EP0093264A2 - Méthode et appareil pour nettoyer des particules en métal - Google Patents

Méthode et appareil pour nettoyer des particules en métal Download PDF

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Publication number
EP0093264A2
EP0093264A2 EP83103031A EP83103031A EP0093264A2 EP 0093264 A2 EP0093264 A2 EP 0093264A2 EP 83103031 A EP83103031 A EP 83103031A EP 83103031 A EP83103031 A EP 83103031A EP 0093264 A2 EP0093264 A2 EP 0093264A2
Authority
EP
European Patent Office
Prior art keywords
drum
particles
solution
interior
section
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP83103031A
Other languages
German (de)
English (en)
Other versions
EP0093264A3 (fr
Inventor
Lyle Carman
Nelson Eugene Wittman
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ransohoff Inc
Original Assignee
Ransohoff Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ransohoff Inc filed Critical Ransohoff Inc
Publication of EP0093264A2 publication Critical patent/EP0093264A2/fr
Publication of EP0093264A3 publication Critical patent/EP0093264A3/fr
Withdrawn legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B08—CLEANING
    • B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04—Cleaning involving contact with liquid
    • B08B3/041—Cleaning travelling work
    • B08B3/042—Cleaning travelling work the loose articles or bulk material travelling gradually through a drum or other container, e.g. by helix or gravity

