ECSP20048510A - Colesterol de aceite de pescado - Google Patents

Colesterol de aceite de pescado

Info

Publication number
ECSP20048510A
ECSP20048510A ECSENADI202048510A ECDI202048510A ECSP20048510A EC SP20048510 A ECSP20048510 A EC SP20048510A EC SENADI202048510 A ECSENADI202048510 A EC SENADI202048510A EC DI202048510 A ECDI202048510 A EC DI202048510A EC SP20048510 A ECSP20048510 A EC SP20048510A
Authority
EC
Ecuador
Prior art keywords
phase
cholesterol
fish oil
organic
distillate
Prior art date
Application number
ECSENADI202048510A
Other languages
English (en)
Inventor
Glade Thomas Francis Härting
Rojas Alejandro Markovits
Eckman Steven Lee Härting
Original Assignee
Haerting Glade Thomas Francis
Haerting Eckman Steven Lee
Rojas Alejandro Markovits
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Haerting Glade Thomas Francis, Haerting Eckman Steven Lee, Rojas Alejandro Markovits filed Critical Haerting Glade Thomas Francis
Publication of ECSP20048510A publication Critical patent/ECSP20048510A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • C07J9/005—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane containing a carboxylic function directly attached or attached by a chain containing only carbon atoms to the cyclopenta[a]hydrophenanthrene skeleton
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/04—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping pipe stills
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06—Flash distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/12—Refining fats or fatty oils by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • C11C1/025—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by saponification and release of fatty acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Fats And Perfumes (AREA)
  • Steroid Compounds (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Edible Oils And Fats (AREA)

Abstract

Se describe un proceso para producir colesterol a partir de aceite de pescado, que incluye los siguientes pasos:(a) destilar aceite de pescado en una columna de destilación al vacío para obtener un primer residuo y un primer destilado, (b) destilar el primer destilado en una columna de destilación al vacío para obtener un segundo destilado y un segundo residuo, (c) poner en contacto el segundo residuo con un álcali para producir una mezcla saponificada, (d) poner en contacto la mezcla saponificada con un solvente orgánico no polar o una mezcla de solventes orgánicos no polares para producir una fase orgánica y una fase acuosa, (e) separar la fase orgánica de la fase acuosa, (f) enfriar la fase orgánica para formar una fase sólida y una fase líquida, y (g) separar la fase sólida de la fase orgánica, en donde la fase sólida separada incluye colesterol.
ECSENADI202048510A 2018-02-14 2020-08-12 Colesterol de aceite de pescado ECSP20048510A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US15/896,263 US10196583B1 (en) 2018-02-14 2018-02-14 Fish oil cholesterol

Publications (1)

Publication Number Publication Date
ECSP20048510A true ECSP20048510A (es) 2020-12-31

Family

ID=65200044

Family Applications (1)

Application Number Title Priority Date Filing Date
ECSENADI202048510A ECSP20048510A (es) 2018-02-14 2020-08-12 Colesterol de aceite de pescado

Country Status (14)

