DD202141A5 - Verfahren zur herstellung von 3,3-dimethylglutarsaeure - Google Patents

Verfahren zur herstellung von 3,3-dimethylglutarsaeure Download PDF

Info

Publication number: DD202141A5
Authority: DD; German Democratic Republic
Prior art keywords: acid; isophorone; hydrogen peroxide; preparation; dimethylglutaric acid
Prior art date: 1981-05-12

Application number

DD82239719A

Other languages

German (de)

English (en)

Inventor

Pavel Lehky

Volker Franzen

Original Assignee

Lonza Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-05-12

Filing date

1982-05-10

Publication date

1983-08-31

1982-05-10 Application filed by Lonza Ag filed Critical Lonza Ag

1983-08-31 Publication of DD202141A5 publication Critical patent/DD202141A5/de

Links

238000000034 method Methods 0.000 title claims abstract description 11
238000002360 preparation method Methods 0.000 title claims description 5
DUHQIGLHYXLKAE-UHFFFAOYSA-N 3,3-dimethylglutaric acid Chemical compound OC(=O)CC(C)(C)CC(O)=O DUHQIGLHYXLKAE-UHFFFAOYSA-N 0.000 title abstract description 4
HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 claims abstract description 33
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 26
239000002253 acid Substances 0.000 claims abstract description 18
150000007513 acids Chemical class 0.000 claims abstract description 6
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 11
238000004519 manufacturing process Methods 0.000 abstract description 2
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
BTUDGPVTCYNYLK-UHFFFAOYSA-N 2,2-dimethylglutaric acid Chemical compound OC(=O)C(C)(C)CCC(O)=O BTUDGPVTCYNYLK-UHFFFAOYSA-N 0.000 description 8
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
239000013078 crystal Substances 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 3
238000001704 evaporation Methods 0.000 description 3
230000008020 evaporation Effects 0.000 description 3
239000000203 mixture Substances 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
239000000243 solution Substances 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 description 2
229910000147 aluminium phosphate Inorganic materials 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
238000001816 cooling Methods 0.000 description 2
150000002148 esters Chemical class 0.000 description 2
239000012452 mother liquor Substances 0.000 description 2
150000002978 peroxides Chemical class 0.000 description 2
239000002002 slurry Substances 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 1
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
239000005708 Sodium hypochlorite Substances 0.000 description 1
239000000654 additive Substances 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 1
SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 1
229940092714 benzenesulfonic acid Drugs 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
238000004587 chromatography analysis Methods 0.000 description 1
DGJMPUGMZIKDRO-UHFFFAOYSA-N cyanoacetamide Chemical compound NC(=O)CC#N DGJMPUGMZIKDRO-UHFFFAOYSA-N 0.000 description 1
230000006378 damage Effects 0.000 description 1
BADXJIPKFRBFOT-UHFFFAOYSA-N dimedone Chemical compound CC1(C)CC(=O)CC(=O)C1 BADXJIPKFRBFOT-UHFFFAOYSA-N 0.000 description 1
ZIUSEGSNTOUIPT-UHFFFAOYSA-N ethyl 2-cyanoacetate Chemical compound CCOC(=O)CC#N ZIUSEGSNTOUIPT-UHFFFAOYSA-N 0.000 description 1
238000000605 extraction Methods 0.000 description 1
239000007789 gas Substances 0.000 description 1
MWVFCEVNXHTDNF-UHFFFAOYSA-N hexane-2,3-dione Chemical compound CCCC(=O)C(C)=O MWVFCEVNXHTDNF-UHFFFAOYSA-N 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000000543 intermediate Substances 0.000 description 1
125000006838 isophorone group Chemical group 0.000 description 1
239000010687 lubricating oil Substances 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
239000000575 pesticide Substances 0.000 description 1
239000000047 product Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
150000003460 sulfonic acids Chemical class 0.000 description 1
YNJBWRMUSHSURL-UHFFFAOYSA-N trichloroacetic acid Chemical compound OC(=O)C(Cl)(Cl)Cl YNJBWRMUSHSURL-UHFFFAOYSA-N 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/285—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with peroxy-compounds

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Detergent Compositions (AREA)

DD82239719A 1981-05-12 1982-05-10 Verfahren zur herstellung von 3,3-dimethylglutarsaeure DD202141A5 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CH3062/81A CH650762A5 (de)	1981-05-12	1981-05-12	Verfahren zur herstellung von 3,3-dimethylglutarsaeure.

Publications (1)

Publication Number	Publication Date
DD202141A5 true DD202141A5 (de)	1983-08-31

Family

ID=4247770

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DD82239719A DD202141A5 (de)	1981-05-12	1982-05-10	Verfahren zur herstellung von 3,3-dimethylglutarsaeure

Country Status (11)

Country	Link
EP (1)	EP0064633B1 (da)
JP (1)	JPS57192330A (da)
AT (1)	ATE9324T1 (da)
CA (1)	CA1183868A (da)
CH (1)	CH650762A5 (da)
DD (1)	DD202141A5 (da)
DE (1)	DE3260707D1 (da)
DK (1)	DK197982A (da)
HU (1)	HU190009B (da)
IL (1)	IL65734A (da)
SU (1)	SU1099841A3 (da)

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB740747A (en) *	1951-08-18	1955-11-16	Distillers Co Yeast Ltd	Preparation of alpha-omega-dicarboxylic acids

1981
- 1981-05-12 CH CH3062/81A patent/CH650762A5/de not_active IP Right Cessation
1982
- 1982-04-21 DE DE8282103380T patent/DE3260707D1/de not_active Expired
- 1982-04-21 EP EP82103380A patent/EP0064633B1/de not_active Expired
- 1982-04-21 AT AT82103380T patent/ATE9324T1/de not_active IP Right Cessation
- 1982-05-03 DK DK197982A patent/DK197982A/da unknown
- 1982-05-10 HU HU821458A patent/HU190009B/hu unknown
- 1982-05-10 DD DD82239719A patent/DD202141A5/de unknown
- 1982-05-11 IL IL65734A patent/IL65734A/xx not_active IP Right Cessation
- 1982-05-11 CA CA000402662A patent/CA1183868A/en not_active Expired
- 1982-05-11 JP JP57079086A patent/JPS57192330A/ja active Pending
- 1982-05-11 SU SU3433200A patent/SU1099841A3/ru active

Also Published As

Publication number	Publication date
IL65734A0 (en)	1982-08-31
CA1183868A (en)	1985-03-12
EP0064633B1 (de)	1984-09-12
ATE9324T1 (de)	1984-09-15
EP0064633A1 (de)	1982-11-17
DE3260707D1 (en)	1984-10-18
SU1099841A3 (ru)	1984-06-23
IL65734A (en)	1986-01-31
JPS57192330A (en)	1982-11-26
DK197982A (da)	1982-11-13
CH650762A5 (de)	1985-08-15
HU190009B (en)	1986-08-28

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