DK2770017T3 - Ny overfladebehandling af hvide mineralmaterialer til anvendelse i plast - Google Patents
Ny overfladebehandling af hvide mineralmaterialer til anvendelse i plast Download PDFInfo
- Publication number
- DK2770017T3 DK2770017T3 DK13156349.6T DK13156349T DK2770017T3 DK 2770017 T3 DK2770017 T3 DK 2770017T3 DK 13156349 T DK13156349 T DK 13156349T DK 2770017 T3 DK2770017 T3 DK 2770017T3
- Authority
- DK
- Denmark
- Prior art keywords
- phosphoric acid
- ester
- mineral material
- white mineral
- containing particles
- Prior art date
Links
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
- C08J2323/04—Homopolymers or copolymers of ethene
- C08J2323/06—Polyethene
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Claims (16)
1. Polymersammensætning omfattende a) mindst et polymerresin, og b) fra 0,1 til 95 vægtprocent, baseret på den samlede vægt af polymersammensætningen, af mindst et overfladereaktivt hvidt mineralmateriale, hvor det mindst ene overfladereaktive hvide mineralmateriale i) omfatter overfladereaktive hvide mineralmateriale-indeholdende partikler har en vægtgennemsnitlig partikelstørrelse cfeo på < 7,5 pm, og har en opløselighed i vand ved 20 °C (± 2 °C) på under 0,1 vægtprocent, baseret på den samlede tørvægt af de overfladereaktive hvide mineralmateriale-indeholdende partikler, ii) har en fugtopsamlingsmodtagelighed på < 0,8 mg/g, iii) har en svingende starttemperatur på > 250 °C, og iv) har en hydrofilicitet på under 8 : 2 volumetrisk forhold afvand : ethanol målt ved +23 °C (± 2 °C) med sedimentationsfremgangsmåden, hvor det mindst ene overfladereaktive hvide mineralmateriale omfattende på mindst en del af overfladen af de overfladereaktive hvide mineralmateriale-indeholdende partikler en fosforsyreesterblanding af en eller flere fosforsyremonoester og saltede reaktionsprodukter deraf og en eller flere fosforsyre di-ester og saltede reaktionsprodukter deraf, hvor molforholdet mellem den ene eller flere fosforsyremonoester og saltede reaktionsprodukter deraf og den ene eller flere fosforsyre di-ester og saltede reaktionsprodukter deraf i fosforsyreesterblandingen er fra 1:1 til 1:100 og hvor det mindst ene overfladereaktive hvide mineralmateriale omfatter fosforsyreesterblandingen i en mængde på mindst 0,1 vægtprocent, baseret på den samlede tørvægt af det mindst ene overfladereaktive hvide mineralmateriale.
2. Polymersammensætningen ifølge krav 1, hvor de overfladereaktive hvide mineralmateriale-indeholdende partikler af det mindst ene overfladereaktive hvide mineralmateriale er mineral partikler har en klarhed på mindst 70 % målt i forhold til DIN 53163, fortrinsvis de overfladereaktive hvide mineralmateriale-indeholdende partikler af det mindst ene overfladereaktive hvide mineralmateriale er calciumkarbonat-indeholdende partikler, mere fortrinsvis de calciumkarbonat-indeholdende partikler af det mindst ene overfladereaktive hvide mineralmateriale er valgt fra blandt formalet calciumkarbonat (GCC), præcipiteret calciumkarbonat (PCC) og blandinger deraf.
3. Polymersammensætningen ifølge et hvilket som helst af de foregående krav, hvor det mindst ene overfladereaktive hvide mineralmateriale omfatter i) overfladereaktive hvide mineralmateriale-indeholdende partikler i en mængde på > 90 vægtprocent, fortrinsvis på > 95 vægtprocent og mest fortrinsvis på > 97.5 vægtprocent, baseret på den samlede tørvægt af det mindst ene overfladereaktive hvide mineralmateriale, og/eller ii) fosforsyreesterblandingen i en mængde på fra 0,1 til 5 vægtprocent, fortrinsvis på fra 0,2 til 3 vægtprocent og mest fortrinsvis på fra 0,3 til 2 vægtprocent, baseret på den samlede tørvægt af det mindst ene overfladereaktive hvide mineralmateriale.