Country Link
US (1) US10196583B1 (es)
EP (1) EP3666867B8 (es)
JP (1) JP6616030B2 (es)
KR (1) KR102027319B1 (es)
CN (1) CN110156861B (es)
AU (1) AU2019201053B1 (es)
CA (1) CA3032846C (es)
CL (1) CL2019000404A1 (es)
DK (1) DK3666867T3 (es)
EC (1) ECSP20048510A (es)
ES (1) ES2896247T3 (es)
MX (1) MX2019001730A (es)
PE (1) PE20211311A1 (es)
WO (1) WO2019159020A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10196586B1 (en) * 2018-02-14 2019-02-05 Golden Omega S.A. Feed ingredient
US10196583B1 (en) * 2018-02-14 2019-02-05 Alejandro Markovits Rojas Fish oil cholesterol
US10836701B2 (en) 2019-04-04 2020-11-17 Alejandro Markovits Rojas Fish oil cholesterol
PE20231711A1 (es) * 2020-09-30 2023-10-23 Naturmega S A Proceso de obtencion de colesterol presente en aceite de pescado
CN114478675B (zh) * 2022-01-25 2023-05-23 淮北师范大学 一种从鱼油下脚料中分离胆固醇的方法
CN116693588A (zh) * 2022-02-28 2023-09-05 浙江金朗博药业有限公司 一种从鱼油残液中提取高纯度胆固醇的方法
CN114751952A (zh) * 2022-05-17 2022-07-15 安徽丰本生物科技有限公司 富集甾体醇生产工艺
WO2024018254A1 (en) * 2022-07-19 2024-01-25 American Bioprocess Limitada Cholesterol recovery from fish oil residues
CN117126224B (zh) * 2023-08-04 2025-07-11 河南省科学院高新技术研究中心 一种从鱼油残液中反应挤出提取胆固醇联产脂肪酸钙的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL47083C (es) 1936-01-31
GB489623A (en) 1936-02-06 1938-07-29 Eastman Kodak Co Improvements in high vacuum distillation of materials containing sterols and related compounds
GB526951A (en) 1938-05-03 1940-09-30 Armour & Co Improvements in or relating to the preparation of cholesterol from materials containing same
US2536753A (en) 1948-02-09 1951-01-02 Veenendaalsche Sajet En Vijfsc Recovery and purification of sterols
CA1064907A (en) 1976-11-19 1979-10-23 Alexander G. Fallis Cholesterol separation process
JPS62145099A (ja) * 1985-12-19 1987-06-29 Nippon Suisan Kaisha Ltd コレステロ−ルの分離精製法
JPS62273995A (ja) * 1986-05-23 1987-11-28 Hitachi Ltd 油脂原料中のステロイド分離方法
JPS63174997A (ja) 1987-01-12 1988-07-19 Hitachi Ltd 油脂原料からの有価物の抽出分離方法
BR0106522A (pt) * 2001-12-17 2003-09-09 Resitec Ind Quimica Ltda Processo para separar produtos valiosos insaponificáveis obtidos de matérias primas diversas
SE0202188D0 (sv) * 2002-07-11 2002-07-11 Pronova Biocare As A process for decreasing environmental pollutants in an oil or a fat, a volatile fat or oil environmental pollutants decreasing working fluid, a health supplement, and an animal feed product
EP2295529B2 (en) * 2002-07-11 2022-05-18 Basf As Use of a volatile environmental pollutants-decreasing working fluid for decreasing the amount of pollutants in a fat for alimentary or cosmetic use
US20110207952A1 (en) 2010-02-22 2011-08-25 Rafael Avila Cholesterol extraction from algae and preparation of vegan vitamin d3
WO2012002210A1 (ja) * 2010-07-01 2012-01-05 日本水産株式会社 魚由来コレステロールを用いた乳化化粧料
US8258330B1 (en) * 2012-01-04 2012-09-04 Naturalis, S.A. Carrier fluid composition comprising fatty acids ethyl esters and process for reducing the concentration of persistent organic pollutants in fish oil
WO2016096989A1 (en) 2014-12-19 2016-06-23 Dsm Ip Assets B.V. Method of extracting cholesterol from fish oil residue
US10190074B1 (en) * 2018-02-14 2019-01-29 Golden Omega S.A. Composition comprising cholesterol
US10196583B1 (en) * 2018-02-14 2019-02-05 Alejandro Markovits Rojas Fish oil cholesterol

Also Published As

Publication number Publication date
AU2019201053B1 (en) 2019-08-08
CL2019000404A1 (es) 2019-05-31
BR102019003063A2 (pt) 2019-10-01
CN110156861B (zh) 2020-09-08
JP2019137687A (ja) 2019-08-22
CA3032846C (en) 2019-10-29
KR20190098716A (ko) 2019-08-22
EP3666867A1 (en) 2020-06-17
WO2019159020A1 (en) 2019-08-22
ES2896247T3 (es) 2022-02-24
CN110156861A (zh) 2019-08-23
EP3666867B1 (en) 2021-07-28
KR102027319B1 (ko) 2019-10-01
US10196583B1 (en) 2019-02-05
JP6616030B2 (ja) 2019-12-04
PE20211311A1 (es) 2021-07-22
EP3666867B8 (en) 2021-11-24
MX2019001730A (es) 2019-10-02
CA3032846A1 (en) 2019-04-15
DK3666867T3 (da) 2021-10-25

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