Definitions

  • the present invention relates to a method and apparatus for cleaning cutting oil, dirt and the like from metallic fines, as well as from larger metallic particles such as chips, turnings or borings, and even bushelings.
  • metalworking results in the generation of relatively large quantities of metallic fines, chips, turnings, borings and other metallic waste.
  • the metal workpiece is coated with a cutting oil, both to reduce wear on the metalworking machinery and to reduce heating of the cutting tool machinery and the workpiece.
  • the fines and other metallic waste particles of the operation are coated with oil. Additionally, any dirt with which the metal may come in contact will be held by the oil.
  • the solution to the above-mentioned problems is to remove the cutting oil and dirt from the metal particles prior to the remelting process. Besides avoiding the disadvantages discussed above, if such a process is also capable of separating the cutting oil from the dirt, the oil may be reused as well.
  • the pipe is positioned parallel to the axis of the drum, and steam leaves the pipe through a series of holes defined along its surface.
  • the cleaned chips are collected into a hopper.
  • U.S. patent No. 3,544,369 discloses a method for cleaning metallic waste, similar to that shown in the Goodstein patent, wherein the chips are carried along by a screw type conveyor. Rather than a rotating drum, however, an open inclined trough is provided wherein the screw is mounted to a rotating shaft. The chips to be cleaned are dumped into the lower end of the trough, and are moved upwardly therealong by the screw conveyor. A heated detergent solution is continuously poured into the upper end of the trough, and is allowed to form a pool at the lower end. The pool level is such that the solution overflows the lower end plate of the trough, and the chips are moved upwardly out of the pool, exiting the trough at its upper end.
  • a third device, having a continuous helical flange, is shown in U.S. patent No. 3,754,559, issued August 28, 1973 to Seiwert.
  • the flange is mounted to the interior of a rotatable drum, which is slightly inclined.
  • the chips to be cleaned are introduced at the lower end and are carried by the flange to the upper end.
  • the drum is formed of alternating sections of solid and perforated wall.
  • the wash solution is introduced to the drum interior in the solid sections, and the chips are drained during their passage through the perforated sections.
  • Baffles are mounted to the drum interior adjacent the perforated sections, so as to deflect the chips away from the perforations.while permitting the accumulated liquid to flow out of the drum.
  • Another known device for cleaning metallic waste which has been sold by the assignee of the present application, includes a three-section rotatable drum.
  • a continuous helical flange is mounted along the entire length of the drum.
  • the drum is mounted with its axis horizontal, but the first two sections of the drum are tapered such that the drum diameter at the entrance to the first section is larger than the diameter of the third section.
  • the taper effectively provides an inclined path for the waste particles, which are fed into the device at the entrance to the first section.
  • the wash solution is sprayed into the first section, and the particles are drained during their passage through the second section, with the liquid flowing out the wide ends of the first and second sections to exit the drum.
  • the particles are heated during their passage through the third section for drying.
  • While presently known devices such as those discussed above are generally effective in cleaning particles of.a relatively large size, they are generally not usable with small particles such as metallic fines, i.e., those particles having a size generally less than 60 mesh (60 openings per linear inch, or 23.4 openings per linear cm).
  • the flow direction of the detergent solution is opposite the direction of movement of the metal chips. Because of the small size of metallic fines, they tend to become suspended in the cleaning solution. Therefore, upon introduction into the drum or trough, some of the fines will become suspended in the solution, and carried thereby out the lower end of the system.
  • the method disclosed in the Keogh patent also provides for recovery of the oil from the cleaning solution. This is accomplished by directing solution after exposure to the chips to a settling tank, where the solution is allowed to stand while the oil forms a separate layer on the top of the solution due to the lower specific gravity of the oil. The oil is drawn off, and the solution is returned to the trough.
  • Such a method is disadvantageous, however, since it requires the use of a relatively large settling tank to allow the solution to become relatively quiescent for a period of time to allow proper settling. This in turn requires the use of a relatively large quantity of detergent solution.
  • Such a method and apparatus should be capable of cleaning fines with a recovery of substantially all fines from the detergent solution. Separation of oil and dirt from the used solution should be provided for, to enable reuse of the solution for further cleaning, as well as for recovery and reuse of the oil.
  • the method should also provide a continuous, rather than batch, operation.
  • the present invention discloses a method and apparatus particularly suited for cleaning metallic fines, but also useful in the cleaning of other metallic particles such as chips, turnings, borings, bushelings and the like.