4. Polymersammensætningen ifølge et hvilket som helst af de foregående krav, hvor molforholdet af den ene eller flere fosforsyremonoester og saltede reaktionsprodukter deraf til den ene eller flere fosforsyre di-ester og saltede reaktionsprodukter deraf i fosforsyreesterbland ingen er fra 1 : 1,1 til 1 : 80, fortrinsvis fra 1 : 1,1 til 1 : 60, mere fortrinsvis fra 1:1,1 1 til 1 : 40, endnu mere fortrinsvis fra 1 : 1,1 til 1 : 20 og mest fortrinsvis fra 1 : 1,1 til 1 : 10.
5. Polymersammensætningen ifølge et hvilket som helst af de foregående krav, hvor fosforsyreesterblandingen yderligere omfatter en eller flere fosforsyre tri-ester og/eller fosforsyre og saltede reaktionsprodukter deraf.
6. Polymersammensætningen ifølge et hvilket som helst af de foregående krav, hvor i) den ene eller flere fosforsyremonoester består af et o-fosforsyre molekyle mono-esterificeret med et alkoholmolekyle valgt fra umættede eller mættede, forgrenede eller lineære, alifatiske eller aromatiske alkoholer med en samlet mængde af kulstofatomer fra C6 til C30, fortrinsvis fra C8 til C22, mere fortrinsvis fra C8 til C20 og mest fortrinsvis fra C8 til C18 i alkoholsubstituenten, og/eller ii) den ene eller flere fosforsyre di-ester består af et o-fosforsyremolekyle di-esterificeret med to alkoholmolekyler valgt fra den samme eller en anden, umættede eller mættede, forgrenede eller lineære, alifatiske eller aromatiske fedtalkoholer med en samlet mængde af kulstofatomer fra C6 til C30, fortrinsvis fra C8 til C22, mere fortrinsvis fra C8 til C20 og mest fortrinsvis fra C8 til C18 i alkoholsubstituenten, og/eller iii) den ene eller flere fosforsyre tri-ester består af et o-fosforsyremolekyle tri-esterificeret med tre alkoholmolekyler valgt fra den samme eller en anden, umættede eller mættede, forgrenede eller lineære, alifatiske eller aromatiske fedtalkoholer med en samlet mængde af kulstofatomer fra C6 til C30, fortrinsvis fra C8 til C22, mere fortrinsvis fra C8 til C20 og mest fortrinsvis fra C8 til C18 i alkoholsubstituenten.
7. Polymersammensætningen ifølge et hvilket som helst af de foregående krav, hvor fosforsyreesterblandingen omfatter saltede reaktionsprodukter såsom en eller flere strontium-, calcium-, magnesium- og/eller aluminiumsalte af fosforsyre mono-esters og en eller flere strontium-, calcium-, magnesium- og/eller aluminiumsalte af fosforsyre di-ester og eventuelt en eller flere strontium-, calcium-, magnesium- og/eller aluminiumsalte af fosforsyre.
8. Polymersammensætningen ifølge et hvilket som helst af de foregående krav, hvor det mindst ene polymerresin er mindst en termoplastisk polymer, fortrinsvis en termoplastisk polymer valgt fra gruppen omfattende homopolymerer og/eller copolymerer af polyolefiner, polyamideer, halogen-indeholdende polymerer og/eller polyestere.
