DK0448413T3 - Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler - Google Patents
Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og diolerInfo
- Publication number
- DK0448413T3 DK0448413T3 DK91302546.6T DK91302546T DK0448413T3 DK 0448413 T3 DK0448413 T3 DK 0448413T3 DK 91302546 T DK91302546 T DK 91302546T DK 0448413 T3 DK0448413 T3 DK 0448413T3
- Authority
- DK
- Denmark
- Prior art keywords
- acylation
- diols
- selective
- dialkyltin oxides
- cyclic adducts
- Prior art date
Links
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title 1
- 229930006000 Sucrose Natural products 0.000 title 1
- 238000005917 acylation reaction Methods 0.000 title 1
- 125000004122 cyclic group Chemical group 0.000 title 1
- 150000002009 diols Chemical class 0.000 title 1
- 230000001404 mediated effect Effects 0.000 title 1
- 239000005720 sucrose Substances 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2224—Compounds having one or more tin-oxygen linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Saccharide Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/499,731 US5089608A (en) | 1990-03-23 | 1990-03-23 | Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK0448413T3 true DK0448413T3 (da) | 1995-07-10 |
Family
ID=23986463
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK91302546.6T DK0448413T3 (da) | 1990-03-23 | 1991-03-22 | Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5089608A (da) |
| EP (1) | EP0448413B1 (da) |
| JP (1) | JP3064462B2 (da) |
| CA (1) | CA2038740C (da) |
| DE (1) | DE69109719T2 (da) |
| DK (1) | DK0448413T3 (da) |
| ES (1) | ES2072541T3 (da) |
| GR (1) | GR910100124A (da) |
| IE (1) | IE66892B1 (da) |
| PT (1) | PT97115B (da) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5034551A (en) * | 1990-04-23 | 1991-07-23 | Noramco, Inc. | Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds |
| US5298611A (en) * | 1993-03-12 | 1994-03-29 | Mcneil-Ppc, Inc. | Sucralose pentaester production |
| AU3006095A (en) | 1994-07-11 | 1996-02-09 | United States Of America, As Represented By The Secretary Of Agriculture, The | Chemically synthesized sugar esters for the control of soft-bodied arthropods |
| US6608039B1 (en) | 1994-07-11 | 2003-08-19 | The United States Of America As Represented By The Secretary Of Agriculture | Chemically synthesized sugar esters for the control of soft-bodied arthropods |
| US5498709A (en) * | 1994-10-17 | 1996-03-12 | Mcneil-Ppc, Inc. | Production of sucralose without intermediate isolation of crystalline sucralose-6-ester |
| RU2159773C2 (ru) * | 1995-11-28 | 2000-11-27 | МакНЕЙЛ-ППС, ИНК. | Способы получения сложного эфира сахарозы по положению 6 |
| US6121430A (en) * | 1998-12-28 | 2000-09-19 | University Of Iowa Research Foundation | Regiospecific synthesis of glucose-based surfactants |
| US20090105470A1 (en) * | 2005-02-22 | 2009-04-23 | Pharmed Medicare Private Limited , A Corporation | Tin Mediated Regioselective Synthesis of Sucrose-6-Esters |
| US20060276639A1 (en) * | 2005-06-01 | 2006-12-07 | Healthy Brands, Llc | Conversion of sucralose-6-ester to sucralose |
| CN100418976C (zh) * | 2006-04-03 | 2008-09-17 | 广州科宏食品添加物有限公司 | 一种三氯蔗糖的制备方法 |
| EP2084129B1 (en) * | 2006-11-17 | 2016-07-27 | Janssen Pharmaceutica NV | Process for regioselective mono-tosylation of diols |
| GB0702854D0 (en) * | 2007-01-09 | 2007-03-28 | Tate & Lyle Plc | Method for the synthesis of sucrose-6-esters |
| GB0702857D0 (en) * | 2007-01-19 | 2007-03-28 | Tate & Lyle Plc | Improved sucralose production method |
| US20080227971A1 (en) * | 2007-01-19 | 2008-09-18 | Leinhos Duane A | Deacylation of sucralose-6-acylates |
| CN100420695C (zh) * | 2007-02-02 | 2008-09-24 | 上海迪赛诺医药发展有限公司 | 制备三氯蔗糖的方法 |
| US20090076261A1 (en) * | 2007-09-13 | 2009-03-19 | Polymed Therapeutics, Inc. | Novel process for preparing sucrose-6-esters |
| AR070082A1 (es) * | 2008-01-04 | 2010-03-10 | Tate & Lyle Technology Ltd | Metodo para la produccion de sucralosa |
| US8557976B2 (en) * | 2008-03-13 | 2013-10-15 | Tate & Lyle Technology Limited | Microbial consortia and methods for their use |
| WO2009117317A1 (en) * | 2008-03-20 | 2009-09-24 | Tate & Lyle Technology Ltd | Removal of acids from tertiary amide solvents |
| US8436157B2 (en) * | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
