EP0390419A2 - Articles à fumer - Google Patents
Articles à fumer Download PDFInfo
- Publication number
- EP0390419A2 EP0390419A2 EP19900303067 EP90303067A EP0390419A2 EP 0390419 A2 EP0390419 A2 EP 0390419A2 EP 19900303067 EP19900303067 EP 19900303067 EP 90303067 A EP90303067 A EP 90303067A EP 0390419 A2 EP0390419 A2 EP 0390419A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- tobacco
- humectant
- smoking article
- article according
- loading level
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES OF CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/42—Treatment of tobacco products or tobacco substitutes by chemical substances by organic and inorganic substances
Definitions
- the invention the subject of this application relates to cigarettes and similar smoking articles.
- the subject invention provides a smoking article comprising a tobacco rod, which rod comprises cut tobacco and a paper wrapper circumscribing said tobacco, a major portion at least of said tobacco having been treated with a humectant to provide a loading level of said humectant of 4% to 15% by weight.
- the loading level of the humectant on the tobacco is not less than 5% and does not exceed 12%. More suitably, the loading level is in the range of 7 - 10%, 9% for example.
- the humectant is suitably one or more of glycerol, propylene glycol, sorbitol and diethylene glycol.
- the humectant is applied to the tobacco prior to the tobacco being subjected to an expansion process.
- the loading level of the humectant on the tobacco prior to expansion may be in a range of about 5% to about 20% in order to result in a post expansion level of 4% to 15%.
- the humectant is applied to the tobacco by being sprayed thereon, advantageously in aqueous solution.
- the humectant should, before the tobacco is subjected to the expansion process, be distributed of the tobacco with a significant degree of uniformity, which objective may be furthered by tumbling the tobacco and/or allowing the tobacco to stand in bulk for a sufficient time after the application of the humectant.
- Tobacco of smoking articles according to the subject invention which is to be subjected to an expansion process is suitably pre-conditioned to a moisture content in a range of 22% to 30% and preferably to a moisture content in a range of 26% to 30%.
- Tobacco of smoking articles according to the subject invention which is subjected to an expansion process may be lamina and/or stem tobacco.
- the expanded tobacco advantageously comprises a lamina tobacco the product of a tobacco expansion process which is effective to provide a high degree of expansion in tobacco subjected to the process.
- High expansion processes are disclosed, for example, in the specification of United States Reissue Patent No. 30,693 and in United Kingdom Patent Specifications Nos. 1,570,270 and 2 160 408A.
- tobacco expansion values in terms of filling value increase, of from about, typically, 75% and even up to about 125% may be obtained.
- Tobacco which has been subjected to a high expansion process may have a bulk density of, for example, from about 100 mg/cc to about 200 mg/cc, and preferably not less than 150 mg/cc, as measured using a Borgwaldt Densimeter.
- a minor proportion of the smoking material of smoking articles according to the subject invention may take the form of reconstituted tobacco and/or tobacco substitute material.
- the smoking material should be wholly natural cut tobacco. It is also preferable that the whole or a substantial proportion of the cut tobacco of smoking articles according to the subject invention should be expanded tobacco and that the whole of this expanded tobacco should have been treated with humectant prior to being expanded.
- at least 65% of the tobacco is treated expanded tobacco, and more suitably 70% is treated expanded tobacco.
- the weight of the smoking material in a cigarette according to the subject invention is suitably in a range of 500 to 800 mg.
- the packing density of the smoking material of smoking articles according to the subject invention does not exceed 210 mg/cc.
- the value obtained includes a proportion of the humectant. It may thus be of interest to express particulate matter delivery on a water, nicotine and humectant free basis (PMWNHF).
- PMWNHF to nicotine delivery ratio of smoking articles according to the subject invention is not more than 8 to 1 and is preferably in the region of 6 to 1, and more preferably in the region of about 5 to 1
- the humectant in the mainstream smoke of cigarettes according to the subject invention preferably forms not less than 15%, and more preferably not less than 20%, of the mainstream PMWNF. Yet more preferably the mainstream smoke humectant forms approximately 25% of the mainstream PMWNF.
- the mainstream smoke humectant may also be in the range 24% to 26%, 24% for example.
- a burn retardant may be used in smoking articles in accordance with the subject invention.
