DK0440074T3 - Process for preparing a glucose, fructose and sucrose-low inulooligosaccharide product - Google Patents
Process for preparing a glucose, fructose and sucrose-low inulooligosaccharide productInfo
- Publication number
- DK0440074T3 DK0440074T3 DK91100776.3T DK91100776T DK0440074T3 DK 0440074 T3 DK0440074 T3 DK 0440074T3 DK 91100776 T DK91100776 T DK 91100776T DK 0440074 T3 DK0440074 T3 DK 0440074T3
- Authority
- DK
- Denmark
- Prior art keywords
- fructose
- glucose
- sucrose
- inulooligosaccharide
- product
- Prior art date
Links
- 229930091371 Fructose Natural products 0.000 title abstract 4
- 239000005715 Fructose Substances 0.000 title abstract 4
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title abstract 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 title abstract 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 title abstract 4
- 239000008103 glucose Substances 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title 1
- 229920001202 Inulin Polymers 0.000 abstract 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract 3
- 229930006000 Sucrose Natural products 0.000 abstract 3
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 abstract 3
- 229940029339 inulin Drugs 0.000 abstract 3
- 239000005720 sucrose Substances 0.000 abstract 3
- 238000004587 chromatography analysis Methods 0.000 abstract 2
- 230000002255 enzymatic effect Effects 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 102000004190 Enzymes Human genes 0.000 abstract 1
- 108090000790 Enzymes Proteins 0.000 abstract 1
- 102100024295 Maltase-glucoamylase Human genes 0.000 abstract 1
- 108010028144 alpha-Glucosidases Proteins 0.000 abstract 1
- 230000002452 interceptive effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000009928 pasteurization Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Saccharide Compounds (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention relates to a process which starts from inulin-containing plant material and produces an inulooligosaccharide product which is low in glucose, fructose and sucrose. This is achieved by subjecting the inulin-containing plant material directly after comminution and pasteurisation to an enzymatic treatment with endo-inulinase and choosing conditions for this which minimise the glucose, fructose and sucrose contents, and then removing interfering glucose and fructose by chromatography. The sucrose can be removed by adding alpha -glucosidase, especially before the chromatography. Selected conditions for the enzymatic treatment are: maintaining the pH constant between 5.0 and 5.6, and the temperature between 50 and 60 DEG C and using 1.8 to 2.4 enzyme units of endo-inulinase per gram of inulin.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4003140A DE4003140A1 (en) | 1990-02-02 | 1990-02-02 | METHOD FOR THE PRODUCTION OF A GLUCOSE, FRUCTOSE AND SACCHAROSEARM INULOOLIGOSACCHARIDE PRODUCT |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK0440074T3 true DK0440074T3 (en) | 1994-07-25 |
Family
ID=6399314
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK91100776.3T DK0440074T3 (en) | 1990-02-02 | 1991-01-22 | Process for preparing a glucose, fructose and sucrose-low inulooligosaccharide product |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0440074B1 (en) |
| JP (1) | JPH04211388A (en) |
| AT (1) | ATE103987T1 (en) |
| DE (2) | DE4003140A1 (en) |
| DK (1) | DK0440074T3 (en) |
| ES (1) | ES2052285T3 (en) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4134922C1 (en) * | 1991-10-23 | 1992-12-03 | Anatoli 3013 Barsinghausen De Stobbe | |