  • a gravity flow of a detergent solution is provided along an inclined path toward a first point from an elevated second point.
  • the dirty metallic particles are continuously introduced into the detergent flow at a point along the path intermediate the two points.
  • the particles are then caused to flow or progress as a moving agitated bed in counter-current fashion through the detergent flow toward the second path point.
  • the method may be accomplished by introducing the particles into a rotating drum equipped with a continuous helical baffle or internal worm, such that the drum interior defines an inclined path extending from the first end to the second end of the drum.
  • the particles are introduced intermediate the ends of the drum, and are caused to flow or progress as a moving. agitated bed in a rising direction.
  • the detergent solution is introduced along the flowing bed of particles and is drained from the drum at a location downstream of the point of introduction of the particles.
  • the cleansed particles are then recovered at the second or discharge end of the drum.
  • the present invention also includes a novel method for performing this task.
  • a rotating drum equipped with a continuous helical baffle or internal worm is provided, defining an inclined path along the interior of the drum, and the fluid flow containing the metallic particles is introduced into the drum interior at a point along the path remote from the lower end.
  • the separated particles are then recovered at the second or discharge end of the drum, while the fluid is drained away near the first or lower end of the drum.
  • the oil and dirt carried by particles to be cleaned by the disclosed method may be recovered through additional steps to the method.
  • the detergent solution is directed to a separation tank adapted for separating oil and dirt from the solution.
  • the solution is continuously flowed through the separation tank, and is then returned to the point at which the fluid is introduced to the drum interior.
  • An apparatus for cleaning metallic particles includes a rotatable hollow drum having a first end and a second end.
  • the drum defines an inclined flow path along its interior with the second end slightly elevated with respect to the first end.
  • a means for rotating the drum is provided, as well as a means for introducing the metallic particles into the interior of the drum at a point along the flow path intermediate the first and second ends.
  • a continuous helical baffle or internal worm is mounted to the interior of the drum and extends from the first to the second end. for transporting the metallic particles along the flow path in the form of an essentially continuously moving, agitated bed of particles progressing toward exit from the drum at its second end.
  • a detergent solution is introduced into the interior of the drum to cause a counterflow of solution through the moving bed of particles.
  • a means for draining the detergent solution is provided near the first end of the drum.
  • the apparatus may further include a means for continuously separating oil and dirt from the drained detergent solution.
  • the detergent solution is collected at the first end of the drum and directed to the separating means, after which the detergent solution from the separating means is recirculated to the point at which the solution is introduced to the drum interior.
  • a funnel member is included having a relatively wide open end and a relatively narrow open end, the wide end being of substantially the same size and shape as the cross-section of the drum.
  • the wide end of the funnel member is mounted to the interior of the drum, and the narrow end is directed toward the second or elevated drum end.
  • the funnel member thus defines first and second sections of the drum, and the means for introducing the metallic particles extends into the first section of the drum to a point along the flow path remote from the first end of the drum.
  • the helical baffle or worm is mounted to the interior of the drum and the funnel member, extending from the first end along the drum interior and along the funnel member to the narrow funnel end.
  • a second helical baffle or worm is mounted to the interior of the drum and extends from the funnel member along the drum interior to the second or discharge end.
  • the first and second. worms are each thus operative in response to rotation of the drum for transporting the metallic particles along the drum interior toward the second end.
  • a further means for introducing a second solution into the second drum section, and a means for draining the second solution from the second drum section are also provided.
  • a means for draining the solution away from the particles within the funnel member and back into the first drum section is also included.
  • metallic fines describes metallic particles of a size approximately 200 mesh (200 openings per linear inch, or 78 openings per cm) , and larger. It will be further recognized, however, that use of the term metallic fines in describing the method and apparatus of the present invention does not represent an intention to limit use of the present invention to metallic fines. While the present invention is particularly well suited for cleaning fines, it is equally usable with larger metallic waste particles, such as chips, turnings, borings, bushelings and the like.
  • the apparatus 10 for cleaning metallic fines may be seen generally in Fig. 1.