- the burn retardant may be, for example, magnesium chloride, sodium chloride, ammonium sulphate, ammonium lactate, or mixtures thereof, applied to the smoking material.
- the subject invention provides a tobacco treatment comprising the application of a humectant to tobacco and, subsequent to said application, the expanding of said tobacco, the application level of said humectants to said tobacco before the expansion step being such that the loading level of said humectant after said tobacco has been expanded is in a range of 4% to 15% by weight.
- glycerol at a 10% loading level and magnesium chloride at a 1% loading level.
- the blend was conditioned to 25% moisture content, the blend being thereafter subjected to a high level expansion process.
- the glycerol loading on the expanded tobacco was about 6%.
- Each cigarette comprised a 64 mm long tobacco rod consisting of 100% of the expanded tobacco and of wrapper of a standard commercial cigarette paper.
- the packing density of the tobacco in the tobacco rods was about 145 mg/cc.
- a tipping wrapper To each of the tobacco rods there was attached, by a tipping wrapper, a 20 mm long cellulose acetate filter plug. The cigarettes were laser ventilated at the filters to provide a ventilation value of 55%.
- the PMWNHF to nicotine ratio was 4.8. It may also be observed that the glycerol delivery represented 31% of the PMWNF delivery.
- glycerol at a 6% loading level and ammonium lactate at a 2% loading level.
- the blend was conditioned to a 30% moisture content, the blend being thereafter subjected to the high level DIET expansion process.
- the glycerol loading level on the expanded tobacco was 4.4%.
- a second cut tobacco blend comprised 50% burley lamina and 50% sun cured oriental lamina.
- the second blend was not subjected to an expansion process.
- the first and second blends were combined in the proportions 70% first to 30% second and to the thus obtained combined blend was added propylene glycol at a 1.5% loading level.
- the total loading level of humectant, glycerol plus propylene glycol was 4.6%.
- each cigarette comprised a 59 mm long tobacco rod and a standard commercial cigarette paper.
- the packing density of the tobacco in the rods was 190 mg/cc.
- the cigarettes were laser ventilated at the cellulose acetate sections of the filters to provide a ventilation of 60%.
- a commercially available cigarette of similar delivery namely Camel Lights (Trade Mark) was found to have a mainstream glycerol delivery of 0.39 mg, this representing 8% of the PMWNF delivery.
- the PMWNHF to nicotine ratio of Camel Lights was 9.7.
- a cut tobacco blend comprised 25% burley lamina, 40% flue cured lamina, 25% water treated stem and 10% sun cured oriental lamina.
- To this blend was added glycerol at a 10% loading level and magnesium chloride at a 1% loading level. The blend was thereafter subjected to a high level expansion process. The glycerol loading level on the expanded tobacco was 8%.
Landscapes
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB8907255 | 1989-03-31 | ||
| GB898907255A GB8907255D0 (en) | 1989-03-31 | 1989-03-31 | Improvements relating to smoking articles |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| EP0390419A2 true EP0390419A2 (fr) | 1990-10-03 |
| EP0390419A3 EP0390419A3 (fr) | 1991-04-03 |
| EP0390419B1 EP0390419B1 (fr) | 1994-05-04 |
| EP0390419B2 EP0390419B2 (fr) | 1997-09-17 |
Family
ID=10654230
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP90303067A Expired - Lifetime EP0390419B2 (fr) | 1989-03-31 | 1990-03-21 | Articles à fumer |
Country Status (12)
| Country | Link |
|---|---|
| EP (1) | EP0390419B2 (fr) |
| JP (1) | JP3113984B2 (fr) |
| AR (1) | AR244956A1 (fr) |
| AT (1) | ATE105149T1 (fr) |
| AU (1) | AU637089B2 (fr) |
| BR (1) | BR9001661A (fr) |
