DK0520377T3 - Fremgangsmåde til selektiv fremstilling af 4,4-methylen-bis-(N-phenylalkylcarbamat) - Google Patents
Fremgangsmåde til selektiv fremstilling af 4,4-methylen-bis-(N-phenylalkylcarbamat)Info
- Publication number
- DK0520377T3 DK0520377T3 DK92110570.6T DK92110570T DK0520377T3 DK 0520377 T3 DK0520377 T3 DK 0520377T3 DK 92110570 T DK92110570 T DK 92110570T DK 0520377 T3 DK0520377 T3 DK 0520377T3
- Authority
- DK
- Denmark
- Prior art keywords
- phenylalkylcarbamate
- methylene
- bis
- selective preparation
- filtrating
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 239000011260 aqueous acid Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000007859 condensation product Substances 0.000 abstract 1
- 239000003456 ion exchange resin Substances 0.000 abstract 1
- 229920003303 ion-exchange polymer Polymers 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 239000012022 methylating agents Substances 0.000 abstract 1
- 239000003880 polar aprotic solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C269/00—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C269/06—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups by reactions not involving the formation of carbamate groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019910010676A KR940010279B1 (ko) | 1991-06-26 | 1991-06-26 | N-페닐알킬카바메이트의 축합에 의한 4,4-메틸렌-비스(n-페닐 알킬카바메이트)의 선택적 제조방법 |
| KR1019910024291A KR950012535B1 (ko) | 1991-12-24 | 1991-12-24 | 4,4-메틸렌-비스-(n-페닐알킬카바메이트)의 선택적 제조방법 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK0520377T3 true DK0520377T3 (da) | 1998-04-14 |
Family
ID=26628663
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK92110570.6T DK0520377T3 (da) | 1991-06-26 | 1992-06-23 | Fremgangsmåde til selektiv fremstilling af 4,4-methylen-bis-(N-phenylalkylcarbamat) |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5384424A (da) |
| EP (1) | EP0520377B1 (da) |
| JP (1) | JP2599865B2 (da) |
| AT (1) | ATE163407T1 (da) |
| DE (1) | DE69224495T2 (da) |
| DK (1) | DK0520377T3 (da) |
| ES (1) | ES2113388T3 (da) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995020590A1 (en) * | 1994-01-27 | 1995-08-03 | The Trustees Of Columbia University In The City Of New York | Enantioselective receptors for amino acid derivatives, and other compounds |
| WO2013067679A1 (zh) * | 2011-11-08 | 2013-05-16 | 中国科学院过程工程研究所 | 制备多亚甲基多苯基多氨基甲酸酯的方法 |
| CN117185962A (zh) * | 2022-08-30 | 2023-12-08 | 海南华盛水泥投资有限公司 | 高效制备二苯甲烷二氨基甲酸甲酯的方法及其制备的产物和应用 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2946768A (en) * | 1957-08-12 | 1960-07-26 | Bayer Ag | Condensation products of carbamic acid esters |
| GB1398975A (en) * | 1971-08-16 | 1975-06-25 | Ici Ltd | Heat treatment and distillation of methylene bridged polyphenyl polyisocyanates |
| DD130143B1 (de) * | 1975-08-15 | 1979-12-27 | Guenter Muecke | Verfahren zur kontinuierlichen thermischen abtrennung organischer isocyanate aus fluessigem destillationsrueckstand |
| US4162362A (en) * | 1978-10-20 | 1979-07-24 | Atlantic Richfield Company | Process for the preparation of diphenylmethane dicarbamates and polymethylene polyphenyl carbamates |
| US4230877A (en) * | 1979-03-22 | 1980-10-28 | Atlantic Richfield Company | Method for increasing the 4,4'dicarbamate isomer of the diphenylmethane dicarbamates during preparation thereof |
| CA1150293A (en) * | 1979-10-01 | 1983-07-19 | Keisuke Wada | Process for the production of methylenedicarbanilates |
| US4287132A (en) * | 1980-09-29 | 1981-09-01 | Atlantic Richfield Company | Preparation of polyisocyanates from polycarbamates |
| US4303794A (en) * | 1980-12-22 | 1981-12-01 | The Dow Chemical Company | Separation and recovery of 4,4'-methylene dimethyl diphenyldicarbamate |
| JPS57171953A (en) * | 1981-04-15 | 1982-10-22 | Asahi Chem Ind Co Ltd | Improved method for condensing n-phenylcarbamic acid ester |
| JPS5862151A (ja) * | 1981-10-12 | 1983-04-13 | Asahi Chem Ind Co Ltd | N−フエニルカルバミン酸エステルの縮合方法 |
| JPS59172451A (ja) * | 1983-03-18 | 1984-09-29 | Asahi Chem Ind Co Ltd | ポリイソシアナ−ト類の製造方法 |
| JPS60231640A (ja) * | 1984-05-02 | 1985-11-18 | Asahi Chem Ind Co Ltd | イソシアナ−トの連続的製法 |
| JPH0240061B2 (ja) * | 1984-05-10 | 1990-09-10 | Asahi Chemical Ind | Isoshianaatonorenzokutekiseizohoho |
| JPS6267059A (ja) * | 1985-09-18 | 1987-03-26 | Nippon Kokan Kk <Nkk> | ジフエニルメタンジカルバミン酸エステル類の製造方法 |
-
1992
- 1992-06-23 ES ES92110570T patent/ES2113388T3/es not_active Expired - Lifetime
- 1992-06-23 DE DE69224495T patent/DE69224495T2/de not_active Expired - Fee Related
- 1992-06-23 DK DK92110570.6T patent/DK0520377T3/da active
- 1992-06-23 AT AT92110570T patent/ATE163407T1/de not_active IP Right Cessation
- 1992-06-23 EP EP92110570A patent/EP0520377B1/en not_active Expired - Lifetime
- 1992-06-25 JP JP4167504A patent/JP2599865B2/ja not_active Expired - Fee Related
- 1992-06-25 US US07/904,736 patent/US5384424A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0520377B1 (en) | 1998-02-25 |
| ATE163407T1 (de) | 1998-03-15 |
| JP2599865B2 (ja) | 1997-04-16 |
| EP0520377A2 (en) | 1992-12-30 |
| JPH0687816A (ja) | 1994-03-29 |
| EP0520377A3 (en) | 1993-06-16 |
| US5384424A (en) | 1995-01-24 |
| ES2113388T3 (es) | 1998-05-01 |
| DE69224495T2 (de) | 1998-08-13 |
| DE69224495D1 (de) | 1998-04-02 |
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