| US20090299055A1 (en) * | 2008-04-03 | 2009-12-03 | Tate & Lyle Technology Limited | Purification of Sucralose Containing Feed Streams for Sucralose Crystallization |
| US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
| AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
| US8212022B2 (en) * | 2008-04-03 | 2012-07-03 | Tate & Lyle Technology Limited | Effect of carbohydrate concentration on sucralose extraction efficiency |
| US20090259036A1 (en) * | 2008-04-03 | 2009-10-15 | Tate & Lyle Technology Limited | Extraction of less polar impurities from sucralose containing aqueous feed streams |
| GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
| GB2469158B (en) * | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
| GB2471348B (en) | 2009-06-22 | 2011-12-14 | Tate & Lyle Technology Ltd | A method for producing sucralose-6-acylate |
| GB2474311B (en) | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
| GB2474310B (en) | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
| GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
| CN102796145B (zh) * | 2012-06-19 | 2015-04-15 | 天津北方食品有限公司 | 一种蔗糖-6-苯甲酸酯的制备方法 |
| CN105829332B (zh) | 2013-12-16 | 2018-10-02 | 塔特和莱利技术有限公司 | 蔗糖-6-酯的氯化 |
| WO2016020635A1 (en) | 2014-08-08 | 2016-02-11 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
| GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
| GB2551591B (en) | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
| CN107459540A (zh) * | 2017-08-28 | 2017-12-12 | 山东三和维信生物科技有限公司 | 用于三氯蔗糖生产的节省dmf及提高蔗糖‑6‑酯产率的方法 |
| CN112218874A (zh) | 2020-09-10 | 2021-01-12 | 安徽金禾实业股份有限公司 | 一种蔗糖-6-酯的制备方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2583084A (en) * | 1948-12-15 | 1952-01-22 | Union Carbide & Carbon Corp | Hydrocarbon tin alcoholates |
| US2789994A (en) * | 1952-07-11 | 1957-04-23 | Metal & Thermit Corp | Polyhydric alcohol-organotin derivatives |
| DE3065399D1 (en) * | 1979-12-18 | 1983-11-24 | Tate & Lyle Plc | Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| EP0031651B1 (en) * | 1979-12-20 | 1983-03-23 | TATE & LYLE PUBLIC LIMITED COMPANY | Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
| DE3165986D1 (en) * | 1980-07-08 | 1984-10-18 | Tate & Lyle Plc | Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs) |
| US4360670A (en) * | 1981-02-02 | 1982-11-23 | Air Products And Chemicals, Inc. | Amino and amido dialkyl tin carboxylates |
| US4464490A (en) * | 1981-02-02 | 1984-08-07 | Air Products And Chemicals, Inc. | Amino and amido dialkyl tin carboxylates and their use in preparing polyurethane products |
| US4430456A (en) * | 1981-02-02 | 1984-02-07 | Air Products And Chemicals, Inc. | Polyurethane-forming process using amino and amido dialkyl tin carboxylates |
| US4465828A (en) * | 1982-12-23 | 1984-08-14 | The Procter & Gamble Company | Process of preparing alkylsaccharides |
| GB8622345D0 (en) * | 1986-09-17 | 1986-10-22 | Tate & Lyle Plc | Sucrose derivatives |
| US4950746A (en) * | 1988-07-18 | 1990-08-21 | Noramco, Inc. | Process for synthesizing sucrose derivatives by regioselective reaction |
-
1990
- 1990-03-23 US US07/499,731 patent/US5089608A/en not_active Expired - Lifetime
-
1991
- 1991-03-14 GR GR910100124A patent/GR910100124A/el not_active IP Right Cessation
- 1991-03-20 JP JP3080358A patent/JP3064462B2/ja not_active Expired - Fee Related
- 1991-03-21 CA CA002038740A patent/CA2038740C/en not_active Expired - Lifetime
- 1991-03-22 EP EP91302546A patent/EP0448413B1/en not_active Expired - Lifetime
- 1991-03-22 DE DE69109719T patent/DE69109719T2/de not_active Expired - Fee Related
- 1991-03-22 IE IE96291A patent/IE66892B1/en not_active IP Right Cessation
- 1991-03-22 ES ES91302546T patent/ES2072541T3/es not_active Expired - Lifetime
- 1991-03-22 DK DK91302546.6T patent/DK0448413T3/da active
- 1991-03-22 PT PT97115A patent/PT97115B/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JPH04217993A (ja) | 1992-08-07 |
| DE69109719T2 (de) | 1996-01-04 |
| EP0448413B1 (en) | 1995-05-17 |
| EP0448413A1 (en) | 1991-09-25 |
| US5089608A (en) | 1992-02-18 |
| PT97115A (pt) | 1991-11-29 |
| CA2038740A1 (en) | 1991-09-24 |
| IE66892B1 (en) | 1996-02-07 |
| IE910962A1 (en) | 1991-09-25 |
| ES2072541T3 (es) | 1995-07-16 |
| DE69109719D1 (de) | 1995-06-22 |
| CA2038740C (en) | 2001-10-23 |
| PT97115B (pt) | 1998-08-31 |
| GR910100124A (el) | 1992-06-30 |
| JP3064462B2 (ja) | 2000-07-12 |
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