| CA (1) | CA2013427C (fr) |
| DE (1) | DE69008602T3 (fr) |
| DK (1) | DK0390419T3 (fr) |
| ES (1) | ES2054241T5 (fr) |
| GB (1) | GB8907255D0 (fr) |
| GR (1) | GR3025017T3 (fr) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006046149A3 (fr) * | 2004-10-25 | 2006-07-13 | Philip Morris Prod | Additifs pour scaferlati |
| CN103859581A (zh) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | 一种分子量梯度分布的烟草保润剂 |
| CN108254233A (zh) * | 2017-12-29 | 2018-07-06 | 国家烟草质量监督检验中心 | 一种烟碱溶液标准物质及其制备方法和应用 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2057962C (fr) * | 1991-01-05 | 1999-08-10 | Larry Bowen | Nouveau produit pour les fumeurs |
| TW201032738A (en) * | 2009-01-23 | 2010-09-16 | Japan Tobacco Inc | Cigarette |
| GB201012090D0 (en) * | 2010-07-19 | 2010-09-01 | British American Tobacco Co | Cellulosic material |
| CN102640981B (zh) * | 2012-04-23 | 2014-04-16 | 湖北中烟工业有限责任公司 | 一种提高再造烟叶松厚度的方法 |
| FR3041507B1 (fr) * | 2015-09-25 | 2019-08-30 | Ltr Industries | Tabac reconstitue pour les dispositifs chauffant le tabac sans le bruler |
| GB201520056D0 (en) * | 2015-11-13 | 2015-12-30 | British American Tobacco Co | Tobacco blend |
| IT201800010532A1 (it) * | 2018-11-23 | 2020-05-23 | Magg Consulting S R L | Metodo perfezionato per la preparazione di prodotti solidi da fumo. |
| CN114868954A (zh) * | 2022-03-22 | 2022-08-09 | 上海龙殷生物科技有限公司 | 一种烟用保润剂及提高烟草润感的方法 |
| WO2025181881A1 (fr) * | 2024-02-27 | 2025-09-04 | 日本たばこ産業株式会社 | Composition de tabac, article à fumer de type à chauffage sans combustion et procédé de stockage de composition de tabac |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4310006A (en) * | 1978-03-31 | 1982-01-12 | American Brands, Inc. | Method and apparatus for expanding tobacco |
| US4449541A (en) * | 1981-06-02 | 1984-05-22 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
| US4827949A (en) * | 1987-09-16 | 1989-05-09 | Sunas Ernest C | Method of treating tobacco and tobacco produced thereby |
-
1989
- 1989-03-31 GB GB898907255A patent/GB8907255D0/en active Pending
-
1990
- 1990-03-21 DE DE69008602T patent/DE69008602T3/de not_active Expired - Lifetime
- 1990-03-21 EP EP90303067A patent/EP0390419B2/fr not_active Expired - Lifetime
- 1990-03-21 AT AT9090303067T patent/ATE105149T1/de not_active IP Right Cessation
- 1990-03-21 ES ES90303067T patent/ES2054241T5/es not_active Expired - Lifetime
- 1990-03-21 DK DK90303067.4T patent/DK0390419T3/da active
- 1990-03-29 CA CA002013427A patent/CA2013427C/fr not_active Expired - Lifetime
- 1990-03-29 AU AU52395/90A patent/AU637089B2/en not_active Expired
- 1990-03-30 AR AR90316523A patent/AR244956A1/es active
- 1990-03-30 BR BR909001661A patent/BR9001661A/pt not_active IP Right Cessation
- 1990-03-30 JP JP02087295A patent/JP3113984B2/ja not_active Expired - Lifetime
-
1997
- 1997-10-14 GR GR970402662T patent/GR3025017T3/el unknown
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006046149A3 (fr) * | 2004-10-25 | 2006-07-13 | Philip Morris Prod | Additifs pour scaferlati |
| US9894928B2 (en) | 2004-10-25 | 2018-02-20 | Philip Morris Usa Inc. | Additives for tobacco cut filler |
| US10188139B2 (en) | 2004-10-25 | 2019-01-29 | Philip Morris Usa Inc. | Additives for tobacco cut filler |
| CN103859581A (zh) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | 一种分子量梯度分布的烟草保润剂 |
| CN103859581B (zh) * | 2014-03-26 | 2016-04-13 | 安徽中烟工业有限责任公司 | 一种分子量梯度分布的烟草保润剂 |
| CN108254233A (zh) * | 2017-12-29 | 2018-07-06 | 国家烟草质量监督检验中心 | 一种烟碱溶液标准物质及其制备方法和应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2054241T5 (es) | 1997-11-16 |
| DE69008602D1 (de) | 1994-06-09 |
| EP0390419B2 (fr) | 1997-09-17 |
| AU5239590A (en) | 1990-10-04 |
| CA2013427C (fr) | 1996-09-10 |
| JP3113984B2 (ja) | 2000-12-04 |
| ATE105149T1 (de) | 1994-05-15 |
| DE69008602T3 (de) | 1998-01-08 |
