DD149793A5 - Verfahren zur herstellung aktiver hydroxyl-und halogenhaltiger phosphornitride - Google Patents
Verfahren zur herstellung aktiver hydroxyl-und halogenhaltiger phosphornitride Download PDFInfo
- Publication number
- DD149793A5 DD149793A5 DD80219565A DD21956580A DD149793A5 DD 149793 A5 DD149793 A5 DD 149793A5 DD 80219565 A DD80219565 A DD 80219565A DD 21956580 A DD21956580 A DD 21956580A DD 149793 A5 DD149793 A5 DD 149793A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- phosphorus
- halogen
- temperature
- weight
- ammonium chloride
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title description 2
- TUJKJAMUKRIRHC-UHFFFAOYSA-N hydroxyl Chemical class [OH] TUJKJAMUKRIRHC-UHFFFAOYSA-N 0.000 title 1
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 22
- 239000011574 phosphorus Substances 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 16
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052736 halogen Inorganic materials 0.000 claims abstract description 12
- 150000002367 halogens Chemical class 0.000 claims abstract description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 10
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical group [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000460 chlorine Substances 0.000 claims abstract description 10
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000001301 oxygen Substances 0.000 claims abstract description 7
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 7
- 238000002360 preparation method Methods 0.000 claims abstract description 7
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 5
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical class ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 claims abstract description 5
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 26
- 239000007795 chemical reaction product Substances 0.000 claims description 16
- 235000019270 ammonium chloride Nutrition 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 230000007062 hydrolysis Effects 0.000 claims description 6
- 238000006460 hydrolysis reaction Methods 0.000 claims description 6
- ZSTLPJLUQNQBDQ-UHFFFAOYSA-N azanylidyne(dihydroxy)-$l^{5}-phosphane Chemical compound OP(O)#N ZSTLPJLUQNQBDQ-UHFFFAOYSA-N 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 3
- 238000000859 sublimation Methods 0.000 claims description 2
- 230000008022 sublimation Effects 0.000 claims description 2
- -1 phosphorus nitrides Chemical class 0.000 abstract description 12
- 239000004744 fabric Substances 0.000 abstract description 11
- 239000003063 flame retardant Substances 0.000 abstract description 9
- 229920003043 Cellulose fiber Polymers 0.000 abstract description 5
- 125000005843 halogen group Chemical group 0.000 abstract description 5
- 150000001875 compounds Chemical class 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 10
- 230000000694 effects Effects 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 5
- 229920002678 cellulose Polymers 0.000 description 4
- 239000001913 cellulose Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 230000004584 weight gain Effects 0.000 description 3
- 235000019786 weight gain Nutrition 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 150000004767 nitrides Chemical class 0.000 description 2
- 125000004437 phosphorous atom Chemical group 0.000 description 2
- 238000003303 reheating Methods 0.000 description 2
- 230000002269 spontaneous effect Effects 0.000 description 2
- 239000004114 Ammonium polyphosphate Substances 0.000 description 1
- 235000019826 ammonium polyphosphate Nutrition 0.000 description 1
- 229920001276 ammonium polyphosphate Polymers 0.000 description 1
- 238000005915 ammonolysis reaction Methods 0.000 description 1
- UXJHQBVRZUANLK-UHFFFAOYSA-N azanylidyne(dichloro)-$l^{5}-phosphane Chemical compound ClP(Cl)#N UXJHQBVRZUANLK-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 239000004627 regenerated cellulose Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/097—Compounds containing nitrogen and non-metals and optionally metals containing phosphorus atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/667—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing phosphorus in the main chain
- D06M15/673—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing phosphorus in the main chain containing phosphorus and nitrogen in the main chain
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S428/00—Stock material or miscellaneous articles
