DK0795535T3 - Fremgangsmåde og anlæg til kontinuerlig fremstilling af alkylestere af (meth)acrylsyre - Google Patents

Fremgangsmåde og anlæg til kontinuerlig fremstilling af alkylestere af (meth)acrylsyre

Info

Publication number: DK0795535T3
Authority: DK; Denmark
Prior art keywords: meth; plant; acrylic acid; alkyl esters; continuous preparation
Prior art date: 1996-02-06

Application number

DK97101728T

Other languages

English (en)

Inventor

Albrecht Dams

Heinrich Aichinger

Gerhard Nestler

Herbert Exner

Gabriele Iffland

Alexander Weck

Holger Herbst

Original Assignee

Basf Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1996-02-06

Filing date

1997-02-04

Publication date

2001-11-19

1997-02-04 Application filed by Basf Ag filed Critical Basf Ag

2001-11-19 Application granted granted Critical

2001-11-19 Publication of DK0795535T3 publication Critical patent/DK0795535T3/da

Links

CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 title 1
125000005907 alkyl ester group Chemical group 0.000 title 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Crystallography & Structural Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

DK97101728T 1996-02-06 1997-02-04 Fremgangsmåde og anlæg til kontinuerlig fremstilling af alkylestere af (meth)acrylsyre DK0795535T3 (da)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19604252A DE19604252A1 (de)	1996-02-06	1996-02-06	Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure

Publications (1)

Publication Number	Publication Date
DK0795535T3 true DK0795535T3 (da)	2001-11-19

Family

ID=7784648

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DK97101728T DK0795535T3 (da)	1996-02-06	1997-02-04	Fremgangsmåde og anlæg til kontinuerlig fremstilling af alkylestere af (meth)acrylsyre

Country Status (16)

Country	Link
US (1)	US5945560A (da)
EP (1)	EP0795535B1 (da)
JP (1)	JPH101455A (da)
KR (1)	KR970061851A (da)
CN (1)	CN1137875C (da)
BR (1)	BR9703407A (da)
CA (1)	CA2196915A1 (da)
CZ (1)	CZ33597A3 (da)
DE (2)	DE19604252A1 (da)
DK (1)	DK0795535T3 (da)
ES (1)	ES2163671T3 (da)
ID (1)	ID15885A (da)
MX (1)	MX9700899A (da)
MY (1)	MY121248A (da)
SG (1)	SG85587A1 (da)
TW (1)	TW374082B (da)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE19851983A1 (de) *	1998-11-11	2000-05-18	Basf Ag	Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure
US6172258B1 (en) *	1999-09-14	2001-01-09	Celanese International Corporation	Process for the production and purification of n-butyl acrylate
US6180820B1 (en) *	1999-09-14	2001-01-30	Celanese International Corporation	Process for the production and purification of N-butyl acrylate
US6982026B2 (en) *	2001-03-15	2006-01-03	Tate & Lyle Ingredients Americas, Inc.	Azeotropic distillation process for producing organic acids or organic acid amides
US6926810B2 (en) *	2001-03-15	2005-08-09	A. E. Staley Manufacturing Co.	Process for obtaining an organic acid from an organic acid ammonium salt, an organic acid amide, or an alkylamine organic acid complex
DE10127941A1 (de)	2001-06-08	2002-05-29	Basf Ag	Verfahren zur Herstellung von (Meth)acrylsäureestern
DE102004038013A1 (de)	2004-08-04	2006-03-16	Basf Ag	Verfahren zur Herstellung von (Meth)acrylsäureestern
DE102005010588A1 (de) *	2005-03-08	2006-05-24	Basf Ag	Verfahren zur Herstellung von Alkylestern der (Meth)acrylsäure
DE102005010587A1 (de) *	2005-03-08	2006-06-08	Basf Ag	Verfahren zur Herstellung von Alkylestern der (Meth)acrylsäure
CN101041621B (zh) *	2006-11-24	2010-12-01	中国石油集团工程设计有限责任公司东北分公司	制备（甲基）丙烯酸丁酯的方法
US7857944B2 (en) *	2007-04-25	2010-12-28	National Taiwan University	Method and apparatus for esterification
US8765217B2 (en)	2008-11-04	2014-07-01	Entrotech, Inc.	Method for continuous production of (meth)acrylate syrup and adhesives therefrom
DE102008060218A1 (de)	2008-12-04	2010-06-10	Evonik Stockhausen Gmbh	Aufarbeitungsverfahren bei der Herstellung von (Meth)Acrylsäurealkylestern
US8329079B2 (en)	2009-04-20	2012-12-11	Entrochem, Inc.	Method and apparatus for continuous production of partially polymerized compositions and polymers therefrom
DE102010062601A1 (de)	2010-12-08	2012-06-14	Evonik Stockhausen Gmbh	Verfahren zur Herstellung von (Meth)Acrylsäureestern
CN102627716A (zh) *	2012-03-29	2012-08-08	沈阳长城润滑油制造有限公司	一种聚甲基丙烯酸酯降凝剂的制备方法
CN103254072A (zh) *	2013-05-14	2013-08-21	江门谦信化工发展有限公司	一种连续生产丙烯酸丁酯粗产品的变压工艺
CN104418922B (zh) *	2013-08-23	2016-12-28	河北科技大学	采用一步法连续合成烷基糖苷的苷化反应器
JP6287269B2 (ja) *	2014-01-30	2018-03-07	三菱ケミカル株式会社	アクリル酸ブチルの製造方法
FR3083233B1 (fr) *	2018-06-27	2020-05-29	Arkema France	Procede de purification d'acrylates legers.
CN113574047A (zh) *	2019-04-16	2021-10-29	罗门哈斯公司	由丙烯酸和甲醇进行的酸催化的丙烯酸甲酯合成
EP3956285B1 (en) *	2019-04-16	2023-04-26	Rohm and Haas Company	Acid catalyzed synthesis of methyl acrylate from acrylic acid and methanol
KR20240041972A (ko)	2021-07-29	2024-04-01	바스프 에스이	아크릴레이트의 연속 증류 방법
WO2025131961A1 (en) *	2023-12-21	2025-06-26	Basf Se	Device and process for manufacture of (meth)acrylates