| JPH02286068A (ja) | 1990-11-26 |
| DE69008602T2 (de) | 1994-10-27 |
| AU637089B2 (en) | 1993-05-20 |
| BR9001661A (pt) | 1991-05-14 |
| ES2054241T3 (es) | 1994-08-01 |
| GB8907255D0 (en) | 1989-05-17 |
| DK0390419T3 (da) | 1994-10-31 |
| EP0390419B1 (fr) | 1994-05-04 |
| CA2013427A1 (fr) | 1990-09-30 |
| AR244956A1 (es) | 1993-12-30 |
| GR3025017T3 (en) | 1998-01-30 |
| EP0390419A3 (fr) | 1991-04-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5249588A (en) | Smoking articles | |
| US3385303A (en) | Reconstituted tobacco product | |
| US5031646A (en) | Cigarette | |
| US4830028A (en) | Salts provided from nicotine and organic acid as cigarette additives | |
| US6397852B1 (en) | Smokable filler material for smoking articles | |
| US4878507A (en) | Smoking articles | |
| US5107865A (en) | Smoking articles | |
| EP0283672A2 (fr) | Cigarette | |
| CA2013427C (fr) | Produits pour fumeur | |
| US4133317A (en) | Smokable material and method for preparing same | |
| CA1332335C (fr) | Produits du tabac aromatises aux agrumes | |
| DE3067665D1 (en) | Flavourant composition for tobacco, method for its production and tobacco product containing said composition | |
| US3411514A (en) | Method of making improved shreds from rolled tobacco stems | |
| JP2002501736A (ja) | 喫煙物 | |
| EP0413536B1 (fr) | Articles à fumer | |
| HU215714B (hu) | Ventilált füstszűrős cigaretta | |
| HK1003973B (en) | Improvements relating to smoking articles | |
| EP0514804B1 (fr) | Améliorations concernant des articles à fumer | |
| US3750674A (en) | Tobacco product | |
| US3828795A (en) | Tobacco product | |
| US3730189A (en) | Tobacco product | |
| US3381690A (en) | Tobacco product | |
| SU1623555A3 (ru) | Сигарета | |
| KR880001822B1 (ko) | 담배제품의 맛 또는 향기를 개선시키는 방법 | |
| US3545451A (en) | Flavorant for tobacco products |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
| 17P | Request for examination filed |
Effective date: 19900328 |
|
| AK | Designated contracting states |
Kind code of ref document: A2 Designated state(s): AT BE CH DE DK ES FR GB GR IT LI LU NL SE |
|
| PUAL | Search report despatched |
Free format text: ORIGINAL CODE: 0009013 |
|
| AK | Designated contracting states |
Kind code of ref document: A3 Designated state(s): AT BE CH DE DK ES FR GB GR IT LI LU NL SE |
|
| RAP3 | Party data changed (applicant data changed or rights of an application transferred) |
Owner name: BRITISH-AMERICAN TOBACCO COMPANY LIMITED |
|
| 17Q | First examination report despatched |
Effective date: 19920409 |
|
| GRAA | (expected) grant |
Free format text: ORIGINAL CODE: 0009210 |
|
| AK | Designated contracting states |
Kind code of ref document: B1 Designated state(s): AT BE CH DE DK ES FR GB GR IT LI LU NL SE |
|
| REF | Corresponds to: |
Ref document number: 105149 Country of ref document: AT Date of ref document: 19940515 Kind code of ref document: T |
|
| REF | Corresponds to: |
Ref document number: 69008602 Country of ref document: DE Date of ref document: 19940609 |
|
| ITF | It: translation for a ep patent filed | ||
| REG | Reference to a national code |
Ref country code: ES Ref legal event code: FG2A Ref document number: 2054241 Country of ref document: ES Kind code of ref document: T3 |
|
| ET | Fr: translation filed | ||
| REG | Reference to a national code |
Ref country code: GR Ref legal event code: FG4A Free format text: 3012065 |
|
| REG | Reference to a national code |
Ref country code: DK Ref legal event code: T3 |
|
| EAL | Se: european patent in force in sweden |
Ref document number: 90303067.4 |
|
| PLBI | Opposition filed |
Free format text: ORIGINAL CODE: 0009260 |
|
| 26 | Opposition filed |
Opponent name: H.F. & PH.F. REEMTSMA GMBH & CO Effective date: 19950203 |
|
| NLR1 | Nl: opposition has been filed with the epo |
