EP0197732A2 - Fabrication de petits récipients de liquides gazeux - Google Patents
Fabrication de petits récipients de liquides gazeux Download PDFInfo
- Publication number
- EP0197732A2 EP0197732A2 EP19860302341 EP86302341A EP0197732A2 EP 0197732 A2 EP0197732 A2 EP 0197732A2 EP 19860302341 EP19860302341 EP 19860302341 EP 86302341 A EP86302341 A EP 86302341A EP 0197732 A2 EP0197732 A2 EP 0197732A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- liquid
- nitrogen
- bottle
- beer
- cans
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 37
- 238000004519 manufacturing process Methods 0.000 title description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 83
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 40
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 14
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 9
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 9
- 238000009924 canning Methods 0.000 claims abstract description 4
- 238000007789 sealing Methods 0.000 claims abstract description 4
- 235000013405 beer Nutrition 0.000 claims description 35
- 239000012263 liquid product Substances 0.000 claims description 11
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 claims description 2
- 238000005187 foaming Methods 0.000 abstract description 7
- 239000006260 foam Substances 0.000 description 20
- 235000013361 beverage Nutrition 0.000 description 9
- 238000012360 testing method Methods 0.000 description 9
- 239000007789 gas Substances 0.000 description 8
- 235000014171 carbonated beverage Nutrition 0.000 description 7
- 239000011521 glass Substances 0.000 description 6
- 239000000243 solution Substances 0.000 description 5
- 239000003570 air Substances 0.000 description 3
- 235000015095 lager Nutrition 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- -1 0.25 gm Chemical compound 0.000 description 1
- 239000012080 ambient air Substances 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B31/00—Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
- B65B31/006—Adding fluids for preventing deformation of filled and closed containers or wrappers
Definitions
- This invention relates to the manufacture of small containers containing carbonated liquids and has a particularly useful but not exclusive application in relation to small (i.e. single portion) containers of beer and other carbonated beverages.
- Such containers may be in the form of ring-pull cans, or bottles with crown closures, for example which cannot be charged with additional gas after the container has been closed.
- Foam is an important element in the consumer- appeal of most beers and of some other carbonated beverages and other carbonated liquids.
- the most important means by which foam is produced by any of these liquids is the release of carbon dioxide from super-saturated solution.
- Super-saturation arises when a previously-closed, pressurized container is opened to atmosphere or when the liquid contents are discharged from within it through a tap or similar device. Bubbles of carbon dioxide gas are then released by turbulent flow, by nucleation on solid surfaces or particles, or by diffusion into existing gas bubbles.
- volume, stability, bulk viscosity and lacing of foam are governed by a number of factors, important among which are the content of solutes in the aqueous phase and the size-distribution of gas bubbles.
- small gas bubbles with suitable colloids adsorbed at the gas/liquid interface tend to produce the most stable and viscous foams; moreover the fine texture of these foams reflects incident light in a manner that is pleasing to the eye.
- Nitrogen is however relatively insoluble in water, and equilibrates between the beverage and the sealed headspace (vacuity) above it, the volume of which is commonly in the range 5% - 10% of the total container volume, so that much more nitrogen is required than will actually dissolve in the beverage. Furthermore, if nitrogen is dissolved in the beverage in a reservoir before a filling operation carried out in currently used equipment for filling small containers with carbonated beverages, most of the nitrogen is removed by 'gas washing' because due to the much lower solubility of nitrogen than carbon dioxide in the liquid, any bubbles liberated by liquid movement entrain nitrogen leaving the nitrogen content of the solution depleted.
- a method of canning or bottling a liquid product in a small (e.g. one-portion) non-valved can or bottle in which method the can or bottle is almost filled with the liquid product and a quantity of liquid nitrogen is then added to the liquid product in the container, and the container is then immediately sealed.
- the containers Since the contents of one-portion containers of beverages are intended to be consumed entirely, and not re-sealed in the container, the containers are non-valved and there is no requirement for the beverage to be capable of re-generating a head pressure of gaseous nitrogen after the container has been opened.
- the mass of liquid nitrogen injected per container must be sufficient, after it has boiled and dissolved, to satisfy the headspace and solution requirements without exceeding the container's bursting pressure at any time in its subsequent history.
- a limiting requirement will usually be survival in a pasteurizer at about 60°C.
- a bottle of brimful capacity 400ml, containing 380ml of lager beer was passed along a powered conveyor below a constant jet of liquid nitrogen.
- the size of the jet and the speed of the conveyor were selected so that 0.25 grammes of liquid nitrogen fell into the beer.
- the bottle was immediately capped and transported to a testing laboratory. There it was subjected to a standard pouring test as 18°C, the whole volume being transferred to a drinking glass, steadily, during 7 seconds.
- the same test was applied to a control bottle, identical in all respects other than the nitrogen injection.
- the nitrogen-treated beer gave a finer-textured foam which collapsed at about half the rate of the control; when poured from the glass it left an extensive pattern of lacing whereas the control did not.
- a seamless one-piece aluminium can of 440-ml capacity was filled up to about 3mm (1/8 inch) from the brim with lager beer.
- 0.25 gm liquid nitrogen in the form of a thin jet was added to the beer, following which a current of nitrogen gas was directed across the surface of the beer and the can was then immediately sealed in the conventional manner by the application of a lid thereto.
- the sealed can was then inverted and the contents pasteurized at 60°C.
- the weight of the can was then checked to ensure that there was no leakage of its contents. Subsequently the can was opened for testing of the foaming qualities of the beer by the Trufoam test described by P J Wilcon and A P Mundy in the Journal of the Institute of Brewing 1984 Vol.
