DK3582886T4 - Fremgangsmåde til at maksimere methanoludbytte ved at anvende katalysatorlag - Google Patents

Fremgangsmåde til at maksimere methanoludbytte ved at anvende katalysatorlag Download PDF

Info

Publication number: DK3582886T4
Authority: DK; Denmark
Prior art keywords: maximizing; catalyst beds; methanol yield; methanol; yield
Prior art date: 2017-02-15

Application number

DK18705374.9T

Other languages

English (en)

Other versions

DK3582886T3 (da

Inventor

Hannsjörg Freund

Robert Frind

Markus Kaiser

Timm Schuhmann

Wolfgang Seuffert

Sebastian Werner

Tobias Henkel

Original Assignee

Clariant Int Ltd

Air Liquide

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2017-02-15

Filing date

2018-02-13

Publication date

2023-08-07

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=61226573&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DK3582886(T4) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

2018-02-13 Application filed by Clariant Int Ltd, Air Liquide filed Critical Clariant Int Ltd

2021-02-22 Publication of DK3582886T3 publication Critical patent/DK3582886T3/da

2023-08-07 Application granted granted Critical

2023-08-07 Publication of DK3582886T4 publication Critical patent/DK3582886T4/da

Links

OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title 3
239000003054 catalyst Substances 0.000 title 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/153—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the catalyst used
- C07C29/154—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the catalyst used containing copper, silver, gold, or compounds thereof
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0492—Feeding reactive fluids
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/153—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the catalyst used
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
- B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
- B01J8/0457—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being placed in separate reactors
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0496—Heating or cooling the reactor
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/1516—Multisteps
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/152—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/0053—Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00654—Controlling the process by measures relating to the particulate material
- B01J2208/00672—Particle size selection
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
- B01J2208/023—Details
- B01J2208/024—Particulate material
- B01J2208/025—Two or more types of catalyst
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
- B01J2208/023—Details
- B01J2208/027—Beds
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Catalysts (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

DK18705374.9T 2017-02-15 2018-02-13 Fremgangsmåde til at maksimere methanoludbytte ved at anvende katalysatorlag DK3582886T4 (da)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE102017001520.1A DE102017001520A1 (de)	2017-02-15	2017-02-15	Reaktor und Verfahren zur Maximierung der Methanolausbeute durch Einsatz von Katalysatorschichten
PCT/EP2018/053518 WO2018149811A1 (en)	2017-02-15	2018-02-13	Reactor and method for maximizing methanol yield by using catalyst layers

Publications (2)

Publication Number	Publication Date
DK3582886T3 DK3582886T3 (da)	2021-02-22
DK3582886T4 true DK3582886T4 (da)	2023-08-07

Family

ID=61226573

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DK18705374.9T DK3582886T4 (da)	2017-02-15	2018-02-13	Fremgangsmåde til at maksimere methanoludbytte ved at anvende katalysatorlag

Country Status (11)

Country	Link
US (1)	US10737230B2 (da)
EP (1)	EP3582886B2 (da)
CN (2)	CN108424351B (da)
CA (1)	CA3050609C (da)
DE (1)	DE102017001520A1 (da)
DK (1)	DK3582886T4 (da)
MY (1)	MY188899A (da)
PL (1)	PL3582886T5 (da)
RU (1)	RU2728351C1 (da)
SA (1)	SA519402409B1 (da)
WO (1)	WO2018149811A1 (da)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US11738317B2 (en) *	2021-01-15	2023-08-29	CRI, hf	Reactor for synthesizing methanol or other products
CN113926391A (zh) *	2021-11-11	2022-01-14	四川天人能源科技有限公司	一种催化剂易热失活的放热催化反应改进工艺
WO2024083780A1 (en)	2022-10-18	2024-04-25	Basf Se	Improved catalyst shapes for heat transfer and pressure-drop in the syngas conversion
CN116212752B (zh) *	2023-04-04	2024-05-24	常州新日催化剂股份有限公司	一种低压型丁烷法顺酐催化剂的装填方法
WO2025141140A1 (en)	2023-12-29	2025-07-03	Basf Se	Process for preparing an activated catalyst and process for preparing methanol using a co2-containing feed stream

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1300917B (de) *	1967-12-30	1969-08-14	Metallgesellschaft Ag	Verfahren zur Herstellung von Methanol
IT1078798B (it) *	1976-09-24	1985-05-08	Tecnimont Spa	Reattore per reazioni esotermiche catalizzate
US4372920A (en) *	1979-07-13	1983-02-08	Ammonia Casale S.A.	Axial-radial reactor for heterogeneous synthesis
JP2560311B2 (ja) *	1987-02-27	1996-12-04	三菱瓦斯化学株式会社	メタノ−ルないし混合アルコ−ルの製造法
DE19605572A1 (de)	1996-02-15	1997-08-21	Metallgesellschaft Ag	Verfahren zum Erzeugen von Methanol
EP0931586B1 (en) *	1997-11-28	2005-03-16	Ammonia Casale S.A.	Method for in-situ modernization of a heterogeneous exothermic synthesis reactor
WO2009082930A1 (en) *	2007-12-17	2009-07-09	Accelergy Shanghai R & D Center Co., Ltd.	Methods and apparatus for exothermic catalystic process
DE102010008857A1 (de) *	2010-02-22	2011-08-25	Lurgi GmbH, 60439	Verfahren zur Herstellung von Methanol
DK3334704T3 (da) *	2015-08-12	2023-07-31	Topsoe As	Hidtil ukendt fremgangsmåde til fremstilling af methanol fra syntesegas af lav kvalitet

2017
- 2017-02-15 DE DE102017001520.1A patent/DE102017001520A1/de not_active Withdrawn
2018
- 2018-02-13 US US16/485,848 patent/US10737230B2/en active Active
- 2018-02-13 CN CN201810149682.0A patent/CN108424351B/zh active Active
- 2018-02-13 MY MYPI2019004635A patent/MY188899A/en unknown
- 2018-02-13 RU RU2019128573A patent/RU2728351C1/ru active
- 2018-02-13 PL PL18705374.9T patent/PL3582886T5/pl unknown
- 2018-02-13 CN CN201820258184.5U patent/CN208532645U/zh active Active
- 2018-02-13 EP EP18705374.9A patent/EP3582886B2/en active Active
- 2018-02-13 DK DK18705374.9T patent/DK3582886T4/da active
- 2018-02-13 CA CA3050609A patent/CA3050609C/en active Active
- 2018-02-13 WO PCT/EP2018/053518 patent/WO2018149811A1/en not_active Ceased
2019
- 2019-08-06 SA SA519402409A patent/SA519402409B1/ar unknown

Also Published As

Publication number	Publication date
PL3582886T3 (pl)	2021-08-02
US20200001261A1 (en)	2020-01-02
RU2728351C1 (ru)	2020-07-29
EP3582886A1 (en)	2019-12-25
CN108424351A (zh)	2018-08-21
CA3050609C (en)	2021-07-13
CA3050609A1 (en)	2018-08-23
DK3582886T3 (da)	2021-02-22
EP3582886B2 (en)	2023-07-12
CN108424351B (zh)	2023-02-17
DE102017001520A1 (de)	2018-08-16
US10737230B2 (en)	2020-08-11
PL3582886T5 (pl)	2023-10-09
CN208532645U (zh)	2019-02-22
EP3582886B1 (en)	2020-12-30
SA519402409B1 (ar)	2022-11-10
MY188899A (en)	2022-01-13
WO2018149811A1 (en)	2018-08-23

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