CS30791A2 - Method of 1,1,1-trio (4-hydroxyphenyl) ethane purification - Google Patents

Method of 1,1,1-trio (4-hydroxyphenyl) ethane purification Download PDF

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Publication number
CS30791A2
CS30791A2 CS91307A CS30791A CS30791A2 CS 30791 A2 CS30791 A2 CS 30791A2 CS 91307 A CS91307 A CS 91307A CS 30791 A CS30791 A CS 30791A CS 30791 A2 CS30791 A2 CS 30791A2
Authority
CS
Czechoslovakia
Prior art keywords
tris
hydroxyphenyl
ethane
washed
crude mixture
Prior art date
Application number
CS91307A
Other languages
Czech (cs)
English (en)
Inventor
Heinz Strutz
Werner H Mueller
Original Assignee
Hoechst Celanese Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Celanese Corp filed Critical Hoechst Celanese Corp
Publication of CS30791A2 publication Critical patent/CS30791A2/cs

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/12—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings
    • C07C39/15—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings with all hydroxy groups on non-condensed rings, e.g. phenylphenol
    • C07C39/16—Bis-(hydroxyphenyl) alkanes; Tris-(hydroxyphenyl)alkanes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/685—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/82—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CS91307A 1990-02-09 1991-02-08 Method of 1,1,1-trio (4-hydroxyphenyl) ethane purification CS30791A2 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/478,072 US4992598A (en) 1990-02-09 1990-02-09 Purification of 1, 1, 1-tris(4'-hydroxyphenyl)ethane

Publications (1)

Publication Number Publication Date
CS30791A2 true CS30791A2 (en) 1991-09-15

Family

ID=23898403

Family Applications (1)

Application Number Title Priority Date Filing Date
CS91307A CS30791A2 (en) 1990-02-09 1991-02-08 Method of 1,1,1-trio (4-hydroxyphenyl) ethane purification

Country Status (11)

Country Link
US (1) US4992598A (de)
EP (1) EP0441648A1 (de)
JP (1) JPH04211032A (de)
KR (1) KR910015518A (de)
CN (1) CN1053918A (de)
BR (1) BR9100414A (de)
CA (1) CA2034705A1 (de)
CS (1) CS30791A2 (de)
HU (1) HUT57692A (de)
IE (1) IE910418A1 (de)
PL (1) PL288833A1 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5202505A (en) 1992-03-24 1993-04-13 Hoechst Celanese Corporation Purification of hydroxyphenyl alkanes
US5300698A (en) * 1993-05-27 1994-04-05 Hoechst Celanese Corporation Process for the prepartion of 1,3,5-tris(4'-hydroxyaryl)benzene
US5312988A (en) * 1993-05-28 1994-05-17 Hoechst Celanese Corporation Amines derived from THPE
US5756781A (en) * 1995-09-29 1998-05-26 General Electric Company Method for making tris(hydroxyphenyl) compounds using ion exchange
EP0782978B1 (de) * 1996-01-05 2000-04-05 General Electric Company Verfahren zur Herstellung und Reinigung von 1,1,1-Tris(4-hydroxyphenyl)ethan
US5672776A (en) * 1996-09-27 1997-09-30 General Electric Company Method for purifying 1,1,1-tris(4-hydroxyphenyl)-alkanes
US5763686A (en) * 1996-12-16 1998-06-09 General Electric Company Method for preparing 1,1,1-tris(4-hydroxyphenyl)ethane
KR100512061B1 (ko) * 2002-05-02 2005-09-05 재원산업 주식회사 노말 헵탄의 정제방법
BRPI0509507B1 (pt) 2004-03-31 2021-02-23 Research Institute Of Petroleum Processing, Sinopec catalisador de conversão de hidrocarbonetos contendo zeólito, o processo de preparação dos mesmos, e um processo para converter óleos hidrocarbonados com o catalisador
US20060004214A1 (en) * 2004-06-30 2006-01-05 Gurram Kishan Methods for preparing 1,1,1-tris(4-hydroxyphenyl)alkanes
US7304189B2 (en) * 2005-01-31 2007-12-04 General Electric Company Methods for preparing 1,1,1-tris(4-hydroxyphenyl)alkanes
EP2374784A1 (de) * 2010-04-07 2011-10-12 Bayer MaterialScience AG Reinigung von Tris-hydroxyaryl-Verbindungen
CN105541561B (zh) * 2016-02-04 2017-08-15 常州市天华制药有限公司 一种1,1,1‑三(4‑羟基苯基)乙烷的合成及纯化方法
CN114573425B (zh) * 2022-03-16 2022-12-09 安徽觅拓材料科技有限公司 一种1，1，1-三(4-羟基苯基)化合物的提纯方法及用途

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2789143A (en) * 1954-08-17 1957-04-16 Texas Co Manufacture of alkyl phenols
US3544514A (en) * 1965-01-15 1970-12-01 Bayer Ag Process for the production of thermoplastic polycarbonates
US3644538A (en) * 1967-08-22 1972-02-22 Exxon Research Engineering Co Hindered trisphenols
US3579542A (en) * 1968-06-26 1971-05-18 Hoechst Co American 4,4',4''-trihydroxytriphenylmethyl-methane
US4394496A (en) * 1971-08-19 1983-07-19 The Dow Chemical Company Epoxidation products of 1,1,1-tri-(hydroxyphenyl) alkanes
US3969421A (en) * 1974-02-21 1976-07-13 Labofina S.A. Process for producing ethylphenols
US4049721A (en) * 1976-09-07 1977-09-20 General Electric Company Purification of crude 9,9-bis-(4-hydroxyphenyl)-fluorene
FR2376109A1 (fr) * 1976-12-30 1978-07-28 Gen Electric Procede de purification des diphenols bruts
US4385191A (en) * 1979-12-19 1983-05-24 Standard Oil Company (Indiana) Recovery of BF3 -free alkylphenol product
US4337369A (en) * 1981-01-30 1982-06-29 Texaco Inc. Method of decolorizing mixtures of t-butyl alkylphenols

Also Published As

Publication number Publication date
PL288833A1 (en) 1991-11-04
BR9100414A (pt) 1991-10-22
CN1053918A (zh) 1991-08-21
US4992598A (en) 1991-02-12
CA2034705A1 (en) 1991-08-10
HU910173D0 (en) 1991-08-28
JPH04211032A (ja) 1992-08-03
IE910418A1 (en) 1991-08-14
EP0441648A1 (de) 1991-08-14
HUT57692A (en) 1991-12-30
KR910015518A (ko) 1991-09-30

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