  • Oil-saturated, dirty fines are loaded into hopper 12, from which the fines are passed into the lower end of a rotatable, slightly inclined drum 14.
  • Drum 14 functions as a conveyor for the fines during cleaning, carrying the fines along the length of the interior of the drum 14.
  • Cleaning fluids are applied to the fines while within drum 14. The fluid is drained from the interior of drum 14, and the cleaned fines are passed out of the drum 14 at its upper end 16.
  • drum 14 is generally cylindrical in shape, it will be recognized that the requisite characteristic is that the conveyor path formed by drum 14 for transporting the fines be inclined. This will allow drainage of. the fluid from the fines to the lower end of the drum 14, thereby providing separation of the fluid from the fines. Accordingly, any shape for drum 14 in addition to an inclined cylinder, for example a conical drum having its axis horizontal to the ground, that provides an inclined path for the fines may be used.
  • Drum 14 is shown in detail in Fig. 2.
  • a frame 20 for supporting drum 14 is provided, to which is mounted a pair of cradle members 22, only one of. which is shown.
  • a pair of support rings 24 are mounted about the exterior-of drum 14, shown also in Fig. 5, resting within one cradle member 22, freely movable therein and guided thereby during rotation of drum 14.
  • Frame 20 is further constructed so as to maintain drum 14 at a slight angle 26 with respect to the ground 28, preferably on the order of 2 to 7°.
  • a means for rotating drum 14 is provided, including a motor 30 driving a gear 32 through an appropriate gear reduction (not shown), which in turn engages sprocket ring 34 mounted, as shown in Fig. 4, about the exterior of drum.14.
  • Motor 30 is selectively actuated so as to rotate drum 14 in the direction indicated by arrow 36, preferably at a rotational speed in the approximate range of 1/2 to 5 rpm.
  • drum 14 The interior of drum 14 is divided generally into a first section 38 and a second section 40.
  • Each section 38 and 40 of drum 14 includes a helical worm 42 and 44, respectively, mounted along the entire length of the section.
  • Drum sections 38 and 40 are substantially similar, and the details shown with respect to drum section 40 in Fig. 2 generally apply to drum section 38 as well.
  • Drum section 40 extends from a lower end at which a section of perforated wall 46 is provided as a portion of the exterior of drum 14, to an upper end at which a cone-shaped funnel member 48 is provided.
  • the helical worm 44 extends along the length of drum section 40, from a point adjacent the perforated wall section 46, along the interiors of drum 14 and funnel member 48.
  • Worm 44 is generally of a solid structure, but includes a perforated section 50 as that portion of worm 44 contained within funnel member 48, as is also shown in Fig. 6.
  • drum section 38 includes a perforated section 52 of the exterior of drum 14'as its lower end.
  • a cone-shaped funnel member 54 defines the upper end of drum section 38, and, as also shown in Fig. 7, the helical worm extending along drum section 38 includes a perforated section 56 as that portion of worm 42 contained within funnel member 54.
  • Funnel member 54 additionally serves as a divider between the drum sections 38 and 40.
  • the fines to be cleaned are introduced to the interior of first section 38 of drum 14 by a conveyor 58.
  • the fines are deposited within section 38 at a point beyond the perforated wall section 52 and several flights along worm 42.
  • Rotation of drum 14 causes worm 42 to advance the fines along drum section 38 toward funnel member 54.
  • a detergent solution is supplied to drum section 38 by a conduit 60 extending into the interior of drum 14 from the lower end thereof.
  • Conduit 60 has a plurality of orifices defined therealong, such that the detergent solution is applied to the fines in the form of spray jets, indi - cated generally as 62.
  • the detergent solution provided to drum section 38 as spray jets 62 travels along drum section 38 in a direction generally opposite to that of the metallic fines, and exits section 38 through perforated wall section 52 as indicated by arrows 64, seen also in Fig. 3.
  • a drain housing 66 is provided about the perforated wall section 52 of drum 14, so as to channel the used detergent solution into a sump 68.
  • drum 14 causes the fines to be tumbled and agitated as they are moved along the path defined by worm 42.
  • the opposite flow of detergent solution will cause some of the fines to become suspended within the solution.
  • conveyor 58 By providing conveyor 58 such that the fines are introduced to drum section 38 at a point several flights along the worm 42, however, sufficient path length is provided for the suspended fines to settle from the solution prior to the solution's exit from drum section 38 through the perforated wall section 52.
  • the fines are conveyed along drum section 38 by worm 42, and then traverse the interior of funnel member 54.
  • the fines are carried along funnel member 54 by the perforated section 56 of worm 42, whereby any detergent solution still carried by worm 42 may be drained away from the fines. Any liquid so drained flows from funnel member 54 back into drum section 38.
  • the fines Upon reaching the narrow end of funnel member 54, the fines are dumped into the second drum section 40. As in the first drum section 38, the fines are deposited into drum section 40 along worm 44, both , beyond perforated wall section 46 and several flights along worm 44. The fines are advanced by worm 44 toward funnel member 48, and a second cleansing liquid, which may be used as a rinse solution, is applied to the fines, supplied through a conduit 70 extending into drum section 40 from the upper end 16 of the drum 14. Conduit 70 has a plurality of orifices defined therealong, such that the liquid is applied to the fines in the form of spray jets, indicated generally as 72.
