EP0055701A1 - Verfahren zum Regeln eines Druckbehälters zur Behandlung von Zellstoff - Google Patents
Verfahren zum Regeln eines Druckbehälters zur Behandlung von Zellstoff Download PDFInfo
- Publication number
- EP0055701A1 EP0055701A1 EP81890204A EP81890204A EP0055701A1 EP 0055701 A1 EP0055701 A1 EP 0055701A1 EP 81890204 A EP81890204 A EP 81890204A EP 81890204 A EP81890204 A EP 81890204A EP 0055701 A1 EP0055701 A1 EP 0055701A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- pulp
- liquid
- withdrawn
- controlling
- flow rate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims description 39
- 239000007788 liquid Substances 0.000 claims abstract description 53
- 239000000126 substance Substances 0.000 claims abstract description 25
- 238000000605 extraction Methods 0.000 claims abstract description 24
- 230000008569 process Effects 0.000 claims description 11
- 230000004044 response Effects 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000000654 additive Substances 0.000 claims description 2
- 238000005259 measurement Methods 0.000 claims 2
- 230000000087 stabilizing effect Effects 0.000 claims 1
- 238000006073 displacement reaction Methods 0.000 description 10
- 230000001276 controlling effect Effects 0.000 description 9
- 238000007599 discharging Methods 0.000 description 8
- 239000000706 filtrate Substances 0.000 description 8
- 238000007792 addition Methods 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 230000014759 maintenance of location Effects 0.000 description 5
- 239000000725 suspension Substances 0.000 description 5
- 239000002131 composite material Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 239000013461 intermediate chemical Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000006096 absorbing agent Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
- D21C9/02—Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
Definitions
- This invention relates to a method for maintaining all flows in and out of pressurized diffuser machines constant and continuous and of stabilized consistency thereby facilitating incorporation of such a machine or machines in a pulp mill process.
- the conventional filtrate tanks also require adequate pump capacity and pressure head controls to both dilute the incoming stock and circulate the excess (surplus) liquor countercurrently back into the process.
- Considerable pressure head on the pump or pumps is required since the pressure process is conventionally kept well above the static head of the filtrate tank which was exposed to the atmosphere.
- the conventional diffusers needed extraction liquor flow control and separate wash liquor flow control to the preceding stage in multi-stage arrangements.
- the present invention cover a method for controlling the continuous flow of cellulosic material suspensions of medium consistency (8% to 15% BD) in pulp processing to achieve simpler and more efficient dewatering.
- This method of treating cellulosic pulp suspensions flowing in a relatively continuous stream through pressurized diffusers equipped with pulp inlets and outlets along with treatment liquid inlets and outlets comprises feeding the pulp stream through the pulp inlet into the diffuser, withdrawing the treated pulp through the pulp outlet, governing the pulp withdrawal flow rate through the pulp outlet by controlling the pulp feed flow rate into the pulp inlet, establishing consistency control over pulp withdrawn through the pulp outlet by controlling the liquid flow rate from the liquid outlet.
- Additional cellulosic flow treatment comprises feeding treatment liquid through the liquid inlet and may also include chemical admission and/or temperature control over the treatment (wash-displacement) liquid relative to the characteristics of the pulp withdrawn through the pulp outlet.
- adapting the method to a multi-stage pressurized diffuser system comprises connecting the desired number of such diffusers in series using the pulp withdrawn from one diffuser as the pulp feed for the succeeding diffuser with optional intermediate temperature and chemical control of the treatment liquid relative to the pulp flow through the pulp outlet. Further, passing the pulp through an enlarged portion of the feed pipe or a vessel between the diffusers provides a desired retention time between liquid extractions.
- the agitator in the outlet end of the first diffuser in series measures pulp concentration.
- FIGURE 1 An exemplary diffuser utilizable in practicing the present invention is illustrated in FIGURE 1.
- the exemplary diffuser 10 illustrated in FIGURE 1 comprises a conical housing 11 with top part 11' and bottom part 1111 having a pulp inlet 12 and outlet 13, with a powered rotatable scraper 14 mounted in the bottom of housing 11 facilitating discharge of pulp from the housing 11 after treatment.