9. Fremgangsmåde til fremstilling af et overfladereaktivt hvidt mineralmateriale ifølge et hvilket som helst af kravene 1 til 7, fremgangsmåden omfattende trinnene: (a) at tilvejebringe overfladereaktive hvide mineralmateriale-indeholdende partikler med en vægtgennemsnitlig partikelstørrelse cfeo på < 7,5 pm, og med en opløselighed i vand ved 20 °C (± 2 °C) på under 0,1 vægtprocent, baseret på den samlede tørvægt af de overfladereaktive hvide mineralmateriale-indeholdende partikler, ifølge et hvilket som helst af kravene 1 eller 2; (b) at tilvejebringe en fosforsyreesterblanding omfattende en eller flere fosforsyremonoester og en eller flere fosforsyre di-ester, og eventuelt en eller flere fosforsyre tri-ester og/eller fosforsyre, hvor molforholdet af den ene eller flere fosforsyremonoester til den ene eller flere fosforsyre di-ester i fosforsyreesterblandingen er fra 1:1 til 1:100; (c) at bringe i kontakt de overfladereaktive hvide mineralmateriale-indeholdende partikler af trin (a), i et eller flere trin, med fosforsyreesterblandingen af trin (b) således at en fosforsyreesterblanding omfattende en eller flere fosforsyremonoester og saltede reaktionsprodukter deraf og en eller flere fosforsyre di-ester og saltede reaktionsprodukter deraf og eventuelt en eller flere fosforsyre tri-ester og/eller fosforsyre og saltede reaktionsprodukter deraf dannes på mindst en del af overfladen af de overfladereaktive hvide mineralmateriale-indeholdende partikler af trin (a); hvor, før og/eller under trin (c), temperaturen justeres således at fosforsyreesterblandingen af trin (b) er flydende.
10. Fremgangsmåden ifølge krav 9, hvor at bringe de overfladereaktive hvide mineralmateriale-indeholdende partikler i kontakt med fosforsyreesterblandingen ifølge trin (c) udføres ved en temperatur på fra 20 til 200 °C, fortrinsvis på fra 90 til 200 °C, mere fortrinsvis på fra 100 til 150 °C og mest fortrinsvis på fra 110 til 130 °C.
11. Fremgangsmåden ifølge krav 9 eller 10, hvor i) den ene eller flere fosforsyremonoester består af et o-fosforsyremolekyle mono-esterificeret med et alkoholmolekyle valgt fra umættede eller mættede, forgrenede eller lineære, alifatiske eller aromatiske alkoholer med en samlet mængde af kulstofatomer fra C6 til C30, fortrinsvis fra C8 til C22, mere fortrinsvis fra C8 til C20 og mest fortrinsvis fra C8 til C18 i alkoholsubstituenten, og/eller ii) den ene eller flere fosforsyre di-ester består af et o-fosforsyremolekyle di-esterificeret med to alkoholmolekyler valgt fra den samme eller en anden, umættede eller mættede, forgrenede eller lineære, alifatiske eller aromatiske fedtalkoholer med en samlet mængde af kulstofatomer fra C6 til C30, fortrinsvis fra C8 til C22, mere fortrinsvis fra C8 til C20 og mest fortrinsvis fra C8 til C18 i alkoholsubstituenten og/eller iii) den ene eller flere fosforsyre tri-ester består af et o-fosforsyremolekyle tri-esterificeret med tre alkoholmolekyler valgt fra den samme eller en anden, umættede eller mættede, forgrenede eller lineære, alifatiske eller aromatiske fedtalkoholer med en samlet mængde af kulstofatomer fra C6 til C30, fortrinsvis fra C8 til C22, mere fortrinsvis fra C8 til C20 og mest fortrinsvis fra C8 til C18 i alkoholsubstituenten.
12. Fremgangsmåde til fremstilling af en fiber og/eller filament og/eller film og/eller tråd og/eller åndbar film omfattende mindst trinnene: a) at tilvejebringe polymersammensætningen ifølge et hvilket som helst af kravene 1 til 8, og b) at udsætte polymersammensætningen af trin a) for forhold under hvilke polymersammensætningen konverteres til en fiber og/eller filament og/eller film og/eller tråd og/eller åndbar film.
13. Overfladereaktivt hvidt mineralmateriale opnåelig med fremgangsmåden ifølge et hvilket som helst af kravene 9 til 11.
14. Fiber og/eller filament og/eller film og/eller tråd og/eller åndbar film omfattende polymersammensætningen ifølge et hvilket som helst af kravene 1 til 8 og/eller det overfladereaktive hvide mineralmateriale ifølge krav 13.