  • a drain housing 76 encloses perforated wall section 46, so as to channel used solution into a second sump 78.
  • funnel member 54 as the divider between drum sections 38 and 40 enables two separate solutions to be applied to the fines and maintained as separate solutions within a single drum.
  • the fines are deposited into drum section 40 at a point several flights along worm 44, the fines may be transported without being carried out of drum section 40 by the flow.of liquid.
  • the fines are moved into funnel member 48, where the perforated section 50 of worm 44 along the interior of funnel member 48 allows the liquid to be drained from the fines.
  • the fines are then delivered to the upper end 16 of the drum 14.
  • Appropriate apparatus may be provided such that upon emergence from upper end 16 of drum 14, the cleaned fines may be deposited within a hopper (not shown). Alternatively, the chips may be supplied to.a conveyor (also not shown), and may be delivered to a means for drying the fines.
  • the supply of cleansing liquids to drum sections 38 and 40 is arranged such that first drum section 38 functions as a wash section for the metallic fines, while section 40 serves as a rinse section.
  • Both the wash fluid and the rinse fluid are a heated alkaline water- base solution, with the alkaline detergent preferably being in an approximate concentration of 22g per liter (3 oz. per gallon).
  • the fines to be cleaned are supplied to drum section 38 of drum 14 from hopper 12 by conveyor 58..
  • the wash solution is applied to the fines, supplied to drum section 38 as indicated schematically'at 80.
  • the fines are transported through drum section 38 and deposited into drum section 40, where the rinse solution is applied to the fines, supplied to drum section 40 through a supply line indicated schematically at 82.
  • the fines are then delivered from the drum 14 at the upper end 16.
  • the used wash solution is drained from drum 14 through perforated wall section 52 into sump 68.
  • the liquid is then removed from sump 68 by pump 84, and passed through a heat exchange 86.
  • Heat exchange 86 lowers the temperature of the wash solution, so that the subsequent separation of oil and dirt from the wash solution will be facilitated.
  • the wash solution is directed to separation tank 88.
  • the wash solution is continuously passed through separation tank 88, wherein the oil is removed from the solution, collecting at the top of the separation tank 88, while the dirt accumulates at the bottom.
  • the cleaned solution is then passed to a heat tank 90, where the solution is heated to the cleaning temperature.
  • the wash solution is then returned to the first section 38 of drum 14 by pump 92.
  • the used rinse solution is drained through perforated wall section 46 into sumps 78.
  • the used solution is transported by pump 94 through a heat exchange 96 and passed through separa-' tion tank 98.
  • the fluid is directed to heat tank 100 whereafter it is delivered by pump 102 back to drum section 40.
  • Separator 104 contained within each of separation tanks 88 and 98 may be partially seen in Fig. 9.
  • Separator 104 includes a frame 106 to which is mounted a plurality of corrugated plates 108.
  • the plates 108 are mounted within frame 106 so as to be mutually parallel, and are further mounted in an inclined orientation with the corrugations extending from the upper to the lower edge of each plate 108.
  • the fluid to be separated is directed into separator 104 as generally indicated by arrows 110, such that the fluid flows between the plates 108 in a direction perpendicular to the corrugations of plates 108.
  • the oil l12 is able to move upwardly along each corrugation of plates 108, as shown by arrows 120, until arriving the top of separation tank 88 or 98, where it forms an upper layer on the solution contained therein.
  • the dirt 116 travels in a downward direction along the corrugations of plates 108, as shown by arrows 122, until reaching the bottom of separation tank 88 or 98.
  • the oil collected at the top of separation tank 88 is drawn off as indicated at 124.
  • the oil from the top of separation tank 98 is drawn off as indicated at 126.
  • the dirt collected at the bottom of separation tank 88 is removed therefrom by an auger (not shown) as indicated at 128, while the dirt collected at the bottom of separation tank 98 is similarly removed as indicated at 130.
  • the dirt collected from both tanks 88 and 98 is supplied to a filter unit 132, where any remaining liquid is removed from the dirt.
  • the dirt is then collected from filter unit 132 at 134, while the liquid is directed by pump 136 back into separation tank 88.
  • the apparatus 10 may also be modified for use in separating small particles such as fines from a slurry.
  • a drum similar to drum 14 having only a single section is used.
  • the slurry is provided as a stream into the uppermost end of the drum, so as to provide the maximum drum interior length for separation of the fines from the fluid in which they are suspended.
  • the fines separated from the fluid are recovered as they exit the upper end of the drum, while the fluid is drained away through a perforated wall section at the lower end of the drum.

