DK2038388T3 - Fremgangsmåde til ekstraktion af vandig olie fra oliefrø-udgangsmateriale - Google Patents
Fremgangsmåde til ekstraktion af vandig olie fra oliefrø-udgangsmateriale Download PDFInfo
- Publication number
- DK2038388T3 DK2038388T3 DK07763817.9T DK07763817T DK2038388T3 DK 2038388 T3 DK2038388 T3 DK 2038388T3 DK 07763817 T DK07763817 T DK 07763817T DK 2038388 T3 DK2038388 T3 DK 2038388T3
- Authority
- DK
- Denmark
- Prior art keywords
- oil
- slurry
- protein
- starting material
- water
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 65
- 239000007858 starting material Substances 0.000 title claims description 30
- 239000002002 slurry Substances 0.000 claims description 62
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 57
- 102000004169 proteins and genes Human genes 0.000 claims description 56
- 108090000623 proteins and genes Proteins 0.000 claims description 56
- 239000007787 solid Substances 0.000 claims description 42
- 235000004977 Brassica sinapistrum Nutrition 0.000 claims description 32
- 239000007788 liquid Substances 0.000 claims description 24
- 238000000605 extraction Methods 0.000 claims description 23
- 235000014698 Brassica juncea var multisecta Nutrition 0.000 claims description 21
- 235000006008 Brassica napus var napus Nutrition 0.000 claims description 21
- 235000006618 Brassica rapa subsp oleifera Nutrition 0.000 claims description 21
- 244000188595 Brassica sinapistrum Species 0.000 claims description 21
- 239000003960 organic solvent Substances 0.000 claims description 21
- 240000002791 Brassica napus Species 0.000 claims description 13
- 239000011343 solid material Substances 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 8
- 238000005119 centrifugation Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000004925 denaturation Methods 0.000 claims description 4
- 230000036425 denaturation Effects 0.000 claims description 4
- 230000001376 precipitating effect Effects 0.000 claims description 4
- 244000068988 Glycine max Species 0.000 claims description 3
- 235000010469 Glycine max Nutrition 0.000 claims description 3
- 244000000231 Sesamum indicum Species 0.000 claims description 3
- 235000003434 Sesamum indicum Nutrition 0.000 claims description 3
- 235000004426 flaxseed Nutrition 0.000 claims description 3
- MJYQFWSXKFLTAY-OVEQLNGDSA-N (2r,3r)-2,3-bis[(4-hydroxy-3-methoxyphenyl)methyl]butane-1,4-diol;(2r,3r,4s,5s,6r)-6-(hydroxymethyl)oxane-2,3,4,5-tetrol Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O.C1=C(O)C(OC)=CC(C[C@@H](CO)[C@H](CO)CC=2C=C(OC)C(O)=CC=2)=C1 MJYQFWSXKFLTAY-OVEQLNGDSA-N 0.000 claims 2
- 229920000742 Cotton Polymers 0.000 claims 2
- 244000299507 Gossypium hirsutum Species 0.000 claims 2
- 244000020551 Helianthus annuus Species 0.000 claims 2
- 235000003222 Helianthus annuus Nutrition 0.000 claims 2
- 239000003921 oil Substances 0.000 description 96
- 235000019198 oils Nutrition 0.000 description 96
- 239000007791 liquid phase Substances 0.000 description 21
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 18
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 239000012071 phase Substances 0.000 description 18
- 235000019784 crude fat Nutrition 0.000 description 17
- 238000011084 recovery Methods 0.000 description 17
- 239000000284 extract Substances 0.000 description 16
- 238000011282 treatment Methods 0.000 description 14
- 239000000463 material Substances 0.000 description 9
- 238000000926 separation method Methods 0.000 description 9
- 239000002904 solvent Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 7
- 102000004190 Enzymes Human genes 0.000 description 6
- 108090000790 Enzymes Proteins 0.000 description 6
- 239000012634 fragment Substances 0.000 description 6
- 238000010979 pH adjustment Methods 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- 210000004027 cell Anatomy 0.000 description 5