- a withdrawn liquid outlet 17 extends from the top part of the housing 11.
- a screen body 18 is mounted inside and substantially concentric with the housing 11, the body 18 having perforations or apertures formed therein to allow passage of liquid therethrough but prevent the passage of suspended solids therethrough.
- the bearings 19 and 19' are provided between the body 18 and housing 11 to allow relative linear movement of screen 18 with respect to housing 11 in dimension "A".
- the screen 18 is rigidly attached to one end thereof to a reciprocal shaft 23, which shaft 23 passes through a seal 24 at the top of the housing 11.
- a conventional drive device 25 (such as shown in U.S. Patent 4,041,560) reciprocates the shaft 23 in dimension A. Normally, drive 25 will operate to move the screen 18 downwardly at about the same speed as the pulp flow from inlet 12 to outlet 13, and then move it upwardly much more quickly, and then restart the downward movement.
- the speed and nature of operation of the drive 25 may be varied as desired to accomplish the objectives of the present invention, as may be the details, dimensions, and relative spacings, of the housing 11 and screen 18.
- a treatment liquid inelt 26 is provided for treatment of suspension passing through the housing 11.
- Treatment liquid introduced through inlet 26 is spread out by baffles 27 arranged circumferentially around a concentric liquid distribution body 15 fastened to the housing part 1111 by three arms 15' of which one is hollow and in connection with inlet 26.
- exemplary apparatus utilizable in practicing the method of the invention includes pressurized diffuser 10, and associated inlet and outlet flow controls and the like.
- the pulp flow (slurry) from a continuous digester, a storage tower or the like enters pipeline 28, flows through stock pump 29 (which alternatively may comprise a valve), and enters the top of the vertically aligned pressurized diffuser 10 and flows past movable screen 18 therein.
- the pulp flow entering pressurized diffuser 10, possibly of varying consistency, is stabilized in consistency under its passage through the diffuser 10 by means of fine adjustment of the extraction flow 30 through outlet 17 relative to wash liquor flow 31 into inlets 26 of said pressurized diffuser 10.
- the bottom discharging agitator 14 of pressurized diffuser 10 gives a very reliable output signal for consistency control to a consistency controller 22 and control ratio relay 33.
- This signal adjusts the set point of control ratio relay 33 between the wash liquor flow control FIC 34 and the extraction liquor flow control FIC 35.
- Control ratio relay 33 may have a limited range, for example, 0.9-1.3, to keep extraction flow deviations within the desired tolerances.
- the discharge flow 36 from outlet 13 is measured by pulp discharge flow monitor 37 and a signal is transmitted to pre-set pulp flow controller FIC 38 which controls the stock pump 29 feeding the diffuser 10 [or controls a valve, depending on the pressure in the preceding vessel and the pressure demand for succeeding processes]. From pulp flow controller FIC 38, a proportional signal is transmitted to pulp flow ratio relay 39 which in turn controls the set point of the wash liquor controller FIC 34 which governs the wash liquid flow to the pressure diffuser 10.
- Wash (or displacement) liquor flow controller FIC 34 receives signals from wash liquor sensing means 40 and pulp flow ratio relay 39 to send a composite signal to control ratio relay 33.
- the composite signal through wash liquor controller FIC 34 governs the flow of wash liquor to the pressurized diffuser 10 through wash liquor control means 41.
- the composite signal is sent from wash liquor controller FIC 34 to control ratio relay 33.
- a signal is then transmitted from control ratio relay 33 to extraction flow controller FIC 35.
- the combination of the signals from extraction flow sensing means 42 and from the control ratio relay 33 through extraction flow controller FIC 35 governs the extraction flow control means 43.
- simultaneous pulp flow and consistency control is achieved by regulating the extraction liquor flow relative to the wash liquor flow with reference to the pulp discharge flow, which in turn governs inlet pulp flow and wash liquor flow. That is, if the consistency of the incoming pulp stream tends to drop, the extraction flow will increase to maintain constant discharge consistency, while the pulp flow entering the diffuser will increase correspondingly so as to maintain a constant fiber flow discharging from the diffuser.