| BE1006377A3 (en) * | 1992-11-24 | 1994-08-09 | Raffinerie Tirlemontoise Sa | SEPARATION METHOD OF polydispersed composition SACCHARIDES, PRODUCTS OBTAINED BY THE METHOD AND USE OF PRODUCTS OBTAINED IN FOOD COMPOSITIONS. |
| DE4316425C2 (en) * | 1993-05-17 | 1998-05-20 | Suedzucker Ag | Process for the production of long-chain inulin, the inulin thus produced and its use |
| DE4341780A1 (en) * | 1993-12-08 | 1995-06-14 | Suedzucker Ag | Hydrogenated fructooligosaccharides |
| JPH07274990A (en) * | 1994-04-15 | 1995-10-24 | Mitsubishi Kasei Eng Co | Method for purifying cyclic inulooligosaccharide |
| EP2179726A3 (en) | 1995-12-26 | 2012-09-26 | Block Drug Company, Inc. | Dietary fiber inulin delivery system |
| BE1010449A3 (en) * | 1996-08-01 | 1998-08-04 | Raffinerie Tirlemontoise Sa | PROCESS FOR PREPARING A COMPOSITION SACCHARIDES POLYDIPERSEE, COMPOSITION polydispersed saccharide, PRODUCTS, PHARMACEUTICAL AND / OR COSMETIC COMPOSITION COMPRISING polydisperse. |
| ES2159174T3 (en) | 1997-02-27 | 2001-09-16 | Tiense Suikerraffinaderij Nv | LOW DENSITY AND COMPOSITION FRUCTANE THAT CONTAINS IT. |
| EP1076716A1 (en) | 1998-05-05 | 2001-02-21 | McNeil Speciality Products Company Division of McNeil-PPC Inc. | Functional sugar polymers from inexpensive sugar sources and apparatus for preparing same |
| US7045166B2 (en) | 1998-08-27 | 2006-05-16 | Silver Barnard S | Sweetener compositions containing fractions of inulin |
| US6569488B2 (en) | 1998-08-27 | 2003-05-27 | Barnard Stewart Silver | Processes for making novel inulin products |
| US6399142B1 (en) | 1998-08-27 | 2002-06-04 | Barnard Stewart Silver | Liquid food products |
| US6419978B1 (en) | 1998-08-27 | 2002-07-16 | Barnard Stewart Silver | Inulin fractions |
| WO2010106077A1 (en) | 2009-03-17 | 2010-09-23 | Dequest Ag | Composition for inhibiting calcium salt scale formation |
| JP6174996B2 (en) | 2010-05-19 | 2017-08-02 | イタルマッチ ケミカルズ ソチエタ ペル アツィオーニ | Cleaning composition with improved stain removal |
| EP2388308A1 (en) | 2010-05-19 | 2011-11-23 | Dequest AG | Cleaning composition with improved stain removal |
| EP2790654A2 (en) | 2011-12-12 | 2014-10-22 | Italmatch Chemicals S.P.A. | Cosmetic composition for skin or hair care |
| EP2626373A1 (en) | 2012-02-08 | 2013-08-14 | Dequest AG | Method for the manufacture of concentrated aqueous solutions of alkali metal salt of carboxymethyl fructan |
| EP3135693A1 (en) | 2015-08-05 | 2017-03-01 | Tiense Suikerraffinaderij N.V. | Inulin product |
| EP3561031B1 (en) | 2018-04-27 | 2025-06-04 | The Procter & Gamble Company | Alkaline hard surface cleaners comprising alkylpyrrolidones |
| EP4234668A3 (en) | 2018-04-27 | 2023-10-04 | The Procter & Gamble Company | Hard surface cleaners comprising carboxylated fructan |
| EP3561032A1 (en) | 2018-04-27 | 2019-10-30 | The Procter & Gamble Company | Antimicrobial hard surface cleaners comprising alkylpyrrolidones |
| MA53323A (en) | 2018-07-31 | 2021-11-03 | Bayer Ag | USE OF A CATIONIC POLYSACCHARIDE COMPOUND AS A FUNGICIDE, PESTICIDE, ALGAECIDE, DEHYDRANT AND FOR PROLONGING THE STORAGE LIFE OF FRUITS AND VEGETABLES |
| WO2023227708A1 (en) | 2022-05-25 | 2023-11-30 | Bayer Aktiengesellschaft | Biobased larvicides |
| EP4484535A1 (en) | 2023-06-28 | 2025-01-01 | The Procter & Gamble Company | Hard surface cleaners comprising carboxylated fructan |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2072679B (en) * | 1980-03-31 | 1983-11-09 | Meiji Seika Kaisha | Sweetener |
| JPH0631285B2 (en) * | 1984-02-09 | 1994-04-27 | 株式会社林原生物化学研究所 | Method for producing high-purity oligoglucosylfructoside |
