH Mepe3 τι2πζιοοομοηηι4Χ <9) c opocMTeaeM aecopaepacpeaHero aaBaeHUP <1'). pecopauun 143 noaaoHa aecopaepa <1> aan OTaaMinTenaa Mepe3 TenaooaMeHHMX pacTBopa <9 '> on exoae pacTBopa and pecopauMOHHyp cTynent »<26). hBbixoa pacTopa 143 pecopauHOHHOft CTynenw <26) cepaan c opocuiTeaeM aecopaepa <1> Mepes Hacoc <24) 14 aasr noraouieHMSi Ten / ia Mepes TenaooaneHHHx pacTBopa <9 ‘>. opumch roaooxa aecopaepa <1) coe «MH8HB c enycxoM napa 0 Typical c OTaopow (4) Mepeo neperpeBaTeaui <10, 3) 14 rioaaonaecopaepa cpeaHero aaeaeHinp <1 '> coeauiHen c bxoaom pacTBopa b CTyneHb Hinaxoro aanziem4íiaacopaepa <5) Mepea npeaoapHTeab ). TenaooaMenHkix <9) ara οταβμμ renzia 143caaaoro pacTBopa 14, npi4 Heoaxoai4MOCTH, Mepe3 oxaaaaaniUHe ycTprjflcTBa <14). 10 266 351

4. yuTpottcTBO no nyHKTaM 1 - 3. oTjtMMa»uieecH Ten, mto nocjie Buxona pacroopa tn ciyneHM4. yuTpottcTBO no nyHKTaM 1 - 3. oTjtMMa »uieecH Ten, Buxona pacroopa tn ciyneHM

Mcopiiepa <5. 5', 5' ’ >. ηρε«ηοΜΤΜΤβΛΐ>Ηο πβαβ CTyneHM bucokoto λοβλοημϊι aacoprfepa (5'').Mcopiiepa <5. 5 ', 5' '>. ηρε «ηοΜΤΜΤβΛΐ> πο πβαβ CTyneHM bucokoto λοβλοημϊι aacoprfepa (5 '').

TpycsonpoBon pa3.ne.neH Ha nee butom. o«na ββτβι. ra kotopux cnennnena nepea τ6:πλοο«μοηιι0κ (9) copocMTejieM necopesepa cpexnero nae-neni/iíi ď). γολοβκβ κοτορογο ΜΜββτ ccieni/ineni/ie κ BiiycK.y napab pecoprtUHOHityo CTyrienb (26), b to bpbmsi ksk npyras» bbtbp npojioxewa κ exony pacroopa bpecopesmnoHH.yo CTynetib (26) in euxon pacToopa otočí crynenin coenniiEH nepea τοιίΛοοΰΜΟΗΗΐηκpacTBopa (9‘) λλϊι nor/iomeHH« Tenna c opoct/ire-neM «ecopeepa (1). πρμμομ nowtati neeopdcpacpemero xaoaeMMR <1') coemHen c βχολομ pacroopa b cTynmb wniwro xasneHHH aouopesepa (5)nepea «ccopaep μοοτριμηογο ηοτοκα ιη τβΓυιοοβΜβΗΗΜΚ (9)0, πριη hgooxoauimoctm, nepea ox/iaxAaoiwneycTpoňcTBa (14). a noraoH necoptsepa (1) «Λ5, οτλομη Teruia coenMHCtt c βχολομ pacTenpn o unny μ,ίcrynenočí aocopoepa (5', 5’’) Μβρβ3 τβπ,ηοοώΜβΗΗΗΚ pacroopa O') in. ripw ηοολχολμμοοt0. «tepe:»oxjiaxnaoiuine ycTpoftCTBa (14'). 5. ycTpoWcTBO no nyHKTaM 1 - 4. OT-nuv-iaumeecsi Ten, mto nepen βχολομ pacTBopa o CTynenb atscopaepa (5. 5'. 5''. 5' ' ') pacravioxeH an0aesaT0MecK0či aecopeep (23). a κ bwxow pacTBopa 03CTynenin ημ3κογο naBnewifl aescopdepa (5) πολκλομβη eme ολμη an0aaaT0MecK0či aecopesep (25).ηρΜΜβΜ γολοβκθ οτογο aescopeepa (25) coeni/iHeHa c BnycKOM napa b aeeoppep (5) 0 npenycMOTpeHOcoexnnenne CTyneHH nwaKoro naeneHMfr TypdMHU c οτΰοροΜ (4) c BnycxoM napa b aíMaóarwHecKHÍíaescopesep (25).TpycsonpoBon pa3.ne.neH Ha nee butom. o «to ββτβι. ra kotopux cnennnena nepea τ6: «« μ ο (9) copocMTejieM necopesepa cpexnero nae-neni / iíi ď). γολοβκβ κοτορογο ΜΜββτ ccieni / Ineni / IE κ BiiycK.y napab pecoprtUHOHityo CTyrienb (26), b that bpbmsi ksk npyras »bbtbp npojioxewa κ exons pacroopa bpecopesmnoHH.yo CTynetib (26) rotates in euxon pacToopa crynenin coenniiEH NEP τοιίΛοοΰΜΟΗΗΐηκpacTBopa (9 ') λλϊι nor / iomeHH «Tenna c opoct / ire-ne« ecopeepa (1). now eop eop)))))))) em em em em em em em em em em em em em em em em em em em em ac,,,,,,,,,,,,,,, a noraoH necoptsepa (1) «Λ5, οτλομη Teruia coenMHCtt c β pacTenpn o unny μ, ίcrynenočí aocopoepa (5 ', 5'’) Μβρβ3 τβπ, ηοοώΜβΗΗΗΚ pacroopa O ') in. ripw ηοολχολμμοοt0. «Heat:» oxjiaxnaoiuine ycTpoftCTBa (14 '). 5. ycTpoWcTBO no nyHKTaM 1 - 4. OT-nuv-iaumeecsi This, unpopular, pacTBopa o CTynenb atscopaepa (5, 5 ', 5' ', 5' '), is a cytoplasmic antioxidant (23). and κ bwxow pacTBopa 03CTynenin ημ3κογο naBnewifl aescopdepa (5) πολκλομβη EME ολμη an0aaaT0MecK0či aecopesep (25) .ηρΜΜβΜ γολοβκθ οτογο aescopeepa (25) Coen / c iHeHa BnycKOM b aeeoppep hood (5) 0 npenycMOTpeHOcoexnnenne CTyneHH nwaKoro naeneHMfr TypdMHU οτΰοροΜ C (4) C BnycxoM napa b aíMaóarwHecKHÍíaescopesep (25).