- Y10S428/92—Fire or heat protection feature
- Y10S428/921—Fire or flameproofing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/20—Coated or impregnated woven, knit, or nonwoven fabric which is not [a] associated with another preformed layer or fiber layer or, [b] with respect to woven and knit, characterized, respectively, by a particular or differential weave or knit, wherein the coating or impregnation is neither a foamed material nor a free metal or alloy layer
- Y10T442/2631—Coating or impregnation provides heat or fire protection
- Y10T442/2639—Coated or impregnated asbestos fabric
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/40—Knit fabric [i.e., knit strand or strip material]
- Y10T442/419—Including strand precoated with other than free metal or alloy
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polyesters Or Polycarbonates (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Graft Or Block Polymers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19792909600 DE2909600A1 (de) | 1979-03-12 | 1979-03-12 | Aktive hydroxyl- und halogenhaltige phosphornitride und verfahren zur herstellung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD149793A5 true DD149793A5 (de) | 1981-07-29 |
Family
ID=6065116
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD80219565A DD149793A5 (de) | 1979-03-12 | 1980-03-10 | Verfahren zur herstellung aktiver hydroxyl-und halogenhaltiger phosphornitride |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4276343A (fr) |
| EP (1) | EP0015546B1 (fr) |
| AT (1) | ATE847T1 (fr) |
| BR (1) | BR8001454A (fr) |
| CA (1) | CA1128287A (fr) |
| DD (1) | DD149793A5 (fr) |
| DE (2) | DE2909600A1 (fr) |
| SU (1) | SU1056892A3 (fr) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2918940C2 (de) * | 1979-05-10 | 1984-08-09 | Max Planck Gesellschaft zur Förderung der Wissenschaften e.V., 3400 Göttingen | Festes Ionenleitermaterial, seine Verwendung und Verfahren zu seiner Herstellung |
| US4741971A (en) * | 1986-05-23 | 1988-05-03 | The Dow Chemical Company | Method for imparting flame resistance to wood surfaces |
| EP0983208A1 (fr) * | 1998-03-05 | 2000-03-08 | International Business Machines Corporation | Materiau a absorption optique reduite |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1225073A (fr) * | 1959-02-13 | 1960-06-29 | Cfmc | Nouveaux composés du phosphore, leurs procédés de préparation et leurs applications dans l'ignifugation |
| US3669633A (en) * | 1970-08-19 | 1972-06-13 | Continuous process for the preparation of phosphonitrilic chloride cyclic polymers | |
| DE2159431A1 (de) * | 1971-12-01 | 1973-06-07 | Knapsack Ag | Verfahren zur herstellung von phospham |
| US3869294A (en) * | 1973-03-05 | 1975-03-04 | Ethyl Corp | Phosphonitrile polymer |
| AT333932B (de) * | 1974-08-20 | 1976-12-27 | Chemiefaser Lenzing Ag | Verfahren zur herstellung flammfester celluloseregeneratfasern |
| DE2608018C2 (de) * | 1976-02-27 | 1982-04-15 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von Phosphornitriden |
| GB1527153A (en) * | 1975-04-17 | 1978-10-04 | Hoechst Ag | Production of phosphorous nitrides |
| DE2516915C3 (de) * | 1975-04-17 | 1981-09-03 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von Phosphornitriden |
| US4175113A (en) * | 1978-04-20 | 1979-11-20 | The Firestone Tire & Rubber Company | Purification of crude chlorophosphazene compounds by treatment with water |
-
1979
- 1979-03-12 DE DE19792909600 patent/DE2909600A1/de not_active Withdrawn
-
1980
- 1980-03-10 US US06/128,385 patent/US4276343A/en not_active Expired - Lifetime
- 1980-03-10 DD DD80219565A patent/DD149793A5/de unknown
- 1980-03-10 AT AT80101111T patent/ATE847T1/de not_active IP Right Cessation
- 1980-03-10 DE DE8080101111T patent/DE3060287D1/de not_active Expired
- 1980-03-10 EP EP80101111A patent/EP0015546B1/fr not_active Expired
- 1980-03-12 BR BR8001454A patent/BR8001454A/pt unknown
- 1980-03-12 SU SU802893255A patent/SU1056892A3/ru active
- 1980-03-12 CA CA347,483A patent/CA1128287A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2909600A1 (de) | 1980-09-18 |
| EP0015546B1 (fr) | 1982-04-14 |
| CA1128287A (fr) | 1982-07-27 |
| US4276343A (en) | 1981-06-30 |
| SU1056892A3 (ru) | 1983-11-23 |
| EP0015546A2 (fr) | 1980-09-17 |
| EP0015546A3 (en) | 1981-01-21 |
| DE3060287D1 (en) | 1982-05-27 |
| BR8001454A (pt) | 1980-11-11 |
| ATE847T1 (de) | 1982-04-15 |
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