DK0659733T3 - Fremgangsmåde til påvirkning af cis-/trans-isomerforholdet af 3-aminomethyl-3,5,5-trimethylcyclohexylamin ved fremstilling heraf ud fra 3-cyano-3,5,5-trimethylcyclohexanon - Google Patents
Fremgangsmåde til påvirkning af cis-/trans-isomerforholdet af 3-aminomethyl-3,5,5-trimethylcyclohexylamin ved fremstilling heraf ud fra 3-cyano-3,5,5-trimethylcyclohexanonInfo
- Publication number
- DK0659733T3 DK0659733T3 DK94118077.0T DK94118077T DK0659733T3 DK 0659733 T3 DK0659733 T3 DK 0659733T3 DK 94118077 T DK94118077 T DK 94118077T DK 0659733 T3 DK0659733 T3 DK 0659733T3
- Authority
- DK
- Denmark
- Prior art keywords
- cis
- trans isomer
- trimethylcyclohexylamine
- trimethylcyclohexanone
- aminomethyl
- Prior art date
Links
- RNLHGQLZWXBQNY-UHFFFAOYSA-N 3-(aminomethyl)-3,5,5-trimethylcyclohexan-1-amine Chemical compound CC1(C)CC(N)CC(C)(CN)C1 RNLHGQLZWXBQNY-UHFFFAOYSA-N 0.000 title abstract 5
- DYLIWHYUXAJDOJ-OWOJBTEDSA-N (e)-4-(6-aminopurin-9-yl)but-2-en-1-ol Chemical compound NC1=NC=NC2=C1N=CN2C\C=C\CO DYLIWHYUXAJDOJ-OWOJBTEDSA-N 0.000 title abstract 3
- JJDFVIDVSCYKDS-UHFFFAOYSA-N 1,3,3-trimethyl-5-oxocyclohexane-1-carbonitrile Chemical compound CC1(C)CC(=O)CC(C)(C#N)C1 JJDFVIDVSCYKDS-UHFFFAOYSA-N 0.000 title abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 229920003002 synthetic resin Polymers 0.000 abstract 1
- 239000000057 synthetic resin Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
- C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4343891A DE4343891A1 (de) | 1993-12-22 | 1993-12-22 | Verfahren zur Beeinflussung des cis-/trans-Isomerenverhältnisses von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin bei dessen Herstellung aus 3-Cyano-3,5,5-trimethylcyclohexanon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK0659733T3 true DK0659733T3 (da) | 1998-01-05 |
Family
ID=6505810
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK94118077.0T DK0659733T3 (da) | 1993-12-22 | 1994-11-17 | Fremgangsmåde til påvirkning af cis-/trans-isomerforholdet af 3-aminomethyl-3,5,5-trimethylcyclohexylamin ved fremstilling heraf ud fra 3-cyano-3,5,5-trimethylcyclohexanon |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5583260A (cs) |
| EP (1) | EP0659733B1 (cs) |
| JP (1) | JPH07206787A (cs) |
| AT (1) | ATE156801T1 (cs) |
| DE (2) | DE4343891A1 (cs) |
| DK (1) | DK0659733T3 (cs) |
| SG (1) | SG46215A1 (cs) |
| TW (1) | TW263492B (cs) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19507398C1 (de) * | 1995-03-03 | 1996-09-12 | Basf Ag | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| JP3973719B2 (ja) * | 1996-08-22 | 2007-09-12 | 花王株式会社 | 第１級アミンの製法 |
| DE19747913C1 (de) * | 1997-10-30 | 1999-02-11 | Degussa | Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Iminen oder Nitrilen, insbesondere zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin (Isophorondiamin) aus 3-Cyano-3,5,5-trimethylcyclohexanimin (Isophoronnitril-imin) durch Hydrierung in Gegenwart eines quaternären Ammoniumhydroxids |
| DE19756400A1 (de) * | 1997-12-18 | 1999-06-24 | Basf Ag | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin mit einem cic/trans-Isomerenverhältnis von mindestens 70/30 |