- the flow control system operates generally according to the description of FIGURE 2, moreover to optimize performance of pressurized diffuser 10, the speed of screen 18 may be automatically adjusted to match that of the average pulp stream speed through pressurized diffuser 10 by means of a pressure differential control PDC 44 which regulates the drive 25 (e.g., regulates the flow of oil when drive 25 is a hydraulic cylinder) relative to the pressure differential between the top and bottom, of diffuser 10, taken at points 45, 46.
- the optimization process is independent of the flow and consistency control system described in FIGURE 2.
- FIGURE 4 shows the flow and consistency control system as shown in FIGURE 2 and the pressure differential control PDC 44 optimization method shown in FIGURE 3 with the addition of chemical admission controller FIC 47 and stock temperature controler TIC 48 which are connected to the wash liquor line 31 just prior to the wash liquor control 41. Displacement or wash liquor enters pipeline 49 and chemical additions made at point 50 are controlled by chemical admission controller FIC 47 which receives the necessary data, for example, on pH or conductivity, from transmitter 51 which may be located directly in the discharging pulp stream 36.
- the chemical admission controller combines the signal from transmitter 51 with one from chemical flow sensor means 52 to determine the amount of chemical admissions through chemical flow control 53 (which may be a valve or pump).
- Passing wash (displacement) liquor through heat exchanger 54 permits the indirect heating or cooling of the pulp stream itself passing through the pressurized diffuser 10.
- the temperature of the heat exchange medium is regulated through temperature controller TIC 48 and attendant flow control 55 wherein the temperature data transmitter 56 may be located in the discharging pulp stream 36. The location of the temperature data transmitter 56 allows automatic temperature control of the pulp stream entering succeeding treatment steps by controlling the temperature of the pulp stream discharging from the preceding diffuser.
- FIGURE 5 illustrates a multi-stage arrangement.
- the wash liquid flow controller 34 of Section A becomes the extraction flow controller for diffuser 10' of Section B, and similarly the wash liquid flow controller 34' of Section B becomes the extraction flow controller for diffuser 10" of Section C.
- the ratio relay 39 sends identical signals to the subsequent flow controllers 34', 34" , so that they are automatically set at the same flow rate.
- booster pumps 58, 58', 58" only have pressure heads sufficient to compensate for decreases in pressure through, for example, control valves 41, 41' and 41' ' and pipings.
- booster pumps 58, 58', 58" can raise the wash (displacement) liquor pressure from diffuser 10' to that in the preceding diffuser 10. This additional pressure head need basically correspond to pulp line friction losses between the diffusers.
- extraction flow 30 from the first pressurized diffuser 10 which governs the pulp flow consistency of the system should be free of surge effects.
- extraction flow 30 from diffuser 10 should enter a surge or liquor tank 59.
- Tank 59 the only one required in the flow control system, may be pressurized if the diffusers 10, 10', 10" are connected in the blow line from a pressurized vessel (e.g., continuous digester or oxygen reactor).
- a vapor or gas cushion 60 acting on the gas relief flow 61 through valve 62 enables tank 59 to absorb surges.
- Gas analyzers 63 may be incorporated in the gas relief line 61 if desired. This prevents surge flow variances from affecting succeeding process steps.
- the other constant flow and consistency effects are obtained according to the steps described with FIGURE 2.
- FIGURE 6 A multiple stage arrangement employing the flow control method with intermediate chemical admission to the wash (displacement) liquor is illustrated in FIGURE 6.
- the chemical admission controller 47' operates in a similar manner to that described with FIGURE 4.
- the indirect heating and cooling of the wash (displacement) liquor in the heat exchange 54, and associated components also operate in the same manner as in FIGURE 4.
- Utilization of the optional hydraulically filled retention vessel 66 necessitates that the chemical admission controller FIC 47' combines the signals received from transmitter 52 and ratio relay 67 which in turn receives a signal proportional to the pulp flow in line 36. A change in the pulp flow will thus result in an immediate and proportional change in chemical admission flow.
