DE69918081D1 - Reinigung von pentafluorophenyl borverbindungen - Google Patents
Reinigung von pentafluorophenyl borverbindungenInfo
- Publication number
- DE69918081D1 DE69918081D1 DE69918081T DE69918081T DE69918081D1 DE 69918081 D1 DE69918081 D1 DE 69918081D1 DE 69918081 T DE69918081 T DE 69918081T DE 69918081 T DE69918081 T DE 69918081T DE 69918081 D1 DE69918081 D1 DE 69918081D1
- Authority
- DE
- Germany
- Prior art keywords
- cleaning
- boron compounds
- pentafluorophenyl boron
- pentafluorophenyl
- compounds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- ZOICEQJZAWJHSI-UHFFFAOYSA-N (2,3,4,5,6-pentafluorophenyl)boron Chemical class [B]C1=C(F)C(F)=C(F)C(F)=C1F ZOICEQJZAWJHSI-UHFFFAOYSA-N 0.000 title 1
- 238000004140 cleaning Methods 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C07F5/027—Organoboranes and organoborohydrides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US58408 | 1998-04-09 | ||
| US09/058,408 US5959151A (en) | 1998-04-09 | 1998-04-09 | Process for the purification of pentafluorophenyl boron compounds |
| PCT/US1999/004871 WO1999052914A1 (en) | 1998-04-09 | 1999-03-02 | Purification of pentafluorophenyl boron compounds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69918081D1 true DE69918081D1 (de) | 2004-07-22 |
| DE69918081T2 DE69918081T2 (de) | 2005-06-16 |
Family
ID=22016638
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69918081T Expired - Fee Related DE69918081T2 (de) | 1998-04-09 | 1999-03-02 | Reinigung von pentafluorophenyl borverbindungen |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5959151A (de) |
| EP (1) | EP1070071B1 (de) |
| JP (1) | JP2002511472A (de) |
| CA (1) | CA2327402A1 (de) |
| DE (1) | DE69918081T2 (de) |
| ES (1) | ES2221368T3 (de) |
| WO (1) | WO1999052914A1 (de) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1998040389A1 (en) * | 1997-03-10 | 1998-09-17 | Nippon Shokubai Co., Ltd. | Method for purifying tetrakis(fluoroaryl) borate/magnesium halide, tetrakis(fluoroaryl) borate/ether complex and process for preparing the same, and process for preparing tetrakis(fluoroaryl) borate derivative |
| US6150560A (en) * | 1999-04-22 | 2000-11-21 | Albemarle Corporation | Recovery of tris(aryl)borane from their tetrahydrofuran complexes |
| US6476271B2 (en) | 2000-06-19 | 2002-11-05 | Honeywell International, Inc. | Process for the preparation of ether-free salts of tetrakis(pentafluorophenyl) borate |
| US6461481B1 (en) * | 2000-08-31 | 2002-10-08 | E. I. Du Pont De Nemours And Company | Process for removing water from organoborane compounds |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE69333541T2 (de) * | 1992-06-23 | 2004-09-30 | The Dow Chemical Company, Midland | Verfahren zur Herstellung von Tetrakisfluorphenylboraten |
| DE4235092A1 (de) * | 1992-10-17 | 1994-04-21 | Solvay Deutschland | Verfahren zur Herstellung von Ph¶3¶C[B(C¶6¶F¶5¶)¶4¶] |
| US5399780A (en) * | 1992-11-02 | 1995-03-21 | Tosoh Akzo Corporation | Method of producing triarylborane |
| US5493056A (en) * | 1992-12-28 | 1996-02-20 | Tosoh Akzo Corporation | Method of producing tetrakis (pentafluorophenyl) borate derivatives using pentafluorophenyl alkali metal salt prepared from pentafluorobenzene |
| EP0604962A1 (de) * | 1992-12-28 | 1994-07-06 | Tosoh Akzo Corporation | Verfahren zur Herstellung von Tris(Pentafluorphenyl)boran unter Verwendung eines Alkalisalzes von Pentafluorphenyl hergestellt aus Pentafluorbenzol |
| US5510536A (en) * | 1992-12-28 | 1996-04-23 | Tosoh Akzo Corporation | Production method of tris(pentafluorophenyl)borane using pentafluorophenylmagnesium derivatives prepared from pentafluorobenzene |
| US5362423A (en) * | 1992-12-28 | 1994-11-08 | Tosoh Akzo Corporation | Method of producing pentafluorophenylmagnesium derivatives using pentafluorobenzene |
| JP2868202B2 (ja) * | 1992-12-28 | 1999-03-10 | 東ソー・アクゾ株式会社 | ペンタフルオロベンゼンより調製したペンタフルオロフェニルアルカリ金属塩を用いたトリス(ペンタフルオロフェニル)ボランの製造方法 |
| JP2790605B2 (ja) * | 1992-12-28 | 1998-08-27 | 東ソー・アクゾ株式会社 | ペンタフルオロフェニルマグネシウム誘導体を用いたテトラキス(ペンタフルオロフェニル)ボレート誘導体の製造方法 |
| US5600004A (en) * | 1995-02-21 | 1997-02-04 | Albemarle Corporation | Process for preparing pentafluorophenyl compounds |
| US5693261A (en) * | 1995-02-21 | 1997-12-02 | Albemarle Corporation | Preparation of pentafluorophenyl compounds |
| US5473036A (en) * | 1995-03-03 | 1995-12-05 | Akzo Nobel N.V. | Process for forming a bromomagnesium tetrakis (fluorophenyl) borate |
| JP3456394B2 (ja) * | 1996-12-20 | 2003-10-14 | 住友化学工業株式会社 | ホウ素化合物の供給方法 |
-
1998
- 1998-04-09 US US09/058,408 patent/US5959151A/en not_active Expired - Fee Related
-
1999
- 1999-03-02 CA CA002327402A patent/CA2327402A1/en not_active Abandoned
- 1999-03-02 DE DE69918081T patent/DE69918081T2/de not_active Expired - Fee Related
- 1999-03-02 JP JP2000543470A patent/JP2002511472A/ja active Pending
- 1999-03-02 ES ES99911142T patent/ES2221368T3/es not_active Expired - Lifetime
- 1999-03-02 WO PCT/US1999/004871 patent/WO1999052914A1/en not_active Ceased
- 1999-03-02 EP EP99911142A patent/EP1070071B1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE69918081T2 (de) | 2005-06-16 |
| JP2002511472A (ja) | 2002-04-16 |
| EP1070071B1 (de) | 2004-06-16 |
| ES2221368T3 (es) | 2004-12-16 |
| CA2327402A1 (en) | 1999-10-21 |
| WO1999052914A1 (en) | 1999-10-21 |
| EP1070071A1 (de) | 2001-01-24 |
| US5959151A (en) | 1999-09-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |