DK1165231T3 - Nikkelkatalysator til hydrogenering af funktionelle grupper og fremgangsmåde til fremstilling heraf - Google Patents

Nikkelkatalysator til hydrogenering af funktionelle grupper og fremgangsmåde til fremstilling heraf

Info

Publication number
DK1165231T3
DK1165231T3 DK00909274T DK00909274T DK1165231T3 DK 1165231 T3 DK1165231 T3 DK 1165231T3 DK 00909274 T DK00909274 T DK 00909274T DK 00909274 T DK00909274 T DK 00909274T DK 1165231 T3 DK1165231 T3 DK 1165231T3
Authority
DK
Denmark
Prior art keywords
hydrogenation
processes
preparation
functional groups
nickel catalyst
Prior art date
Application number
DK00909274T
Other languages
English (en)
Inventor
Peter Birke
Reinhard Geyer
Peter Kraak
Rainer Schoedel
Original Assignee
Kataleuna Gmbh Catalysts
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kataleuna Gmbh Catalysts filed Critical Kataleuna Gmbh Catalysts
Application granted granted Critical
Publication of DK1165231T3 publication Critical patent/DK1165231T3/da

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/755—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J33/00—Protection of catalysts, e.g. by coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B01J35/393—Metal or metal oxide crystallite size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/396—Distribution of the active metal ingredient
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • B01J35/77—Compounds characterised by their crystallite size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/031—Precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B01J37/18—Reducing with gases containing free hydrogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DK00909274T 1999-03-03 2000-03-01 Nikkelkatalysator til hydrogenering af funktionelle grupper og fremgangsmåde til fremstilling heraf DK1165231T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19909177A DE19909177A1 (de) 1999-03-03 1999-03-03 Katalysator zur Hydrierung funktioneller Gruppen und Verfahren zu seiner Herstellung
PCT/EP2000/001708 WO2000051727A1 (de) 1999-03-03 2000-03-01 Nickel-katalysator zur hydrierung funktioneller gruppen und verfahren zu seiner herstellung

Publications (1)

Publication Number Publication Date
DK1165231T3 true DK1165231T3 (da) 2004-03-01

Family

ID=7899484

Family Applications (1)

Application Number Title Priority Date Filing Date
DK00909274T DK1165231T3 (da) 1999-03-03 2000-03-01 Nikkelkatalysator til hydrogenering af funktionelle grupper og fremgangsmåde til fremstilling heraf

Country Status (8)

Country Link
US (1) US6677271B1 (da)
EP (1) EP1165231B1 (da)
JP (1) JP4711513B2 (da)
KR (1) KR100606990B1 (da)
CN (1) CN1125678C (da)
DE (2) DE19909177A1 (da)
DK (1) DK1165231T3 (da)
WO (1) WO2000051727A1 (da)

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DE10224802A1 (de) * 2002-05-23 2003-12-11 Messer Griesheim Gmbh Nickelhaltige Gasreinigungsmasse
US6995115B2 (en) * 2003-09-23 2006-02-07 Catalytic Materials, Llc Catalyst for the generation of CO-free hydrogen from methane
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US8981155B2 (en) 2010-12-06 2015-03-17 Basf Se Process for preparing aromatic amines
KR20140015473A (ko) 2011-03-16 2014-02-06 바스프 에스이 니트로방향족의 수소화에 의해 방향족 아민을 제조하는 방법을 위한 반응물의 최적 계량
US8835688B2 (en) 2011-03-16 2014-09-16 Basf Se Optimized introduction of the starting materials for a process for preparing aromatic amines by hydrogenation of nitroaromatics
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US8895783B2 (en) 2012-02-07 2014-11-25 Basf Se Monitoring of the stoichiometric ratio in the reaction of nitroaromatics with hydrogen
US9295971B2 (en) 2013-01-11 2016-03-29 Basf Se Apparatus and process for the continuous reaction of liquids with gases
US9302237B2 (en) 2013-01-11 2016-04-05 Basf Se Apparatus and process for the continuous reaction of liquids with gases
WO2014108351A1 (de) 2013-01-11 2014-07-17 Basf Se Vorrichtung und verfahren zur kontinuierlichen umsetzung von flüssigkeiten mit gasen
CN103288608B (zh) * 2013-05-29 2016-03-30 扬州大学 纳米氧化镍催化醇类物质选择性氧化的新方法
DE102013214229A1 (de) * 2013-07-19 2015-01-22 Bayer Materialscience Ag Verfahren zur Herstellung eines effizienten Katalysators für die Produktion mehrwandiger Kohlenstoffnanoröhrchen, mehrwandiges Kohlenstoffnanoröhrchen und Kohlenstoffnanoröhrchenpulver
EP3445488A1 (en) * 2016-04-22 2019-02-27 INVISTA Textiles (U.K.) Limited Heterogeneous catalyst process and nickel catalyst
CN109803949B (zh) 2016-10-10 2023-04-14 巴斯夫欧洲公司 在硝基化合物的连续液相氢化中使用碱金属离子、碱土金属离子或稀土金属离子进行催化剂改性
CN107011107A (zh) * 2017-05-16 2017-08-04 中国科学技术大学 一种采用负载型金属催化剂制备醇的方法
EP3697753B1 (de) 2017-10-16 2025-10-01 Basf Se Erhöhung der katalysatorselektivität bei der kontinuierlichen hydrierung von nitroverbindungen durch zugabe von ammoniak
CN108525669B (zh) * 2018-05-04 2020-11-13 贵州大学 一种高度分散二氧化硅纳米管负载镍催化剂及其制备方法
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US20240226858A1 (en) * 2021-05-06 2024-07-11 Basf Se A catalytic material suitable for hydrogenation reactions comprising ni, one or more additional metals m, and a specific oxidic support material
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Also Published As

Publication number Publication date
KR20010113721A (ko) 2001-12-28
KR100606990B1 (ko) 2006-07-31
CN1349433A (zh) 2002-05-15
EP1165231A1 (de) 2002-01-02
DE19909177A1 (de) 2000-09-07
JP2002537973A (ja) 2002-11-12
JP4711513B2 (ja) 2011-06-29
DE50004157D1 (de) 2003-11-27
EP1165231B1 (de) 2003-10-22
US6677271B1 (en) 2004-01-13
CN1125678C (zh) 2003-10-29
WO2000051727A1 (de) 2000-09-08

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