Opponent name: H.F.& PH.F.REEMTSMA GMBH & CO |
|
| PLAW | Interlocutory decision in opposition |
Free format text: ORIGINAL CODE: EPIDOS IDOP |
|
| PLAW | Interlocutory decision in opposition |
Free format text: ORIGINAL CODE: EPIDOS IDOP |
|
| ITF | It: translation for a ep patent filed | ||
| PUAH | Patent maintained in amended form |
Free format text: ORIGINAL CODE: 0009272 |
|
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: PATENT MAINTAINED AS AMENDED |
|
| 27A | Patent maintained in amended form |
Effective date: 19970917 |
|
| AK | Designated contracting states |
Kind code of ref document: B2 Designated state(s): AT BE CH DE DK ES FR GB GR IT LI LU NL SE |
|
| REG | Reference to a national code |
Ref country code: CH Ref legal event code: AEN Free format text: MAINTIEN DU BREVET DONT L'ETENDUE A ETE MODIFIEE |
|
| REG | Reference to a national code |
Ref country code: DK Ref legal event code: T4 |
|
| NLR2 | Nl: decision of opposition | ||
| ET3 | Fr: translation filed ** decision concerning opposition | ||
| REG | Reference to a national code |
Ref country code: ES Ref legal event code: DC2A Kind code of ref document: T5 Effective date: 19971017 |
|
| REG | Reference to a national code |
Ref country code: GR Ref legal event code: FG4A Free format text: 3025017 |
|
| NLR3 | Nl: receipt of modified translations in the netherlands language after an opposition procedure | ||
| REG | Reference to a national code |
Ref country code: GB Ref legal event code: IF02 |
|
| PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: ES Payment date: 20090327 Year of fee payment: 20 Ref country code: DK Payment date: 20090313 Year of fee payment: 20 Ref country code: LU Payment date: 20090316 Year of fee payment: 20 Ref country code: AT Payment date: 20090317 Year of fee payment: 20 |
|
| PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: NL Payment date: 20090317 Year of fee payment: 20 |
|
| PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: GB Payment date: 20090325 Year of fee payment: 20 Ref country code: CH Payment date: 20090316 Year of fee payment: 20 Ref country code: GR Payment date: 20090316 Year of fee payment: 20 |
|
| PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: DE Payment date: 20090320 Year of fee payment: 20 Ref country code: IT Payment date: 20090325 Year of fee payment: 20 Ref country code: SE Payment date: 20090312 Year of fee payment: 20 |
|
| PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: BE Payment date: 20090430 Year of fee payment: 20 |
|
| PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: FR Payment date: 20090312 Year of fee payment: 20 |
|
| BE20 | Be: patent expired |
Owner name: BRITISH-AMERICAN *TOBACCO CY LTD Effective date: 20100321 |
|
| REG | Reference to a national code |
Ref country code: NL Ref legal event code: V4 Effective date: 20100321 Ref country code: CH Ref legal event code: PL |
|
| REG | Reference to a national code |
Ref country code: DK Ref legal event code: EUP |
|
| REG | Reference to a national code |
Ref country code: GB Ref legal event code: PE20 Expiry date: 20100320 |
|
| EUG | Se: european patent has lapsed | ||
| REG | Reference to a national code |
Ref country code: ES Ref legal event code: FD2A Effective date: 20100322 |
|
| PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: GB Free format text: LAPSE BECAUSE OF EXPIRATION OF PROTECTION Effective date: 20100320 |
|
| PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: NL Free format text: LAPSE BECAUSE OF EXPIRATION OF PROTECTION Effective date: 20100321 Ref country code: ES Free format text: LAPSE BECAUSE OF EXPIRATION OF PROTECTION Effective date: 20100322 |
|
| PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: DE Free format text: LAPSE BECAUSE OF EXPIRATION OF PROTECTION Effective date: 20100321 |