15. Genstand omfattende polymersammensætningen ifølge et hvilket som helst af kravene 1 til 8 og/eller det overfladereaktive hvide mineralmateriale ifølge krav 13 og/eller fiberen og/eller filamentet og/eller filmen og/eller tråden og/eller den åndbare film ifølge krav 14, hvor genstanden er valgt fra gruppen omfattende hygiejneprodukter, medicinal- og sundhedsprodukter, filterprodukter, geotekstilprodukter, landbrugs- og gartneriprodukter, beklædning, fodtøj og baggageprodukter, husholdnings- og industrielle produkter, indpakningsprodukter, konstruktionsprodukter og lignende.
16. Anvendelse afen fosforsyreesterblanding ifølge krav 9 til at mindske hydrofiliciteten og/eller fugtopsamlingsmodtageligheden af den overfladereaktive hvide mineralmateriale-indeholdende partikeloverflade.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP13156349.6A EP2770017B1 (en) | 2013-02-22 | 2013-02-22 | New surface treatment of white mineral materials for application in plastics |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK2770017T3 true DK2770017T3 (da) | 2015-12-14 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK13156349.6T DK2770017T3 (da) | 2013-02-22 | 2013-02-22 | Ny overfladebehandling af hvide mineralmaterialer til anvendelse i plast |
Country Status (18)
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|---|---|
| US (1) | US10066086B2 (da) |
| EP (2) | EP2770017B1 (da) |
| JP (1) | JP6235617B2 (da) |
| KR (1) | KR101856832B1 (da) |
| CN (1) | CN105073864B (da) |
| BR (1) | BR112015020123B8 (da) |
| CA (1) | CA2899282C (da) |
| DK (1) | DK2770017T3 (da) |
| ES (1) | ES2550679T3 (da) |
| HU (1) | HUE026774T2 (da) |
| MX (1) | MX360394B (da) |
| PH (1) | PH12015501670A1 (da) |
| PL (1) | PL2770017T3 (da) |
| PT (1) | PT2770017E (da) |
| RU (1) | RU2630548C2 (da) |
| SI (1) | SI2770017T1 (da) |
| TW (1) | TWI510533B (da) |
| WO (1) | WO2014128087A1 (da) |
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| PT2963162T (pt) * | 2014-07-01 | 2018-10-19 | Omya Int Ag | Fibras multifilamento de poliéster |
| EP3012223A1 (en) | 2014-10-24 | 2016-04-27 | Omya International AG | PCC with reduced portlandite content |
| SI3018174T1 (en) | 2014-11-07 | 2018-07-31 | Omya International Ag | METHOD FOR THE PRODUCTION OF SUSPENSION CONTAINING MATERIAL CONTAINING CALCIUM CARBONATE |
| EP3025786A1 (en) | 2014-11-28 | 2016-06-01 | Omya International AG | Apparatus for simultaneous grinding and froth flotation |
| EP3028830B1 (en) * | 2014-12-02 | 2017-11-22 | Omya International AG | Process for producing a compacted material, material so produced and its use |
| ES2728380T3 (es) | 2015-01-07 | 2019-10-24 | Omya Int Ag | Proceso para obtener un CCM ultrafino con propiedades de elevada dispersión de luz y elevado contenido de sólidos |
| EP3072687A1 (en) | 2015-03-24 | 2016-09-28 | Omya International AG | Easy to disperse calcium carbonate to improve hot tack strength |
| EP3088475A1 (en) | 2015-04-27 | 2016-11-02 | Omya International AG | Modified mineral-based filler comprising copper salts |
| EP3098202A1 (en) | 2015-05-28 | 2016-11-30 | Omya International AG | Process for increasing opacity of precipitated calcium carbonate |
| EP3109274B1 (en) | 2015-06-23 | 2018-06-13 | Omya International AG | Surface treated filler material product for alpha-nucleation of polyolefins |
| PT3118161T (pt) | 2015-07-17 | 2018-10-08 | Omya Int Ag | Pcc com alto teor de sólidos com celulose carboxilada despolimerizada |