Claims (6)

.11 cs 266351 B1 PŘEDMĚT . VYNÁLEZU.11 en 266351 B1 SUBJECT. THE INVENTION 1. Zařízení pro využití odpadního tepla níuké teplotníhladiny k výrobě mechanické nebo elektrické energie sesoučasnou výrobou chladu na principu sorpčních zařízenípoužívající páry pracovní látky o vysokém tlaku, kde pra-covní látka je uvolňována desorpcí a po přehřevu sr ukonče-ní práce expanduje ve vícestupňové turbině s odběrem, vy-značující se tím, že vana desorbéru (1) je pro přidánítepla ze slabého roztoku spojena se vstupem ohřívacísekce desorbéru částečného proudu (22) nebo s přehříva-čem (10), jejichž výstupy jsou spojeny s místem vstupuroztoku do stupně nízkého tlaku absorbéru (5) přes vý»5—nik tepla (9) a v případě potřeby přes chladicí zařízení(14) pro další odvod tepla ze slabého roztoku a současněje spojena hlavice desorbéru (1) se vstupem páry do více-stupňové turbiny s odběrem (4), přičemž pro případ částečnédodávky parotvorné látky do turbiny s odběrem (4) je přesabsorpční chladicí zařízení provedeno přídavné spojeníhlavice desorbéru se vstupem páry do stupně nízkého tlakuabsorbéru (5), přičemž ke každému tlakovému stupni tur-biny s odběrem (4) patří odpovídající stupeň absorbéru(5,5*» 5”9 5"') a výstup roztoku z každého stupně ab-sorbéru (5, 5\ 5") je spojen přes čerpadlo (6, 6', 6")se vstupem roztoku do stupně absorbéru o vyšším tlaku zaúčelem zvýšení tlaku a existuje neregulované spojení prv-ního stupně (nízkého tlaku) turbiny s. odběren se vstupempáry do stupně nízkého tlaku absorbéru za účelem odvodupracovní látky expandované na tomto tlakovém stupni vli-vem vykonávané práce..a zároveň lze expandovanou pracovnílátku odpovídajícího tlaku z jiných tlakových stupňůturbiny (4) odvádět spojovacím potrubím do odpovídající-ho stupně . absorbéru (5\ 5", 5'")» přičemž výstup roz-toku z posledního stupně (vysokého tlaku) absorbéru CS 256351 B1 12 (5Z<Z) je spojen se zvlhčovačem desorbéru (1) a vpřípadě nutnosti a se zvlhčovačem desorbéru částečnéhoproudu (22) přes čerpadlo (&amp;'"') a pro pohlcení teplaze slabého.roztoku i přes výměník tepla (9).An apparatus for utilizing waste heat of a low temperature level to produce mechanical or electrical energy by co-producing cold based on the principle of sorption devices using high pressure steam of a working substance where the working substance is released by desorption and expands in a multistage turbine after heating. by collecting, characterized in that the desorber tub (1) is connected to a weak solution desorption port (22) or a superheater (10) for the addition of the weak solution, the outlets of which are connected to the inlet flow point to the low pressure stage an absorber (5) through a heat exchanger (9) and, if necessary, through a cooling device (14) for further heat dissipation from the weak solution, and at the same time the desorber head (1) is connected to the steam inlet into a multi-stage turbine with extraction ( 4), wherein p is p for the partial delivery of vaporising agent to the turbine with extraction (4) the esabsorption cooling device has an additional connection of the desorber head with the steam inlet to the low pressure stage of the absorber (5), with a corresponding absorber stage (5.5 * 5 ”9 5” ') for each pressure stage (4) and outlet The solution from each stage of the sorbers (5, 5 ") is connected via a pump (6, 6 ', 6") to the inlet of the solution to the higher pressure stage of the absorber to increase the pressure and there is an unregulated first stage (low pressure) of the turbine with the intake to the absorber low pressure stage in order to remove the treatment agent expanded at this pressure stage by the work carried out, and at the same time, the expanded workpiece corresponding to the pressure from the other pressure stages (4) can be discharged to the corresponding degree. the absorber (5 ", 5 &quot;) " wherein the outlet of the last stage (high pressure) absorber CS 256351 B1 12 (5Z < Z) is coupled to the desorber humidifier (1) and, if necessary, to the partial flow desorber (22) via the pump (&amp; &quot; &quot;) and to absorb the heat of the weak solution through the heat exchanger (9). 