| DE10142635A1 (de) | 2001-08-31 | 2003-03-20 | Basf Ag | Verfahren zur Herstellung von Isophorondiamin (IPDA, 3-Aminomethyl-3,5,5,-trimethylcyclohexylamin) |
| DE10236675A1 (de) * | 2002-08-09 | 2004-02-19 | Basf Ag | Verfahren zur Herstellung von Isophorondiamin(IPDA, 3-Aminomethyl-3,5,5-trimethylcyclohexylamin) mit einem hohen cis/trans-Isomerenverhältnis |
| DE10236674A1 (de) * | 2002-08-09 | 2004-02-19 | Basf Ag | Destillative Verfahren zur Herstellung von IPDA mit einem hohen cis/trans-Isomerenverhältnis |
| EP3050870B1 (de) | 2015-01-30 | 2024-11-27 | Evonik Operations GmbH | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| CN107428674B (zh) | 2015-03-09 | 2021-01-29 | 三菱瓦斯化学株式会社 | 1,3,3-三甲基-1-(氨甲基)氨基环己烷的异构化方法 |
| CN106977422B (zh) * | 2017-03-06 | 2018-12-04 | 万华化学集团股份有限公司 | 一种连续生产异佛尔酮腈的方法 |
| CN108017547B (zh) * | 2017-12-22 | 2019-07-02 | 浙江新和成股份有限公司 | 一种异佛尔酮腈亚胺加氢还原制备异佛尔酮二胺的方法 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1229078B (de) * | 1961-10-18 | 1966-11-24 | Hibernia Chemie Ges Mit Beschr | Verfahren zur Herstellung von 3-(Aminomethyl)-3, 5, 5-trimethylcyclohexylderivaten |
| DE3011656A1 (de) * | 1980-03-26 | 1981-10-01 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 3-aminomethyl-3-5-5-trimethyl-cyclohexylamin |
| DE3021955A1 (de) * | 1980-06-12 | 1981-12-24 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung primaerer mono- und diamine aus oxoverbindungen |
| KR900016106A (ko) * | 1989-04-25 | 1990-11-12 | 마릴린 클로스티 | 카보닐니트릴 및 이와 유사한 화합물의 환원적 아민화 방법 |
| DE3942371A1 (de) * | 1989-12-21 | 1991-06-27 | Degussa | Verfahren zur herstellung von 1,3,3-trimethyl-5-oxo-cyclohexan-carbonitril |
| DE4010227A1 (de) * | 1990-03-30 | 1991-10-02 | Basf Ag | Verfahren zur herstellung von 3-aminomethyl-3,5,5-trimethyl-cyclohexylamin |
| DE4106882C2 (de) * | 1991-03-05 | 1994-02-03 | Degussa | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin durch reduktive Aminierung von 1,3,3-Trimethyl-5-oxocyclohexan-carbonitril |
| KR930005965A (ko) * | 1991-09-25 | 1993-04-20 | 에토 다케토시 | 3-아미노메틸-3,5,5-트리알킬사이클로헥실아민의 제조방법 |
| DE4211454C2 (de) * | 1992-04-06 | 1995-11-02 | Degussa | Verfahren zum Verlängern der Topfzeit bei der Härtung von Epoxidharzen mit Isophorondiamin-Isomerengemischen |
-
1993
- 1993-12-22 DE DE4343891A patent/DE4343891A1/de not_active Withdrawn
-
1994
- 1994-09-30 TW TW083109048A patent/TW263492B/zh active
- 1994-11-17 DK DK94118077.0T patent/DK0659733T3/da active
- 1994-11-17 EP EP94118077A patent/EP0659733B1/de not_active Expired - Lifetime
- 1994-11-17 AT AT94118077T patent/ATE156801T1/de not_active IP Right Cessation
- 1994-11-17 DE DE59403724T patent/DE59403724D1/de not_active Expired - Lifetime
- 1994-11-17 SG SG1996000932A patent/SG46215A1/en unknown
- 1994-12-19 JP JP6315106A patent/JPH07206787A/ja active Pending
- 1994-12-22 US US08/361,437 patent/US5583260A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE59403724D1 (de) | 1997-09-18 |
| EP0659733B1 (de) | 1997-08-13 |
| SG46215A1 (en) | 1998-02-20 |
| US5583260A (en) | 1996-12-10 |
| TW263492B (cs) | 1995-11-21 |
| EP0659733A1 (de) | 1995-06-28 |
| JPH07206787A (ja) | 1995-08-08 |
| ATE156801T1 (de) | 1997-08-15 |
| DE4343891A1 (de) | 1995-06-29 |
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