- the systems as described above are capable of practicing the method of the invention so that the flow rate of the pulp being withdrawn through the pulp outlet 36 by controlling the flow rate (by conrol of pump 29) of pulp fed into the first stage diffuser 10; and are capable of setting and controlling the consistency of the pulp being withdrawn through outlets 36, 36', 36" by controlling the flow rate (via flow controller 35) of withdrawn liquid from outlet 17 of first stage diffuser 10 through conduit 30.
- the nature of the pulp treatment and the qualities of the pulp withdrawn from each stage are controlled by adding desired chemicals to the treatment liquids introduced into inlets 26, 26', 26" through lines 31, 31', 32", and controlling the temperature of the treatment liquid via temperature controllers 48, 48', 48" and associated heat exchangers 54, 54', 54".
- the qualities of the withdrawn pulp in lines 36, 36', 36" are sensed (by components 51, 51', 51" and 56, 56', 56") , and control of the treatment liquid chemical addition and temperature is effected in response to such sensing.
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Paper (AREA)
- Immobilizing And Processing Of Enzymes And Microorganisms (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
- Fittings On The Vehicle Exterior For Carrying Loads, And Devices For Holding Or Mounting Articles (AREA)
- Processing Of Color Television Signals (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Materials For Medical Uses (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT81890204T ATE16614T1 (de) | 1980-12-31 | 1981-12-18 | Verfahren zum regeln eines druckbehaelters zur behandlung von zellstoff. |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US22181280A | 1980-12-31 | 1980-12-31 | |
| US221812 | 1980-12-31 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP0055701A1 true EP0055701A1 (de) | 1982-07-07 |
| EP0055701B1 EP0055701B1 (de) | 1985-11-21 |
Family
ID=22829494
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP81890204A Expired EP0055701B1 (de) | 1980-12-31 | 1981-12-18 | Verfahren zum Regeln eines Druckbehälters zur Behandlung von Zellstoff |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP0055701B1 (de) |
| JP (1) | JPS57133292A (de) |
| AT (1) | ATE16614T1 (de) |
| BR (1) | BR8108558A (de) |
| CA (1) | CA1173603A (de) |
| DE (1) | DE3173030D1 (de) |
| FI (1) | FI69139C (de) |
| NO (1) | NO157626C (de) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2639050A1 (fr) * | 1988-11-11 | 1990-05-18 | Kamyr Ab | Procede de stabilisation des conditions de pression et de debit dans un appareil de classage, et appareil de classage le mettant en oeuvre |
| EP0343393A3 (de) * | 1987-11-27 | 1991-07-10 | KAMYR Aktiebolag | Druckverteiler mit mehreren Sieben |
| EP0356415A3 (de) * | 1988-08-18 | 1991-08-28 | Kvaerner Pulping Technologies AB | Drucksiebdiffusionsanlage mit Zurückströmung |
| WO2022200687A1 (en) * | 2021-03-25 | 2022-09-29 | Titoff Matias | Method and apparatus for treating mixtures of liquids and solids |
| US12630976B2 (en) | 2021-03-25 | 2026-05-19 | Lean Pulp Oy | Method and apparatus for treating mixtures of liquids and solids |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5021127A (en) * | 1987-12-01 | 1991-06-04 | Kamyr, Inc. | Extended delignification in pressure diffusers |
| US5066362A (en) * | 1987-12-01 | 1991-11-19 | Kamyr, Inc. | Extended delignification in pressure diffusers |
| US4975148A (en) * | 1988-12-06 | 1990-12-04 | Ahlstromforetagen Svenska Ab | Cold blow system for batch production of pulp |
| FI82082C (fi) * | 1989-03-29 | 1991-12-10 | Ahlstroem Oy | Foerfarande och anordning foer behandling av massa. |
| US5538632A (en) * | 1993-10-28 | 1996-07-23 | Beloit Technologies, Inc. | Multiple filter dynamic washer |