- 239000000835 fiber Substances 0.000 description 5
- 238000012986 modification Methods 0.000 description 5
- 230000004048 modification Effects 0.000 description 5
- 230000006920 protein precipitation Effects 0.000 description 5
- 238000007906 compression Methods 0.000 description 4
- 230000006835 compression Effects 0.000 description 4
- 230000000593 degrading effect Effects 0.000 description 4
- 235000013372 meat Nutrition 0.000 description 4
- 238000003825 pressing Methods 0.000 description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 description 4
- 240000006240 Linum usitatissimum Species 0.000 description 3
- 235000004431 Linum usitatissimum Nutrition 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 235000019197 fats Nutrition 0.000 description 3
- 150000002632 lipids Chemical class 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000008188 pellet Substances 0.000 description 3
- 239000006228 supernatant Substances 0.000 description 3
- 235000011293 Brassica napus Nutrition 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 230000001143 conditioned effect Effects 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000000194 supercritical-fluid extraction Methods 0.000 description 2
- 235000009027 Amelanchier alnifolia Nutrition 0.000 description 1
- 244000068687 Amelanchier alnifolia Species 0.000 description 1
- 108091005658 Basic proteases Proteins 0.000 description 1
- 235000011331 Brassica Nutrition 0.000 description 1
- 241000219198 Brassica Species 0.000 description 1
- 235000003255 Carthamus tinctorius Nutrition 0.000 description 1
- 244000020518 Carthamus tinctorius Species 0.000 description 1
- 229920000715 Mucilage Polymers 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 210000003850 cellular structure Anatomy 0.000 description 1
- 238000010960 commercial process Methods 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000011534 incubation Methods 0.000 description 1
- 239000002198 insoluble material Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 230000002934 lysing effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 229940064639 minipress Drugs 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- WFXFYZULCQKPIP-UHFFFAOYSA-N prazosin hydrochloride Chemical compound [H+].[Cl-].N=1C(N)=C2C=C(OC)C(OC)=CC2=NC=1N(CC1)CCN1C(=O)C1=CC=CO1 WFXFYZULCQKPIP-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000000135 prohibitive effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 230000003381 solubilizing effect Effects 0.000 description 1
- 239000002195 soluble material Substances 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000002569 water oil cream Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biochemistry (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
- Peptides Or Proteins (AREA)
Claims (13)
1. Fremgangsmåde til vandig ekstraktion af en olie fra et oliefrø-udgangsmateriale uden anvendelse af et organisk opløsningsmiddel omfattende de følgende trin: (a) at uddrive et oliefrø-udgangsmateriale for at fremstille en olie og et faststofmateriale, der indeholder restolie; (b) at opslæmme faststofmaterialet med vand for at danne en opslæmning; (c) at tilsætte tilstrækkelig alkalisk forbindelse til opslæmningen for at øge opslæmningens pH-værdi til en pH-værdi på 8 eller højere; (d) at fraseparere opslæmningen til en uopløselig protein-beriget fraktion og en flydende olie-i-vand-fase; og (e) at fraseparere olien fra den flydende olie-i-vand-fase, hvor oliefrø-udgangsmaterialet er udvalgt blandt sojabønne, raps og rapsfrø, solsikke, bomuldsfrø, sesam og hørfrø.
2. Fremgangsmåde ifølge krav 1 omfattende de yderligere følgende trin: (f) at udfælde opløseligt protein fra opslæmningen i trin (c); (g) at fraseparere det udfældede opløselige protein fra opslæmningen med den uopløselige protein-berigede fraktion, i trin (d).