| EP3124436A1 (en) | 2015-07-31 | 2017-02-01 | Omya International AG | Precipitated calcium carbonate with improved resistance to structural breakdown |
| EP3133127B1 (en) | 2015-08-21 | 2018-08-08 | Omya International AG | Process for the preparation of a mineral filler product |
| PL3156369T3 (pl) | 2015-10-16 | 2019-01-31 | Omya International Ag | PCC o dużej zawartości części stałych z dodatkiem kopolimerowym |
| EP3176204A1 (en) | 2015-12-02 | 2017-06-07 | Omya International AG | Surface-treated fillers for ultrathin breathable films |
| EP3184644A1 (en) | 2015-12-22 | 2017-06-28 | Omya International AG | Microbial cell viability assay for detection of or determining slurry contamination |
| EP3192838A1 (en) | 2016-01-14 | 2017-07-19 | Omya International AG | Treatment of surface-reacted calcium carbonate |
| ES2944933T3 (es) | 2016-01-14 | 2023-06-27 | Omya Int Ag | Tratamiento con alcoxisilano de un material que comprende carbonato de calcio |
| EP3192850B1 (en) | 2016-01-14 | 2018-10-03 | Omya International AG | Use of surface-treated calcium carbonate as oxygen scavenger |
| EP3269361A1 (en) * | 2016-07-14 | 2018-01-17 | Omya International AG | Dosage form |
| EP3272524A1 (en) | 2016-07-21 | 2018-01-24 | Omya International AG | Calcium carbonate as cavitation agent for biaxially oriented polypropylene films |
| EP3275946A1 (en) | 2016-07-25 | 2018-01-31 | Omya International AG | Post treatment of surface-reacted calcium carbonate with different functional cations |
| EP3275947A1 (en) | 2016-07-25 | 2018-01-31 | Omya International AG | Surface-reacted calcium carbonate with functional cations |
| EP3275838A1 (en) | 2016-07-25 | 2018-01-31 | Omya International AG | Production of amorphous calcium carbonate |
| EP3293322A1 (en) | 2016-09-13 | 2018-03-14 | Omya International AG | Slip resistant product |
| WO2018095515A1 (en) | 2016-11-22 | 2018-05-31 | Omya International Ag | Surface-treated fillers for biaxially oriented polyester films |
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2013
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- 2013-02-22 PT PT131563496T patent/PT2770017E/pt unknown
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- 2013-02-22 SI SI201330069T patent/SI2770017T1/sl unknown
- 2013-02-22 PL PL13156349T patent/PL2770017T3/pl unknown
- 2013-02-22 DK DK13156349.6T patent/DK2770017T3/da active
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| BR112015020123B8 (pt) | 2022-01-18 |
| EP2770017A1 (en) | 2014-08-27 |
| PH12015501670A1 (en) | 2015-10-19 |
| CN105073864B (zh) | 2018-05-08 |
| CA2899282A1 (en) | 2014-08-28 |
| MX2015010610A (es) | 2015-12-16 |
| SI2770017T1 (sl) | 2015-11-30 |
| MX360394B (es) | 2018-10-31 |
| US20160115302A1 (en) | 2016-04-28 |
| EP2770017B1 (en) | 2015-09-02 |
| CA2899282C (en) | 2017-10-17 |
| EP2958958A1 (en) | 2015-12-30 |
| BR112015020123A2 (pt) | 2017-07-18 |
| TWI510533B (zh) | 2015-12-01 |
| TW201443118A (zh) | 2014-11-16 |
| RU2630548C2 (ru) | 2017-09-11 |
| PL2770017T3 (pl) | 2016-02-29 |
| ES2550679T3 (es) | 2015-11-11 |
| HUE026774T2 (en) | 2016-08-29 |
| BR112015020123B1 (pt) | 2021-12-07 |
| PT2770017E (pt) | 2015-11-30 |
| WO2014128087A1 (en) | 2014-08-28 |
| JP6235617B2 (ja) | 2017-11-22 |
| US10066086B2 (en) | 2018-09-04 |
| KR20150133715A (ko) | 2015-11-30 |
| KR101856832B1 (ko) | 2018-05-10 |
| CN105073864A (zh) | 2015-11-18 |
| JP2016513159A (ja) | 2016-05-12 |
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