2. Zařízení podle bodu 1, vyznačující se tím, že pří-vod roztoku je rozdělen do dvou větví, z nichž prvníje spojena se vstupem roztoku do stupně vysokého tlakuabsorbéru {5'") a druhá větev je spojená se zvlhčova-čem desorbéru středního tlaku přes desorbér částečnéhoproudu nebo výměník tepla roztoku (9) za účelem pohlce-ní tepla z roztoku desorbéru středního tlaku (1'), jehožhlavice je spojena se vstupem páry do stupně vysokéhotlaku absorbéru (5"') a zároveň od vany desorbéru střed-ního tlaku (1") veďě potrubí přes výměník tepla roztoku(9') ke spojovacímu potrubí vany desorbéru (1) se vstupemroztoku do absorbéru nízkého tlaku (5).2. Apparatus according to claim 1, characterized in that the supply of the solution is divided into two branches, the first of which is connected to the inlet of the solution to the high pressure stage and the second branch is connected to the medium pressure desorber humidifier. via a partial-flow desorber or a heat exchanger of the solution (9) to absorb heat from the medium pressure desorber solution (1 '), the head of which is connected to the steam inlet to the high pressure stage of the absorber (5' ') and at the middle pressure desorber bath (1 ") through the heat exchanger of the solution (9 ') to the conduit of the desorber tank (1) with the inlet to the low pressure absorber (5). 3. Zařízení podle bodu 1, vyznačující se tím, že k.se-kundárnímu stlačení pracovní látky slouží dvoustupňovýtermický kompresor a výstup roztoku z vysokotlakého stup-ně absorbéru (5") je spojen přes výměník tepla (9) sezvlhčovačem desorbéru středního tlaku (1*), jehož hla-vice je spojena se vstupem páry do resorpčního stupně(26) a slabý roztok je do resorpce přiváděn z vany de-sorbéru (1) za účelem odvodu tepla přes výměník teplaroztoku (9*), přičemž výstup roztoku z resorpčního stup-ně (26) je spojen se zvlhčovačem desorbéru (1) přesčerpadlo (24) a přes výměník tepla (9*)» přičemž hlavi-ce desorbéru (1) je spojena se vstupem páry do turbiny(4) přes přehřívače (10, 3) a vana desorbéru středníhotlaku ď) je spojena se vstupem roztoku do stupně níz-kého tlaku absorbéru (5) přes předřazený přehřívač (10), 13 CS 266351 B1 výměník-tepla (9) a v případě nutnosti přes chladicízařízení (14).3. Apparatus according to claim 1, characterized in that the two-stage compressor compresses the working medium and the outlet of the high-pressure absorber (5 ") is connected via a heat exchanger (9) to a medium pressure desorber (1). *), the level of which is associated with the introduction of steam into the resorption step (26) and the weak solution is brought to resorption from the sorbent tub (1) to dissipate heat through the heat exchanger (9 *), leaving the solution from the resorption step (26) is connected to the desorber humidifier (1) via a pump (24) and via a heat exchanger (9 *), wherein the head of the desorber (1) is connected to the steam inlet of the turbine (4) via superheaters (10, 3) and the medium pressure depressor duct d1) is connected to the inlet of the absorber to the low pressure stage of the absorber (5) via a pre-heater (10), CS 266351 B1 of the heat exchanger (9) and, if necessary, via a cooling device (14). 