3. Fremgangsmåde til vandig ekstraktion af en olie fra et oliefrø-udgangsmateriale uden anvendelse af et organisk opløsningsmiddel omfattende de følgende trin: (a) at uddrive et oliefrø-udgangsmateriale for at fremstille en olie og et faststofmateriale, der indeholder restolie; (b) at opslæmme faststofmaterialet med vand for at danne en opslæmning; (c) at fjerne fibrøse faststoffer fra opslæmningen i trin (b) for at generere en fibrøs fraktion og et protein plus flydende olie-i-vand-fase; (d) at tilsætte tilstrækkelig alkalisk forbindelse til proteinet plus flydende olie-i-vand-fase i trin (c) for at øge pH-værdien til en pH-værdi på 8 eller højere; (e) at fraseparere opslæmningen fra trin (d) til en uopløselig protein-beriget fraktion og en flydende olie-i-vand-fase; og (f) at fraseparere olien fra den flydende olie-i-vand-fase i trin (e), hvor oliefrøudgangsmaterialet er udvalgt blandt sojabønne, raps og rapsfrø, solsikke, bomuldsfrø, sesam og hørfrø.
4. Fremgangsmåde ifølge krav 3 omfattende de yderligere følgende trin: (g) at udfælde opløseligt protein fra opslæmningen i trin (d); (h) at fraseparere det udfældede opløselige protein med det den uopløselige protein-berigede fraktion, i trin (e).
5. Fremgangsmåde ifølge krav 2 eller 4, hvor proteinet udfældes ved varme-induceret denaturering.
6. Fremgangsmåde ifølge et af kravene 1-5, hvor den protein-berigede fraktion frasepareres ved centrifugering.
7. Fremgangsmåde ifølge et af kravene 1-5, hvor den protein-berigede fraktion frasepareres ved filtrering.
8. Fremgangsmåde ifølge et af kravene 1-7, hvor et forhold mellem vand og fast materiale i trin (b) er lig med eller større end mellem ca. 3,5-7:1.
9. Fremgangsmåde ifølge krav 8, hvor et forhold mellem vand og fast materiale i trin (b) er ca. 5:1.
10. Fremgangsmåde ifølge et af kravene 1-8, hvor den alkaliske forbindelse tilsættes for at øge pFI-værdien af opslæmningen til en pFI-værdi på 9.
11. Fremgangsmåde ifølge et af kravene 1-8, hvor den alkaliske forbindelse tilsættes for at øge pFI-værdien af opslæmningen til en pFI-værdi på 10.
12. Fremgangsmåde ifølge et af kravene 1-11, hvor oliefrø-udgangsmaterialet er rapsfrø.
13. Fremgangsmåde ifølge et af kravene 1-11, hvor oliefrø-udgangsmaterialet er raps.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA002551070A CA2551070A1 (en) | 2006-06-27 | 2006-06-27 | Process for aqueous oil extraction from oilseed starting material |
| PCT/CA2007/001147 WO2008000077A1 (en) | 2006-06-27 | 2007-06-27 | Process for aqueous oil extraction from oilseed starting material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK2038388T3 true DK2038388T3 (da) | 2015-12-07 |
Family
ID=38834876
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK07763817.9T DK2038388T3 (da) | 2006-06-27 | 2007-06-27 | Fremgangsmåde til ekstraktion af vandig olie fra oliefrø-udgangsmateriale |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20100040748A1 (da) |
| EP (1) | EP2038388B1 (da) |
| AU (1) | AU2007264359B9 (da) |
| CA (2) | CA2551070A1 (da) |
| DK (1) | DK2038388T3 (da) |
| ES (1) | ES2555178T3 (da) |
| PL (1) | PL2038388T3 (da) |
| WO (1) | WO2008000077A1 (da) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9155323B2 (en) | 2009-05-15 | 2015-10-13 | Siebte Pmi Verwaltungs Gmbh | Aqueous process for preparing protein isolate and hydrolyzed protein from an oilseed |