- the test involves pouring a standard quantity of the beer into a standard glass under standard temperature conditions, the glass and its contents being disposed between a vertically aligned light source and a photoelectric cell.
- the foam on the beer forms a barrier between the light source and the cell.
- the cell emits a signal, and the time taken from the pouring of the beer to the emission of the signal indicates the life of the foam.
- each of the cans A was a control sample in which gaseous nitrogen was blown across the surface of the beer immediately before the can was sealed, but no liquid nitrogen was added to the beer.
- Cans B and C were treated in the same manner but 0.25 gm of liquid nitrogen was added to the beer in cans B and 0.5 gm of liquid nitrogen was added to the beer in cans C before the lids were sealed on the cans.
- empty one-piece aluminium cans 10 of one-portion (440-ml) capacity are fed along a conveyor on to the turntable 11 of a rotary filling machine of the carousel type which initially fills the cans with beer 12 to a level about 1/8" from the brim.
- the cans of beer are then transferred to an output conveyor 11a and pass under a nozzle 13 which is emitting a continuous jet 14 of liquid nitrogen, the flow of nitrogen being adjusted in relation to the time taken for a can to pass under the nozzle so as to add the required weight of liquid nitrogen, e.g. 0.25 gm, to the beer in the can.
- the cans are transferred sequentially to the turntable 11b of a sealing machine in which gaseous nitrogen or carbon dioxide 15 is then blown across the surface of the beer and a lid 16 is immediately sealed on the can. Subsequently the cans are inverted and passed through a pasteurizing apparatus.
- the process is equally applicable to bottles of one-portion capacity containing beers or other carbonated or non-carbonated liquids which are required to have good foaming qualities.
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Basic Packing Technique (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB858508835A GB8508835D0 (en) | 1985-04-04 | 1985-04-04 | Small container of carbonated liquids |
| GB8508835 | 1985-04-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP0197732A2 true EP0197732A2 (fr) | 1986-10-15 |
Family
ID=10577211
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP19860302341 Withdrawn EP0197732A2 (fr) | 1985-04-04 | 1986-03-27 | Fabrication de petits récipients de liquides gazeux |
Country Status (3)
| Country | Link |
|---|---|
| EP (1) | EP0197732A2 (fr) |
| AU (1) | AU5560286A (fr) |
| GB (1) | GB8508835D0 (fr) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2619550A1 (fr) * | 1987-08-17 | 1989-02-24 | Air Liquide | Installation de conditionnement de produits dans des recipients |
| US4865088A (en) * | 1986-09-29 | 1989-09-12 | Vacuum Barrier Corporation | Controller cryogenic liquid delivery |
| DE19538216A1 (de) * | 1995-10-13 | 1997-04-17 | Schmalbach Lubeca | Verfahren zum Herstellen von mit Bier befüllten Dosen |
| US6024996A (en) * | 1995-05-29 | 2000-02-15 | Sara Lee/De N.V. | Packaged carbonated coffee beverage |
| WO2001032530A1 (fr) * | 1999-11-05 | 2001-05-10 | Nytrotec Beverages Ltd | Distribution de boisson et contenants a boisson |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0525089A4 (en) * | 1990-04-19 | 1993-09-22 | Weir & Harrod Machinery Pty. Limited | Drum closure |
| WO1999002406A1 (fr) * | 1997-07-10 | 1999-01-21 | Amcor Packaging (Australia) Pty. Ltd. | Production de produits liquides contenus dans des canettes, bouteilles et autres recipients appropries |
| AU753940B2 (en) * | 1997-07-10 | 2002-10-31 | Amcor Packaging (Australia) Pty Ltd | Producing liquid products contained in cans, bottles and other suitable containers |
-
1985
- 1985-04-04 GB GB858508835A patent/GB8508835D0/en active Pending
-
1986
- 1986-03-27 EP EP19860302341 patent/EP0197732A2/fr not_active Withdrawn
- 1986-04-01 AU AU55602/86A patent/AU5560286A/en not_active Abandoned
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4865088A (en) * | 1986-09-29 | 1989-09-12 | Vacuum Barrier Corporation | Controller cryogenic liquid delivery |
| FR2619550A1 (fr) * | 1987-08-17 | 1989-02-24 | Air Liquide | Installation de conditionnement de produits dans des recipients |
| EP0306379A1 (fr) * | 1987-08-17 | 1989-03-08 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Installation de conditionnement de produits dans des récipients |
| US4977723A (en) * | 1987-08-17 | 1990-12-18 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Plant for packing products in containers |
| US6024996A (en) * | 1995-05-29 | 2000-02-15 | Sara Lee/De N.V. | Packaged carbonated coffee beverage |
| DE19538216A1 (de) * | 1995-10-13 | 1997-04-17 | Schmalbach Lubeca | Verfahren zum Herstellen von mit Bier befüllten Dosen |
| WO2001032530A1 (fr) * | 1999-11-05 | 2001-05-10 | Nytrotec Beverages Ltd | Distribution de boisson et contenants a boisson |
| EP1486432A1 (fr) * | 1999-11-05 | 2004-12-15 | Nytrotec Beverages Ltd | Distribution de boisson et récipient pour boisson |
Also Published As
| Publication number | Publication date |
|---|---|
| AU5560286A (en) | 1986-10-09 |
| GB8508835D0 (en) | 1985-05-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
| AK | Designated contracting states |
Kind code of ref document: A2 Designated state(s): BE DE FR GB NL |
|
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION HAS BEEN WITHDRAWN |
|
| 18W | Application withdrawn |
Withdrawal date: 19870302 |
|
| RIN1 | Information on inventor provided before grant (corrected) |
Inventor name: WREN, JOHN JOSIAH |