DD283793A5 - Verfahren zur herstellung von beta-siliziumkarbid - Google Patents
Verfahren zur herstellung von beta-siliziumkarbid Download PDFInfo
- Publication number
- DD283793A5 DD283793A5 DD89327987A DD32798789A DD283793A5 DD 283793 A5 DD283793 A5 DD 283793A5 DD 89327987 A DD89327987 A DD 89327987A DD 32798789 A DD32798789 A DD 32798789A DD 283793 A5 DD283793 A5 DD 283793A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- mixture
- nitrogen
- carbon
- silicon carbide
- silicon
- Prior art date
Links
- 229910010271 silicon carbide Inorganic materials 0.000 title abstract description 56
- 238000004519 manufacturing process Methods 0.000 title abstract description 13
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 title description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 103
- 239000000203 mixture Substances 0.000 claims abstract description 68
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 50
- 238000000034 method Methods 0.000 claims abstract description 40
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000001301 oxygen Substances 0.000 claims abstract description 29
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 29
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 27
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 26
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 26
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 26
- 239000010703 silicon Substances 0.000 claims abstract description 26
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 26
- 239000007789 gas Substances 0.000 claims abstract description 21
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 45
- 238000005275 alloying Methods 0.000 claims description 20
- 239000000126 substance Substances 0.000 claims description 20
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 16
- 239000001569 carbon dioxide Substances 0.000 claims description 15
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 14
- 229910002090 carbon oxide Inorganic materials 0.000 claims description 14
- 239000010425 asbestos Substances 0.000 claims description 9
- 229910052895 riebeckite Inorganic materials 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 8
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 claims description 7
- 239000004202 carbamide Substances 0.000 claims description 7
- 235000013877 carbamide Nutrition 0.000 claims description 7
- 239000000123 paper Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 4
- 239000011111 cardboard Substances 0.000 claims description 4
- 239000001099 ammonium carbonate Substances 0.000 claims description 3
- 235000012501 ammonium carbonate Nutrition 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 3
- WIGIZIANZCJQQY-UHFFFAOYSA-N 4-ethyl-3-methyl-N-[2-[4-[[[(4-methylcyclohexyl)amino]-oxomethyl]sulfamoyl]phenyl]ethyl]-5-oxo-2H-pyrrole-1-carboxamide Chemical compound O=C1C(CC)=C(C)CN1C(=O)NCCC1=CC=C(S(=O)(=O)NC(=O)NC2CCC(C)CC2)C=C1 WIGIZIANZCJQQY-UHFFFAOYSA-N 0.000 claims 1
- 239000003082 abrasive agent Substances 0.000 abstract description 4
- 229910045601 alloy Inorganic materials 0.000 abstract description 3
- 239000000956 alloy Substances 0.000 abstract description 3
- 239000000919 ceramic Substances 0.000 abstract description 3
- 239000004744 fabric Substances 0.000 abstract description 3
- 239000011819 refractory material Substances 0.000 abstract description 2
- 229910010293 ceramic material Inorganic materials 0.000 abstract 1
- 229910021483 silicon-carbon alloy Inorganic materials 0.000 abstract 1
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 18
- 238000004458 analytical method Methods 0.000 description 10
- 229910052786 argon Inorganic materials 0.000 description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 239000006229 carbon black Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 239000010445 mica Substances 0.000 description 3
- 229910052618 mica group Inorganic materials 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- HZVOZRGWRWCICA-UHFFFAOYSA-N methanediyl Chemical compound [CH2] HZVOZRGWRWCICA-UHFFFAOYSA-N 0.000 description 2
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 238000003892 spreading Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000006004 Quartz sand Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910021383 artificial graphite Inorganic materials 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000010891 electric arc Methods 0.000 description 1