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB1017522A (en) *	1963-09-26	1966-01-19	Distillers Co Yeast Ltd	Improvements in or relating to the production of butyl acrylate
DE1468932B2 (de) *	1965-09-23	1976-01-22	Röhm GmbH, 6100 Darmstadt	Verfahren zur kontinuierlichen herstellung von niedermolekularen aliphatischen acrylsaeureestern
DE2226829A1 (de) *	1972-06-02	1973-12-20	Knapsack Ag	Verfahren zur herstellung von acrylsaeureestern
US3776947A (en) *	1972-10-10	1973-12-04	Nippon Catalytic Chem Ind	Continuous esterification process
DE2548561C2 (de) *	1975-10-30	1983-09-29	Hoechst Ag, 6230 Frankfurt	Verfahren zur kontinuierlichen Herstellung dioctylätherfreien 2-Äthyl- hexylacrylats
DE2552987C2 (de) *	1975-11-26	1983-09-29	Hoechst Ag, 6230 Frankfurt	Verfahren zur kontinuierlichen Herstellung ätherfreier Acrylsäurealkylester
US4733004A (en) *	1986-06-23	1988-03-22	Ashland Oil, Inc.	Continuous esterification of methacrylic acid and product recovery
FR2723089B1 (fr) *	1994-07-28	1996-09-06	Atochem Elf Sa	Procede de fabrication de l'acrylate de butyle par esterification directe
DE19510891A1 (de) *	1995-03-24	1996-09-26	Basf Ag	Verfahren zur kontinuierlicheen Herstellung von Alkylestern der (Meth)acrylsäure
DE19536178A1 (de) *	1995-09-28	1997-04-03	Basf Ag	Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure

1996
- 1996-02-06 DE DE19604252A patent/DE19604252A1/de not_active Withdrawn
1997
- 1997-01-28 US US08/791,054 patent/US5945560A/en not_active Expired - Lifetime
- 1997-01-31 TW TW860101154A patent/TW374082B/zh active
- 1997-02-04 DK DK97101728T patent/DK0795535T3/da active
- 1997-02-04 DE DE59704499T patent/DE59704499D1/de not_active Expired - Lifetime
- 1997-02-04 SG SG9700250A patent/SG85587A1/en unknown
- 1997-02-04 MX MX9700899A patent/MX9700899A/es unknown
- 1997-02-04 EP EP97101728A patent/EP0795535B1/de not_active Expired - Lifetime
- 1997-02-04 ES ES97101728T patent/ES2163671T3/es not_active Expired - Lifetime
- 1997-02-05 CN CNB971031843A patent/CN1137875C/zh not_active Expired - Lifetime
- 1997-02-05 CA CA002196915A patent/CA2196915A1/en not_active Abandoned
- 1997-02-05 MY MYPI97000436A patent/MY121248A/en unknown
- 1997-02-05 CZ CZ97335A patent/CZ33597A3/cs unknown
- 1997-02-05 JP JP9022994A patent/JPH101455A/ja not_active Withdrawn
- 1997-02-05 ID IDP970346A patent/ID15885A/id unknown
- 1997-02-05 KR KR1019970003628A patent/KR970061851A/ko not_active Ceased
- 1997-05-27 BR BR9703407A patent/BR9703407A/pt unknown