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  • Cleaning By Liquid Or Steam (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
EP83103031A 1982-04-30 1983-03-26 Méthode et appareil pour nettoyer des particules en métal Withdrawn EP0093264A3 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US37347382A 1982-04-30 1982-04-30
US373473 1982-04-30

Publications (2)

Publication Number Publication Date
EP0093264A2 true EP0093264A2 (fr) 1983-11-09
EP0093264A3 EP0093264A3 (fr) 1984-07-11

Family

ID=23472571

Family Applications (1)

Application Number Title Priority Date Filing Date
EP83103031A Withdrawn EP0093264A3 (fr) 1982-04-30 1983-03-26 Méthode et appareil pour nettoyer des particules en métal

Country Status (2)

Country Link
EP (1) EP0093264A3 (fr)
JP (1) JPS58204184A (fr)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1985003661A1 (fr) * 1984-02-20 1985-08-29 Michel Thonney Procede de traitement par brassage en vrac de pieces brutes moulees ou usinees et machine pour la mise en oeuvre de ce procede
EP0308382A1 (fr) * 1987-09-14 1989-03-22 Lars Ake Hilmer Hakansson Dispositif pour le traitement de petits articles
US5174315A (en) * 1990-04-13 1992-12-29 Durr Gmbh System for cleaning objects
EP0557672A1 (fr) * 1992-02-24 1993-09-01 Oddino Dorigo Appareil pour le traitement continu au moyen de liquides d'objets de petite taille alimentés en vrac
CN103386412A (zh) * 2013-07-09 2013-11-13 慈溪市共力磁业有限公司 一种钕铁硼废料的清洁回收工艺
CN108126956A (zh) * 2017-06-14 2018-06-08 南宁盛世凌云电子科技有限公司 一种改进型除尘器设备
CN114160480A (zh) * 2021-12-06 2022-03-11 鹤山市联发商品混凝土有限公司 一种混凝土用砂粉分离设备及其方法
CN117644058A (zh) * 2024-01-30 2024-03-05 安徽精诚食品科技有限公司 一种用于色选机的多层筛选装置
CN121490475A (zh) * 2026-01-12 2026-02-10 江苏长三角环境科学技术研究院有限公司 基于高压冲洗的滤料重金属清洗装置

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63162084A (ja) * 1986-12-26 1988-07-05 ジヤパン・フイ−ルド株式会社 洗浄装置

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB584744A (en) * 1944-06-16 1947-01-22 Curran Brothers Ltd Improvements in or relating to apparatus for cleaning and otherwise treating small articles by spraying liquid thereon
GB1558566A (en) * 1975-09-26 1980-01-03 Wiggin & Co Ltd Henry Apparatus for treating small articles with liquid

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1985003661A1 (fr) * 1984-02-20 1985-08-29 Michel Thonney Procede de traitement par brassage en vrac de pieces brutes moulees ou usinees et machine pour la mise en oeuvre de ce procede
EP0308382A1 (fr) * 1987-09-14 1989-03-22 Lars Ake Hilmer Hakansson Dispositif pour le traitement de petits articles
US5174315A (en) * 1990-04-13 1992-12-29 Durr Gmbh System for cleaning objects
EP0557672A1 (fr) * 1992-02-24 1993-09-01 Oddino Dorigo Appareil pour le traitement continu au moyen de liquides d'objets de petite taille alimentés en vrac
CN103386412A (zh) * 2013-07-09 2013-11-13 慈溪市共力磁业有限公司 一种钕铁硼废料的清洁回收工艺
CN103386412B (zh) * 2013-07-09 2015-07-15 慈溪市共力磁业有限公司 一种钕铁硼废料的清洁回收工艺
CN108126956A (zh) * 2017-06-14 2018-06-08 南宁盛世凌云电子科技有限公司 一种改进型除尘器设备
CN114160480A (zh) * 2021-12-06 2022-03-11 鹤山市联发商品混凝土有限公司 一种混凝土用砂粉分离设备及其方法
CN114160480B (zh) * 2021-12-06 2022-07-12 鹤山市联发商品混凝土有限公司 一种混凝土用砂粉分离设备及其方法
CN117644058A (zh) * 2024-01-30 2024-03-05 安徽精诚食品科技有限公司 一种用于色选机的多层筛选装置
CN117644058B (zh) * 2024-01-30 2024-04-02 安徽精诚食品科技有限公司 一种用于色选机的多层筛选装置
CN121490475A (zh) * 2026-01-12 2026-02-10 江苏长三角环境科学技术研究院有限公司 基于高压冲洗的滤料重金属清洗装置

Also Published As

Publication number Publication date
EP0093264A3 (fr) 1984-07-11
JPS58204184A (ja) 1983-11-28

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