DD283732A7 - Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes - Google Patents
Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes Download PDFInfo
- Publication number
- DD283732A7 DD283732A7 DD88320967A DD32096788A DD283732A7 DD 283732 A7 DD283732 A7 DD 283732A7 DD 88320967 A DD88320967 A DD 88320967A DD 32096788 A DD32096788 A DD 32096788A DD 283732 A7 DD283732 A7 DD 283732A7
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- formaldehyde
- urea
- molar ratio
- solution
- condensation
- Prior art date
Links
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 128
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000004202 carbamide Substances 0.000 claims abstract description 27
- 229920001807 Urea-formaldehyde Polymers 0.000 claims abstract description 15
- -1 methylol groups Chemical group 0.000 claims abstract description 14
- 238000009833 condensation Methods 0.000 claims abstract description 12
- 230000005494 condensation Effects 0.000 claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 230000002378 acidificating effect Effects 0.000 claims abstract description 11
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 claims abstract description 7
- 239000011093 chipboard Substances 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims description 14
- 239000003292 glue Substances 0.000 claims description 10
- 239000008098 formaldehyde solution Substances 0.000 claims description 9
- ODGAOXROABLFNM-UHFFFAOYSA-N polynoxylin Chemical compound O=C.NC(N)=O ODGAOXROABLFNM-UHFFFAOYSA-N 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 4
- 239000011541 reaction mixture Substances 0.000 claims description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 235000019253 formic acid Nutrition 0.000 claims 1
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 1
- 239000011707 mineral Substances 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 230000009257 reactivity Effects 0.000 abstract description 7
- 238000002360 preparation method Methods 0.000 abstract description 2
- 239000000853 adhesive Substances 0.000 abstract 2
- 230000001070 adhesive effect Effects 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 23
- 238000006243 chemical reaction Methods 0.000 description 8
- NNFCIKHAZHQZJG-UHFFFAOYSA-N potassium cyanide Chemical compound [K+].N#[C-] NNFCIKHAZHQZJG-UHFFFAOYSA-N 0.000 description 7
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000007859 condensation product Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 238000004513 sizing Methods 0.000 description 4
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical class OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000003776 cleavage reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000007017 scission Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- KSPIHGBHKVISFI-UHFFFAOYSA-N Diphenylcarbazide Chemical compound C=1C=CC=CC=1NNC(=O)NNC1=CC=CC=C1 KSPIHGBHKVISFI-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 244000154870 Viola adunca Species 0.000 description 1
- 235000005811 Viola adunca Nutrition 0.000 description 1
- 235000013487 Viola odorata Nutrition 0.000 description 1
- 235000002254 Viola papilionacea Nutrition 0.000 description 1
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L97/00—Compositions of lignin-containing materials
- C08L97/02—Lignocellulosic material, e.g. wood, straw or bagasse
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/04—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08G12/10—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with acyclic compounds having the moiety X=C(—N<)2 in which X is O, S or —N
- C08G12/12—Ureas; Thioureas
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C09J161/22—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C09J161/24—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with urea or thiourea
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2666/00—Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
- C08L2666/02—Organic macromolecular compounds, natural resins, waxes or and bituminous materials
- C08L2666/26—Natural polymers, natural resins or derivatives thereof according to C08L1/00 - C08L5/00, C08L89/00, C08L93/00, C08L97/00 or C08L99/00
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DD88320967A DD283732A7 (de) | 1988-10-21 | 1988-10-21 | Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes |
| AT89114038T ATE80906T1 (de) | 1988-10-21 | 1989-07-29 | Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes. |
| DE8989114038T DE58902334D1 (de) | 1988-10-21 | 1989-07-29 | Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes. |
| EP89114038A EP0366879B1 (fr) | 1988-10-21 | 1989-07-29 | Procédé de préparation de colles réactives à base de résines urée-formaldéhyde |
| ES89114038T ES2052834T3 (es) | 1988-10-21 | 1989-07-29 | Procedimiento para la obtencion de una cola reactiva de resina de urea-formaldehido. |
| FI895004A FI93550C (fi) | 1988-10-21 | 1989-10-20 | Menetelmä reaktiivisen urea/formaldehydi-hartsiliiman valmistamiseksi |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DD88320967A DD283732A7 (de) | 1988-10-21 | 1988-10-21 | Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD283732A7 true DD283732A7 (de) | 1990-10-24 |
Family
ID=5603320
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD88320967A DD283732A7 (de) | 1988-10-21 | 1988-10-21 | Verfahren zur herstellung eines reaktiven harnstoff-formaldehyd-harz-leimes |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0366879B1 (fr) |
| AT (1) | ATE80906T1 (fr) |
| DD (1) | DD283732A7 (fr) |
| DE (1) | DE58902334D1 (fr) |
| ES (1) | ES2052834T3 (fr) |
| FI (1) | FI93550C (fr) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1038100C (zh) * | 1992-09-30 | 1998-04-22 | 杭州市化工研究所 | 一种饲料粘合剂的生产方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1209203B (it) * | 1980-04-10 | 1989-07-16 | Montedison Spa | Collante ureico a basso sviluppo di formaldeide ed alto valore di tack. |
| ES8106163A1 (es) * | 1980-08-18 | 1981-08-01 | Patentes Novedades Sa | Procedimiento de preparacion de una resina ureaformaldehido de baja pegajosidad |
| DD160384A3 (de) * | 1980-10-01 | 1983-07-06 | Joachim Barse | Verfahren zur herstellung von harnstoff-formaldehyd-harz-leimen |
| GB2150939B (en) * | 1983-12-09 | 1987-02-04 | Enigma Nv | A process for preparing urea-formaldehyde resins |
| GB8519392D0 (en) * | 1985-08-01 | 1985-09-04 | Bip Chemicals Ltd | Solid uf |
-
1988
- 1988-10-21 DD DD88320967A patent/DD283732A7/de not_active IP Right Cessation
-
1989
- 1989-07-29 ES ES89114038T patent/ES2052834T3/es not_active Expired - Lifetime
- 1989-07-29 DE DE8989114038T patent/DE58902334D1/de not_active Expired - Fee Related
- 1989-07-29 EP EP89114038A patent/EP0366879B1/fr not_active Expired - Lifetime
- 1989-07-29 AT AT89114038T patent/ATE80906T1/de not_active IP Right Cessation
- 1989-10-20 FI FI895004A patent/FI93550C/fi not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI895004A0 (fi) | 1989-10-20 |
| EP0366879A2 (fr) | 1990-05-09 |
| FI93550B (fi) | 1995-01-13 |
| ATE80906T1 (de) | 1992-10-15 |
| EP0366879B1 (fr) | 1992-09-23 |
| DE58902334D1 (de) | 1992-10-29 |
| EP0366879A3 (en) | 1990-09-05 |
| FI93550C (fi) | 1995-04-25 |
| ES2052834T3 (es) | 1994-07-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RPI | Change in the person, name or address of the patentee (searches according to art. 11 and 12 extension act) | ||
| ENJ | Ceased due to non-payment of renewal fee |