- 238000010892 electric spark Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- CSJDCSCTVDEHRN-UHFFFAOYSA-N methane;molecular oxygen Chemical compound C.O=O CSJDCSCTVDEHRN-UHFFFAOYSA-N 0.000 description 1
- -1 nitrogen ions Chemical class 0.000 description 1
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229910021332 silicide Inorganic materials 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/90—Carbides
- C01B32/914—Carbides of single elements
- C01B32/956—Silicon carbide
- C01B32/963—Preparation from compounds containing silicon
- C01B32/984—Preparation from elemental silicon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU884409571A SU1706963A1 (ru) | 1988-04-28 | 1988-04-28 | Способ получени @ -карбида кремни |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD283793A5 true DD283793A5 (de) | 1990-10-24 |
Family
ID=21368455
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD89327987A DD283793A5 (de) | 1988-04-28 | 1989-04-26 | Verfahren zur herstellung von beta-siliziumkarbid |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP0364592A4 (cs) |
| JP (1) | JPH03500528A (cs) |
| CN (1) | CN1037689A (cs) |
| CS (1) | CS274745B2 (cs) |
| DD (1) | DD283793A5 (cs) |
| HU (1) | HUT52738A (cs) |
| SU (1) | SU1706963A1 (cs) |
| WO (1) | WO1989010329A1 (cs) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1058692C (zh) * | 1995-10-26 | 2000-11-22 | 北京有色金属研究总院 | 离心自蔓延制取陶瓷衬管的点火方法 |
| JP3296998B2 (ja) * | 1997-05-23 | 2002-07-02 | 日本ピラー工業株式会社 | 単結晶SiCおよびその製造方法 |
| RU2163563C1 (ru) * | 1999-08-18 | 2001-02-27 | ЗАО НПП "Шунгитовые технологии" | Способ получения карбида кремния |
| RU2169701C2 (ru) * | 1999-08-18 | 2001-06-27 | ЗАО НПП "Шунгитовые технологии" | Способ получения бета-карбида кремния |
| CN1304286C (zh) * | 2004-12-30 | 2007-03-14 | 清华大学 | 一种SiC微米粉体的制备方法 |
| CN101343062B (zh) * | 2007-07-13 | 2012-02-29 | 贾玉东 | 一种冶炼绿色碳化硅磨料的方法 |
| CN101648709B (zh) * | 2008-08-16 | 2011-09-14 | 贾玉东 | 一种冶炼绿色碳化硅磨料的方法 |
| US20110250117A1 (en) * | 2010-04-07 | 2011-10-13 | Ge Investment Co., Ltd. | Method for fabricating silicon carbide material |
| CN102863953A (zh) * | 2012-10-16 | 2013-01-09 | 桂林理工大学 | 自蔓延高温合成致白光LED用红色荧光粉Sr2Si5N8:Eu2+的方法 |
| CN103058192B (zh) * | 2013-01-06 | 2016-05-25 | 河北同光晶体有限公司 | 一种用于碳化硅晶体生长的碳化硅微粉的制备方法 |
| CN105293499B (zh) * | 2015-11-30 | 2017-10-24 | 西安电子科技大学 | 一种b、n共掺杂碳化硅纳米吸波材料的制备方法 |
| DE112023001291T5 (de) * | 2022-03-09 | 2025-01-23 | Tohoku University | Verfahren zum Recycling von Kohlendioxid und Verfahren zum Erzeugen eines festen Carbids |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3535080A (en) * | 1969-02-18 | 1970-10-20 | Norton Co | Apparatus and method for the continuous furnacing of borides,carbides and silicides |
| JPS5325300A (en) * | 1976-08-20 | 1978-03-08 | Nippon Crucible Co | Process for preparing betaatype silicon carbide particle |
| JPS5850929B2 (ja) * | 1978-03-10 | 1983-11-14 | 株式会社東芝 | 炭化ケイ素粉末の製造方法 |
| DE2922280C2 (de) * | 1979-05-31 | 1982-07-22 | Nippon Crucible Co., Ltd., Tokyo | Verfahren zum Herstellen von pulverförmigem ß-Siliziumcarbid |
| US4217335A (en) * | 1979-06-14 | 1980-08-12 | Nippon Crucible Co., Ltd. | Process for producing β-silicon carbide fine powder |
| JPS5684310A (en) * | 1979-12-14 | 1981-07-09 | Hiroshige Suzuki | Manufacture of betaatype silicon carbide |
-
1988
- 1988-04-28 SU SU884409571A patent/SU1706963A1/ru active
- 1988-12-14 JP JP1502225A patent/JPH03500528A/ja active Pending
- 1988-12-14 HU HU891329A patent/HUT52738A/hu unknown
- 1988-12-14 EP EP19890902352 patent/EP0364592A4/de not_active Ceased
- 1988-12-14 WO PCT/SU1988/000256 patent/WO1989010329A1/ru not_active Ceased
-
1989
- 1989-04-19 CN CN89103262A patent/CN1037689A/zh active Pending
- 1989-04-26 DD DD89327987A patent/DD283793A5/de not_active IP Right Cessation
- 1989-04-28 CS CS263089A patent/CS274745B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN1037689A (zh) | 1989-12-06 |
| EP0364592A1 (de) | 1990-04-25 |
| HUT52738A (en) | 1990-08-28 |
| HU891329D0 (en) | 1990-07-28 |
| EP0364592A4 (en) | 1991-08-28 |
| CS274745B2 (en) | 1991-10-15 |
| SU1706963A1 (ru) | 1992-01-23 |
| CS263089A2 (en) | 1990-10-12 |
| WO1989010329A1 (fr) | 1989-11-02 |
| JPH03500528A (ja) | 1991-02-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |