DK1061067T3 - Fremgangsmåde til krystallisering og opsamling af basiske N-omega-trifluoracetylerede aminosyrer - Google Patents
Fremgangsmåde til krystallisering og opsamling af basiske N-omega-trifluoracetylerede aminosyrerInfo
- Publication number
- DK1061067T3 DK1061067T3 DK00120296T DK00120296T DK1061067T3 DK 1061067 T3 DK1061067 T3 DK 1061067T3 DK 00120296 T DK00120296 T DK 00120296T DK 00120296 T DK00120296 T DK 00120296T DK 1061067 T3 DK1061067 T3 DK 1061067T3
- Authority
- DK
- Denmark
- Prior art keywords
- basic
- omega
- amino acid
- basic amino
- crystallization
- Prior art date
Links
- 150000001413 amino acids Chemical class 0.000 title abstract 6
- 238000002425 crystallisation Methods 0.000 title 1
- 230000008025 crystallization Effects 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 239000007788 liquid Substances 0.000 abstract 3
- 150000002148 esters Chemical class 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000003002 pH adjusting agent Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/22—Separation; Purification; Stabilisation; Use of additives
- C07C231/24—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5184696 | 1996-03-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK1061067T3 true DK1061067T3 (da) | 2004-04-05 |
Family
ID=12898225
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK97905454T DK0826664T3 (da) | 1996-03-08 | 1997-03-06 | Fremgangsmåde til fremstilling af N-omega-trifluoracetylerede, basiske aminosyrer |
| DK00120296T DK1061067T3 (da) | 1996-03-08 | 1997-03-06 | Fremgangsmåde til krystallisering og opsamling af basiske N-omega-trifluoracetylerede aminosyrer |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK97905454T DK0826664T3 (da) | 1996-03-08 | 1997-03-06 | Fremgangsmåde til fremstilling af N-omega-trifluoracetylerede, basiske aminosyrer |
Country Status (9)
| Country | Link |
|---|---|
| EP (2) | EP1061067B1 (da) |
| JP (1) | JP3788996B2 (da) |
| AT (2) | ATE202334T1 (da) |
| DE (2) | DE69705275T2 (da) |
| DK (2) | DK0826664T3 (da) |
| ES (2) | ES2209744T3 (da) |
| PT (1) | PT1061067E (da) |
| SG (1) | SG82013A1 (da) |
| WO (1) | WO1997032841A1 (da) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU3075300A (en) * | 1999-01-21 | 2000-08-07 | Kaneka Corporation | Method for isolation of n-protected s-phenylcysteine |
| CN105348134B (zh) * | 2015-12-09 | 2017-06-06 | 九江天赐高新材料有限公司 | 一种n‑酰基氨基酸的精制纯化方法 |
| CN111470993A (zh) * | 2020-05-22 | 2020-07-31 | 安徽安力肽生物科技有限公司 | 一种不结块Beta-丙氨酸制备方法 |
| CN118108617B (zh) * | 2024-03-05 | 2024-10-15 | 山东极地医药科技有限公司 | 一种三氟乙酰赖氨酸的生产工艺 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1080564B (de) * | 1959-02-17 | 1960-04-28 | Hoechst Ag | Verfahren zur N-Trifluoracetylierung von Aminosaeuren und Peptiden |
| JPS62226952A (ja) * | 1986-03-27 | 1987-10-05 | Kanegafuchi Chem Ind Co Ltd | Nω−トリフルオロアセチル−アミノ酸の製造方法 |
| FR2609985B1 (fr) * | 1987-01-26 | 1989-04-14 | Rhone Poulenc Chimie | Procede de n-o trifluoroacetylation des a, o diaminoacides monocarboxyliques aliphatiques satures |
-
1997
- 1997-03-06 DK DK97905454T patent/DK0826664T3/da active
- 1997-03-06 WO PCT/JP1997/000690 patent/WO1997032841A1/ja not_active Ceased
- 1997-03-06 DE DE69705275T patent/DE69705275T2/de not_active Expired - Fee Related
- 1997-03-06 EP EP00120296A patent/EP1061067B1/en not_active Expired - Lifetime
- 1997-03-06 EP EP97905454A patent/EP0826664B1/en not_active Revoked
- 1997-03-06 PT PT00120296T patent/PT1061067E/pt unknown
- 1997-03-06 AT AT97905454T patent/ATE202334T1/de not_active IP Right Cessation
- 1997-03-06 DE DE1997627324 patent/DE69727324T2/de not_active Expired - Fee Related
- 1997-03-06 JP JP53167097A patent/JP3788996B2/ja not_active Expired - Fee Related
- 1997-03-06 AT AT00120296T patent/ATE258162T1/de not_active IP Right Cessation
- 1997-03-06 DK DK00120296T patent/DK1061067T3/da active
- 1997-03-06 ES ES00120296T patent/ES2209744T3/es not_active Expired - Lifetime
- 1997-03-06 ES ES97905454T patent/ES2157555T3/es not_active Expired - Lifetime
- 1997-03-06 SG SG9903657A patent/SG82013A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DK0826664T3 (da) | 2001-09-03 |
| JP3788996B2 (ja) | 2006-06-21 |
| ATE202334T1 (de) | 2001-07-15 |
| SG82013A1 (en) | 2001-07-24 |
| DE69705275T2 (de) | 2002-05-16 |
| DE69705275D1 (de) | 2001-07-26 |
| ATE258162T1 (de) | 2004-02-15 |
| EP0826664B1 (en) | 2001-06-20 |
| EP1061067A2 (en) | 2000-12-20 |
| ES2157555T3 (es) | 2001-08-16 |
| WO1997032841A1 (en) | 1997-09-12 |
| PT1061067E (pt) | 2004-06-30 |
| EP0826664A1 (en) | 1998-03-04 |
| DE69727324T2 (de) | 2004-11-18 |
| DE69727324D1 (de) | 2004-02-26 |
| EP1061067A3 (en) | 2001-01-17 |
| ES2209744T3 (es) | 2004-07-01 |
| EP0826664A4 (en) | 1998-04-29 |
| EP1061067B1 (en) | 2004-01-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0220958A2 (en) | Selective chemical removal of a protein amino-terminal residue | |
| OTSUKA et al. | Synthetic studies on an antitumor antibiotic, Bleomycin. XII. Preparation of an l-2, 3-diaminopropionic acid derivative as a synthetic intermediate | |
| Olsen et al. | Synthesis of N. alpha., N. delta.-protected N. delta.-hydroxy-L-ornithine from L-glutamic acid | |
| US4782139A (en) | Selective chemical removal of a protein amino-terminal residue | |
| Valerio et al. | Synthesis of peptide analogues using the multipin peptide synthesis method | |
| EP0335483A3 (en) | Condensed imidazole derivatives, process and intermediates for their preparation and pharmaceutical compositions containing them. | |
| ATE278650T1 (de) | Ein verfahren zur herstellung von carbonsäure- derivaten und ein kondensationshilfsmittel mit einem quarternären ammonium-salz | |
| CA1326036C (en) | Process for the production of alkali metal salts of 2-pyrrolidon-5-carboxylic acid | |
| DE58904546D1 (de) | 1-chlorpyrimidinyl-1h-1,2,4-triazol-3-sulfonsaeureamide, verfahren zu ihrer herstellung und ihre verwendung als mittel mit herbizider wirkung. | |
| DK1061067T3 (da) | Fremgangsmåde til krystallisering og opsamling af basiske N-omega-trifluoracetylerede aminosyrer | |
| DK159441C (da) | 11-substituerede 5,11-dihydro-6h-dibenz(b,e)azepin-6-on-derivater, laegemidler indeholdende disse forbindelser og analogifremgangsmaade til forbindelsernes fremstilling | |
| Nielsen et al. | Reagents for photoaffinity labeling. I. Photobinding efficiency of aryl azido-, diazocyclopentadienyl-and ethyl diazomalonyl-derivatives of 9-aminoacridine | |
| US4921971A (en) | Method of preparing alkaline earth metal salts of 2-pyrrolidone-5-carboxylic acid | |
| Schneider et al. | Synthesis of D-leucine-oxytocin, a biologically active diastereoisomer of oxytocin, and demonstration of its separability from oxytocin upon countercurrent distribution | |
| DE69513673D1 (de) | Verfahren zur herstellung von cyclopropancarbonsäure und ihre derivaten | |
| Ghosh et al. | One pot amide/peptide synthesis via two redox reactions | |
| Sypniewski et al. | (R)-tert-Butoxycarbonylamino-fluorenylmethoxycarbonyl-glycine from (S)-Benzyloxycarbonyl-serine or from Papain Resolution of the Corresponding Amide or Methyl Ester | |
| O'donnell et al. | Synthetic of α-Methylhistidine by Catalytic Phase-Transfer Alkylations | |
| Kessler et al. | 4-Diazocyclohexa-2, 5-dienones as photoaffinity reagents for proteins | |
| Cheikh et al. | Polymerization of amino acids containing nucleotide bases | |
| NO874374L (no) | Fremstilling av peptid-aminoalkylamider og peptid-hydrazider ved hjelp av fastfasemetoden. | |
| Steinfeld et al. | Anticandidal activity of 5-fluorocytosine-peptide conjugates | |
| Jiang et al. | Kinetic and mechanistic investigation of the selective acidolysis of the C‐terminal amide bond of N‐acyl‐N, α, α‐trialkyl glycine amides | |
| Irie et al. | Validity of Methoxycarbonyl as an N-Protecting Group in Peptide Synthesis: New Synthesis of MSH-Release Inhibiting Factor | |
| RU2227141C2 (ru) | Способ получения соединения бензиламина |