| CA2961573C (en) * | 2014-09-18 | 2023-01-24 | Dsm Ip Assets B.V. | Method for producing an oil seed protein mix |
| CN113278463A (zh) * | 2021-04-27 | 2021-08-20 | 东北农业大学 | 一种利用水酶法制备核桃油副产物水包油乳液的方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3732108A (en) * | 1971-12-17 | 1973-05-08 | Canadian Patents Dev | Recovery of and seed meat from thioglucoside-containing oilseed |
| US3865802A (en) * | 1972-08-08 | 1975-02-11 | Us Agriculture | Process for obtaining full-fat oilseed-protein beverages using water and initial acid pH |
| US4188399A (en) * | 1974-12-23 | 1980-02-12 | Miles Laboratories, Inc. | Process for preparing a heat coagulable viscous protein |
| IE43623B1 (en) * | 1975-09-18 | 1981-04-22 | Taylor P Co Inc | Improvements in or relating to edible oilseed extracts |
| CA1099576A (en) * | 1978-03-23 | 1981-04-21 | Chester D. Myers | Improved process for isolation of proteins |
| US4361081A (en) * | 1980-08-11 | 1982-11-30 | Howard James R | Apparatus for processing oilseed and grain mash products |
| US4530788A (en) * | 1982-12-03 | 1985-07-23 | Stauffer Chemical Company | Oil seed proteins evidencing improved functionality |
| US5035910A (en) * | 1990-02-14 | 1991-07-30 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Agricuture | Separation of oilseed components in solvent phase |
| FI100089B (fi) * | 1995-01-20 | 1997-09-30 | Markku Anttila | Pellavavalmiste, sen käyttö ja valmistus |
| US5936069A (en) * | 1995-12-06 | 1999-08-10 | Iowa State University Research Foundation | Process for producing improved soy protein concentrate from genetically-modified soybeans |
| US5934188A (en) * | 1997-01-14 | 1999-08-10 | Pioneer Hi-Bred International, Inc. | Oilseed press |
| SE524075C2 (sv) * | 2001-10-04 | 2004-06-22 | Bjurenvall Ingemar | Förfarande för fraktionering av oljefröpresskakor och mjöl |
| CA2363451C (en) * | 2001-11-20 | 2005-05-10 | Mcn Bioproducts Inc. | Oilseed processing |
| US20070207254A1 (en) * | 2006-03-03 | 2007-09-06 | Specialty Protein Producers, Inc. | Methods of separating fat from soy materials and compositions produced therefrom |
-
2006
- 2006-06-27 CA CA002551070A patent/CA2551070A1/en not_active Abandoned
-
2007
- 2007-06-27 US US12/305,343 patent/US20100040748A1/en not_active Abandoned
- 2007-06-27 AU AU2007264359A patent/AU2007264359B9/en not_active Ceased
- 2007-06-27 CA CA2653743A patent/CA2653743C/en active Active
- 2007-06-27 PL PL07763817T patent/PL2038388T3/pl unknown
- 2007-06-27 WO PCT/CA2007/001147 patent/WO2008000077A1/en not_active Ceased
- 2007-06-27 DK DK07763817.9T patent/DK2038388T3/da active
- 2007-06-27 EP EP07763817.9A patent/EP2038388B1/en active Active
- 2007-06-27 ES ES07763817.9T patent/ES2555178T3/es active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2038388A4 (en) | 2010-09-22 |
| CA2551070A1 (en) | 2007-12-27 |
| CA2653743A1 (en) | 2008-01-03 |
| US20100040748A1 (en) | 2010-02-18 |
| ES2555178T3 (es) | 2015-12-29 |
| EP2038388B1 (en) | 2015-09-16 |
| AU2007264359B9 (en) | 2014-01-23 |
| CA2653743C (en) | 2014-12-23 |
| EP2038388A1 (en) | 2009-03-25 |
| PL2038388T3 (pl) | 2016-04-29 |
| WO2008000077A1 (en) | 2008-01-03 |
| AU2007264359A1 (en) | 2008-01-03 |
| AU2007264359B2 (en) | 2013-12-05 |
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