Also Published As

Publication number	Publication date
BR9703407A (pt)	1999-01-05
MY121248A (en)	2006-01-28
DE59704499D1 (de)	2001-10-11
US5945560A (en)	1999-08-31
CA2196915A1 (en)	1997-08-07
DE19604252A1 (de)	1997-08-07
EP0795535A1 (de)	1997-09-17
CN1168370A (zh)	1997-12-24
CZ33597A3 (en)	1997-09-17
CN1137875C (zh)	2004-02-11
TW374082B (en)	1999-11-11
ES2163671T3 (es)	2002-02-01
KR970061851A (ko)	1997-09-12
JPH101455A (ja)	1998-01-06
SG85587A1 (en)	2002-01-15
ID15885A (id)	1997-08-14
EP0795535B1 (de)	2001-09-05
MX9700899A (es)	1997-08-30

Publication	Publication Date	Title
DK0795535T3 (da)	2001-11-19	Fremgangsmåde og anlæg til kontinuerlig fremstilling af alkylestere af (meth)acrylsyre
DK0784046T3 (da)	2001-04-30	Fremgangsmåde til fremstilling af acrylsyre og estere deraf
SG80565A1 (en)	2001-05-22	Continuous preparation of alkyl esters of (meth)acrylic acid
SG74578A1 (en)	2000-08-22	Continuous preparation of alkyl esters of (meth) acrylic acid
SG72705A1 (en)	2000-05-23	Continuous preparation of alkyl esters of (meth)acrylic acid and apparatus for this purpose
DE69505303D1 (de)	1998-11-19	Verfahren zur Polymerisationsinhibierung von (Meth-)Acrylsäure und ihrer Ester
DE69405801D1 (de)	1997-10-30	Verfahren zur Polymerisationsinhibierung von (Meth-) Acrylsäure und ihrer Ester
DK0822935T3 (da)	2001-12-27	Fremgangsmåde til fremstilling af rene enantiomerer af tropasyreestere
DE59907520D1 (de)	2003-12-04	Verfahren zur kontinuierlichen Gewinnung von (Meth)acrylsäure
DE59405832D1 (de)	1998-06-04	Verfahren zur Reinigung von Roh-(Meth)acrylsäure
DE59904311D1 (de)	2003-03-27	Verfahren zur Herstellung von Estern der (Meth)acrylsäure
DE59910285D1 (de)	2004-09-23	Verfahren zur herstellung von (meth)acrylsäure und (meth)acrylsäureestern
DE69701590D1 (de)	2000-05-11	Verfahren zur Polymerisationsinhibierung von (Meth-)Acrylsäure und ihrer Ester
DE59602043D1 (de)	1999-07-08	Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure
DK0780359T3 (da)	2000-08-07	Fremgangsmåde til forestring af (meth)acrylsyre med en alkanol
DK0788310T3 (da)	2002-09-16	Fremgangsmåde til inhibering af plantesygdom
GB2316680B (en)	1999-12-08	Method for preparing (meth)acrylic acid ester
SG85160A1 (en)	2001-12-19	Method for production of (meth) acrylic acid and/or (meth) acrylic esters
DE69705192D1 (de)	2001-07-19	Verfahren zur Herstellung von (Meth)acrylsäure
DK0713854T3 (da)	1998-10-19	Fremgangsmåde til oprensning af rå-(meth)acrylsyre
DK0780360T3 (da)	2000-08-07	Fremgangsmåde til forestering af (meth)acrylsyre med en alkanol
DK0889873T3 (da)	2001-01-02	Fremgangsmåde til fremstilling af alkoxylerede fedtsyrealkylestere
SG50766A1 (en)	1998-07-20	Preparation of alkyl esters of (meth) acrylic acid
US5183539B1 (en)	1997-02-04	Method of purifying crude glycidyl (meth) acrylate
DK0589832T3 (da)	1999-12-20	Fremgangsmåde og anlæg til deoxidation af vand