4. Zařízení podle bodů 1 až 3, vyznačující se tím,že po výstupu roztoku ze scupně absorbéru (5*, 5', 5"), zejména ze stupně vysokého tlaku absorbéru (5"),je potrubí rozděleno do dvou větví, z nichž první jespojena přes výměník tepla (9) se zvlhčovačem desorbérustředního tlaku (lý jehož hlavice je spojena se vstu-pem páry do resorpčního stupně (26) a druhá část potru-bí je připojena ke vstupu roztoku do resorpčního stup-ně (26) a výstup roztoku z tohoto stupně je spojen přesvýměník tepla (9') se zvlhčovačem desorbéru (1), při-čemž vana desorbéru středního tlaku ď) je spojena sevstupem roztoku do stupně nízkého tlaku absorbéru (5)přes desorbér částečného proudu a výměník tepla (9) av případě nutnosti přes chladicí zařízení (14) a vanadesorbéru (1) je za účelem odvodu tepla spojena se vstupem roztoku do jednoho ze stupňů absorbéru (5', 5")přes výměník tepla roztoku (9) a v případě nutnostipřes chladicí zařízení (14').4. Apparatus according to claim 1, characterized in that after the solution has been discharged from the absorber (5 *, 5 ', 5 "), in particular from the high pressure stage of the absorber (5"), the conduit is divided into two branches. which first is connected via a heat exchanger (9) to a medium pressure desorber humidifier (whose head is connected to the steam inlet to the resorption stage (26) and the second portion of the tube is connected to the solution inlet to the resorption step (26) and the outlet of the solution from this stage is connected to a heat exchanger (9 ') with a desorber humidifier (1), wherein the medium pressure desorber bath d1 is connected to the low pressure stage of the absorber (5) via a partial flow desorber and a heat exchanger (9). ) and, if necessary, through the cooling device (14) and the vanadium absorber (1) is connected to the inlet of the solution to one of the absorber stages (5 ', 5 ") via the solution heat exchanger (9) and in case of necessity via a cooling device (14 '). 5 <. Zařízení podle bodů 1 až 4, vyznačující se tím, žepřed vstupem roztoku do stupně absorbéru (5, 5'» 5",5"'} je umístěn adiabatický absorbér (2) a k výstupuroztoku ze stupně nízkého tlaku absorbéru (5) je při-pojen ještě jeden adiabatický absorbér (25), jehož hla-vice je spojena se^vstupem páry do absorbéru (5) a stu-peň nízkého tlaku turbiny s odběrem (4) je spojen sevstupem páry do adiabatického absorbéru (25).5 <. A device according to claims 1 to 4, characterized in that an adiabatic absorber (2) is placed in front of the absorber (5, 5 ' 5 &apos;, 5 &apos; ', 5 &apos; &apos; &apos; &apos; &apos;, 5 &apos;) and yet another adiabatic absorber (25) is bonded, the pressure of which is coupled to the inlet of steam into the absorber (5), and the low pressure stage of the extraction turbine (4) is coupled to the adiabatic absorber (25) by vapor entering. 6 výkresů6 drawings
CS811828A 1980-04-08 1981-03-11 Apparatus using exhaust heat of low temperature or electric energy for producing mechanic energy and cooling CS266351B1 (en)

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US4546620A (en) * 1984-11-05 1985-10-15 The United States Of America As Represented By The United States Department Of Energy Absorption machine with desorber-resorber
US4586340A (en) * 1985-01-22 1986-05-06 Kalina Alexander Ifaevich Method and apparatus for implementing a thermodynamic cycle using a fluid of changing concentration
DE3525721A1 (en) * 1985-07-18 1987-01-29 Linde Ag Process for utilizing waste heat
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US7735325B2 (en) * 2002-04-16 2010-06-15 Research Sciences, Llc Power generation methods and systems
DE102010046584A1 (en) 2010-09-25 2012-03-29 Hans Förster Method for generating mechanical or electrical energy from waste heat or renewable heating using thermodynamic cyclic process, involves liquefying thermal back compression of efficiently expanded working medium vapor in absorber
EP2803923B1 (en) * 2013-05-15 2017-11-29 Ago Ag Energie + Anlagen Absorption process and machine

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