| WO2015080190A1 (ja) * | 2013-11-29 | 2015-06-04 | 三菱化学株式会社 | スラリーの洗浄装置及び洗浄システム |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1468440A (fr) * | 1965-02-17 | 1967-02-03 | Kamyr Ab | Procédé pour agir sur la consistance de pulpe cellulosique dans des installations de blanchiment |
| US3398412A (en) * | 1964-12-17 | 1968-08-27 | Aremaa Toivo Ensio | Method for precipitation or washing of materials containing cellulose |
| US3807202A (en) * | 1969-09-30 | 1974-04-30 | K Gunkel | Continuous washing apparatus for pulp stock and the like |
| US4041560A (en) * | 1975-04-15 | 1977-08-16 | Kamry Ab | Method and device for dewatering of suspensions in movement |
| GB1566099A (en) * | 1976-11-11 | 1980-04-30 | Largo Lintec Ltd | Pulping cellulosic material |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4212239A (en) * | 1979-02-15 | 1980-07-15 | Hobart Corporation | Method and apparatus for removing moisture from wet pulp |
-
1981
- 1981-12-18 CA CA000392616A patent/CA1173603A/en not_active Expired
- 1981-12-18 AT AT81890204T patent/ATE16614T1/de not_active IP Right Cessation
- 1981-12-18 DE DE8181890204T patent/DE3173030D1/de not_active Expired
- 1981-12-18 EP EP81890204A patent/EP0055701B1/de not_active Expired
- 1981-12-28 NO NO814440A patent/NO157626C/no not_active IP Right Cessation
- 1981-12-28 FI FI814173A patent/FI69139C/fi not_active IP Right Cessation
- 1981-12-30 BR BR8108558A patent/BR8108558A/pt not_active IP Right Cessation
- 1981-12-31 JP JP56216193A patent/JPS57133292A/ja active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3398412A (en) * | 1964-12-17 | 1968-08-27 | Aremaa Toivo Ensio | Method for precipitation or washing of materials containing cellulose |
| FR1468440A (fr) * | 1965-02-17 | 1967-02-03 | Kamyr Ab | Procédé pour agir sur la consistance de pulpe cellulosique dans des installations de blanchiment |
| US3807202A (en) * | 1969-09-30 | 1974-04-30 | K Gunkel | Continuous washing apparatus for pulp stock and the like |
| US4041560A (en) * | 1975-04-15 | 1977-08-16 | Kamry Ab | Method and device for dewatering of suspensions in movement |
| GB1566099A (en) * | 1976-11-11 | 1980-04-30 | Largo Lintec Ltd | Pulping cellulosic material |
Non-Patent Citations (1)
| Title |
|---|
| Tappi, Journal of the Technical Association of the Pulp and Paper Industry, Volume 60, No. 9 September 1977 Atlanta (GA) US A. TOMIAK et al.: "Countercurrent Pulp Washing Theory: an Attempt at a Synthesis", pages 148-150 * the entire article * * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0343393A3 (de) * | 1987-11-27 | 1991-07-10 | KAMYR Aktiebolag | Druckverteiler mit mehreren Sieben |
| EP0356415A3 (de) * | 1988-08-18 | 1991-08-28 | Kvaerner Pulping Technologies AB | Drucksiebdiffusionsanlage mit Zurückströmung |
| FR2639050A1 (fr) * | 1988-11-11 | 1990-05-18 | Kamyr Ab | Procede de stabilisation des conditions de pression et de debit dans un appareil de classage, et appareil de classage le mettant en oeuvre |
| WO2022200687A1 (en) * | 2021-03-25 | 2022-09-29 | Titoff Matias | Method and apparatus for treating mixtures of liquids and solids |
| US12630976B2 (en) | 2021-03-25 | 2026-05-19 | Lean Pulp Oy | Method and apparatus for treating mixtures of liquids and solids |
Also Published As
| Publication number | Publication date |
|---|---|
| BR8108558A (pt) | 1982-10-19 |
| FI69139C (fi) | 1985-12-10 |
| DE3173030D1 (en) | 1986-01-02 |
| FI69139B (fi) | 1985-08-30 |
| NO157626C (no) | 1988-04-20 |
| NO814440L (no) | 1982-07-01 |
| ATE16614T1 (de) | 1985-12-15 |
| NO157626B (no) | 1988-01-11 |
| EP0055701B1 (de) | 1985-11-21 |
| CA1173603A (en) | 1984-09-04 |
| JPS57133292A (en) | 1982-08-17 |
| FI814173L (fi) | 1982-07-01 |
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