| JPS6140754A (en) * | 1984-07-31 | 1986-02-27 | Meiji Seika Kaisha Ltd | Feed containing inulooligosaccharide and method of raising domestic animal using same |
| DE3580350D1 (en) * | 1985-01-18 | 1990-12-06 | Satoru Shinohara | METHOD FOR PRODUCING A FRUKTO OLIGOSACCHAROSE. |
| DE3874613T2 (en) * | 1987-06-05 | 1993-05-13 | Mitsui Toatsu Chemicals | ADDITIVES FOR CATTLE FEED, ADDITIONAL CATTLE FEED AND METHOD FOR PRODUCING AN ADDITIONAL ADDITIVE. |
| JPH06140754A (en) * | 1992-10-26 | 1994-05-20 | Matsushita Electric Works Ltd | Switchable printed wiring board |
-
1990
- 1990-02-02 DE DE4003140A patent/DE4003140A1/en not_active Ceased
-
1991
- 1991-01-22 AT AT91100776T patent/ATE103987T1/en not_active IP Right Cessation
- 1991-01-22 DK DK91100776.3T patent/DK0440074T3/en active
- 1991-01-22 EP EP91100776A patent/EP0440074B1/en not_active Expired - Lifetime
- 1991-01-22 DE DE91100776T patent/DE59101299D1/en not_active Expired - Fee Related
- 1991-01-22 ES ES91100776T patent/ES2052285T3/en not_active Expired - Lifetime
- 1991-01-30 JP JP3029479A patent/JPH04211388A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| JPH04211388A (en) | 1992-08-03 |
| EP0440074A1 (en) | 1991-08-07 |
| ATE103987T1 (en) | 1994-04-15 |
| ES2052285T3 (en) | 1994-07-01 |
| DE59101299D1 (en) | 1994-05-11 |
| DE4003140A1 (en) | 1991-08-08 |
| EP0440074B1 (en) | 1994-04-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ATE103987T1 (en) | PROCESS FOR MANUFACTURING A LOW GLUCOSE, FRUCTOSE, AND SUCCHROSE INULOOLIGOSACCHARIDE PRODUCT. | |
| FR2626583B1 (en) | PROCESS FOR THE ENZYMATIC PREPARATION OF OLIGODEXTRANES USEFUL IN THE MANUFACTURE OF SUGAR SUBSTITUTES AND NEW OLIGODEXTRANES | |
| ATE314463T1 (en) | MALTOSE-TREHALOSE CONVERTING ENZYME, PRODUCTION AND USE THEREOF | |
| DK0627490T3 (en) | Process for preparing long-chain inuli n | |
| GR3001580T3 (en) | Aqueous ink compositions and method of manufacturing them | |
| KR940008603A (en) | Non-Random Decomposition of Starch and the Low Dextrose Equivalent Starch Conversion Product Produced thereby | |
| AU8314587A (en) | New oligosaccharides, immunogens and vaccines, and methods for preparing such oligosaccharides, immunogens and vaccines | |
| EP0252799A3 (en) | Process for preparing enzymatically a sugar mixture having a high content of isomaltose from sucrose and the obtained products | |
| NO875319D0 (en) | PROCEDURE FOR EXTRACELLULAR PREPARATION OF HOMOPOLYSACCARIDES. | |
| KR970043056A (en) | Extraction method of useful components in cultured mycelium | |
| ATE238683T1 (en) | METHOD FOR PRODUCING A FERMENTED DRINK. | |
| KR100913587B1 (en) | Method of Making Inulin | |
| EP0290768A3 (en) | Process for the production of glucose dehydrogenase from bacillus megaterium | |
| EP0301522A3 (en) | Process for producton of isomaltulose | |
| DK655187A (en) | METHOD OF TREATING MAIZE WATER | |
| DK165843C (en) | ENZYMATIC PROCEDURE FOR PREPARING A SYRUP WITH A HIGH CONTENT OF DEXTROSE | |
| IL31438A (en) | A method for converting glucose into fructose using microorganisms in which a glucose isomerizing enzyme has been fixed | |
| EP0175582A3 (en) | Stabilized enzymes, their production and use | |
| JPH06102033B2 (en) | Method for producing inulooligosaccharide | |
| AU1093392A (en) | Method for improving the flavour of starch by treatment with enzymatically active cell preparation | |
| ES2022934B3 (en) | ENZYMES MODIFIED WITH POLYURETHANE. | |
| MY129615A (en) | Method of removing off-notes from cocoa products | |
| ATE22702T1 (en) | PRODUCTION OF GLUCOSE DEHYDROGENASE. | |
| DE69427232D1 (en) | METHOD FOR PRODUCING DISACCHARIDES AND SACCHARIDES | |
| ES2009245A6 (en) | Process for improving quality of fruit |